CN103301044A - Tea oil skin-moistening emulsion and preparation method thereof - Google Patents
Tea oil skin-moistening emulsion and preparation method thereof Download PDFInfo
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- CN103301044A CN103301044A CN2012100666210A CN201210066621A CN103301044A CN 103301044 A CN103301044 A CN 103301044A CN 2012100666210 A CN2012100666210 A CN 2012100666210A CN 201210066621 A CN201210066621 A CN 201210066621A CN 103301044 A CN103301044 A CN 103301044A
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Abstract
The invention discloses a tea oil skin-moistening emulsion and a preparation method thereof. The tea oil skin-moistening emulsion is characterized by comprising the following raw materials in parts by weight: 5-15 parts of tea oil, 3 parts of fatty alcohol-polyoxyethylene ether, 1 part of hexadecyl glucoside, 0.50-1 part of cetearyl alcohol, 3-6 parts of isopropyl myristate, 4-7 parts of isopropyl palmitate, 1-3 parts of caprylic capric triglyceride, 0.20 part of methylparaben, 0.10 part of propylparaben, 1.50-2.50 parts of polydimethyl siloxane fluid, 0.05-0.10 part of Carbopol940 (acrylic polymer), 0.10-0.50 part of Carbopol305 (acrylic polymer), 2-3 parts of glycerinum, 0.15 part of essences, 0.20 part of diazolidinyl urea and 63.30-74.20 parts of water; the preparation method is also characterized by comprising the following steps of: preparing an oil phase, preparing a water phase, emulsifying, cooling, ageing and filling to obtain the fished tea oil skin-moistening emulsion product. The tea oil skin-moistening emulsion is mainly used for cosmetics and the technical scheme is applied to the preparation method of the tea oil skin-moistening emulsion.
Description
Technical field
The present invention relates to a kind of Oleum Camelliae moisturizer and preparation method thereof.
Background technology
Along with improving constantly of the current living standard of people, the cosmetics take natural plant extracts as primary raw material have become the main flow of market comsupton, the consumption figure increase year after year.Oleum Camelliae is rich in oleic acid, linoleic acid, can form hydrophobic film at skin surface, when giving skin softness, lubricated and glossiness, can also effectively prevent the intrusion of outside harmful substance; Can suppress the evaporation of moisture, prevent chapped skin, make the horny layer of dry skin and sclerosis rehydrated, recover cuticular softness and elasticity, make skin smooth, soft and moist and have elasticity, keep the good health status of skin.Oleum Camelliae also contains higher natural Vitamin E, has the ability of good non-oxidizability and removing oxygen-derived free radicals, can protect skin to preserve from; Important polyphenoils and membrane stabilizer in vitamin E or the cell membrane has the expansion blood capillary, improves sanguimotor effect.Therefore, Oleum Camelliae will become a kind of important natural material of cosmetics industry as a kind of desirable skin care item component.
Summary of the invention
The object of the present invention is to provide a kind of Oleum Camelliae moisturizer and preparation method thereof, to satisfy people to the demand of natural plant extracts as the cosmetics of primary raw material.
