CN103169627A - Tea oil moisturizer and preparation method thereof - Google Patents

Tea oil moisturizer and preparation method thereof Download PDF

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Publication number
CN103169627A
CN103169627A CN2011104374062A CN201110437406A CN103169627A CN 103169627 A CN103169627 A CN 103169627A CN 2011104374062 A CN2011104374062 A CN 2011104374062A CN 201110437406 A CN201110437406 A CN 201110437406A CN 103169627 A CN103169627 A CN 103169627A
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preparation
raw material
oil
water
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CN103169627B (en
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李加兴
李敬业
陈双平
张娟
孙金玉
黄诚
张朝晖
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HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co Ltd
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HUNAN XIANGCHUN AGRICULTURAL TECHNOLOGY Co Ltd
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Abstract

The invention discloses a tea oil moisturizer and a preparation method of the tea oil moisturizer. The tea oil moisturizer is characterized by being prepared from the following materials and steps that: the materials include 5-15 parts of tea oil, 1-4 parts of glycerin monostearate, 0.5-1.5 parts of methl glucse sesquistearate, 1-2 parts of polyoxyethylene stearates, 12-18 parts of white oil, 3-6 parts of isopropyl palmitate, 2-4 parts of isopropyl myristate, 2-3 parts of caprylic/capric triglyceride, 2 parts of stearic acid, 0.5-2 parts of cetostearyl alcohol, 0.2 part of methylparaben, 0.1 part of propylparaben, 2 parts of glycerol, 2-3 parts of glyceryl polymethacrylate, 0.3-0.5 part of triethanolamine, 0.2 part of diazolidinyl urea, and 0.15 part of essence; and the steps include preparing an oil phase, preparing a water phase, emulsifying, cooling, aging and bulking to form the product. The tea oil moisturizer is mainly applied to cosmetics and preparation of the cosmetics.

