CN105232364A - Oil-control balancing and refirming emulsion and preparation method thereof - Google Patents
Oil-control balancing and refirming emulsion and preparation method thereof Download PDFInfo
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- CN105232364A CN105232364A CN201510460408.1A CN201510460408A CN105232364A CN 105232364 A CN105232364 A CN 105232364A CN 201510460408 A CN201510460408 A CN 201510460408A CN 105232364 A CN105232364 A CN 105232364A
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Abstract
The invention provides oil-control balancing and refirming emulsion and a preparation method thereof. The oil-control balancing and refirming emulsion is prepared from a skin conditioning agent, a moisturizing agent, emulsifying thickener acrylic acids (esters)/C10-30 alkanol acrylate cross-linked polymers, PH regulator triethanolamine, preservatives, odorant essences, a chelating agent, a coloring agent and the balance deionized water solvent. The preparation method includes: weighing raw materials, heating deionized water, forming a first mixture, carrying out vacuum homogeneous emulsification, stirring, cooling and the like. The oil-control balancing and refirming emulsion has the advantages of moderate cost, mildness, easiness in absorption, effectiveness in grease balance and skin refirming, inhibition of bacterial reproduction, removal of redundant grease, prevention of acnes and realization of skin smoothing and skin brightening. In addition, the preparation method of the oil-control balancing and refirming emulsion has the advantages of low processing cost and high production efficiency.
Description
Technical field
The present invention relates to daily washing articles for use technical field, be specifically related to a kind of control oil balance Firm breast and preparation method thereof.
Background technology
Controlling oil balance Firm breast is arrive skincare product through conventional in people's daily life, the Main Function of Firm breast is pore refining, generally all contain ethanol, refrigerant dry and comfortable sensation is had after using, simultaneously can also the breeding of anti-bacteria effectively, prevent growing of comedo, skin is made to become smoothly glossy, effectively can also dispel excess oil in addition, but ethanol has certain zest to skin, in prior art Firm breast often gentle not, cost is higher, price comparison is expensive, and there is certain chemical composition being not easy to be absorbed by the skin.
Summary of the invention
Technical problem to be solved by this invention is control oil balance Firm breast providing a kind of moderate cost, skin tightening effect good for above-mentioned the deficiencies in the prior art and preparation method thereof.
The present invention for the adopted technical scheme that solves the problem is:
A control oil balance Firm breast, its component and raw material weight percentage ratio are:
Skin conditioning agent 2% ~ 30%,
Wetting agent 1% ~ 30%,
Emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.1% ~ 5%,
PH regulator triethanolamine 0.5% ~ 10%,
Antiseptic 0.1% ~ 2%,
Odorant essence 0.02% ~ 2%,
Chelating agen EDETATE SODIUM 0.01% ~ 2%,
Coloring agent 0.00001% ~ 1.0%, surplus is deionized water solvent.
Further, described skin conditioning agent is one or more in Hamamelis virginiana extract, dimethione, squalane, ethoxy urea, allantoin.
Further, described wetting agent is one or both in betanin, propylene glycol.
Further, described antiseptic is one or more in methyl hydroxybenzoate, diazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate.
Further, described coloring agent is one or both in CI15985, CI16035.
Control a preparation method for oil balance Firm breast, comprise the following steps:
(1) raw material is taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionized water and be heated to 90 ~ 100 DEG C, the deionized water that unlatching vacuum pump extraction part has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent, antiseptic and chelating agen EDETATE SODIUM again, be heated to 85 ~ 90 DEG C, stir formation first mixture;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with described first mixture, rapid stirring is even, homogenizing 1 ~ 3min, stir 5 ~ 10min again and form the second mixture, start cooling;
(5) when described second mixture is cooled to 70 ~ 85 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2 ~ 5min, stirring 10 ~ 20min to evenly forming the 3rd mixture;
(6), when described 3rd mixture is cooled to 50 ~ 55 DEG C, to stir adding emulsifying pot with the good antiseptic solution of deionized water dissolving and colourant solution formation 4 mixture;
(7) when described 4 mixture is cooled to 40 ~ 50 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) described 5th mixture is cooled to 30 ~ 40 DEG C and adds in emulsifying pot by essence, stirs 15 ~ 20min, to completely evenly obtaining required product.
