CN103169627B - Tea oil moisturizer and preparation method thereof - Google Patents

Tea oil moisturizer and preparation method thereof Download PDF

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Publication number
CN103169627B
CN103169627B CN201110437406.2A CN201110437406A CN103169627B CN 103169627 B CN103169627 B CN 103169627B CN 201110437406 A CN201110437406 A CN 201110437406A CN 103169627 B CN103169627 B CN 103169627B
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parts
oil
preparation
raw material
stearic acid
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CN103169627A (en
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李加兴
李敬业
陈双平
张娟
孙金玉
黄诚
张朝晖
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HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co Ltd
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HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co Ltd
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Abstract

The invention discloses a tea oil moisturizer and a preparation method of the tea oil moisturizer. The tea oil moisturizer is characterized by being prepared from the following materials and steps that: the materials include 5-15 parts of tea oil, 1-4 parts of glycerin monostearate, 0.5-1.5 parts of methl glucse sesquistearate, 1-2 parts of polyoxyethylene stearates, 12-18 parts of white oil, 3-6 parts of isopropyl palmitate, 2-4 parts of isopropyl myristate, 2-3 parts of caprylic/capric triglyceride, 2 parts of stearic acid, 0.5-2 parts of cetostearyl alcohol, 0.2 part of methylparaben, 0.1 part of propylparaben, 2 parts of glycerol, 2-3 parts of glyceryl polymethacrylate, 0.3-0.5 part of triethanolamine, 0.2 part of diazolidinyl urea, and 0.15 part of essence; and the steps include preparing an oil phase, preparing a water phase, emulsifying, cooling, aging and bulking to form the product. The tea oil moisturizer is mainly applied to cosmetics and preparation of the cosmetics.

