CN107213040A - A kind of natural no added camellia moisturiser and preparation method thereof - Google Patents

A kind of natural no added camellia moisturiser and preparation method thereof Download PDF

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Publication number
CN107213040A
CN107213040A CN201710590029.3A CN201710590029A CN107213040A CN 107213040 A CN107213040 A CN 107213040A CN 201710590029 A CN201710590029 A CN 201710590029A CN 107213040 A CN107213040 A CN 107213040A
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moisturiser
added
phase components
natural
camellia
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郑生华
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/39Derivatives containing from 2 to 10 oxyalkylene groups
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/42Amides
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70Biological properties of the composition as a whole
    • A61K2800/72Hypo-allergenic

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Abstract

The present invention relates to a kind of natural no added camellia moisturiser, it is characterised in that:Percentage composition includes following components by weight:A phase components:7.0~70.0%;B phase components:20.0~90%;C phase components:0.8~15%;The preparation method of the moisturiser comprises the following steps:A, by A phases component add emulsification pot in, stirring mixed dissolution it is uniform;B, B phases component added in oil phase material pot, stirring mixed dissolution is uniform;Stir pre-emulsification in c, the emulsification pot that the B phases component obtained by step b is pumped into step a, then carries out homogeneous, insulated and stirred, the cooling of vacuum froth breaking;D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;E, detection are qualified, discharging, you can.The advantage of the invention is that:The common moisturiser of in the market is overcome using dangerous chemicals such as ore deposit oil ﹑ silicon oil essence ﹑ color element ﹑ wine essence ﹑ preservatives, being easily caused stimulates the security disadvantages of skin.