Description

A kind of Oleum Camelliae emollient cream and preparation method thereof
Technical field
The present invention relates to a kind of Oleum Camelliae emollient cream and preparation method thereof.
Background technology
Along with improving constantly of the current living standard of people, the cosmetics take natural plant extracts as primary raw material have become the main flow of market comsupton, the consumption figure increase year after year.Oleum Camelliae is rich in oleic acid, linoleic acid, can form hydrophobic film at skin surface, when giving skin softness, lubricated and glossiness, can also effectively prevent the intrusion of outside harmful substance; Can suppress the evaporation of moisture, prevent chapped skin, make the horny layer of dry skin and sclerosis rehydrated, recover cuticular softness and elasticity, make skin smooth, soft and moist and have elasticity, the good health status of maintenance skin.Oleum Camelliae also contains higher natural Vitamin E, has the ability of good non-oxidizability and removing oxygen-derived free radicals, can protect skin to preserve from; Important polyphenoils and membrane stabilizer in vitamin E or cell membrane has the expansion blood capillary, improves sanguimotor effect.Therefore, Oleum Camelliae will become a kind of important natural material of cosmetics industry as a kind of desirable skin care item component.
Summary of the invention
The object of the present invention is to provide a kind of Oleum Camelliae emollient cream and preparation method thereof, to satisfy people to the demand of natural plant extracts as the cosmetics of primary raw material.
For achieving the above object, technical solution of the present invention is: a kind of preparation method of Oleum Camelliae emollient cream, it is characterized in that it is comprised of following raw material and step, and the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part, (2) glyceryl monostearate 1-4 part,
(3) methyl glucoside sesqui-stearate 0.5-1.5 part,
(4) polyoxyethylene stearic acid ester 1-2 part,
(5) white oil 12-18 part, (6) isopropyl palmitate 3-6 part,
(7) isopropyl myristate 2-4 part, (8) sad capric acid triglyceride 2-3 part,
(9) stearic acid is 2 parts, (10) cetostearyl alcohol 0.5-2 part,
(11) methyl hydroxybenzoate is 0.2 part, 0.1 part of (12) propylparaben,
(13) glycerol is 2 parts, (14) polymethyl acid glyceride 2-3 part,
(15) triethanolamine 0.3-0.5 part, 0.2 part of (16) two imidazolidinyl urea,
(17) essence is 0.15 part;
Described each step is as follows:
A. the preparation of oil phase, Oleum Camelliae and other oil-soluble raw material glyceryl monostearates, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, stearic acid, cetostearyl alcohol, the polymethyl acid glyceride mix and blend of aforementioned proportion are heated to 70-75 ℃, it are fully melted or dissolve stand-by;
B. the preparation of water adds water-soluble material glycerol, the triethanolamine of aforementioned proportion in deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
C. emulsifying, after above-mentioned oil phase and water raw material are filtered respectively, sequentially add in the emulsifying pot by water after first oil, stir under temperature 70-80 ℃, after oil, water raw material fully are mixed into emulsion, add again parabens, two imidazolidinyl urea antiseptic, stir, namely complete emulsification procedure;
D. cooling, after the emulsifying that step C is obtained, raw material is cooled to 50-60 ℃, adds essence, then stirs 5 minutes, continues to cool to 35-40 ℃ of discharging;
E. ageing and fill is discharged in storage container, be placed in the storage cream between ageing be no less than 48 hours, carry out fill through after the assay was approved.
Oleum Camelliae emollient cream of method preparation as described herein.
The invention has the beneficial effects as follows: the moistening that the present invention has skin according to Oleum Camelliae, protection, aging resistance activity, carry out emulsion dispersion by adding the compositions such as emulsifying agent, antiseptic, thickening agent, essence, prepare a kind of Oleum Camelliae emollient cream, can make skin moisturizing, moisturizing, smooth.
The specific embodiment
Below in conjunction with embodiment, the present invention and the specific embodiment thereof are described in further detail.The invention is characterized in that it is comprised of following raw material and step, the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part, (2) glyceryl monostearate 1-4 part,
(3) methyl glucoside sesqui-stearate 0.5-1.5 part,
(4) polyoxyethylene stearic acid ester 1-2 part,
(5) white oil 12-18 part, (6) isopropyl palmitate 3-6 part,
(7) isopropyl myristate 2-4 part, (8) sad capric acid triglyceride 2-3 part,