Description

A kind of tea oil moisturizer and preparation method thereof
Technical field
The present invention relates to a kind of tea oil moisturizer and preparation method thereof.
Background technology
Along with improving constantly of the current living standard of people, take natural plant extracts as the main flow that the cosmetics of primary raw material have become market comsupton, consumption figure increases year by year.Oleum Camelliae is rich in oleic acid, linoleic acid, can form hydrophobic film at skin surface, while imparting skin emolliency, lubrication and glossiness, effectively can also prevent the intrusion of harmful environmental material; The evaporation of moisture can be suppressed, prevent chapped skin, make the horny layer of dry skin and sclerosis rehydrated, recover cuticular softness and elasticity, make skin smooth, soft and moist and there is elasticity, keep the health status that skin is good.Oleum Camelliae also containing higher natural Vitamin E, has good non-oxidizability and the ability of scavenging activated oxygen, skin can be protected to preserve from; Important polyphenoils and membrane stabilizer in vitamin E or cell membrane, have expansion blood capillary, improve sanguimotor effect.Therefore, Oleum Camelliae, as a kind of desirable skin care item component, will become a kind of important natural material of cosmetics industry.
Summary of the invention
The object of the present invention is to provide a kind of tea oil moisturizer and preparation method thereof, to meet the demand of people to the cosmetics that natural plant extracts is primary raw material.
For achieving the above object, technical solution of the present invention is: a kind of preparation method of tea oil moisturizer, it is characterized in that it is made up of following raw material and step, and the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part, (2) glyceryl monostearate 1-4 part,
(3) methyl glucoside sesqui-stearate 0.5-1.5 part,
(4) polyoxyethylene stearic acid ester 1-2 part,
(5) white oil 12-18 part, (6) isopropyl palmitate 3-6 part,
(7) isopropyl myristate 2-4 part, (8) caprylic capric triglyceride 2-3 part,
(9) stearic acid 2 parts, (10) cetostearyl alcohol 0.5-2 part,
(11) methyl hydroxybenzoate 0.2 part, (12) propylparaben 0.1 part,
(13) glycerol 2 parts, (14) polyglycerolmethacrylate 2-3 part,
(15) triethanolamine 0.3-0.5 part, (16) two imidazolidinyl urea 0.2 part,
(17) 0.15 part, essence;
Described each step is as follows:
A. the preparation of oil phase, the Oleum Camelliae of aforementioned proportion and other Oil soluble materials glyceryl monostearates, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, caprylic capric triglyceride, stearic acid, cetostearyl alcohol, polyglycerolmethacrylate mix and blend are heated to 70-75 DEG C, make it fully melt or dissolve stand-by;
B. the preparation of aqueous phase, adds in deionized water by the water-soluble material glycerol of aforementioned proportion, triethanolamine, is heated with stirring to 90-100 DEG C, keeps sterilizing in 20 minutes, be then cooled to 70-80 DEG C stand-by;
C. emulsifying, after above-mentioned oil phase and Aqueous Phase Raw Material are filtered respectively, add in emulsifying pot by water order after first oil, stir at temperature 70-80 DEG C, after oil, Aqueous Phase Raw Material are fully mixed into emulsion, add parabens, two imidazolidinyl urea antiseptic again, stir, namely complete emulsification procedure;
D. cool, after the emulsifying obtained by step C, raw material is cooled to 50-60 DEG C, adds essence, then stirs 5 minutes, continues to cool to 35-40 DEG C of discharging;
E. ageing and fill, is discharged in storage container, is placed in ageing between storage cream and is no less than 48 hours, through carrying out fill after the assay was approved.
The tea oil moisturizer prepared of method as described herein.
The invention has the beneficial effects as follows: the moistening that the present invention has skin according to Oleum Camelliae, protection, anti-aging active, emulsion dispersion is carried out by adding the compositions such as emulsifying agent, antiseptic, thickening agent, essence, prepare a kind of tea oil moisturizer, skin moisturizing, moisturizing, smooth can be made.
Detailed description of the invention
Below in conjunction with embodiment, the present invention and detailed description of the invention thereof are described in further detail.The invention is characterized in that it is made up of following raw material and step, the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part, (2) glyceryl monostearate 1-4 part,
(3) methyl glucoside sesqui-stearate 0.5-1.5 part,
(4) polyoxyethylene stearic acid ester 1-2 part,
(5) white oil 12-18 part, (6) isopropyl palmitate 3-6 part,
(7) isopropyl myristate 2-4 part, (8) caprylic capric triglyceride 2-3 part,
