CN109805226A - A kind of health drink and preparation method thereof with anti-aging skin-care functional - Google Patents
A kind of health drink and preparation method thereof with anti-aging skin-care functional Download PDFInfo
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Abstract
A kind of health drink and preparation method thereof with anti-aging skin-care functional, it is related to a kind of health drink, it is combined by ultrasonic wave with dynamic countercurrent circulation, ultrasonic wave auxiliary, aqueous enzymatic extraction and ultrafiltration technology triple combination greatly remain alkali it is fluffy in water-soluble functional components, the fluffy middle polyphenols recovery rate of alkali improves 30%-70% compared to traditional extraction process recovery rate, polyphenol substance in the fluffy stem leaf extract of alkali has very strong inoxidizability, the smoothness of skin can be promoted, U.S. face skin, remove the free radical that human body generates, delaying skin aging, inhibit the decomposition of collagen, play crease-resistant function, the conjugated linoleic acid that common seepweed seeds oil is rich in, jujube in the nutrients such as selenium and flavone compound and ingredient, adlay, donkey-hide gelatin, lily, tremella, aloe combines, it is supported with beauty Face, crease-resistant macrobiosis, nutrition balanced feature comprehensively are suitable for vast female consumer, especially for beautifying face and moistering lotion, crease-resistant have significant health-care effect.
Description
[technical field]
The present invention relates to a kind of health drinks, more particularly, to a kind of health beverage with anti-aging skin-care functional
Material and preparation method thereof.
[background technique]
With the development of modern science and technology, people are higher and higher for the demand of beauty, especially female consumer.People is from out
From raw that time, aging has just been accompanied, meanwhile, the influence of environmental factor and life style can also accelerate aging course,
Cause irreversible transformation, so that people form huge contradiction between the pursuit and irresistible aging of health, beauty,
How pre- anti-aging, anti-aging becomes the hot issue that people inquire into.However, for anti-aging, people are frequently used
Cosmetics and antiaging agent, thus caused health status decline and the following mental wound recognize people gradually
Making up simply can only bring bigger shortcoming.
Currently, more and more people start to praise highly health theory and integration of drinking and medicinal herbs under the influence of Traditional Chinese medical theory
Culture, it is how theoretical with integration of drinking and medicinal herbs, develop a kind of pre- anti-aging, health that delays senescence, green product is society
In a problem urgently to be resolved.
Beautifying face and moistering lotion is the state for making oneself to keep the beautiful youth, is divided into two stages of beauty and beauty treatment.After only focusing on
It maintenance can just possess the perfect skin of health, can just be really achieved radiant.However many people seeking beauties in life, especially
It is Ms, only pays attention to external beauty and maintenance, but ignores inherent conditioning.
Existing beauty skin care product contains chemicals or biological agent mostly, and majority has various side effects, can give skin
Skin brings damage, and cosmetic result relates generally to surface skin, and using effect is difficult to persistently, to be adjusted in terms of constitution
It supports, makes skin is glorious to shine.Studies have shown that nutrition needed for skin is mainly obtained by inside of human body, rather than skin surface.It is former
Because be skin epidermis growth and metabolism required for nutrition mainly by skin corium provide, rather than from skin surface into
Row absorbs.Normal nutrient rich in, plugs skin pore, is deposited in skin surface, be fungus grown in cosmetics
Favourable places threaten skin health over time.
Suaeda salsa is annual herb salification plant, and the fluffy middle nutritional ingredient of alkali is complete and enriches, the fluffy stem leaf protein matter of alkali,
Fat, carbohydrate three nutritious elements content are higher, and seed fat content accounts for the 36.5% of dry matter, are higher than soybean,
The protein content of fresh and tender cauline leaf accounts for the 40% of dry matter, measures 16 kinds of amino acid in Suaeda salsa altogether, wherein there is 8 kinds of human bodies must
Amino acid is needed, and content is higher, there is expansion blood vessel, enhance human immunity, be depressured, the function of hypoglycemic, prevention and cure of cardiovascular disease
Effect；The essential trace elements of the human body and vitamin abundant there are many also containing during alkali is fluffy, wherein calcium, magnesium, zinc, iron, nickel content are rich
Richness, calcium, phosphorus, iron and core yellow cellulose content are higher than or quite much higher than the vegetables such as spinach, tomato and carrot, Vitamin C content
In general vegetables, vitamin B content is 5-8 times of general vegetables, is much higher than spirulina；Invention Announce number is CN106578918
The patent document of A discloses a kind of fluffy healthy and nutritious noodle of selenium-rich alkali and its production technology, and patent document research demonstrates alkali
Fluffy middle high 10 times of the more general food of Se content or so, and selenium is referred to as " king of anti-cancer " in body trace element by scientist,
Have effects that anticancer, pre- preventing tumor, the generation of hepatopathy, raising body immunity；Invention Announce number are as follows: CN103027962A
Patent document disclose a kind of Suaeda salsa extracting flavonoids and content assaying method, patent document research demonstrates saline land alkali
Fluffy (S.salsa) leaf flavonoids content is higher, and has stronger antioxidant activity, and plant flavone has anti-oxidant, antitumor, anti-
The multiple efficacies such as atherosclerosis, anti-inflammatory.