Further, in described step (3), skin conditioning agent is ethoxy urea, allantoin, and antiseptic is methyl hydroxybenzoate.
Further, in described step (4), wetting agent is betanin, propylene glycol.
Further, in described step (5), skin conditioning agent is Hamamelis virginiana extract, dimethione and squalane.
Further, antiseptic described in described step (6) is diazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate; Described coloring agent is CI15985 and CI16035.
Beneficial effect of the present invention is:
One control oil balance Firm breast provided by the invention is moderate, performance is gentle, easily be absorbed by the skin, energy active balance oils and fats, compact skin, the breeding of anti-bacteria and dispel excess oil, prevents growing of comedo, make skin become smoothly glossy, separately this preparation method has the advantage that processing cost is low, production efficiency is high.
Detailed description of the invention
Lower mask body illustrates embodiments of the present invention; the providing of these embodiments is only used to the object illustrated; limitation of the invention can not be interpreted as; only for reference and explanation uses; do not form the restriction to scope of patent protection of the present invention; because without departing from the spirit and scope of the present invention, many changes can be carried out to the present invention.
embodiment 1
In the present embodiment, one control oil balance Firm breast provided by the present invention, its component and raw material weight percentage ratio are:
Skin conditioning agent 20%,
Wetting agent 8%,
Emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.3%,
PH regulator triethanolamine 0.26%,
Antiseptic 0.3%,
Odorant essence 0.2%,
Chelating agen EDETATE SODIUM 0.12%,
Coloring agent 0.004%, surplus is deionized water solvent.
In the present embodiment, skin conditioning agent is in Hamamelis virginiana extract, ethoxy urea, dimethione, squalane, allantoin totally 5 kinds, and the percentage by weight of each assembly is 40:40:10:9:1.
In the present embodiment, wetting agent is betanin, propylene glycol two kinds, and its percentage by weight is 1:3.
In the present embodiment, antiseptic is in methyl hydroxybenzoate, diazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate 3 kinds, and its percentage by weight is 203:96:1.
In the present embodiment, coloring agent is in CI15985, CI16035 two kinds, and its percentage by weight is 1:1.
The preparation method of this Firm breast comprises the following steps:
(1) raw material 10kg is altogether taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionization 7.806kg water and be heated to 98 DEG C, the deionized water that unlatching vacuum pump extraction 7.6kg has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent again, antiseptic and chelating agen EDETATE SODIUM 0.012kg, be heated to 85 DEG C, and stir formation first mixture; In the present embodiment, skin conditioning agent is 0.8kg ethoxy urea and each 0.02kg of allantoin; In the present embodiment, antiseptic is 0.0203kg methyl hydroxybenzoate;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.003kg wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with the first mixture, rapid stirring is even, homogenizing 2min, stir 6min again and form the second mixture, start cooling; In the present embodiment, wetting agent is 0.6kg propylene glycol, 0.2kg betanin;
When (5) second mixture are cooled to 80 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2min, stirring 10min to evenly forming the 3rd mixture; In the present embodiment, skin conditioning agent is 0.8kg Hamamelis virginiana extract, 0.2kg dimethione and 0.18kg squalane;
(6), when in the present embodiment, the 3rd mixture is cooled to 52 DEG C, to stir adding emulsifying pot with deionized water and the solution of antiseptic that dissolved and the solution of coloring agent formation 4 mixture; Antiseptic is 0.0096kg diazolidinyl urea and 0.0001kg iodine propilolic alcohol butyl mephenesin Carbamate; Coloring agent is each 0.0002kg of CI15985 and CI16035;
When (7) 4 mixtures are cooled to 45 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine 0.0038kg, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) the 5th mixture are cooled to 30 DEG C and add in emulsifying pot by 0.02kg essence, stir 16min, to completely evenly obtaining required product.
