CN109745264A - A kind of preparation method of the mild moisturiser of no anti-corrosion addition - Google Patents
A kind of preparation method of the mild moisturiser of no anti-corrosion addition Download PDFInfo
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- CN109745264A CN109745264A CN201910232147.6A CN201910232147A CN109745264A CN 109745264 A CN109745264 A CN 109745264A CN 201910232147 A CN201910232147 A CN 201910232147A CN 109745264 A CN109745264 A CN 109745264A
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Abstract
The present invention relates to technical field of daily necessities, and in particular to a kind of preparation method for the mild moisturiser that no anti-corrosion is added cooperates sodium hydroxide and purslane extract that a kind of mild moisturiser that no anti-corrosion is added is prepared using oily mutually with water phase as raw material.Have the characteristics that excellent biodegradability and natural, mild, safety, be suitable for various types of skins, there is brilliant emulsifying capacity, emulsification system is stablized, and has liquid crystal characteristic, can generate sparkling and crystal-clear bright lotion, soft to moisten.
Description
Technical field
The present invention relates to technical field of daily necessities, and in particular to a kind of preparation side of the mild moisturiser of no anti-corrosion addition
Method.
Background technique
For the purpose of cosmetics preservative refers to the growth and breeding to inhibit microorganism in cosmetics and in cosmetics
The substance of addition.Cosmetics preservative has different mode classifications.Common cosmetics preservative has benzyl alcohol, benzoic acid, water
The substances such as poplar acid, boric acid, sorbic acid and other alcohols, aldehydes.The effect of Determination of Preservatives in Cosmetics mainly inhibits microorganism
Growth and breeding, keep cosmetics property stablize, be unlikely to deteriorate after making its use of uncapping, extend the holding time.Moisture compared with
Demand of more cosmetics to preservative is larger, such as toner, lotion；And closer to ointment or the cosmetics of wax, micro- life
Object is more difficult to survive, and the demand to preservative is relatively small.It is compounded in Cosmetic Manufacture usually using several preservatives, from
And reaches and expand antibacterial range, improves drug effect, anti-secondary pollution and other effects.Preservative in cosmetics can generate 100% work
Property oxygen, is one of arch-criminal of skin aging, how to avoid being a technical problem to be solved urgently in cosmetics using preservative.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of preparation method of the mild moisturiser of no anti-corrosion addition.
Specific technical solution is as follows:
A kind of preparation method of the mild moisturiser of no anti-corrosion addition, using oily mutually with water phase as raw material, cooperation sodium hydroxide
And purslane extract, specific preparation process is as follows:
(1) oil mixes the preparation of liquid
By cetearyl glucoside, cetostearyl alcohol, stearic acid, dimethyl silicone polymer, saualane, sad glycerol three
Ester or Triglyceride DDD, isononyl isononanoate, tocopherol acetate, glycerol caprylate, decoyl hydroximic acid are put into container and stir
Mix be heated to 80-85 DEG C oily mix liquid；
(2) preparation of water phase mixed liquor
Deionized water, moisturizer are put into another container, 80-85 DEG C is heated with stirring to and obtains water phase mixed liquor；
(3) oil that step (1) obtains is mixed liquid to be added in the water phase mixed liquor that step (2) obtains, at 80-85 DEG C
Stirring, is emulsified homogeneous, is cooled to 60-65 DEG C, and sodium hydroxide is added, and is cooled to 40-45 DEG C, and anti-sensitizer is added, and stirring is equal
It is even, it is cooled to 30-40 DEG C of discharging, obtains moisturiser product.
Step (1) the cetearyl glucoside concentration is 1.5-3mol/L, and cetearyl alcohol determining alcohol is 1.5-3mol/
L, stearic acid 1-2mol/L, dimethyl silicone polymer 1-4mol/L, saualane 2-6mol/L, acid glycerol three ester or capric acid glycerol three
Ester 4-8mol/L, isononyl isononanoate 1-5mol/L, tocopherol acetate 0.1-0.5mol/L, glycerol caprylate 0.1-
0.3mol/L, decoyl hydroximic acid 0.1-0.3mol/L.
Step (2) moisturizer is 0.1-0.3moL/L carbomer, 5-10moL/L glycerol, 2-4moL/L 1,3 the third two
Alcohol, 0.1-0.5moL/L Phosphoric acid monohexadecyl ester potassium.
Step (3) the sodium hydroxide molar concentration is 0.01-0.05mol/L.