Description

A kind of natural no added camellia moisturiser and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, particularly a kind of natural no added camellia moisturiser and preparation method thereof.
Background technology
Frost is a kind of chemicals mixed by a variety of chemical substances, and the skin of baby is more tender and lovely, uses some common guarantors Wet frost is possible to cause allergic or stimulation skin.
Camellia oil, also known as tea-seed oil.It is derived from tea oil tree.Tea oil tree, Theaceae, oil tea belongs to evergreen dungarunga.It is that the world four is big One of woody oleiferous plants, it be grown in south China subtropical zone high mountain and hilly country be that the distinctive one kind of China is pure natural Senior oil plant.The manufacturing process of camellia oil can be divided into:Shell, dry, crush, extract oil, filtering, overall process is physical method, Erucic acid, cholesterol, aflatoxins and other additives are free of in tea oil, therefore it is real fully natural green edible oil.Mountain Tea oil is nutritious, and fatty acids (unrighted acid 93%, wherein oleic acid 82%, linoleic acid 11%), camellianin, tea are more Phenol, saponin, tannin, and the squalene rich in antioxidant and with anti-inflammatory effect, squalene and Flavonoid substances, have to anticancer Splendid effect.Camellia oil is also rich in the trace element such as vitamin E and calcium, iron, zinc, is described as by physician and nutritionist " The Zn-ef ficiency of flowers of life ", content is 10 times of soybean oil, in tea oil amino acid contained species be in all edible oil at most 's.Camellia oil have moisturizing, moisten, hair care beautifying function, for taking care of hair, can anti-hairs break and alopecia, rubbed one's body with a towel after bath, strengthen Skin elasticity, and skin pruritus in winter can be prevented and treated.And camellia oil has medicinal and edible performance, with good gentle security Can, it is adaptable to which cosmetic industry is used, it is also adapted to pregnant woman and baby is applicable, the diaper rash, eczema for baby is safe and effective.
Six polyglycerol monostearates, are a kind of emulsifying agents of food-grade, and its HLB value is about 11-12, are usually used in snow Cake, ice lolly, ice cream, vegetable protein beverage, sour milk beverage, maximum usage amount l0.0g/kg is a kind of edible emulsification Agent.Six polyglycerol monostearates, make O/W type emulsifying agents, with good emulsification, it is scattered, stably, the performance such as even bubble.Odorless, taste Micro- sweet tea.Glycerine, benzene, propane diols, the ethanol and cold ethyl acetate of heat are dissolved in, stirring can insoluble in cold water, but in the hot water It is dispersed into emulsion.HLB value is about 11-12.Make emulsifying agent using six polyglycerol monostearates in cosmetics, can be not Add other additives, the material such as silicone oil can also make beautiful cream, and its odorless, not interfere with the smell of cream, and And also have the effect for preventing chapped anti-chap.Polyglycerol ester tool also has certain antibiotic property, can suppress the growth of multiple-microorganism, such as uses In canned and packed food.
PHL composition be decoyl hydroximic acid (CAPRYLHYDROXAMIC ACID), 1,3- propane diols (PROPANEDIOL), 1,2- hexylene glycol (1,2-HEXANEDIOL), be it is a kind of harmless to human body skin, it is safe, not in cosmetics preservative model Farmland, but it plays the role of bacteriostasis antibiosis within validity date.Used suitable for no added cosmetics.This product uses PHL conducts Preservative, other preservatives are not added, can ensure that the security of product.Decoyl hydroximic acid is a kind of preferable organic acid, There is excellent antibacterial, bacteriostasis property at neutral ph, available for without chemical preservative formula system.Decoyl hydroximic acid is The acid organic acid for all keeping not having ionized state to neutral whole process, is optimal antibacterial organic acid.There is highly effective chelating effect, suppress mould The active element that bacterium needs, limits the environment needed for microorganism growth.Decoyl hydroximic acid and raw materials most absolutely have simultaneous dissolubility, Do not influenceed by the raw material such as surfactant, protein in system, can and alcohols, the preservative such as glycols compounding.Can be Added under normal temperature and hot environment.It is widely used in the skincare products and hair care articles such as gel, essence, emulsion, cream, shampoo, shower lotion In.
The content of the invention
It is an object of the invention to the shortcoming for overcoming prior art, there is provided a kind of natural no added camellia moisturiser and its system Preparation Method, solves the safety issue of common baby's moisturiser.
The purpose of the present invention is achieved through the following technical solutions:A kind of natural no added camellia moisturiser, by weight hundred Content is divided to include following components:
A phase components:7.0~70.0%;
B phase components:20.0~90%;
C phase components:0.8~15%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:50.0~70.0%;
Glycerine:10.0~20.0%;
Allantoin:0.01~0.5%;
Hyaluronic acid:10.0~30.0%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:30.0~60.0%;