The fluffy seed of alkali is rich in unsaturated fatty acid and conjugated linoleic acid, and the crude fat content of the fluffy seed of alkali is considerably beyond soybean
(crude fat content 23%-25%), unsaturated fatty acid content is abundant in seed, and the 90% of the total fat of Zhan, wherein needed by human
For the content of fatty acid up to 70% or more, linolenic acid accounts for 6.08%, has flax of important health-care efficacy in common seepweed seeds oil to human body
Acid content is suitable with soybean oil and wheat malt oil up to 6.08%, is much higher than other common edible oils.Common seepweed seeds oil is rich in micro member
Plain Se, and liposoluble vitamin content is higher, and especially vitamin E, content are up to 2mg/g, and numerous studies sufficiently show
Common seepweed seeds oil has high healthy nutritive value, is a kind of table oil, can be used as new oil resource and is developed；Alkali is fluffy
Contain conjugated linoleic acid in seed, the patent document of application publication number CN104710299A discloses the sub- oil of conjugation in a kind of fluffy seed of alkali
The extracting method of acid, which extracts common seepweed seeds oil from the fluffy seed of alkali using low boiling point solvent, then mentions from common seepweed seeds oil
Take purified conjugate linoleic acid；A large amount of scientific research proves that conjugated linoleic acid is with antitumor, anti-oxidant, anti-atherogenic is hard
Change, norcholesterol, anticancer improve immunity, improve a variety of important physiological functions such as skeleton density, prevention and treatment diabetes；And it can also
It reduces animal and body's cholesterol and triglycerides and low density lipoprotein cholesterol, animal and human body rouge can also be reduced
Fat increases muscle.
Haematochrome in the fluffy cauline leaf of saline-alkali land is natural pigment, which is researched and analysed as water-soluble anthocyan color
Element, security performance with higher, and there are the healthcare functions such as anti-mutation, anti-oxidant, blood pressure lowering, protection liver, it is anti-oxidant
Activity analysis shows that alkali is fluffy to O-2Free radical has stronger scavenging effect, and often the red in the edible fluffy cauline leaf of saline-alkali land is known as
Conducive to removing excessive oxygen radical in vivo, to be good for one's health and long-lived；The one kind of pigment as polyphenol, the color during alkali is fluffy
Element is the valuable source of natural pigment, anthocyanidin as natural pigment, security performance with higher, and have anti-mutation,
The healthcare functions such as anti-oxidant, blood pressure lowering, protection liver, belong to functional food additives.Polyphenols is referred to as " the 7th class
Nutrient ".Polyphenol is natural " antioxidant ", possesses superpower oxidation resistance, can prevent body from aoxidizing, and can remove people
The free radical that body generates, delaying skin aging；The decomposition for inhibiting collagen, plays crease-resistant function.
Beauty product currently on the market is many kinds of, although can reach a period of time beautification of skin surface, in its product
Emulsifier, fragrance, pigment, the chemical additives such as preservative are also easy to cause a degree of injury to the person of disappearing, are not achieved and answer
Some safety requirements.Common beautifying and youth-keeping beverage is mostly green tea beverage, black tea drinks, jasmine tea beverage etc. currently on the market,
In kind, it is all relatively simple on taste and in terms of healthcare function, the beverage that special suitable female health is drunk is even more considerably less, very
Difficulty meets the consumption demand of vast female consumer.
[summary of the invention]
In order to overcome the shortcomings in the background art, the present invention develops a kind of guarantor with anti-aging skin-care functional
Strong beverage and preparation method thereof greatly remains alkali by ultrasonic wave auxiliary, aqueous enzymatic extraction and ultrafiltration technology triple combination
Water-soluble functional components in fluffy, the fluffy middle polyphenols recovery rate of alkali are improved compared to traditional extraction process recovery rate
30%-70%, the polyphenol substance during alkali is fluffy have very strong inoxidizability, can promote the smoothness of skin, U.S. face skin, clearly
Except the free radical that human body generates, delaying skin aging inhibits the decomposition of collagen, plays crease-resistant function, and common seepweed seeds oil institute is rich
Jujube in the nutrients such as the conjugated linoleic acid, selenium and the flavone compound that contain and ingredient, adlay, donkey-hide gelatin, lily, tremella,
Aloe combines, and has a beautifying face and moistering lotion, crease-resistant macrobiosis, recuperating qi-blood, and nutrition balanced feature comprehensively is suitable for numerous women
Consumer, especially for beautifying face and moistering lotion, crease-resistant macrobiosis has significant health-care effect.
For achieving the above object, the present invention adopts the following technical scheme:
A kind of health drink and preparation method thereof with anti-aging skin-care functional, includes the following steps:
The fluffy stem leaf extract preparation of saline-alkali land:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, is put into guarantor's food peace food purifying machine and cleans 1 time~3
Time, removal impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper and be cut into every section of 1cm~2cm；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, at colloid mill mashing
It manages to 30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 to 60 mesh~200 mesh using high-accuracy Wet ultrafine grinding equipment；
Step 5, smashed material is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment, by feed liquid mass ratio 1:
20~1:50 adds deionized water, adds 2%~4% (w/w) cellulase, is added 0.05%~0.08% vitamin C, when enzymatic hydrolysis
Between 20min~30min, 30 DEG C~50 DEG C of hydrolysis temperature, ultrasonic power 50w~200w, extraction time be 1~2 time, merge leaching
Extract；
Step 6, the leaching liquor of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, obtains the fluffy cauline leaf of saline-alkali land and extracts
Liquid is spare；
The preparation of salt-soda soil common seepweed seeds oil:
Step 7, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened,
Remove soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is small after screening
In 0.1%；
Step 8, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature
Degree is 40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 9, the fluffy seed of saline-alkali land is crushed after vacuum drying with pulverizer, is crushed to mesh number as 60 mesh to 150
Mesh；
Step 10, the fluffy powder of seeds of saline-alkali land being subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, one
Grade separating still pressure is 8-10MPa, and the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, two fractions
35 DEG C are regulated to from kettle temperature degree, extraction time 2.5h-4.5h；
Step 11, the isolate in level-one separating still and the second-order separation kettle is collected, evaporates separation using spiral evaporator
Then ethyl alcohol in object further removes ethyl alcohol in a vacuum drying oven under the conditions of 40 DEG C；
Step 12, the isolate in level-one separating still and the second-order separation kettle is after step 5 removes ethyl alcohol, in level-one separating still
Isolate directly as salt-soda soil common seepweed seeds oil, the isolate in the second-order separation kettle is centrifuged with centrifuge, centrifugal rotational speed
For 30r/min-50r/min, centrifugation time 20min, upper layer oil reservoir, the saline-alkali land being incorporated in level-one separating still after collection are taken
In fluffy seed oil, it is spare that salt-soda soil common seepweed seeds oil is obtained after mixing；
Step 13, the fluffy stem leaf extract of saline-alkali land and salt-soda soil common seepweed seeds oil mix according to the ratio of 10:1
Mixed liquor A；
Step 14, jujube 35%, adlay 22%, donkey-hide gelatin 8%, lily 15%, tremella 10%, aloe 10% are taken, is cleaned, powder
It is broken, after mixing, 2-3h is added water to cook, residue is filtered, takes supernatant to obtain extracting solution B spare；
Step 15, by mixed liquor A made from step 13 and step 14, extracting solution B and water, honey according to 1:1.2:0.4's
Ratio is mixed to prepare mixed liquor C；
Step 16, mixed liquor C carries out coarse filtration, ultrafiltration by reverse osmosis unit, and sterile filling to obtain the final product.