Step (3) anti-sensitizer is 1-2mol/L purslane extract.
Compared with prior art, the present invention has following advantageous effects:
(1) effect of primary raw material of the present invention:
Glycerol caprylate: pure natural glyceride type multifunctional replacement preservative, the mildness of skin is preferable, wide spectrum it is micro-
Biostatic agent, product stability is high, there is long-term fungistatic effect, while also having the effect of moisturizing, moisturizing, emulsification Sage Extract.
Decoyl hydroximic acid: there is preservative efficacy, but be not listed among preservative.
Phosphoric acid monohexadecyl ester potassium: small to the irritation of skin, similar natural phospholipid, is more mild surfactant.
It is a kind of excellent oil-in-water emulsifiers, there is foaminess abundant, the cleaning strength of good emulsibility and appropriateness.Physics and
Stable chemical performance, salt tolerant is alkaline-resisting, and high temperature resistance is good, and biodegradability is good.
Cetearyl glucoside, cetostearyl alcohol: as emulsifier, emulsion stabilizer.
This product system nonionic glycosyl emulsifier, with excellent biodegradability and natural, mild, safety spy
Point is suitable for various types of skins.With brilliant emulsifying capacity, emulsification system is stablized, has liquid crystal characteristic, can generate crystalline substance
The bright lotion of jade-like stone, it is soft, it moistens.Compatibility is strong.Emulsifying process is simple, easy to operate.
Specific embodiment
The following describes the present invention in detail with reference to examples, but protection scope of the present invention is not limited by embodiment.
Embodiment 1:
A kind of preparation method of the mild moisturiser of no anti-corrosion addition, using oily mutually with water phase as raw material, cooperation sodium hydroxide
And purslane extract, specific preparation process is as follows:
(1) oil mixes the preparation of liquid
By cetearyl glucoside, cetostearyl alcohol, stearic acid, dimethyl silicone polymer, saualane, sad glycerol three
Ester, isononyl isononanoate, tocopherol acetate, glycerol caprylate, decoyl hydroximic acid are put into container for stirring and are heated to 80 DEG C
Oil mixes liquid；
(2) preparation of water phase mixed liquor
Deionized water, moisturizer are put into another container, 80 DEG C is heated with stirring to and obtains water phase mixed liquor；
(3) oil that step (1) obtains is mixed liquid to be added in the water phase mixed liquor that step (2) obtains, is stirred at 80 DEG C
It mixes, homogeneous, emulsified, be cooled to 60 DEG C, sodium hydroxide is added, be cooled to 40 DEG C, anti-sensitizer is added, stirs evenly, cool down
It discharges to 30 DEG C, obtains moisturiser product.
Step (1) the cetearyl glucoside concentration is 1.5mol/L, and cetearyl alcohol determining alcohol is 1.5mol/L, firmly
Resin acid 1mol/L, dimethyl silicone polymer 1mol/L, saualane 2mol/L, Trivent OCG 4mol/L, isononyl isononanoate
1mol/L, tocopherol acetate 0.1mol/L, glycerol caprylate 0.1mol/L, decoyl hydroximic acid 0.1mol/L.
Step (2) moisturizer is 0.1moL/L carbomer, 5moL/L glycerol, 2moL/L1,3 propylene glycol, 0.1moL/L
Phosphoric acid monohexadecyl ester potassium.
Step (3) C is sodium hydroxide, molar concentration 0.01mol/L.
Step (3) anti-sensitizer is 1mol/L purslane extract.
Embodiment 2
A kind of preparation method of the mild moisturiser of no anti-corrosion addition, using oily mutually with water phase as raw material, cooperation sodium hydroxide
And purslane extract, specific preparation process is as follows:
(1) oil mixes the preparation of liquid
By cetearyl glucoside, cetostearyl alcohol, stearic acid, dimethyl silicone polymer, saualane, capric acid glycerol three
Ester, isononyl isononanoate, tocopherol acetate, glycerol caprylate, decoyl hydroximic acid are put into container for stirring and are heated to 82 DEG C
Oil mixes liquid；
(2) preparation of water phase mixed liquor
Deionized water, moisturizer are put into another container, 82 DEG C is heated with stirring to and obtains water phase mixed liquor；
(3) oil that step (1) obtains is mixed liquid to be added in the water phase mixed liquor that step (2) obtains, is stirred at 82 DEG C
It mixes, homogeneous, emulsified, be cooled to 62 DEG C, sodium hydroxide is added, be cooled to 42 DEG C, anti-sensitizer is added, stirs evenly, cool down
It discharges to 35 DEG C, obtains moisturiser product.