embodiment 2
The present embodiment is identical with the formula of embodiment 1, and difference is in preparation process, and technological parameter is different, specific as follows:
Its preparation method comprises the following steps:
(1) raw material 10kg is altogether taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionization 7.806kg water and be heated to 98 DEG C, the deionized water that unlatching vacuum pump extraction 7.6kg has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent again, antiseptic and chelating agen EDETATE SODIUM 0.012kg, be heated to 85 DEG C, and stir formation first mixture; In the present embodiment, skin conditioning agent is 0.8kg ethoxy urea and each 0.02kg of allantoin; In the present embodiment, antiseptic is 0.0203kg methyl hydroxybenzoate;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.003kg wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with the first mixture, rapid stirring is even, homogenizing 1min, stir 10min again and form the second mixture, start cooling; In the present embodiment, wetting agent is 0.6kg propylene glycol, 0.2kg betanin;
When (5) second mixture are cooled to 85 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2min, stirring 10min to evenly forming the 3rd mixture; In the present embodiment, skin conditioning agent is 0.8kg Hamamelis virginiana extract, 0.2kg dimethione and 0.18kg squalane;
(6), when in the present embodiment, the 3rd mixture is cooled to 53 DEG C, to stir adding emulsifying pot with deionized water and the solution of antiseptic that dissolved and the solution of coloring agent formation 4 mixture; Antiseptic is 0.0096kg diazolidinyl urea and 0.0001kg iodine propilolic alcohol butyl mephenesin Carbamate; Coloring agent is each 0.0002kg of CI15985 and CI16035;
When (7) 4 mixtures are cooled to 45 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine 0.0038kg, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) the 5th mixture are cooled to 32 DEG C and add in emulsifying pot by 0.02kg essence, stir 15min, to completely evenly obtaining required product.
embodiment 3
The present embodiment is identical with the formula of embodiment 2 with embodiment 1, and difference is in preparation process, and technological parameter is different, specific as follows:
Its preparation method comprises the following steps:
(1) raw material 10kg is altogether taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionization 7.806kg water and be heated to 98 DEG C, the deionized water that unlatching vacuum pump extraction 7.6kg has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent again, antiseptic and chelating agen EDETATE SODIUM 0.012kg, be heated to 85 DEG C, and stir formation first mixture; In the present embodiment, skin conditioning agent is 0.8kg ethoxy urea and each 0.02kg of allantoin; In the present embodiment, antiseptic is 0.0203kg methyl hydroxybenzoate;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.003kg wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with the first mixture, rapid stirring is even, homogenizing 3min, stir 5min again and form the second mixture, start cooling; In the present embodiment, wetting agent is 0.6kg propylene glycol, 0.2kg betanin;
When (5) second mixture are cooled to 85 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 4min, stirring 10min to evenly forming the 3rd mixture; In the present embodiment, skin conditioning agent is 0.8kg Hamamelis virginiana extract, 0.2kg dimethione and 0.18kg squalane;
(6), when in the present embodiment, the 3rd mixture is cooled to 54 DEG C, to stir adding emulsifying pot with deionized water and the solution of antiseptic that dissolved and the solution of coloring agent formation 4 mixture; Antiseptic is 0.0096kg diazolidinyl urea and 0.0001kg iodine propilolic alcohol butyl mephenesin Carbamate; Coloring agent is each 0.0002kg of CI15985 and CI16035;
When (7) 4 mixtures are cooled to 50 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine 0.0038kg, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) the 5th mixture are cooled to 40 DEG C and add in emulsifying pot by 0.02kg essence, stir 18min, to completely evenly obtaining required product.