For achieving the above object, technical solution of the present invention is: a kind of preparation method of Oleum Camelliae moisturizer, it is characterized in that it is comprised of following raw material and step, and the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part,
(2) fatty alcohol-polyoxyethylene ether is 3 parts,
(3) the cetyl glucoside is 1 part,
(4) cetostearyl alcohol 0.5-1 part,
(5) isopropyl myristate 3-6 part,
(6) isopropyl palmitate 4-7 part,
(7) sad capric acid triglyceride 1-3 part,
(8) methyl hydroxybenzoate is 0.2 part,
(9) propylparaben is 0.1 part,
(10) polydimethyl siloxane fluid 1.5-2.5 part,
(11) Carbopol940 (acrylate copolymer) 0.05-0.1 part,
(12) Carbopol305 (acrylate copolymer) 0.1-0.5 part,
(13) glycerol 2-3 part,
(14) essence is 0.15 part,
(15) two imidazolidinyl urea are 0.2 part,
(16) water 63.3-74.2 part;
Described each step is as follows:
A. the preparation of oil phase, the Oleum Camelliae of aforementioned proportion and other oil-soluble raw material cetostearyl alcohols, isopropyl myristate, isopropyl palmitate, sad capric acid triglyceride, polydimethyl siloxane fluid are heated with stirring to 70-75 ℃, it is fully melted or dissolve evenly stand-by.The preparation of water adds the water-soluble material glycerol of aforementioned proportion, triethanolamine in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilizing in 20 minutes, then be cooled to 70-80 ℃ stand-by;
B. the preparation of water adds water soluble ingredient fatty alcohol-polyoxyethylene ether, cetyl glucoside, acrylate copolymer, glycerol in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
C. emulsifying, after above-mentioned oil phase and water raw material filter, order according to water behind elder generation's oil adds in the emulsifying pot, under 70-80 ℃ of condition, carry out high-speed stirred, after oil, water raw material fully are mixed into the uniform emulsion of dispersion, add again the antiseptic (using first dissolve with ethanol) such as parabens, two imidazolidinyl urea, stir, namely finish emulsification procedure;
D. cooling, raw material is cooled to 50-60 ℃ after the emulsifying that step C is obtained, and adds essence, and restir 5 minutes continues to cool to 35-40 ℃ of discharging;
E. ageing and fill is discharged in the storage container, place the storage cream between ageing be no less than 48 hours, carry out fill through after the assay was approved.
The Oleum Camelliae moisturizer of method preparation as described herein.
The invention has the beneficial effects as follows: the moistening that the present invention has skin according to Oleum Camelliae, protection, aging resistance activity, carry out emulsion dispersion by adding the compositions such as emulsifying agent, antioxidant, antiseptic, essence, prepare a kind of Oleum Camelliae emollient cream that is fluid state, be easy to be absorbed by the skin, and can make skin moisturizing, moisturizing, smooth.
The specific embodiment
Below in conjunction with embodiment the present invention and the specific embodiment thereof are described in further detail.The invention is characterized in that it is comprised of following raw material and step, the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part,
(2) fatty alcohol-polyoxyethylene ether is 3 parts,
(3) the cetyl glucoside is 1 part,
(4) cetostearyl alcohol 0.5-1 part,
(5) isopropyl myristate 3-6 part,
(6) isopropyl palmitate 4-7 part,
(7) sad capric acid triglyceride 1-3 part,
(8) methyl hydroxybenzoate is 0.2 part,
(9) propylparaben is 0.1 part,
(10) polydimethyl siloxane fluid 1.5-2.5 part,
(11) Carbopol940 (acrylate copolymer) 0.05-0.1 part,
(12) Carbopol305 (acrylate copolymer) 0.1-0.5 part
(13) glycerol 2-3 part,
(14) essence is 0.15 part,
(15) two imidazolidinyl urea are 0.2 part,
(16) water 63.3-74.2 part;
Described each step is as follows:
A. the preparation of oil phase, the Oleum Camelliae of aforementioned proportion and other oil-soluble raw material cetostearyl alcohols, isopropyl myristate, isopropyl palmitate, sad capric acid triglyceride, polydimethyl siloxane fluid are heated with stirring to 70-75 ℃, it is fully melted or dissolve evenly stand-by.The preparation of water adds the water-soluble material glycerol of aforementioned proportion, triethanolamine in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilizing in 20 minutes, then be cooled to 70-80 ℃ stand-by;
B. the preparation of water adds water soluble ingredient fatty alcohol-polyoxyethylene ether, cetyl glucoside, acrylate copolymer, glycerol in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
C. emulsifying, after above-mentioned oil phase and water raw material filter, order according to water behind elder generation's oil adds in the emulsifying pot, under 70-80 ℃ of condition, carry out high-speed stirred, after oil, water raw material fully are mixed into the uniform emulsion of dispersion, add again the antiseptic (using first dissolve with ethanol) such as parabens, two imidazolidinyl urea, stir, namely finish emulsification procedure;
D. cooling, raw material is cooled to 50-60 ℃ after the emulsifying that step C is obtained, and adds essence, and restir 5 minutes continues to cool to 35-40 ℃ of discharging;
E. ageing and fill is discharged in the storage container, places the storage bay ageing to be no less than 48 hours, carries out fill through after the assay was approved.