1,3-PD:18.0~40.0%;
1,6- hexylene glycol:18.0~40.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 80~85 DEG C, stirring mixed dissolution is uniform;
B, each material of B phase components added in oil phase material pot, be heated to 80~85 DEG C, stirring mixed dissolution is equal It is even;
Stir 10~15min of pre-emulsification in c, the emulsification pot that the B phases component obtained by step b is pumped into step a, so 5~10min homogeneous, 5~8min of insulated and stirred, the cooling of vacuum froth breaking are carried out afterwards;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
Further, in step a, mixing speed is 20~30rpm, stirs 15~20min.
Further, in step b, mixing speed is 15~20rpm, stirs 14~16min.
The present invention has advantages below:
1st, some ore deposits oil ﹑ silicon oil essence ﹑ color element ﹑ wine essences ﹑ is used instant invention overcomes moisturiser common on existing market The dangerous chemicals such as preservative, being easily caused stimulates the security disadvantages of skin.
2nd, the present invention, which has, grows the gentle effect of the anti-chap safety of the wet ﹑ of profit guarantor.
What the 3rd, effect thing of the present invention was used is all natural plant grease camellia oil, utilizes the polyglycereol list of food grade emulsifier six Stearate, prepares moist moisturizing and the gentle baby's moisturiser of safety.
4th, no added preservative of the invention, can also play anti-corrosion function.
5th, moisturiser of the invention is that one kind may cause uneasiness without preservative, pigment, Dormant oils, essence, alcohol etc. Full material.Natural camellia vegetable oil, you can edible, in cosmetics, also there is the function of skin-moisturizing, skin etc., and color and luster is partially yellow, There is light camellia fragrant.It is used together with the polyglycerol monostearate of food grade emulsifier six, other additions can be not added with The cream that color and luster is beautiful attractive in appearance and smell is simple and elegant is made in the case of agent.And have to the moist moisturizing of infant skin and safety temperature Effect of sum.
Embodiment
With reference to embodiment, the present invention will be further described, but protection scope of the present invention is not limited to following institute State.
【Embodiment 1】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:7.0%;
B phase components:90%;
C phase components:3.0%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:50.0%;
Glycerine:20.0%;
Allantoin:0.5%;
Hyaluronic acid:29.5%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:30.0%;
1,3-PD:40.0%;
1,6- hexylene glycol:30.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 80 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 20rpm, stirring 15min;
B, each material of B phase components added in oil phase material pot, be heated to 80 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 15rpm, 14min is stirred;
Stir pre-emulsification 10min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 5min homogeneous, insulated and stirred 5min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
【Embodiment 2】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:70.0%;
B phase components:20.0%;
C phase components:10.0%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:70.0%;
Glycerine:10.0%;
Allantoin:0.01%;
Hyaluronic acid:19.99%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:60.0%;
1,3-PD:18.0%;
1,6- hexylene glycol:22.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 85 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 30rpm, stirring 20min;
B, each material of B phase components added in oil phase material pot, be heated to 85 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 20rpm, 16min is stirred;
Stir pre-emulsification 15min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 10min homogeneous, insulated and stirred 8min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
【Embodiment 3】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:38.0%;
B phase components:55.0%;
C phase components:7.0%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:60.0%;
Glycerine:15.0%;
Allantoin:0.24%;
Hyaluronic acid:24.76%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:45.0%;
1,3-PD:29.0%;
1,6- hexylene glycol:26.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 82 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 25rpm, stirring 18min;
B, each material of B phase components added in oil phase material pot, be heated to 83 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 17rpm, 15min is stirred;
Stir pre-emulsification 12min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 8min homogeneous, insulated and stirred 6min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
【Embodiment 4】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:9.2%;
B phase components:90%;
C phase components:0.8%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:69.7%;
Glycerine:19.8%;
Allantoin:0.5%;
Hyaluronic acid:10.0%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:45.0%;
1,3-PD:37.0%;
1,6- hexylene glycol:18.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 81 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 22rpm, stirring 19min;
B, each material of B phase components added in oil phase material pot, be heated to 84 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 18rpm, 16min is stirred;