(9) stearic acid is 2 parts, (10) cetostearyl alcohol 0.5-2 part,
(11) methyl hydroxybenzoate is 0.2 part, 0.1 part of (12) propylparaben,
(13) glycerol is 2 parts, (14) polymethyl acid glyceride 2-3 part,
(15) triethanolamine 0.3-0.5 part, 0.2 part of (16) two imidazolidinyl urea,
(17) essence is 0.15 part;
Described each step is as follows:
A. the preparation of oil phase, Oleum Camelliae and other oil-soluble raw material glyceryl monostearates, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, stearic acid, cetostearyl alcohol, the polymethyl acid glyceride mix and blend of aforementioned proportion are heated to 70-75 ℃, it are fully melted or dissolve stand-by;
B. the preparation of water adds water-soluble material glycerol, the triethanolamine of aforementioned proportion in deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
C. emulsifying, after above-mentioned oil phase and water raw material are filtered respectively, sequentially add in the emulsifying pot by water after first oil, stir under temperature 70-80 ℃, after oil, water raw material fully are mixed into emulsion, add again parabens, two imidazolidinyl urea antiseptic, stir, namely complete emulsification procedure;
D. cooling, after the emulsifying that step C is obtained, raw material is cooled to 50-60 ℃, adds essence, then stirs 5 minutes, continues to cool to 35-40 ℃ of discharging;
E. ageing and fill is discharged in storage container, be placed in the storage cream between ageing be no less than 48 hours, carry out fill through after the assay was approved.
Oleum Camelliae emollient cream of method preparation as described herein.
Below provide embodiments of the invention
Example 1
The preparation of oil phase, with 5 parts of Oleum Camelliae, 1 part of glyceryl monostearate, 0.5 part of methyl glucoside sesqui-stearate, 1 part, stearic acid polyoxyethylene fat, 16 parts of white oils (liquid paraffin), 3 parts of isopropyl palmitates, 2 parts of isopropyl myristates, 3 parts of sad capric acid greases, 2 parts of stearic acid, 2 parts of cetostearyl alcohols, 3 parts of polymethyl acid glycerides, mix and blend are heated to 70 ℃.It is fully melted or dissolve stand-by;
The preparation of water, with 2 parts of water-soluble material glycerol, 0.3 part of triethanolamine adds 58.55 parts of deionized waters, is heated with stirring to 100 ℃, keep 20 minutes the sterilization, then be cooled to 80 ℃ stand-by;
Emulsifying, above-mentioned oil phase and water raw material are filtered respectively rear (filtering as centrifuge), order by water after first oil adds in the emulsifying pot, stir under temperature 70 C, after oil, water raw material fully are mixed into emulsion, add again 0.2 part of antiseptic methyl hydroxybenzoate, 0.1 part of propylparaben, 0.2 part of two imidazolidinyl urea, stir, namely complete emulsification procedure;
Cooling, material after above-mentioned emulsifying is cooled to 60 ℃, add 0.15 part, essence, then stirred 5 minutes, continue to cool to 35 ℃ of dischargings;
Ageing and fill are delivered to above-mentioned material in storage container, are placed in that between storage cream, ageing is no less than 48 hours, to carrying out fill after the assay was approved, are product.
Example 2
The preparation of oil phase, 10 parts of Oleum Camelliae, 2 parts of glyceryl monostearates, 1 part of methyl glucoside sesqui-stearate, 1.5 parts, stearic acid polyoxyethylene fat, 15 parts of white oils (liquid paraffin), 4 parts of isopropyl palmitates, 3 parts of isopropyl myristates, 2.5 parts of sad capric acid triglyceride, 2 parts of stearic acid, 1 part of cetostearyl alcohol, 2.5 parts of polymethyl acid glycerides, mix and blend are heated to 72 ℃.
The preparation of water, 2 parts of glycerol, 0.4 part of triethanolamine adds 52.45 parts of deionized waters, is heated with stirring to 95 ℃, then is cooled to 75 ℃;
Stir under 75 ℃ in emulsifying, emulsifying pot;
Cooling, after emulsifying, material is cooled to 55 ℃; Then be cooled to 38 ℃ of dischargings, all the other are with example 1.
Example 3
The preparation of oil phase, 15 parts of Oleum Camelliae, 4 parts of glyceryl monostearates, 1.5 parts of methyl glucoside sesqui-stearate, 2 parts, stearic acid polyoxyethylene fat, 12 parts of white oils (liquid paraffin), 6 parts of isopropyl palmitates, 4 parts of isopropyl myristates, 2 parts of sad capric acid triglyceride, 2 parts of stearic acid, 0.5 part of cetostearyl alcohol, 2 parts of polymethyl acid glycerides, mix and blend are heated to 75 ℃.
The preparation of water, 2 parts of glycerol, 0.5 part of triethanolamine, 45.85 parts of deionized waters are heated with stirring to 90 ℃, then are cooled to 70 ℃.
Stir under 80 ℃ in emulsifying, emulsifying pot;
Cooling, the material of emulsifying is cooled to 50 ℃, then is cooled to 40 ℃ of dischargings, and all the other are with example 1.

