CN1965792A - Moisturizing cream and preparation method thereof - Google Patents

Moisturizing cream and preparation method thereof Download PDF

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Publication number
CN1965792A
CN1965792A CN 200610123391 CN200610123391A CN1965792A CN 1965792 A CN1965792 A CN 1965792A CN 200610123391 CN200610123391 CN 200610123391 CN 200610123391 A CN200610123391 A CN 200610123391A CN 1965792 A CN1965792 A CN 1965792A
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China
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emollient cream
oleum camelliae
vaseline
polyoxyethylene
peg400
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CN 200610123391
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CN100581533C (en
Inventor
何庭玉
陈珊
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South China Agricultural University
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South China Agricultural University
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Abstract

The invention discloses a skin cream and its preparing process, wherein the the formula comprises tea-seed oil 2-6 wt%, vaseline 4-6 wt%, cetyl alcohol 1-2 wt%, dimethyl silicon oil 0.5-1 wt%, stearinic sorbic alcohol and sucrose ester of coconut fatty acid 1.3-1.5 wt%, monoglyceride and polyoxyethylene-100 monostearate 3.8-4.0 wt%, glycerin 3-5 wt%, polyethylene glycol 400 2-3 wt%, sodium carboxymethylcellulose 0.3-0.4 wt%, methylis oxybenzoas 0.15-0.2 wt% and balancing water.