embodiment 4
The present embodiment is identical with the formula of 3 with embodiment 1,2, and difference is in preparation process, and technological parameter is different, specific as follows:
Its preparation method comprises the following steps:
(1) raw material 10kg is altogether taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionization 7.806kg water and be heated to 98 DEG C, the deionized water that unlatching vacuum pump extraction 7.6kg has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent again, antiseptic and chelating agen EDETATE SODIUM 0.012kg, be heated to 85 DEG C, and stir formation first mixture; In the present embodiment, skin conditioning agent is 0.8kg ethoxy urea and each 0.02kg of allantoin; In the present embodiment, antiseptic is 0.0203kg methyl hydroxybenzoate;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.003kg wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with the first mixture, rapid stirring is even, homogenizing 1min, stir 5min again and form the second mixture, start cooling; In the present embodiment, wetting agent is 0.6kg propylene glycol, 0.2kg betanin;
When (5) second mixture are cooled to 71 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2min, stirring 10min to evenly forming the 3rd mixture; In the present embodiment, skin conditioning agent is 0.8kg Hamamelis virginiana extract, 0.2kg dimethione and 0.18kg squalane;
(6), when in the present embodiment, the 3rd mixture is cooled to 50 DEG C, to stir adding emulsifying pot with deionized water and the solution of antiseptic that dissolved and the solution of coloring agent formation 4 mixture; Antiseptic is 0.0096kg diazolidinyl urea and 0.0001kg iodine propilolic alcohol butyl mephenesin Carbamate; Coloring agent is each 0.0002kg of CI15985 and CI16035;
When (7) 4 mixtures are cooled to 40 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine 0.0038kg, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) the 5th mixture are cooled to 32 DEG C and add in emulsifying pot by 0.02kg essence, stir 20min, to completely evenly obtaining required product.
embodiment 5
The present embodiment is not identical with the formula of 4 with embodiment 1,2,3, and difference is skin conditioning agent 30%, and in preparation process, technological parameter is also different, specific as follows:
Its preparation method comprises the following steps:
(1) raw material 10kg is altogether taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionization 6.806kg water and be heated to 98 DEG C, the deionized water that unlatching vacuum pump extraction 6.6kg has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent again, antiseptic and chelating agen EDETATE SODIUM 0.012kg, be heated to 85 DEG C, and stir formation first mixture; In the present embodiment, skin conditioning agent is 1.2kg ethoxy urea and each 0.03kg of allantoin; In the present embodiment, antiseptic is 0.0203kg methyl hydroxybenzoate;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.003kg wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with the first mixture, rapid stirring is even, homogenizing 1min, stir 5min again and form the second mixture, start cooling; In the present embodiment, wetting agent is 0.6kg propylene glycol, 0.2kg betanin;
When (5) second mixture are cooled to 75 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2min, stirring 20min to evenly forming the 3rd mixture; In the present embodiment, skin conditioning agent is 1.2kg Hamamelis virginiana extract, 0.3kg dimethione and 0.27kg squalane;
(6), when in the present embodiment, the 3rd mixture is cooled to 53 DEG C, to stir adding emulsifying pot with deionized water and the solution of antiseptic that dissolved and the solution of coloring agent formation 4 mixture; Antiseptic is 0.0096kg diazolidinyl urea and 0.0001kg iodine propilolic alcohol butyl mephenesin Carbamate; Coloring agent is each 0.0002kg of CI15985 and CI16035;
When (7) 4 mixtures are cooled to 45 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine 0.0038kg, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) the 5th mixture are cooled to 37 DEG C and add in emulsifying pot by 0.02kg essence, stir 19min, to completely evenly obtaining required product.
Carry out hygienic chemistry Indexs measure (table 1) and microbiological indicator detection (table 2) all conformance with standard to the control oil balance Firm breast in embodiment 1, detection method is as shown in table 3.