Claims (2)

1. the preparation method of Oleum Camelliae emollient cream, is characterized in that it is comprised of following raw material and step, and the weight proportion of described each raw material is:
Oleum Camelliae 5-15 part, (2) glyceryl monostearate 1-4 part,
Methyl glucoside sesqui-stearate 0.5-1.5 part,
Polyoxyethylene stearic acid ester 1-2 part,
White oil 12-18 part, (6) isopropyl palmitate 3-6 part,
Isopropyl myristate 2-4 part, (8) sad capric acid triglyceride 2-3 part,
2 parts of stearic acid, (10) cetostearyl alcohol 0.5-2 part,
(11) methyl hydroxybenzoate is 0.2 part, 0.1 part of (12) propylparaben,
(13) glycerol is 2 parts, (14) polymethyl acid glyceride 2-3 part,
(15) triethanolamine 0.3-0.5 part, 0.2 part of (16) two imidazolidinyl urea,
(17) essence is 0.15 part;
Described each step is as follows:
The preparation of oil phase, Oleum Camelliae and other oil-soluble raw material glyceryl monostearates, polyoxyethylene stearic acid ester, methyl glucoside sesqui-stearate, white oil, isopropyl palmitate, isopropyl myristate, sad capric acid triglyceride, stearic acid, cetostearyl alcohol, the polymethyl acid glyceride mix and blend of aforementioned proportion are heated to 70-75 ℃, it are fully melted or dissolve stand-by;
The preparation of water adds water-soluble material glycerol, the triethanolamine of aforementioned proportion in deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
Emulsifying, after above-mentioned oil phase and water raw material are filtered respectively, sequentially add in the emulsifying pot by water after first oil, stir under temperature 70-80 ℃, after oil, water raw material fully are mixed into emulsion, add again parabens, two imidazolidinyl urea antiseptic, stir, namely complete emulsification procedure;
Cooling, after the emulsifying that step C is obtained, raw material is cooled to 50-60 ℃, adds essence, then stirs 5 minutes, continues to cool to 35-40 ℃ of discharging;
Ageing and fill are discharged in storage container, be placed in the storage cream between ageing be no less than 48 hours, carry out fill through after the assay was approved.
2. Oleum Camelliae emollient cream of the method for claim 1 preparation.
CN201110437406.2A 2011-12-23 2011-12-23 Tea oil moisturizer and preparation method thereof Active CN103169627B (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104207987A (en) * 2014-09-02 2014-12-17 杭州陶源秀化妆品厂 Mulberry leaf moisturizing body cream and preparation process thereof
CN104997674A (en) * 2015-07-09 2015-10-28 广东长荣林业发展股份有限公司 Skin moistening cream and preparation method thereof
CN105708973A (en) * 2016-04-11 2016-06-29 赣南医学院 Tea oil ointment for external use and preparation method of tea oil ointment
CN106727025A (en) * 2017-01-13 2017-05-31 华南理工大学 A kind of camellia skin cream and preparation method thereof
CN107080707A (en) * 2017-04-28 2017-08-22 云南健牛生物科技有限公司 Sufficient ointment of a kind of high oil content moisturizing anticracking handguard and preparation method thereof
CN108939966A (en) * 2018-08-07 2018-12-07 陆挚译 A kind of production method of cosmetics
CN110251446A (en) * 2019-08-07 2019-09-20 太仓新亚逊生物科技有限公司 A kind of plant skin cream and preparation method thereof
CN111973465A (en) * 2020-08-29 2020-11-24 荣鼎(广东)生物科技有限公司 Antioxidant oil microemulsion
CN115252483A (en) * 2022-08-31 2022-11-01 于永涛 Ginseng and radix gimeracil fruit oil skin-moistening composition and preparation method thereof

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CN1965792A (en) * 2006-11-07 2007-05-23 华南农业大学 Moisturizing cream and preparation method thereof

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CN1965792A (en) * 2006-11-07 2007-05-23 华南农业大学 Moisturizing cream and preparation method thereof

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104207987A (en) * 2014-09-02 2014-12-17 杭州陶源秀化妆品厂 Mulberry leaf moisturizing body cream and preparation process thereof
CN104997674A (en) * 2015-07-09 2015-10-28 广东长荣林业发展股份有限公司 Skin moistening cream and preparation method thereof
CN105708973A (en) * 2016-04-11 2016-06-29 赣南医学院 Tea oil ointment for external use and preparation method of tea oil ointment
CN106727025A (en) * 2017-01-13 2017-05-31 华南理工大学 A kind of camellia skin cream and preparation method thereof
CN107080707A (en) * 2017-04-28 2017-08-22 云南健牛生物科技有限公司 Sufficient ointment of a kind of high oil content moisturizing anticracking handguard and preparation method thereof
CN108939966A (en) * 2018-08-07 2018-12-07 陆挚译 A kind of production method of cosmetics
CN108939966B (en) * 2018-08-07 2021-04-27 广东圣雪颜生物科技有限公司 Method for producing cosmetics
CN110251446A (en) * 2019-08-07 2019-09-20 太仓新亚逊生物科技有限公司 A kind of plant skin cream and preparation method thereof
CN111973465A (en) * 2020-08-29 2020-11-24 荣鼎(广东)生物科技有限公司 Antioxidant oil microemulsion
CN115252483A (en) * 2022-08-31 2022-11-01 于永涛 Ginseng and radix gimeracil fruit oil skin-moistening composition and preparation method thereof

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