The health drink and preparation method thereof with anti-aging skin-care functional, the fluffy cauline leaf of the alkali mention
Take its mineral composition of liquid and content as follows: Ca2+2985 μ g/L~5200 μ g/L, μ g/L of Mg2+1743 μ g/L~2791, Fe2+
The 162 μ g/L of μ g/L~185, the μ g/L of Mn2+5.11 μ g/L~8.03, the μ g/L of Zn+5.27 μ g/L~8.51, the μ of K+0.8 μ g/L~3.0
G/L, μ g/L of Na+1746 μ g/L~6899,200 μ of μ g/L~400 g/L of total dissolved solid.
The health drink and preparation method thereof with anti-aging skin-care functional, step 6 and step 16 institute
The reverse osmosis unit system configuration stated are as follows: pretreatment system, smart filtration system, corollary system；Pretreatment system is by mechanical filter
Device, adsorption filter, cartridge filter composition；Smart filtration system is made of hollow-fibre ultrafiltration device；Corollary system is by water purification
Tank, electrical control system composition；Mechanical filter filtering can remove body refuse and fiber etc. in extracting solution, after through absorbing and filter
Device filtering can remove oil removal, however can remove the impurity such as algae through mechanical filter filtering.
The health drink and preparation method thereof with anti-aging skin-care functional, step 6 and step 16 institute
Stating ultrafiltration is hollow-fibre membrane ultrafiltration to remove the microorganisms such as bacterium in extracting solution, mould.
The health drink and preparation method thereof with anti-aging skin-care functional, the hollow-fibre membrane are straight
Diameter is 0.01 μm~0.001 μm, and feed rate is 900L/h~1500L/h, pressure 0.045Mpa~0.18Mpa, feed concentration
For the 200 μ g/L of μ g/L~400, ultrafiltration time 100min~400min, backwash cycle 10min~40min, backwash time 20min
~120min, upper operation 10min~40min, upper backwash 20s~120s, lower operation 10min~40min, lower backwash 20s~
120s。
Due to the adoption of the technical scheme as described above, the invention has the following beneficial effects:
1, in the health drink ingredient with anti-aging skin-care functional of the invention select jujube, adlay, donkey-hide gelatin,
Lily, tremella, aloe, jujube contain a variety of amino of protein, fat, carbohydrate, organic acid, vitamin A, vitamin C, micro-calcium
The nutrition abundant such as acid.There are invigorating spleen and reinforcing stomach, tonifying middle-Jiao and Qi, nourishing blood and tranquilization mitigates the function of pharmacological property；Jujube and adlay have
The effect of beautifying face and moistering lotion is good, and adlay, nature and flavor are sweet, light, slightly cold, returns spleen, stomach and lung channel, has clearing damp and promoting diuresis, invigorating the spleen to arrest diarrhea, clearing damp
Only the effect of numbness, clearing away heat and eliminating pus；Donkey-hide gelatin, enriching yin of enriching blood, moisturizes, hemostasis.For blood deficiency chlorosis, dizziness palpitaition, dysphoria and insomnia, lung
Cough caused by dryness is coughed；Lily, nature and flavor are sweet, slightly cold, and return lung and the heart channel of Hang-Shaoyin have effects that moistening lung to arrest cough, clearing away the heart fire and tranquillizing；Tremella is sweet in flavor, light, property
It is flat, nontoxic, the effect of existing tonifying spleen is whetted the appetite, and play the role of QI invigorating gut purge, nourishing Yin and moistening lung, can enhance human immunity and
Tumor patient can be enhanced to the tolerance of Radiotherapy chemotherapy, tremella has the function of enriching yin rich in natural plant colloid, additional its,
It is the good moisturizing food that can be taken for a long time；Aloe contains Anthraquinones abundant, carbohydrate, amino acid, organic acid, cellulose, work
Property substance, microelement etc., in addition, aloe also there is defaecation to rush down under, antitumor, anti-aging, anti-oxidant, antibacterial, liver protection and
Other pharmacological actions；Honey is a kind of natural nutriment, it include can burn high-quality sugar of body energy, vitamin with
And minerals etc., honey contain outstanding bactericidal effect and detoxifying effect, it can allow the waste under stopping in vivo to excrete,
Making the metabolic function of whole body is improved so that those gathered in vivo due to that cannot consume well get off it is extra
Fat is burnt as energy；It is rich in polyphenols in the fluffy stem leaf extract of alkali, there is anti-mutation, anti-oxidant, drop blood
Pressure, liver-protective healthcare function, antioxidant activity is analysis shows alkali is fluffy to O-2Free radical has stronger scavenging effect, through often eating
Be conducive to remove excessive oxygen radical in vivo with the haematochrome in the fluffy cauline leaf of saline-alkali land, thus be good for one's health and long-lived,
Polyphenol in the fluffy stem leaf extract of alkali is natural " antioxidant ", possesses superpower oxidation resistance, can prevent body from aoxidizing,
The free radical of human body generation, delaying skin aging can be removed；The decomposition for inhibiting collagen, plays crease-resistant function, the fluffy seed of alkali
Flavones ingredient has free radical resisting and antioxidation in oil.