Stir pre-emulsification 11min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 9min homogeneous, insulated and stirred 5min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
【Embodiment 5】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:45%;
B phase components:40%;
C phase components:15%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:54.7%;
Glycerine:15.0%;
Allantoin:0.3%;
Hyaluronic acid:30.0%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:30.0%;
1,3-PD:30.0%;
1,6- hexylene glycol:40.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 85 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 25rpm, stirring 18min;
B, each material of B phase components added in oil phase material pot, be heated to 84 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 16rpm, 16min is stirred;
Stir pre-emulsification 15min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 5min homogeneous, insulated and stirred 8min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
【Embodiment 6】:
A kind of natural no added camellia moisturiser, by weight percentage composition includes following components:
A phase components:45%;
B phase components:40%;
C phase components:15%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is sweet by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric Oily three esters composition;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
Further, each composition is constituted by following percentage composition in the A phases component:
Water:54.7%;
Glycerine:15.0%;
Allantoin:0.3%;
Hyaluronic acid:30.0%.
Further, each composition is constituted by following percentage composition in the B phases component:
Further, each composition is constituted by following percentage composition in the C phases component:
Decoyl hydroximic acid:30.0%;
1,3-PD:30.0%;
1,6- hexylene glycol:40.0%.
Further, the water in the A phases component is deionized water.
A kind of preparation method of natural no added camellia moisturiser, it is characterised in that:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 85 DEG C, stirring mixed dissolution is uniform, stirring speed Spend for 25rpm, stirring 18min;
B, each material of B phase components added in oil phase material pot, be heated to 84 DEG C, stirring mixed dissolution is uniform, stirs Speed is mixed for 16rpm, 16min is stirred;
Stir pre-emulsification 15min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 5min homogeneous, insulated and stirred 8min, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
Part raw material sources and model are shown in Table 1 in various embodiments above:
Table 1:
Measure of merit:
Skin moisturizing moisturizing, anti-chap maintenance measure of merit:
Clinical trial subjects measures of effectiveness
From double blinding, random, comparative study test;Object (n=20) uses the cream and in the market ratio of Application Example 3 More popular common baby's moisturiser does placebo, twice a day, continuous surrounding.Volunteer is that healthy baby is virgin, the age At 0-16 Sui, using the cream of Application Example 2 in left face region, using placebo cream in right face region.
Tested under the environment that winter conditions are dried.Tester is scored and tested not using skin moisture analyzer Evaluated with region water content method
Wherein:Test result is scored with 5 points of full marks processed, preferably 5 points, and worst is 0 point, its assessment result such as table Shown in 2.
Table 2:
Group 1 2 3 4 5 6 7 8 9 10 Average value
Left face 5 4 4 5 4 4 3 5 3 5
Right face 4 4 3 5 3 3 2 3 2 5
Group 11 12 13 14 15 16 17 18 19 20
Left face 4 5 4 5 3 5 4 5 2 5 4.2
Right face 4 4 4 3 3 4 4 3 2 3 3.25
Cutaneous safety is tested:
Clinical trial subjects measures of effectiveness
From double blinding, random, comparative study test;Object (n=20) uses the cream and in the market ratio of Application Example 2 More popular common baby's moisturiser does placebo, twice a day, continuous surrounding.Volunteer is the baby born a pretty, delicate skin Child, the age is relatively popular and common using in the market using the cream of Application Example 2 in left face region at 0-16 Sui Baby's moisturiser placebo blank cream in right face region.
Observation tester's skin whether there is discomfort, and tester's readme is scored and using skin analyzer test different zones skin Being upset property is evaluated.
Wherein:Test result is scored with 5 points of full marks processed, and non-stimulated preferably 5 points, worst is 0 point, and it assesses knot Fruit is as shown in table 3.
Table 3:
Group 1 2 3 4 5 6 7 8 9 10 Average value
Left face 4 4 5 5 5 5 5 5 5 5
Right face 2 2 1 0 3 0 0 1 0 1
Group 11 12 13 14 15 16 17 18 19 20
Left face 5 5 4 4 5 5 4 5 5 5 4.75
Right face 0 1 2 1 2 2 1 1 2 2 1.2
Preservative challenge testing:
Using the cream and in the market of Application Example 3 it is relatively popular be not that no added baby's moisturiser does and pacified Console agent, equivalent and same species of microorganism are inoculated with weekly, observation microorganism growing state is as shown in table 4:
Table 4:
It can to sum up show that moist moistening effect is slightly better than general goods after this product use, and safety is gentle non-stimulated. Although no added preservative, antiseptic property is good, before the deadline can be with safe to use.