(9) stearic acid 2 parts, (10) cetostearyl alcohol 0.5-2 part,
(11) methyl hydroxybenzoate 0.2 part, (12) propylparaben 0.1 part,
(13) glycerol 2 parts, (14) polyglycerolmethacrylate 2-3 part,
(15) triethanolamine 0.3-0.5 part, (16) two imidazolidinyl urea 0.2 part,
(17) 0.15 part, essence;
Described each step is as follows:
A. the preparation of oil phase, the Oleum Camelliae of aforementioned proportion and other Oil soluble materials glyceryl monostearates, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, caprylic capric triglyceride, stearic acid, cetostearyl alcohol, polyglycerolmethacrylate mix and blend are heated to 70-75 DEG C, make it fully melt or dissolve stand-by;
B. the preparation of aqueous phase, adds in deionized water by the water-soluble material glycerol of aforementioned proportion, triethanolamine, is heated with stirring to 90-100 DEG C, keeps sterilizing in 20 minutes, be then cooled to 70-80 DEG C stand-by;
C. emulsifying, after above-mentioned oil phase and Aqueous Phase Raw Material are filtered respectively, add in emulsifying pot by water order after first oil, stir at temperature 70-80 DEG C, after oil, Aqueous Phase Raw Material are fully mixed into emulsion, add parabens, two imidazolidinyl urea antiseptic again, stir, namely complete emulsification procedure;
D. cool, after the emulsifying obtained by step C, raw material is cooled to 50-60 DEG C, adds essence, then stirs 5 minutes, continues to cool to 35-40 DEG C of discharging;
E. ageing and fill, is discharged in storage container, is placed in ageing between storage cream and is no less than 48 hours, through carrying out fill after the assay was approved.
The tea oil moisturizer prepared of method as described herein.
Below provide embodiments of the invention
Example 1
The preparation of oil phase, by Oleum Camelliae 5 parts, glyceryl monostearate 1 part, methyl glucoside sesqui-stearate 0.5 part, 1 part, stearic acid polyoxyethylene fat, white oil (liquid paraffin) 16 parts, isopropyl palmitate 3 parts, isopropyl myristate 2 parts, caprylic capric grease 3 parts, stearic acid 2 parts, cetostearyl alcohol 2 parts, polyglycerolmethacrylate 3 parts, mix and blend is heated to 70 DEG C.Make it fully melt or dissolve stand-by;
The preparation of aqueous phase, by water-soluble material glycerol 2 parts, triethanolamine 0.3 part, adds deionized water 58.55 parts, is heated with stirring to 100 DEG C, keeps sterilizing in 20 minutes, be then cooled to 80 DEG C stand-by;
Emulsifying, after above-mentioned oil phase and Aqueous Phase Raw Material are filtered respectively (as centrifuge filters), add in emulsifying pot by the order of water after first oil, stir under temperature 70 C, after oil, Aqueous Phase Raw Material are fully mixed into emulsion, add antiseptic methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, two imidazolidinyl urea 0.2 part again, stir, namely complete emulsification procedure;
Cooling, is cooled to 60 DEG C by material after above-mentioned emulsifying, adds 0.15 part, essence, then stir 5 minutes, continue to cool to 35 DEG C of dischargings;
Ageing and fill, deliver in storage container by above-mentioned material, being placed in ageing between storage cream and being no less than 48 hours, to carrying out fill after the assay was approved, being product.
Example 2
The preparation of oil phase, Oleum Camelliae 10 parts, glyceryl monostearate 2 parts, methyl glucoside sesqui-stearate 1 part, 1.5 parts, stearic acid polyoxyethylene fat, white oil (liquid paraffin) 15 parts, isopropyl palmitate 4 parts, isopropyl myristate 3 parts, caprylic capric triglyceride 2.5 parts, stearic acid 2 parts, cetostearyl alcohol 1 part, polyglycerolmethacrylate 2.5 parts, mix and blend is heated to 72 DEG C.
The preparation of aqueous phase, glycerol 2 parts, triethanolamine 0.4 part, adds deionized water 52.45 parts, is heated with stirring to 95 DEG C, be then cooled to 75 DEG C;
Emulsifying, stirs at 75 DEG C in emulsifying pot;
Cooling, after emulsifying, material is cooled to 55 DEG C; Then be cooled to 38 DEG C of dischargings, all the other are with example 1.
Example 3
The preparation of oil phase, Oleum Camelliae 15 parts, glyceryl monostearate 4 parts, methyl glucoside sesqui-stearate 1.5 parts, 2 parts, stearic acid polyoxyethylene fat, white oil (liquid paraffin) 12 parts, isopropyl palmitate 6 parts, isopropyl myristate 4 parts, caprylic capric triglyceride 2 parts, stearic acid 2 parts, cetostearyl alcohol 0.5 part, polyglycerolmethacrylate 2 parts, mix and blend is heated to 75 DEG C.
The preparation of aqueous phase, glycerol 2 parts, triethanolamine 0.5 part, deionized water 45.85 parts, is heated with stirring to 90 DEG C, is then cooled to 70 DEG C.
Emulsifying, stirs at 80 DEG C in emulsifying pot;
Cooling, the material of emulsifying is cooled to 50 DEG C, and be then cooled to 40 DEG C of dischargings, all the other are with example 1.