2, simultaneously alkali it is fluffy in also rich in the mineral elements such as calcium, magnesium, iron, manganese, zinc, copper, strontium, sodium, and contain abundant amino
Sour type, up to 18 kinds, including necessary amino acid: threonine, valine, isoleucine, methionine, leucine, phenylpropyl alcohol
Propylhomoserin, lysine, tryptophan.Nonessential amino acid: asparatate, serine, glutamic acid, glycine, alanine, Guang ammonia
Acid, tyrosine, histidine, arginine, proline.Wherein essential amino acids content accounts for total amino acid content difference 35.2%, approaches
The reference model (36%) that FAO is proposed, it is necessary to which the ratio of amino acid and nonessential amino acid is 55%, the ginseng proposed close to FAO
Mode (0.56) is examined, comprehensive and abundant nutrition can be provided for beautifying face and moistering lotion person.
3, polyphenol recovery rate compared to traditional extraction process recovery rate improves 30%- in the fluffy stem leaf extract of alkali of the present invention
70%, it is combined by ultrasonic wave with dynamic countercurrent circulation, so that polyphenol recovery rate greatly improves in the fluffy stem leaf extract of alkali, is risen
To the effect got twice the result with half the effort；It is fluffy that alkali is greatly remained by ultrasonic wave auxiliary, aqueous enzymatic extraction and ultrafiltration technology triple combination
In water-soluble functional components, aqueous enzymatic method combination ultrasonic wave physical process, utilize it generate very big acceleration, strong sky
Change the properties such as effect, high vibration, reduce and asked when extracting, temperature is avoided to change the activity change to effective component；Of the invention
Ultrasonic wave dynamic countercurrent auxiliary enzymes and ultrafiltration technology combine extract the fluffy middle polyphenols of alkali method simple production process,
The consuming time is few, reduces production work intensity, has product effective component high, and it is excellent to reduce temperature change bring adverse effect etc.
Point.
4, the present invention using coarse filtration and ultrafiltration effectively eliminate the impurity such as body refuse, suspended matter, algae in extracting solution and
The microorganisms such as bacterium, mould in extracting solution, high degree remain the fluffy extracting solution of alkali, jujube, adlay, donkey-hide gelatin, lily, silver
Ear, the various nutritional ingredients of extract solution from aloe and microelement, it is easy to operate, it is suitable for industrialized production, compared to traditional mistake
Filtering method, hyperfiltration technique are a kind of purifications for being widely used in water, and pollution-free, low energy consumption, and separator is simple, process is short, operation
Easy, easily controllable and maintenance, installation area are small.It carries out at normal temperature, mild condition is especially fitted without component damage
It is highly effective to the recycling of the micro constitutent in this product preferably to the separation and enrichment of the substance of this product (thermo-responsive).Ultrafiltration
Mechanical filter filtering can remove body refuse and fiber etc. in extracting solution in technique pretreatment system, after through adsorption filter mistake
Filter can remove the impurity such as oil removal and algae, and then by the hollow-fibre membrane ultrafiltration of ultrafiltration technology essence filtration system to go
Except the microorganisms such as bacterium, mould in extracting solution.
5, the fluffy polyphenols recovery rate of alkali may be up to 5.9% in the present invention, and polyphenols is referred to as " the 7th class nutrition
Element ", it is external that polyphenol can promote lipid and bile acid to exclude, and reduce the content of cholesterol and triglycerides in blood plasma and liver, fit
Suitable disease in the liver and gallbladder patient drinks, and has significant health-care effect especially for the elderly, liver and gallbladder patient, helps health.
6, the present invention is directed to the critical CO of the fluffy seed part over-extraction of saline-alkali land2Extraction has extraction efficiency high, solvent-free
Residual toxicity, active skull cap components and heat-sensitive ingredients are not easy the destruction that is decomposed, and can keep the natural of extract to the maximum extent
Feature is, it can be achieved that the advantages of Selective Separation.
7, the fluffy stem and leaf part raw material of alkali chooses alkali fluffy plant of the growth cycle within 45 days in the present invention, and alkali at this time is fluffy
Cauline leaf is fresh and tender, rich in nutritional ingredients such as functional pigmented, vitamin, protein and alkaloids；The fluffy seed of saline-alkali land in the present invention
The fluffy seed of 10-11 month saline-alkali land is selected, the fluffy raw material of alkali selected by the present invention is artificial cultivation, and avoiding wild suaeda glauce raw material can
Heavy metals exceeding standard problem existing for energy, artificial cultivation, good growing environment ensure that the safety of raw material.
8, the health drink to provided by the invention with anti-aging skin-care functional carries out physical and chemical index detection, respectively
Item main indicator is all satisfied requirements of the national standard.
[Detailed description of the invention]
Fig. 1 is influence of the liquid-solid ratio to the fluffy pigment extraction effect of alkali；
Fig. 2 is the response surface that solid-liquid ratio, cellulase, vitamin C and ultrasonic power influence polyphenol content.