Claims (8)

1. a kind of natural no added camellia moisturiser, it is characterised in that:Percentage composition includes following components by weight:
A phase components:7.0~70.0%;
B phase components:20.0~90%;
C phase components:0.8~15%;
Wherein:A phases component is made up of water, glycerine, allantoin and hyaluronic acid;
B phases component is by six polyglycerol monostearates, camellia oil, 1618 alcohol, stearic acid, saualane and caprylic/capric glycerine three Ester is constituted;
C phases component is made up of decoyl hydroximic acid, 1,3-PD and 1,6- propane diols.
2. a kind of natural no added camellia moisturiser according to claim 1, it is characterised in that:It is each in the A phases component Composition is constituted by following percentage composition:
Water:50.0~70.0%;
Glycerine:10.0~20.0%;
Allantoin:0.01~0.5%;
Hyaluronic acid:10.0~30.0%.
3. a kind of natural no added camellia moisturiser according to claim 1, it is characterised in that:It is each in the B phases component Composition is constituted by following percentage composition:
4. a kind of natural no added camellia moisturiser according to claim 1, it is characterised in that:It is each in the C phases component Composition is constituted by following percentage composition:
Decoyl hydroximic acid:30.0~60.0%;
1,3-PD:18.0~40.0%;
1,6- hexylene glycol:18.0~40.0%.
5. a kind of natural no added camellia moisturiser according to claim 1 or 2, it is characterised in that:In the A phases component Water be deionized water.
6. a kind of preparation method of natural no added camellia moisturiser as claimed in any one of claims 1 to 5, wherein, its feature exists In:Comprise the following steps:
A, each material of A phase components added in emulsification pot, be heated to 80~85 DEG C, stirring mixed dissolution is uniform;
B, each material of B phase components added in oil phase material pot, be heated to 80~85 DEG C, stirring mixed dissolution is uniform;
Stir pre-emulsification 10~15min, Ran Houjin in c, the emulsification pot that the B phases component obtained by step b is pumped into step a Row 5~10min homogeneous, 5~8min of insulated and stirred, the cooling of vacuum froth breaking;
D, when being cooled to 45 DEG C, add C phase components stir, be cooled to normal temperature;
E, detection are qualified, discharging, you can.
7. a kind of preparation method of natural no added camellia moisturiser according to claim 6, it is characterised in that:Step a In, mixing speed is 20~30rpm, stirs 15~20min.
8. a kind of preparation method of natural no added camellia moisturiser according to claim 6, it is characterised in that:Step b In, mixing speed is 15~20rpm, stirs 14~16min.
CN201710590029.3A 2017-07-19 2017-07-19 A kind of natural no added camellia moisturiser and preparation method thereof Pending CN107213040A (en)

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CN107669499A (en) * 2017-11-21 2018-02-09 郑生华 A kind of baby's physical sunscreen breast and preparation method
CN109745264A (en) * 2019-03-26 2019-05-14 丹东欣时代生物医药科技有限公司 A kind of preparation method of the mild moisturiser of no anti-corrosion addition
CN110507554A (en) * 2019-09-06 2019-11-29 王文概 A kind of natural no added moisturiser and preparation method thereof containing camellia seed oil
CN111067822A (en) * 2020-01-10 2020-04-28 广州贝玛生物科技有限公司 Shea butter infant moisturizing and wrinkle-preventing cream and preparation method thereof
CN113318063A (en) * 2021-07-07 2021-08-31 江西省康之鑫实业发展有限公司 Camellia oil skin cream and preparation method thereof

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CN106420532A (en) * 2016-11-24 2017-02-22 李心宇 Traditional Chinese herbal medicine essence emulsion with efficacies of freckle removing, whitening, skin moisturizing and inflammation diminishing, preparation method of traditional Chinese herbal medicine essence emulsion and facial mask

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CN107669499A (en) * 2017-11-21 2018-02-09 郑生华 A kind of baby's physical sunscreen breast and preparation method
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CN110507554A (en) * 2019-09-06 2019-11-29 王文概 A kind of natural no added moisturiser and preparation method thereof containing camellia seed oil
CN111067822A (en) * 2020-01-10 2020-04-28 广州贝玛生物科技有限公司 Shea butter infant moisturizing and wrinkle-preventing cream and preparation method thereof
CN113318063A (en) * 2021-07-07 2021-08-31 江西省康之鑫实业发展有限公司 Camellia oil skin cream and preparation method thereof

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Application publication date: 20170929