Step (1) the cetearyl glucoside concentration is 2mol/L, and cetearyl alcohol determining alcohol is 2mol/L, stearic acid
1.5mol/L, dimethyl silicone polymer 2mol/L, saualane 4mol/L, Triglyceride DDD 6mol/L, isononyl isononanoate
3.5mol/L, tocopherol acetate 0.3mol/L, glycerol caprylate 0.2mol/L, decoyl hydroximic acid 0.2mol/L.
Step (2) moisturizer is 0.2moL/L carbomer, 6moL/L glycerol, 3moL/L1,3 propylene glycol, 0.3moL/L
Phosphoric acid monohexadecyl ester potassium.
Step (3) the sodium hydroxide molar concentration is 0.03mol/L.
Step (3) anti-sensitizer is 1.5mol/L purslane extract.
Embodiment 3
A kind of preparation method of the mild moisturiser of no anti-corrosion addition, using oily mutually with water phase as raw material, cooperation sodium hydroxide
And purslane extract, specific preparation process is as follows:
(1) oil mixes the preparation of liquid
By cetearyl glucoside, cetostearyl alcohol, stearic acid, dimethyl silicone polymer, saualane, sad glycerol three
Ester, isononyl isononanoate, tocopherol acetate, glycerol caprylate, decoyl hydroximic acid are put into container for stirring and are heated to 85 DEG C
Oil mixes liquid；
(2) preparation of water phase mixed liquor
Deionized water, moisturizer are put into another container, 85 DEG C is heated with stirring to and obtains water phase mixed liquor；
(3) oil that step (1) obtains is mixed liquid to be added in the water phase mixed liquor that step (2) obtains, is stirred at 85 DEG C
It mixes, homogeneous, emulsified, be cooled to 65 DEG C, sodium hydroxide is added, be cooled to 45 DEG C, anti-sensitizer is added, stirs evenly, cool down
It discharges to 40 DEG C, obtains moisturiser product.
Step (1) the cetearyl glucoside concentration is 3mol/L, and cetearyl alcohol determining alcohol is 3mol/L, stearic acid
2mol/L, dimethyl silicone polymer 4mol/L, saualane 6mol/L, Trivent OCG 8mol/L, isononyl isononanoate 5mol/
L, tocopherol acetate 0.5mol/L, glycerol caprylate 0.3mol/L, decoyl hydroximic acid 0.3mol/L.
Step (2) moisturizer is 0.3moL/L carbomer, 10moL/L glycerol, 4moL/L1,3 propylene glycol, 0.5moL/
L Phosphoric acid monohexadecyl ester potassium.
Step (3) the sodium hydroxide molar concentration is 0.05mol/L.
Step (3) anti-sensitizer is 2mol/L purslane extract.
100 people are randomly selected, moisture of skin is carried out using German CK moisture of skin tester Corneometer CM825 and is contained
Measure examination, with above-described embodiment 1-3 and and commercially available moisturiser 1,2 be applied to 100 30-40 years old dry skins or firmly believe tool
There is the inner forearm of the women user of dry skin, embodiment 1-3 is as shown in table 1 using rear mean skin moisture content:
1 embodiment 1-3 of table uses rear skin moisture content
Seen from table 1,30 minutes skin moisture content ratios use commercially available guarantor after the moisturiser using embodiment 1-3
Skin moisture content has very big promotion after wet frost, and using 4-8 hours latter, the skin moisture content of commercially available moisturiser just has significantly
It falls after rise, and uses 4-8 after the moisturiser of the embodiment of the present invention 1-3, skin moisture content remains at a higher level, do not have
There is apparent falling.Furthermore after the moisturiser of the embodiment of the present invention 1-3 user's skin without allergic reaction.As it can be seen that of the invention
Moisturiser can safely, persistently, efficiently be skin moisture-keeping.