[specific embodiment]
The present invention can be explained in more detail by the following examples, the open purpose of the present invention is intended to protect the present invention
All changes and improvements in range, the invention is not limited to the following examples；
A kind of health drink and preparation method thereof with anti-aging skin-care functional, includes the following steps:
The fluffy stem leaf extract preparation of saline-alkali land:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, is put into guarantor's food peace food purifying machine and cleans 1 time~3
Time, removal impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper and be cut into every section of 1cm~2cm；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, at colloid mill mashing
It manages to 30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 to 60 mesh~200 mesh using high-accuracy Wet ultrafine grinding equipment；
Step 5, smashed material is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment, by feed liquid mass ratio 1:
20~1:50 adds deionized water, adds 2%~4% (w/w) cellulase, is added 0.05%~0.08% vitamin C, when enzymatic hydrolysis
Between 20min~30min, 30 DEG C~50 DEG C of hydrolysis temperature, ultrasonic power 50w~200w, extraction time be 1~2 time, merge leaching
Extract；
Step 6, the leaching liquor of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, obtains the fluffy cauline leaf of saline-alkali land and extracts
Liquid is spare；
The preparation of salt-soda soil common seepweed seeds oil:
Step 7, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened,
Remove soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is small after screening
In 0.1%；
Step 8, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature
Degree is 40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 9, the fluffy seed of saline-alkali land is crushed after vacuum drying with pulverizer, is crushed to mesh number as 60 mesh to 150
Mesh；
Step 10, the fluffy powder of seeds of saline-alkali land being subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, one
Grade separating still pressure is 8-10MPa, and the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, two fractions
35 DEG C are regulated to from kettle temperature degree, extraction time 2.5h-4.5h；
Step 11, the isolate in level-one separating still and the second-order separation kettle is collected, evaporates separation using spiral evaporator
Then ethyl alcohol in object further removes ethyl alcohol in a vacuum drying oven under the conditions of 40 DEG C；
Step 12, the isolate in level-one separating still and the second-order separation kettle is after step 5 removes ethyl alcohol, in level-one separating still
Isolate directly as salt-soda soil common seepweed seeds oil, the isolate in the second-order separation kettle is centrifuged with centrifuge, centrifugal rotational speed
For 30r/min-50r/min, centrifugation time 20min, upper layer oil reservoir, the saline-alkali land being incorporated in level-one separating still after collection are taken
In fluffy seed oil, it is spare that salt-soda soil common seepweed seeds oil is obtained after mixing；
Step 13, the fluffy stem leaf extract of saline-alkali land and salt-soda soil common seepweed seeds oil mix according to the ratio of 10:1
Mixed liquor A；
Step 14, jujube 35%, adlay 22%, donkey-hide gelatin 8%, lily 15%, tremella 10%, aloe 10% are taken, is cleaned, powder
It is broken, after mixing, 2-3h is added water to cook, residue is filtered, takes supernatant to obtain extracting solution B spare；
Step 15, by mixed liquor A made from step 13 and step 14, extracting solution B and water, honey according to 1:1.2:0.4's
Ratio is mixed to prepare mixed liquor C；
Step 16, mixed liquor C carries out coarse filtration, ultrafiltration by reverse osmosis unit, and sterile filling to obtain the final product.
The health drink and preparation method thereof with anti-aging skin-care functional, the fluffy cauline leaf of the alkali mention
Take its mineral composition of liquid and content as follows: Ca2+2985 μ g/L~5200 μ g/L, μ g/L of Mg2+1743 μ g/L~2791, Fe2+
The 162 μ g/L of μ g/L~185, the μ g/L of Mn2+5.11 μ g/L~8.03, the μ g/L of Zn+5.27 μ g/L~8.51, the μ of K+0.8 μ g/L~3.0
G/L, μ g/L of Na+1746 μ g/L~6899,200 μ of μ g/L~400 g/L of total dissolved solid.
The health drink and preparation method thereof with anti-aging skin-care functional, step 6 and step 16 institute
The reverse osmosis unit system configuration stated are as follows: pretreatment system, smart filtration system, corollary system；Pretreatment system is by mechanical filter
Device, adsorption filter, cartridge filter composition；Smart filtration system is made of hollow-fibre ultrafiltration device；Corollary system is by water purification
Tank, electrical control system composition；Mechanical filter filtering can remove body refuse and fiber etc. in extracting solution, after through absorbing and filter
Device filtering can remove oil removal, however can remove the impurity such as algae through mechanical filter filtering.
The health drink and preparation method thereof with anti-aging skin-care functional, step 6 and step 16 institute
Stating ultrafiltration is hollow-fibre membrane ultrafiltration to remove the microorganisms such as bacterium in extracting solution, mould.
The health drink and preparation method thereof with anti-aging skin-care functional, the hollow-fibre membrane are straight
Diameter is 0.01 μm~0.001 μm, and feed rate is 900L/h~1500L/h, pressure 0.045Mpa~0.18Mpa, feed concentration
For the 200 μ g/L of μ g/L~400, ultrafiltration time 100min~400min, backwash cycle 10min~40min, backwash time 20min
~120min, upper operation 10min~40min, upper backwash 20s~120s, lower operation 10min~40min, lower backwash 20s~
120s。
Wherein, water used is deionized water, and the minerals in water have been filtered out in deionized water, have avoided calcium in water, magnesium
The interference of plasma.
Addition vitamin C can play the color protection fluffy to alkali, anti-oxidation efficacy in steps of 5, while also can be realized battalion
Support the purpose strengthened.