Claims (2)

1. a preparation method for tea oil moisturizer, is characterized in that this emollient cream is made up of following raw material, and the weight proportion of each raw material is:
Oleum Camelliae 5-15 part, glyceryl monostearate 1-4 part,
Methyl glucoside sesqui-stearate 0.5-1.5 part,
Polyoxyethylene stearic acid ester 1-2 part,
White oil 12-18 part, isopropyl palmitate 3-6 part,
Isopropyl myristate 2-4 part, caprylic capric triglyceride 2-3 part,
Stearic acid 2 parts, cetostearyl alcohol 0.5-2 part,
Methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part,
Glycerol 2 parts, polyglycerolmethacrylate 2-3 part,
Triethanolamine 0.3-0.5 part, two imidazolidinyl urea 0.2 part,
0.15 part, essence;
Preparation process is as follows:
The preparation of A oil phase, by the Oleum Camelliae of aforementioned proportion and other Oil soluble materials: glyceryl monostearate, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, caprylic capric triglyceride, stearic acid, cetostearyl alcohol, polyglycerolmethacrylate mix and blend are heated to 70-75 DEG C, make it fully melt or dissolve stand-by;
The preparation of B aqueous phase, adds in deionized water by the water-soluble material glycerol of aforementioned proportion, triethanolamine, is heated with stirring to 90-100 DEG C, keeps sterilizing in 20 minutes, be then cooled to 70-80 DEG C stand-by;
C emulsifying, after above-mentioned oil phase and Aqueous Phase Raw Material are filtered respectively, add in emulsifying pot by water order after first oil, stir at temperature 70-80 DEG C, after oil, Aqueous Phase Raw Material are fully mixed into emulsion, add methyl hydroxybenzoate and propylparaben, two imidazolidinyl urea antiseptic again, stir, namely complete emulsification procedure;
D cools, and after the emulsifying obtained by step C, raw material is cooled to 50-60 DEG C, adds essence, then stirs 5 minutes, continues to cool to 35-40 DEG C of discharging;
E ageing and fill, be discharged in storage container, is placed in ageing between storage cream and is no less than 48 hours, through carrying out fill after the assay was approved.
2. the tea oil moisturizer prepared of the method for claim 1.
CN201110437406.2A 2011-12-23 2011-12-23 Tea oil moisturizer and preparation method thereof Active CN103169627B (en)

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Families Citing this family (9)

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Publication number Priority date Publication date Assignee Title
CN104207987A (en) * 2014-09-02 2014-12-17 杭州陶源秀化妆品厂 Mulberry leaf moisturizing body cream and preparation process thereof
CN104997674A (en) * 2015-07-09 2015-10-28 广东长荣林业发展股份有限公司 Skin moistening cream and preparation method thereof
CN105708973B (en) * 2016-04-11 2020-11-03 赣南医学院 External-use tea oil ointment and preparation method thereof
CN106727025A (en) * 2017-01-13 2017-05-31 华南理工大学 A kind of camellia skin cream and preparation method thereof
CN107080707A (en) * 2017-04-28 2017-08-22 云南健牛生物科技有限公司 Sufficient ointment of a kind of high oil content moisturizing anticracking handguard and preparation method thereof
CN108939966B (en) * 2018-08-07 2021-04-27 广东圣雪颜生物科技有限公司 Method for producing cosmetics
CN110251446A (en) * 2019-08-07 2019-09-20 太仓新亚逊生物科技有限公司 A kind of plant skin cream and preparation method thereof
CN111973465A (en) * 2020-08-29 2020-11-24 荣鼎(广东)生物科技有限公司 Antioxidant oil microemulsion
CN115252483A (en) * 2022-08-31 2022-11-01 于永涛 Ginseng and radix gimeracil fruit oil skin-moistening composition and preparation method thereof

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Address after: 410008 first floor, building 2, office building, chunkou Town, Liuyang City, Changsha City, Hunan Province

Patentee after: HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co.,Ltd.

Address before: 4, 410008, Fairview Alex Hua Tian B block 206, Furong Road, Furong Road, Hunan, Changsha

Patentee before: HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co.,Ltd.