Table 1
| Project | Unit | Index request |
| Plumbous | mg/kg | ≤40 |
| Hydrargyrum | mg/kg | ≤1 |
| Arsenic | mg/kg | ≤10 |
Table 2
| Project | Unit | Index request |
| Total plate count | CFU/g | ≤1000 |
| Yeast and mold sum | CFU/g | ≤100 |
| Excrement colibacillus group | — | Must not detect |
| Staphylococcus aureus | — | Must not detect |
| Pseudomonas aeruginosa | — | Must not detect |
Table 3
One control oil balance Firm breast using method provided by the invention is after clean, getting appropriate this product uniform application in face, massaging 1-2 minute gently to fully absorbing.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from spirit of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (10)
1. a control oil balance Firm breast, it is characterized in that, its component and raw material weight percentage ratio are:
Skin conditioning agent 2% ~ 30%,
Wetting agent 1% ~ 30%,
Emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer 0.1% ~ 5%,
PH regulator triethanolamine 0.5% ~ 10%,
Antiseptic 0.1% ~ 2%,
Odorant essence 0.02% ~ 2%,
Chelating agen EDETATE SODIUM 0.01% ~ 2%,
Coloring agent 0.00001% ~ 1.0%,
Surplus is deionized water solvent.
2. one control oil balance Firm breast according to claim 1, is characterized in that: described skin conditioning agent is one or more in Hamamelis virginiana extract, dimethione, squalane, ethoxy urea, allantoin.
3. one control oil balance Firm breast according to claim 1, is characterized in that: described wetting agent is one or both in betanin, propylene glycol.
4. one control oil balance Firm breast according to claim 1, is characterized in that: described antiseptic is one or more in methyl hydroxybenzoate, diazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate.
5. one control oil balance Firm breast according to claim 1, is characterized in that: described coloring agent is one or both in CI15985, CI16035.
6. control a preparation method for oil balance Firm breast, it is characterized in that, comprise the following steps:
(1) raw material is taken according to the percentage by weight of raw material;
(2) in aqueous phase pot, add deionized water and be heated to 90 ~ 100 DEG C, the deionized water that unlatching vacuum pump extraction part has heated is in emulsifying pot;
(3) in emulsifying pot, add skin conditioning agent, antiseptic and chelating agen EDETATE SODIUM again, be heated to 85 ~ 90 DEG C, stir formation first mixture;
(4) after emulsifing thickener acrylic acid (ester) class/C10 ~ 30 alkylol acrylamide acid esters cross linked polymer wetting agent being uniformly dispersed in plastic barrel, add in emulsifying pot and mix with described first mixture, rapid stirring is even, homogenizing 1 ~ 3min, stir 5 ~ 10min again and form the second mixture, start cooling;
(5) when described second mixture is cooled to 70 ~ 85 DEG C, skin conditioning agent being added in emulsifying pot, homogenizing 2 ~ 5min, stirring 10 ~ 20min to evenly forming the 3rd mixture;
(6), when described 3rd mixture is cooled to 50 ~ 55 DEG C, to stir adding emulsifying pot with the good antiseptic solution of deionized water dissolving and colourant solution formation 4 mixture;
(7) when described 4 mixture is cooled to 40 ~ 50 DEG C, add in emulsifying pot after the deionized water dissolving remaining by PH regulator triethanolamine, rapid stirring forms the 5th mixture to the fine and smooth light of emulsion;
(8) described 5th mixture is cooled to 30 ~ 40 DEG C and adds in emulsifying pot by essence, stirs 15 ~ 20min, to completely evenly obtaining required product.
7. one control oil balance Firm breast preparation method according to claim 6, is characterized in that: in described step (3), skin conditioning agent is ethoxy urea, allantoin, and antiseptic is methyl hydroxybenzoate.
8. one control oil balance Firm breast preparation method according to claim 6, is characterized in that: in described step (4), wetting agent is betanin, propylene glycol.
9. one control oil balance Firm breast preparation method according to claim 6, is characterized in that: in described step (5), skin conditioning agent is Hamamelis virginiana extract, dimethione and squalane.
10. one control oil balance Firm breast preparation method according to claim 6, is characterized in that: antiseptic described in described step (6) is diazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate; Described coloring agent is CI15985 and CI16035.
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| CN201510460408.1A CN105232364A (en) | 2015-07-29 | 2015-07-29 | Oil-control balancing and refirming emulsion and preparation method thereof |
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Application publication date: 20160113 |