Description

A kind of emollient cream and preparation method thereof
Technical field
The present invention relates to a kind of cosmetics, particularly a kind of emollient cream and preparation method thereof.
Technical background
In recent years, the psychology that people pursue green cosmetics, back to nature strengthens day by day, and the cosmetic product of therefore seeking natural product with no side effects and be active additive and cosmetic material becomes fine chemicals industry one big focus.Oleum Camelliae belongs to crude vegetal, squeezing from the xylophyta Semen Camelliae and get, and its physicochemical property is similar to olive oil, and iodine number is lower, belongs to non-drying oil, makes with extra care the Oleum Camelliae stable in properties, is difficult for oxidized.Oleum Camelliae fatty acid profile and human body skin are approaching, are easy to skin absorbs, no greasy feeling, and also contain sterilizing and itch-relieving compositions such as the tea polyphenols that do not contain in abundant vitamin and the olive oil, camellianin in the Oleum Camelliae.Therefore, refining Oleum Camelliae can be used as a kind of good used for cosmetic raw material, utilizes Oleum Camelliae can develop good cosmetics.
Summary of the invention
The object of the present invention is to provide a kind of to skin nonirritant, Oleum Camelliae emollient cream that moistness is good.
Another object of the present invention provides the preparation method of above-mentioned Oleum Camelliae emollient cream.
Oleum Camelliae emollient cream of the present invention comprises Oleum Camelliae 2~6% and surplus auxiliary agent, and unit is a mass percent.Its concrete prescription is: Oleum Camelliae 2~6%, vaseline 4~6%, hexadecanol 1~2%, dimethicone 0.5~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester 1.3~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate 3.8~4.0%, glycerol 3~5%, PEG400 2~3%, sodium carboxymethyl cellulose 0.3~0.4%, methyl hydroxybenzoate 0.15~0.2%, excess water.
Described Oleum Camelliae is that the squeezing of natural oil camellia oleosa seed produces, again by filtering and impurity removing, come unstuck, technologies such as deacidification, decolouring, deodorize and dewaxing get faint yellow to colourless liquid.
In above-mentioned Oleum Camelliae emollient cream, the preferred proportion of the amount of described Oleum Camelliae is 2.0~2.2%, 2.8~3.0%, 3.9~4.1%, 4.6~4.8%, 5.0~5.2% or 5.9~6.0%.
In above-mentioned Oleum Camelliae emollient cream, described glycerol and PEG400 are wetting agent, and sodium carboxymethyl cellulose is a thickening agent.
The preparation method of above-mentioned Oleum Camelliae emollient cream comprises the steps:
(1) batching: methyl hydroxybenzoate is dissolved in the small amount of ethanol, and sodium carboxymethyl cellulose adds in 20% the distilled water and is swelling to dissolving fully, and joins mixing in the mixed liquor of glycerol, PEG400 and residue distilled water, is designated as the A phase; With hexadecanol, vaseline and dimethicone heating for dissolving mixing become oil phase, and emulsifying agent stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester and glyceryl monostearate and polyoxyethylene (100) stearate heating mixing are joined in the oil phase, are designated as the B phase;
(2) sterilization: A, B are heated to 90 ℃ respectively, keep after 20min sterilizes Oleum Camelliae is joined mixing among the B;
(3) emulsifying: when A drops to 74~76 ℃ mutually, when B drops to 69~71 ℃ mutually, with B mutually slowly be added to A mutually in and constantly stir, holding temperature is under 70 ℃~75 ℃, shears 15min with the emulsification pretreatment machine under 1500r/min;
(4) cooling packing: stir after the emulsifying and be cooled to 40 ℃ of packaging products.
In above-mentioned preparation method, add distilled water, to replenish the loss of moisture in the sterilization process into 2~3%.
Compared with prior art, the present invention has following beneficial effect: the present invention has adopted the crude vegetal of no side effects---Oleum Camelliae, and choose reasonable its consumption in cosmetics, make it show good quality and skin moistening effect.This Oleum Camelliae milky lotion outward appearance is snow-white glossy, the emulsion particle exquisiteness, and coating is evenly.Feel is cunning, and spreadability is good, more easily absorbs, and to the skin nonirritant, can reach the effect of skin care.
The specific embodiment
Preparation method:
(1) batching: methyl hydroxybenzoate is dissolved in the ethanol, and sodium carboxymethyl cellulose adds in 20% the distilled water and is swelling to dissolving fully, and joins mixing in the mixed liquor of glycerol, PEG400 and residue distilled water, is designated as the A phase; With hexadecanol, vaseline and dimethicone heating for dissolving mixing become oil phase, and emulsifying agent stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester and glyceryl monostearate and polyoxyethylene (100) stearate heating mixing are joined in the oil phase, are designated as the B phase;
(2) sterilization: A, B are heated to 90 ℃, keep after 20min sterilizes Oleum Camelliae is joined mixing among the B;
(3) emulsifying: when water drops to 75 ℃, when oil phase drops to 70 ℃, the oil phase aqueous phase that is added to is slowly also constantly stirred, holding temperature is under 70 ℃~75 ℃, shears 15min with the emulsification pretreatment blender under 1500r/min;
(4) cooling packing: slowly stir after the emulsifying and be cooled to 40 ℃ of dischargings.Detect qualified back packing again through conventional cosmetics quality and safe and sanitary.
Utilize above-mentioned preparation method, preparation embodiment 1~6, as follows:
Embodiment 1
Oleum Camelliae 2.0%, hexadecanol is 2%, and vaseline is 6%, and dimethicone is 1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%, and glycerol is 5%, and PEG400 is 3%, sodium carboxymethyl cellulose is 0.4%, methyl hydroxybenzoate is 0.2%, and distilled water is 75.1%, and unit is a mass percent.
Embodiment 2
Oleum Camelliae 3.0%, hexadecanol is 2%, and vaseline is 5%, and dimethicone is 0.8%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%, glyceryl monostearate and polyoxyethylene (100) stearate is 4.0%, and glycerol is 5%, and PEG400 is 2.5%, sodium carboxymethyl cellulose is 0.35%, methyl hydroxybenzoate is 0.2%, and distilled water is 75.85%, and unit is a mass percent.
Embodiment 3
Oleum Camelliae is 4.1%, hexadecanol is 1%, and vaseline is 5%, and dimethicone is 0.5%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.4%, glyceryl monostearate and polyoxyethylene (100) stearate is 4.0%, and glycerol is 5%, and PEG400 is 2%, sodium carboxymethyl cellulose is 0.4%, methyl hydroxybenzoate is 0.2%, and distilled water is 76.4%, and unit is a mass percent.
Embodiment 4
Oleum Camelliae 4.8%, hexadecanol is 2%, and vaseline is 4%, and dimethicone is 1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 4.0%, and glycerol is 3%, and PEG400 is 3%, sodium carboxymethyl cellulose is 0.3%, methyl hydroxybenzoate is 0.15%, and distilled water is 76.25%, and unit is a mass percent.
Embodiment 5
Oleum Camelliae 5.2%, hexadecanol is 1%, and vaseline is 4%, and dimethicone is 0.5%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.4%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%, and glycerol is 5%, and PEG400 is 2%, sodium carboxymethyl cellulose is 0.3%, methyl hydroxybenzoate is 0.2%, and distilled water is 76.6%, and unit is a mass percent.
Embodiment 6
Oleum Camelliae 6%, hexadecanol is 1%, and vaseline is 5%, and dimethicone is 0.8%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 4.0%, and glycerol is 4.5%, and PEG400 is 3%, sodium carboxymethyl cellulose is 0.3%, methyl hydroxybenzoate is 0.2%, and all the other are 73.7% for distilled water, and unit is a mass percent.