Claims (5)
1. a kind of preparation method of the mild moisturiser of no anti-corrosion addition, it is characterised in that: using oily mutually with water phase as raw material, cooperation
Sodium hydroxide and purslane extract, specific preparation process is as follows:
(1) oil mixes the preparation of liquid
By cetearyl glucoside, cetostearyl alcohol, stearic acid, dimethyl silicone polymer, saualane, Trivent OCG or
Triglyceride DDD, isononyl isononanoate, tocopherol acetate, glycerol caprylate, decoyl hydroximic acid are put into container for stirring and add
Heat to 80-85 DEG C oily mix liquid；
(2) preparation of water phase mixed liquor
Deionized water, moisturizer are put into another container, 80-85 DEG C is heated with stirring to and obtains water phase mixed liquor；
(3) oil that step (1) obtains is mixed liquid to be added in the water phase mixed liquor that step (2) obtains, is stirred at 80-85 DEG C
It mixes, homogeneous, emulsified, be cooled to 60-65 DEG C, sodium hydroxide is added, be cooled to 40-45 DEG C, anti-sensitizer is added, stirring is equal
It is even, it is cooled to 30-40 DEG C of discharging, obtains moisturiser product.
2. the preparation method of the mild moisturiser of no anti-corrosion addition according to claim 1, it is characterised in that: step (1)
The cetearyl glucoside concentration is 1.5-3mol/L, and cetearyl alcohol determining alcohol is 1.5-3mol/L, stearic acid 1-2mol/
L, dimethyl silicone polymer 1-4mol/L, saualane 2-6mol/L, acid glycerol three ester or Triglyceride DDD 4-8mol/L, different nonyl
Acid different nonyl ester 1-5mol/L, tocopherol acetate 0.1-0.5mol/L, glycerol caprylate 0.1-0.3mol/L, decoyl hydroximic acid
0.1-0.3mol/L。
3. the preparation method of the mild moisturiser of no anti-corrosion addition according to claim 1, it is characterised in that: step (2)
The moisturizer is 0.1-0.3moL/L carbomer, 5-10moL/L glycerol, 2-4moL/L1,3 propylene glycol, 0.1-0.5moL/L whale
Ceryl alcohol phosphate potassium.
4. the preparation method of the mild moisturiser of no anti-corrosion addition according to claim 1, it is characterised in that: step (3)
The sodium hydroxide molar concentration is 0.01-0.05mol/L.
5. the preparation method of the mild moisturiser of no anti-corrosion addition according to claim 1, it is characterised in that: step (3)
The anti-sensitizer is 1-2mol/L purslane extract.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910232147.6A CN109745264A (en) | 2019-03-26 | 2019-03-26 | A kind of preparation method of the mild moisturiser of no anti-corrosion addition |
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| CN201910232147.6A CN109745264A (en) | 2019-03-26 | 2019-03-26 | A kind of preparation method of the mild moisturiser of no anti-corrosion addition |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130074983A (en) * | 2011-12-27 | 2013-07-05 | 주식회사 제닉 | Composition of preservatives for cosmetic and cosmetic composition comprising the same |
| CN107213040A (en) * | 2017-07-19 | 2017-09-29 | 郑生华 | A kind of natural no added camellia moisturiser and preparation method thereof |
| CN107669500A (en) * | 2017-11-28 | 2018-02-09 | 广州市花安堂生物科技有限公司 | A kind of moisturizing elite breast and preparation method thereof |
| CN108078841A (en) * | 2017-12-25 | 2018-05-29 | 陕西佰傲再生医学有限公司 | A kind of moisturiser of preservative free and preparation method thereof |
| CN108703930A (en) * | 2018-08-26 | 2018-10-26 | 福建乐伴护理用品有限公司 | A kind of moisturiser and preparation method thereof containing Abelmoschus Esculentus Linn extract |
-
2019
- 2019-03-26 CN CN201910232147.6A patent/CN109745264A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130074983A (en) * | 2011-12-27 | 2013-07-05 | 주식회사 제닉 | Composition of preservatives for cosmetic and cosmetic composition comprising the same |
| CN107213040A (en) * | 2017-07-19 | 2017-09-29 | 郑生华 | A kind of natural no added camellia moisturiser and preparation method thereof |
| CN107669500A (en) * | 2017-11-28 | 2018-02-09 | 广州市花安堂生物科技有限公司 | A kind of moisturizing elite breast and preparation method thereof |
| CN108078841A (en) * | 2017-12-25 | 2018-05-29 | 陕西佰傲再生医学有限公司 | A kind of moisturiser of preservative free and preparation method thereof |
| CN108703930A (en) * | 2018-08-26 | 2018-10-26 | 福建乐伴护理用品有限公司 | A kind of moisturiser and preparation method thereof containing Abelmoschus Esculentus Linn extract |
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