The detection of every physical and chemical index:
For nutritional ingredient composition and content situation in the fluffy stem leaf extract of saline-alkali land and salt-soda soil common seepweed seeds oil, pass through
Micro-kjoldahl method measures crude protein content；Using determination of crude oil by Soxhlet extraction；It is thick using gravimetry
Fiber content；Moisture content is measured using atmosphere pressure desiccation；Carbohydrate content is measured using anthrone colorimetry；Using high temperature
Ash purification determining content of ashes；Amino acid content is measured using Hitachi 835-50 type high-speed amino acid analyzer；Using fluorescence point
Light photometry measures tryptophan composition and content；Using atomic absorption spectroscopy determination mineral element, wherein selenium element is used
Fluorescence spectrophotometry；Every nutritional ingredient and content are shown in Table 1-3 in the common seepweed seeds oil of salt-soda soil, and the fluffy cauline leaf of saline-alkali land mentions
Every nutritional ingredient and content in liquid is taken to be shown in Table 4-6: main nutrient composition content in 1 salt-soda soil common seepweed seeds oil of table
2 salt-soda soil common seepweed seeds oil Mineral Element Contents (μ g/g) of table
The composition and content (mg/g) of amino acid in 3 salt-soda soil common seepweed seeds oil of table
The fluffy stem leaf extract nutrient content of 4 saline-alkali land of table
The fluffy stem leaf extract Mineral Elements in Jadeite Shellfish content of 5 alkali of table
The fluffy stem leaf extract amino acid content of 6 saline-alkali land of table
Pass through nutritional ingredient composition and content situation in the fluffy stem leaf extract of measurement saline-alkali land and salt-soda soil common seepweed seeds oil
It can be seen that
The comparison of table 1 and table 4 can be seen that crude protein, crude fat content in the common seepweed seeds oil of salt-soda soil: 18.75% and
23.46%, much higher than crude protein, crude fat content in the fluffy stem leaf extract of saline-alkali land: 3.020% and 1.380%, and salt
Alkali in common seepweed seeds oil crude fat content account for 23.46%, be higher than soybean (crude fat content 18.80%), be good plant
Oil sources can be used as good protein sources, vitamin in the fluffy stem leaf extract of saline-alkali land since its crude protein content is also higher
Content is higher, in addition, the chemotrophy ingredient of the fluffy seed of saline-alkali land and the fluffy cauline leaf of saline-alkali land is complete and enriches.
The comparison of table 2 and table 5 can be seen that salt-soda soil common seepweed seeds oil Mineral Elements potassium and the content of sodium is the abundantest,
This is related with the saline-alkali environment that it grows, close with human health in salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land
It is higher to cut the constituent contents such as relevant iron, calcium, zinc, copper, manganese, it is seen then that the fluffy seed of saline-alkali land and the fluffy cauline leaf of saline-alkali land are one
Kind good mineral matter nutritional source, in addition, also contain selenium in the common seepweed seeds oil of salt-soda soil, it is micro that selenium by scientist is referred to as human body
" king of anti-cancer " in element therefore develops the fluffy seed of saline-alkali land and can be the mankind using the selenium contained by the fluffy seed of saline-alkali land
Bring high value medical health care.
The comparison of table 3 and table 6, which can be seen that in salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land, contains 18
Middle amino acid, rich content, it is necessary to which amino acid composition is complete, and wherein it is total to account for amino acid for the fluffy seed essential amino acids content of saline-alkali land
The 36.44% of amount is higher than FAO mode (36.00%), while the ratio between the fluffy seed essential amino acid of saline-alkali land and nonessential amino acid
It (E/N) is 0.573, also above FAO mode (0.56), it is seen then that the fluffy seed albumen of alkali belongs to quality plant albumen；The fluffy stem of saline-alkali land
It is 35.5% that essential amino acids content, which accounts for total amino acid content, in leaf, the reference model (36%) proposed close to FAO, it is necessary to amino acid
Ratio with nonessential amino acid is 55.1%, the reference model (0.56) proposed close to FAO；In addition, the research discovery fluffy seed of alkali
The common seepweed seeds oil obtained after processing is refined has the physicochemical property of general edible oil, and it is next to can be used as a kind of new edible oil
Exploitation, it is rich in unsaturated fatty acid in addition, and especially linoleic acid content is higher than many plants, it can be seen that, common seepweed seeds oil is one
Kind of vegetable oil new resources containing high linoleic acid, have important a nutrition health-care functions and biggish Development volue, in common seepweed seeds oil
Rich in unsaturated fatty acid, total unsaturated fatty acid content is up to 90.65%, and wherein linoleic acid content accounts for 68.74%, is current
It was found that one of the higher oil sources of linoleic acid content, physical and chemical index also substantially conforms to edible oil standard, is a kind of ideal
The good material of edible health-care oil and preparation conjugated linoleic acid.
By above-mentioned analysis it is found that the nutritional ingredient being rich in by the fluffy seed of saline-alkali land and the fluffy stem and leaf part of saline-alkali land
It is biased to difference, the present invention can be made by deploying salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land in proportion
Have the health drink of anti-aging skin-care functional, fluffy middle the be rich in nutritional ingredient effect of alkali is maximized, maximum limit
Degree plays the fluffy edible value of saline-alkali land.
The detection of every physical and chemical index:
The health drink with anti-aging skin-care functional of the preparation of preparation method described in Example, by GB/
T12143.1, GB8537-1995, GB4789 examination criteria compare indices, the results are shown in Table 7.
Table 7 has the health drink indices of anti-aging skin-care functional
It is visible each with the health drink with anti-aging skin-care functional according to prepared by the present invention by 1 result of table
Item main indicator is all satisfied requirements of the national standard.