Oleum Camelliae emollient cream of method preparation as described herein.
Below provide embodiments of the invention.
Example 1
The preparation of oil phase, with 5 parts of Oleum Camelliae, 0.5 part of cetostearyl alcohol, 6 parts of isopropyl myristates, 4 parts of isopropyl palmitates, 1 part of sad capric acid triglyceride, 1.5 parts of mix and blends of polydimethyl siloxane fluid are heated to 70 ℃, it is fully melted or dissolve stand-by;
The preparation of water, with 3 parts of water-soluble material fatty alcohol-polyoxyethylene ether, 1 part of cetyl glucoside, 0.05 part of Carbopol940 (acrylate copolymer), 0.1 part of Carbopol305 (acrylate copolymer), 3 parts of glycerol, add 74.2 parts of deionized waters, be heated with stirring to 100 ℃, keep 20 minutes the sterilization, then be cooled to 80 ℃ stand-by;
Emulsifying, above-mentioned oil phase and water raw material are filtered respectively rear (filtering such as centrifuge), order by water behind elder generation's oil adds in the emulsifying pot, under temperature 70 C, stir, after oil, water raw material fully are mixed into emulsion, add again 0.2 part of antiseptic methyl hydroxybenzoate, 0.1 part of propylparaben, 0.2 part of two imidazolidinyl urea, stir, namely finish emulsification procedure;
Cooling is cooled to 60 ℃ with material after the above-mentioned emulsifying, adds 0.15 part in essence, and restir 5 minutes continues to cool to 35 ℃ of dischargings;
Ageing and fill are delivered to above-mentioned material in the storage container, place that ageing is no less than 48 hours between storage cream, to carrying out fill after the assay was approved, are product.
Example 2
The preparation of oil phase, 10 parts of Oleum Camelliae, 0.7 part of cetostearyl alcohol, 4.5 parts of isopropyl myristates, 5 parts of isopropyl palmitates, 2 parts of sad capric acid triglyceride, 2 parts of mix and blends of polydimethyl siloxane fluid are heated to 72 ℃;
The preparation of water, 3 parts of fatty alcohol-polyoxyethylene ether, 1 part of cetyl glucoside, 0.08 part of Carbopol940 (acrylate copolymer), 0.3 part of Carbopol305 (acrylate copolymer), 2.5 parts of glycerol add 68.27 parts of deionized waters, be heated with stirring to 95 ℃, then be cooled to 75 ℃;
75 ℃ of lower stirrings in the emulsifying, emulsifying pot, all the other are with example 1;
Cooling, material is cooled to 55 ℃ after the emulsifying; Then be cooled to 38 ℃ of dischargings, all the other are with example 1.
Example 3
The preparation of oil phase, 15 parts of Oleum Camelliae, 1 part of cetostearyl alcohol, 3 parts of isopropyl myristates, 7 parts of isopropyl palmitates, 3 parts of sad capric acid triglyceride, 2.5 parts of polydimethyl siloxane fluids, mix and blend are heated to 75 ℃;
The preparation of water, 3 parts of fatty alcohol-polyoxyethylene ether, 1 part of cetyl glucoside, 0.1 part of Carbopol940 (acrylate copolymer), 0.5 part of Carbopol305 (acrylate copolymer), 2 parts of glycerol add 63.3 parts of deionized waters, be heated with stirring to 90 ℃, then be cooled to 70 ℃;
80 ℃ of lower stirrings in the emulsifying, emulsifying pot, all the other are with example 1;
Cooling, the material of emulsifying is cooled to 50 ℃, then is cooled to 40 ℃ of dischargings, and all the other are with example 1.