Claims (10)

1, a kind of emollient cream is characterized in that comprising Oleum Camelliae 2%~6% and surplus auxiliary agent, and unit is a mass percent.
2, emollient cream according to claim 1, it is characterized in that prescription consists of: Oleum Camelliae 2%~6%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, glycerol is 3%~5%, PEG400 is 2%~3%, and sodium carboxymethyl cellulose is 0.3%~0.4%, and methyl hydroxybenzoate is 0.15%~0.2%, surplus is a water, and unit is a mass percent.
3, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 2.0%~2.2%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
4, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 2.8%~3.0%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
5, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 3.9%~4.1%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
6, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 4.6%~4.8%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
7, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 5.0%~5.2%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
8, emollient cream according to claim 2, it is characterized in that, the composition of this emollient cream: Oleum Camelliae is 5.9%~6.0%, hexadecanol is 1%~2%, vaseline is 4%~6%, dimethicone is 0.5%~1%, stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester are 1.3%~1.5%, glyceryl monostearate and polyoxyethylene (100) stearate is 3.8%~4.0%, and glycerol is 3%~5%, and PEG400 is 2%~3%, sodium carboxymethyl cellulose is 0.3%~0.4%, methyl hydroxybenzoate is 0.15%~0.2%, and surplus is a water, and unit is a mass percent.
9, the preparation method of the described emollient cream of claim 2 is characterized in that comprising the steps:
(1) batching: methyl hydroxybenzoate is dissolved in the ethanol, and sodium carboxymethyl cellulose adds in 20% the distilled water and is swelling to dissolving fully, and joins mixing in the mixed liquor of glycerol, PEG400 and residue distilled water, is designated as the A phase; With hexadecanol, vaseline and dimethicone heating for dissolving mixing become oil phase, and emulsifying agent stearic acid Pyrusussuriensis alcohol and coconut oil sucrose ester and glyceryl monostearate and polyoxyethylene (100) stearate heating mixing are joined in the oil phase, are designated as the B phase;
(2) sterilization: A, B are heated to 90 ℃ respectively, keep after 20min sterilizes Oleum Camelliae is joined mixing among the B;
(3) emulsifying: when A drops to 74~76 ℃ mutually, when B drops to 69~71 ℃ mutually, with B be added to A mutually in and constantly stir, holding temperature is under 70 ℃~75 ℃, shears 15min with the emulsification pretreatment machine under 1500r/min;
(4) cooling packing: stir after the emulsifying and be cooled to 40 ℃ of packaging products.
10, preparation method according to claim 9 is characterized in that: add the distilled water into 2~3%.
CN200610123391A 2006-11-07 2006-11-07 Moisturizing cream and preparation method thereof Expired - Fee Related CN100581533C (en)

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Application Number Priority Date Filing Date Title
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CN1965792A true CN1965792A (en) 2007-05-23
CN100581533C CN100581533C (en) 2010-01-20

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101305973B (en) * 2008-07-11 2010-12-01 中山大学 Camellia oil for baby skin protection
CN102885749A (en) * 2012-10-15 2013-01-23 管天球 Oil tea cosmetic
CN103169627A (en) * 2011-12-23 2013-06-26 湖南湘纯农业科技有限公司 Tea oil moisturizer and preparation method thereof
CN103301044A (en) * 2012-03-14 2013-09-18 湖南湘纯农业科技有限公司 Tea oil skin-moistening emulsion and preparation method thereof
CN104414880A (en) * 2013-09-08 2015-03-18 范梦天 Health cream rich in yeast polypeptidase
CN105708973A (en) * 2016-04-11 2016-06-29 赣南医学院 Tea oil ointment for external use and preparation method of tea oil ointment
CN107693454A (en) * 2017-11-06 2018-02-16 广州佰泰莱生物科技有限公司 A kind of plant acne eliminating cream and preparation method thereof
CN109288759A (en) * 2018-11-23 2019-02-01 茂名市和香种植科技有限公司 A kind of preparation method of novel agalloch eaglewood body lotion

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101305973B (en) * 2008-07-11 2010-12-01 中山大学 Camellia oil for baby skin protection
CN103169627A (en) * 2011-12-23 2013-06-26 湖南湘纯农业科技有限公司 Tea oil moisturizer and preparation method thereof
CN103169627B (en) * 2011-12-23 2015-01-14 湖南湘纯农业科技有限公司 Tea oil moisturizer and preparation method thereof
CN103301044A (en) * 2012-03-14 2013-09-18 湖南湘纯农业科技有限公司 Tea oil skin-moistening emulsion and preparation method thereof
CN102885749A (en) * 2012-10-15 2013-01-23 管天球 Oil tea cosmetic
CN102885749B (en) * 2012-10-15 2014-03-12 管天球 Oil tea cosmetic
CN104414880A (en) * 2013-09-08 2015-03-18 范梦天 Health cream rich in yeast polypeptidase
CN105708973A (en) * 2016-04-11 2016-06-29 赣南医学院 Tea oil ointment for external use and preparation method of tea oil ointment
CN107693454A (en) * 2017-11-06 2018-02-16 广州佰泰莱生物科技有限公司 A kind of plant acne eliminating cream and preparation method thereof
CN109288759A (en) * 2018-11-23 2019-02-01 茂名市和香种植科技有限公司 A kind of preparation method of novel agalloch eaglewood body lotion

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