In order to determine the solid-liquid ratio in the fluffy stem leaf extract preparation process of alkali, the present invention is directed to the feed liquid of alkali fluffy cauline leaf and water
Than carrying out experimental study, liquid-solid ratio is obtained to the influence diagram of the fluffy pigment extraction effect of alkali, as shown in Figure 1, as shown in Figure 1, with
The absorbance of the increase of liquid-solid ratio, pigment solution gradually rises, and when liquid-solid ratio is 40:1, light absorption value is significantly increased, and obtains alkali
Fluffy pigment recovery rate also significantly increases, and when liquid-solid ratio is greater than 40:1, curve tends towards stability, and absorbance changes less, and synthesis is examined
Consider energy-saving and emission-reduction, selects liquid-solid ratio for 40:1 (mL/g).
On the basis of above-mentioned single factor experiment, solid-liquid ratio, 4 cellulase, vitamin C and ultrasonic power factors are chosen
Box-Behnken design is carried out, the maximum value of polyphenol content in the fluffy stem leaf extract of alkali is studied, the results are shown in Table 8:
8 Box-Behnken experimental design scheme of table and result
Regression fit is carried out to 8 test data of table using 8.0 design software of Design-Expert, obtains polyphenol content pair
Solid-liquid ratio, cellulase, 4 factors of vitamin C and ultrasonic power secondary multinomial regression model:
Polyphenol content=5.55+0.13A+0.19B+0.32C+0.19D-0.33A2-0.39B2-0.28C2-0.96D2
9 response surface design quadratic regression equation model the results of analysis of variance of table
Note: * significant difference p < 0.05；The extremely significant p < 0.01 of * difference.
Make response surface figure according to regression equation, investigate the shape of be fitted response surface, analysis solid-liquid ratio, cellulase,
Fig. 2 is met personally in the influence of vitamin C and ultrasonic power to polyphenol content, response.As shown in Table 9, mutation model p value < 0.0001,
Reach extremely significant level, illustrates that the models fitting degree is fine.It as shown in Figure 2, is 1:50, cellulase 3%, dimension in solid-liquid ratio
Raw element C 0.05%, ultrasonic power 125w, polyphenol content reach peak, and the result and experiment of single factor result one
It causes.
It is above-mentioned the experimental results showed that, the present invention passes through ultrasonic wave auxiliary, aqueous enzymatic extraction and ultrafiltration technology triple combination pole
It is big remain alkali it is fluffy in water-soluble functional components, the fluffy middle polyphenols recovery rate of alkali mentions compared to traditional extraction process
Rate is taken to improve 30%-70%, the fluffy polyphenol recovery rate of alkali of the invention may be up to 5.9%, the polyphenol in the fluffy stem leaf extract of alkali
Substance has very strong inoxidizability, can promote the smoothness of skin, and U.S. face skin is removed the free radical that human body generates, prolonged
Slow skin aging, inhibits the decomposition of collagen, plays crease-resistant function, conjugated linoleic acid that common seepweed seeds oil is rich in, selenium and
The nutrients such as flavone compound are combined with jujube, adlay, donkey-hide gelatin, lily, tremella, aloe in ingredient, are supported with beauty
Face, crease-resistant macrobiosis, recuperating qi-blood, the comprehensive and balanced feature of nutrition are suitable for vast female consumer, support especially for beauty
Face, crease-resistant macrobiosis have significant health-care effect.
Health drink clinical observation data produced by the present invention with anti-aging skin-care functional is as follows:
Liu XX, female, 45 years old, face was dark and gloomy, withered and yellow, dry, there is blocky spot, has successively tried out a few money plaque dispelling skin cares and has produced
Product, but health drink of the present invention all is drunk without effect, 3 times a day, each 220ml adheres to after taking 6 weeks, color spot on the face
Obvious thin out, the colour of skin is ruddy.
Lee XX, female, 47 years old, the colour of skin was dark yellow, and sleep insufficiency with menopause symptom, tried several beauty products, effect
It is unobvious, health drink of the present invention is drunk, 3 times a day, each 220ml adheres to after taking 2 months, and the exquisiteness that skin becomes is pale,
Sleep also makes moderate progress.
Pueraria lobota XX, female 35 years old, cutis laxa was sagging, and the colour of skin is obscure, drank health drink of the present invention, 3 times a day, every time
220ml adheres to after taking 2 months that skin becomes tight, and complexion is ruddy.
Part not in the detailed description of the invention is the prior art.