Claims (2)
1. the preparation method of an Oleum Camelliae moisturizer is characterized in that it is comprised of following raw material and step, and the weight proportion of described each raw material is:
(1) Oleum Camelliae 5-15 part,
(2) fatty alcohol-polyoxyethylene ether is 3 parts,
(3) the cetyl glucoside is 1 part,
(4) cetostearyl alcohol 0.5-1 part,
(5) isopropyl myristate 3-6 part,
(6) isopropyl palmitate 4-7 part,
(7) sad capric acid triglyceride 1-3 part,
(8) methyl hydroxybenzoate is 0.2 part,
(9) propylparaben is 0.1 part,
(10) polydimethyl siloxane fluid 1.5-2.5 part,
(11) Carbopol940 (acrylate copolymer) 0.05-0.1 part,
(12) Carbopol305 (acrylate copolymer) 0.1-0.5 part,
(13) glycerol 2-3 part,
(14) essence is 0.15 part,
(15) two imidazolidinyl urea are 0.2 part,
(16) water 63.3-74.2 part,
Described each step is as follows:
A. the preparation of oil phase, the Oleum Camelliae of aforementioned proportion and other oil-soluble raw material cetostearyl alcohols, isopropyl myristate, isopropyl palmitate, sad capric acid triglyceride, polydimethyl siloxane fluid are heated with stirring to 70-75 ℃, it is fully melted or dissolve evenly stand-by; The preparation of water adds the water-soluble material glycerol of aforementioned proportion, triethanolamine in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilizing in 20 minutes, then be cooled to 70-80 ℃ stand-by;
B. the preparation of water adds water soluble ingredient fatty alcohol-polyoxyethylene ether, cetyl glucoside, acrylate copolymer, glycerol in the deionized water, is heated with stirring to 90-100 ℃, keeps sterilization in 20 minutes, then be cooled to 70-80 ℃ stand-by;
C. emulsifying, after above-mentioned oil phase and water raw material filter, order according to water behind elder generation's oil adds in the emulsifying pot, under 70-80 ℃ of condition, carry out high-speed stirred, after oil, water raw material fully are mixed into the uniform emulsion of dispersion, add again the antiseptic (using first dissolve with ethanol) such as parabens, two imidazolidinyl urea, stir, namely finish emulsification procedure;
D. cooling, raw material is cooled to 50-60 ℃ after the emulsifying that step C is obtained, and adds essence, and restir 5 minutes continues to cool to 35-40 ℃ of discharging;
E. ageing and fill is discharged in the storage container, place the storage cream between ageing be no less than 48 hours, carry out fill through after the assay was approved.
2. the Oleum Camelliae moisturizer of the method for claim 1 preparation.
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| CN2012100666210A CN103301044A (en) | 2012-03-14 | 2012-03-14 | Tea oil skin-moistening emulsion and preparation method thereof |
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| CN2012100666210A CN103301044A (en) | 2012-03-14 | 2012-03-14 | Tea oil skin-moistening emulsion and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103637955A (en) * | 2013-12-18 | 2014-03-19 | 淄博齐鼎立专利信息咨询有限公司 | Skin-moistening emulsion |
| CN105232364A (en) * | 2015-07-29 | 2016-01-13 | 朱耀灯 | Oil-control balancing and refirming emulsion and preparation method thereof |
| CN110538097A (en) * | 2019-09-18 | 2019-12-06 | 郑州轻工业学院 | moisturizing body refreshing lotion |
| CN111973465A (en) * | 2020-08-29 | 2020-11-24 | 荣鼎(广东)生物科技有限公司 | Antioxidant oil microemulsion |
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| CN1965792A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Moisturizing cream and preparation method thereof |
| CN1965791A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Anti-acne moisturizing cream and preparation process thereof |
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| CN1965792A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Moisturizing cream and preparation method thereof |
| CN1965791A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Anti-acne moisturizing cream and preparation process thereof |
| CN101889966A (en) * | 2010-06-21 | 2010-11-24 | 金奇集团金奇日化有限公司 | Preparation method of tea oil anti-cracking cream composition and product thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103637955A (en) * | 2013-12-18 | 2014-03-19 | 淄博齐鼎立专利信息咨询有限公司 | Skin-moistening emulsion |
| CN105232364A (en) * | 2015-07-29 | 2016-01-13 | 朱耀灯 | Oil-control balancing and refirming emulsion and preparation method thereof |
| CN110538097A (en) * | 2019-09-18 | 2019-12-06 | 郑州轻工业学院 | moisturizing body refreshing lotion |
| CN111973465A (en) * | 2020-08-29 | 2020-11-24 | 荣鼎(广东)生物科技有限公司 | Antioxidant oil microemulsion |
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Application publication date: 20130918 |