Claims (5)
1. a kind of health drink and preparation method thereof with anti-aging skin-care functional, it is characterized in that: including following step
It is rapid:
The fluffy stem leaf extract preparation of saline-alkali land:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, is put into guarantor's food peace food purifying machine and cleans 1 time~3 times, go
Except impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper and be cut into every section of cm of 1 cm~2；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, using colloid mill mashing handle to
30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 to 60 mesh~200 mesh using high-accuracy Wet ultrafine grinding equipment；
Step 5, smashed material is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment, by feed liquid mass ratio 1:20~
1:50 adds deionized water, adds 2%~4%(w/w) cellulase, 0.05%~0.08% vitamin C, 20 min of enzymolysis time is added
~30 min, 30 DEG C~50 DEG C of hydrolysis temperature, the ultrasonic power w of 50 w~200, extraction time is 1~2 time, merges extraction
Liquid；
Step 6, the leaching liquor of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, it is standby obtains the fluffy stem leaf extract of saline-alkali land
With；
The preparation of salt-soda soil common seepweed seeds oil:
Step 7, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened, removed
Soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is less than after screening
0.1%；
Step 8, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature is
40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 9, the fluffy seed of saline-alkali land is crushed with pulverizer after vacuum drying, being crushed to mesh number is 60 mesh to 150 mesh；
Step 10, the fluffy powder of seeds of saline-alkali land is subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, a fraction
It is 8-10MPa from kettle pressure, the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, the second-order separation kettle
Temperature is regulated to 35 DEG C, extraction time 2.5h-4.5h；
Step 11, the isolate in level-one separating still and the second-order separation kettle is collected, is evaporated in isolate using spiral evaporator
Ethyl alcohol, then under the conditions of 40 DEG C in a vacuum drying oven further removal ethyl alcohol；
Step 12, point of the isolate in level-one separating still and the second-order separation kettle after step 5 removes ethyl alcohol, in level-one separating still
From object directly as salt-soda soil common seepweed seeds oil, the isolate in the second-order separation kettle is centrifuged with centrifuge, and centrifugal rotational speed is
30r/min -50r/min, centrifugation time 20min take upper layer oil reservoir, the saline-alkali land being incorporated in level-one separating still after collection
In fluffy seed oil, it is spare that salt-soda soil common seepweed seeds oil is obtained after mixing；
Step 13, it carries out the fluffy stem leaf extract of saline-alkali land and salt-soda soil common seepweed seeds oil to mix to obtain mixing according to the ratio of 10:1
Liquid A；
Step 14, jujube 35%, adlay 22%, donkey-hide gelatin 8%, lily 15%, tremella 10%, aloe 10% are taken, is cleaned, is crushed, after mixing,
2-3h is added water to cook, residue is filtered, takes supernatant to obtain extracting solution B spare；
Step 15, by mixed liquor A made from step 13 and step 14, extracting solution B and water, honey according to 1:1.2:0.4 ratio
It is mixed to prepare mixed liquor C；
Step 16, mixed liquor C carries out coarse filtration, ultrafiltration by reverse osmosis unit, and sterile filling to obtain the final product.
2. the health drink and preparation method thereof according to claim 1 with anti-aging skin-care functional, special
Sign is: its mineral composition of the fluffy stem leaf extract of the alkali and content are as follows: 2985 μ g/L of μ g/L~5200 of Ca2+, Mg2
+ 1743 μ g/L of μ g/L~2791,162 the Fe2+ μ g/L of μ g/L~185,5.11 Mn2+ μ g/L of μ g/L~8.03, Zn+
The 5.27 μ g/L of μ g/L~8.51,0.8 the K+ μ g/L of μ g/L~3.0,1746 Na+ μ g/L of μ g/L~6899, dissolubility are total
200 μ of μ g/L~400 g/L of solid.
3. the health drink and preparation method thereof according to claim 1 with anti-aging skin-care functional, special
Sign is: reverse osmosis unit system configuration described in step 6 and step 16 are as follows: pretreatment system, smart filtration system, corollary system；
Pretreatment system is made of mechanical filter, adsorption filter, cartridge filter；Smart filtration system is by hollow-fibre ultrafiltration device
Composition；Corollary system is made of water purification pot, electrical control system；Mechanical filter filtering can remove body refuse and fibre in extracting solution
Dimension etc., after through adsorption filter filtering can remove oil removal, however it is miscellaneous to remove algae etc. through mechanical filter filtering
Matter.
4. the health drink and preparation method thereof according to claim 3 with anti-aging skin-care functional, special
Sign is: ultrafiltration described in step 6 and step 16 is hollow-fibre membrane ultrafiltration to remove the microorganisms such as bacterium in extracting solution, mould.
5. the health drink and preparation method thereof according to claim 3 or 4 with anti-aging skin-care functional,
Be characterized in: the hollow-fibre membrane diameter is 0.01 μm~0.001 μm, and feed rate is the L/h of 900 L/h~1500, pressure
The Mpa of 0.045 Mpa~0.18, feed concentration be the 200 μ g/L of μ g/L~400, ultrafiltration time 100 min~400 min, instead
Wash period 10 min~40 min, backwash time 20 min~120 min, upper operation 10 min~40 min, 20 s of upper backwash
~120 s, lower operation 10 min~40 min, lower backwash 20 s~120 s.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112889970A (en) * | 2021-01-14 | 2021-06-04 | 黄祥 | Preparation process and equipment of seed tea |
| CN115517306A (en) * | 2021-01-23 | 2022-12-27 | 辽宁海水碱蓬生物科技有限公司 | Saline-alkali soil tea |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074405A (en) * | 2007-07-13 | 2007-11-21 | 杨庆利 | Extraction of common seepweed seeds oil by supercritical CO2 fluid |
| CN105029632A (en) * | 2015-07-30 | 2015-11-11 | 潍坊友容实业有限公司 | Suaeda salsa fermented beverage and preparation method thereof |
| CN106071555A (en) * | 2016-06-27 | 2016-11-09 | 青岛铭晨信息技术有限公司 | A kind of Herba suadeae glaucae health beverage with function of delaying senility |
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2017
- 2017-11-22 CN CN201711169445.2A patent/CN109805226A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074405A (en) * | 2007-07-13 | 2007-11-21 | 杨庆利 | Extraction of common seepweed seeds oil by supercritical CO2 fluid |
| CN105029632A (en) * | 2015-07-30 | 2015-11-11 | 潍坊友容实业有限公司 | Suaeda salsa fermented beverage and preparation method thereof |
| CN106071555A (en) * | 2016-06-27 | 2016-11-09 | 青岛铭晨信息技术有限公司 | A kind of Herba suadeae glaucae health beverage with function of delaying senility |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112889970A (en) * | 2021-01-14 | 2021-06-04 | 黄祥 | Preparation process and equipment of seed tea |
| CN115517306A (en) * | 2021-01-23 | 2022-12-27 | 辽宁海水碱蓬生物科技有限公司 | Saline-alkali soil tea |
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