CN107669499A - A kind of baby's physical sunscreen breast and preparation method - Google Patents
A kind of baby's physical sunscreen breast and preparation method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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Abstract
The present invention relates to a kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:A phase components:7.0~70.0 parts of water;1.0~20.0 parts of glycerine;0.1~1.0 part of carbomer;0.1~1.0 part of arginine;1.0~10.0 parts of titanium dioxide;0.5~10.0 part of zinc oxide;B phase components:1.0~50.0 parts of 20 alkyl glucosides of C12;20.0~90.0 parts of cetostearyl alcohol;1.0~50.0 parts of camellia oil;1.0~90.0 parts of jojoba seed oil;5.0~20.0 parts of caprylic/capric triglyceride;C phase components:0.5~1.0 part of decoyl hydroximic acid;0.1~0.2 part of Sensiva SC50;1,2 1.0~2.0 parts of hexylene glycol;Additionally provide its preparation method.The advantage of the invention is that:Overcome the problem of easily being tanned severely when baby travels outdoors; the preventing coating protection of baby, child skin is acted on; also there is certain moist moisture-keeping efficacy; there is the physical characteristic of reflection and scattering using inorganic particles to ultraviolet, visible ray, infra-red radiation, prepare baby's physical sunscreen breast with preventing coating protection effect.
Description
Technical field
The present invention relates to articles for babies technical field, particularly a kind of baby's physical sunscreen breast and preparation method.
Background technology
Outside world beauty is colorful, is easily injured yet with bearing a pretty, delicate skin for baby by the external world, such as vigor four
Penetrate and it is burning can be hard to guard against directly the skin sunburn of baby.The present invention is the physical sunscreen breast that a kind of baby uses,
Reflected using inorganic particles such as titanium dioxide, zinc oxide or scatter most ultraviolet, visible and infra-red radiation, it is non-stimulated to baby
And moisten wound of the moisturizing and can using most ultraviolet, the visible and infra-red radiation reduction of the reflection of physics or scattering to skin
Evil.Therefore a kind of baby's physical sunscreen breast of the present invention adapts to the demand in market.
Zinc oxide:It is a kind of inorganic particles, white powder, odorlessness, 4.0~15.0nm of crystal size, specific area (BET
Method) 90.0~140.0 ㎡/g, the refraction index of zinc oxide is about 2.In sun care preparations, China, European Union and the U.S. allow to use
Highest mass fractions are 25%, and Japan is no to use limitation.UVA/B absorbents are moderate, are comparatively ideal broad spectrum sunscreens,
Also Antifungal activities, with other preservative compatibilities, match somebody with somebody with nonionic surfactant and most of anion surfactants
5.It is disperse easily in each quasi-grease, O/W or W/O emulsions is made.Zinc oxide or a kind of metalloenzyme, it is DNA and RNA synthesis
Required, some lesions physiologically may be relevant with zinc-deficiency, makees Derma-Guard available for skin disease ointment.And zinc oxide
Stability is preferable, can use and preserve for a long time.
Titanium dioxide:It is a kind of inorganic particles, white fine particulate powder is tasteless, 10~25nm of crystal size, compares surface
(BET method) 80~140 ㎡/g, refraction index 2.4~2.7.In sun care preparations, China, European Union and the U.S. allow to use highest
Mass fraction is 25%, and Japan is no to use limitation.Nano level superfine titanium dioxide is to stop UV radiation using light scattering effect,
UVA/B absorbents.The nano titanium oxide that existing market sale is surface-treated with serial of methods, facilitate handy, addition formula
It is middle that transparent or semitransparent state is presented, general white coating will not be produced on skin as pigmentary titanium dioxide;Efficiently, it is easy to add
Formula is added, for cream, emulsion, gel and aqua sunscreen.
The content of the invention
The shortcomings that it is an object of the invention to overcome prior art, there is provided a kind of baby's physical sunscreen breast and preparation method,
Solve the problems, such as that baby dare not easily be gone out by sunburn with baby.
The purpose of the present invention is achieved through the following technical solutions:A kind of baby's physical sunscreen breast, by following parts by weight
Raw material forms:
A phase components
7.0~70.0 parts of water;1.0~20.0 parts of glycerine;0.1~1.0 part of carbomer;0.1~1.0 part of arginine;Dioxy
Change 1.0~10.0 parts of titanium;0.5~10.0 part of zinc oxide;
B phase components
1.0~50.0 parts of C12-20 alkyl glucosides;20.0~90.0 parts of cetostearyl alcohol;1.0~50.0 parts of camellia oil;
1.0~90.0 parts of jojoba seed oil;5.0~20.0 parts of caprylic/capric triglyceride;
C phase components
0.5~1.0 part of decoyl hydroximic acid;0.1~0.2 part of Sensiva SC50;1,2- 1.0~2.0 parts of hexylene glycol.
Further, a kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:
A phase components
27.2 parts of water;11.0 parts of glycerine;0.6 part of carbomer;0.5 part of arginine;6.5 parts of titanium dioxide;Zinc oxide 5.2
Part;
B phase components
20.0 parts of C12-20 alkyl glucosides;55.0 parts of cetostearyl alcohol;25.5 parts of camellia oil;Jojoba seed oil 45.5
Part;12.5 parts of caprylic/capric triglyceride;
C phase components
0.7 part of decoyl hydroximic acid;0.15 part of Sensiva SC50;1,2- 1.5 parts of hexylene glycol.
A kind of preparation method of baby's physical sunscreen breast, comprises the following steps:
S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, then sequentially adds each material of A phase components in emulsification pot,
80~85 DEG C are heated to, is stirred and is uniformly dissolved;
S2, each material of B phase components added in oil phase material pot, be heated to 80~85 DEG C, it is equal to be stirred dissolving
It is even;
S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, the pre-emulsification that stirs 8~12min, Ran Houjin
Row 5~10min homogeneous, 4~6min of insulated and stirred, vacuum defoaming cooling;
S4, when being cooled to 43~47 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature;
S5, detection are qualified, discharging, obtain finished product.
Further, in step S1, the granularity of titanium dioxide, zinc oxide after grinding is 800~1000 mesh.
Further, in step S1, the concrete operation step of heating is:First emulsification pot is heated, emulsification kettle temperature reaches
During to 40~60 DEG C, then A phase components are added into emulsification pot, during stirring, using rotating alternate agitation method, mixing speed 20
~30rpm.
Further, in step S3, the vacuum of vacuum defoaming cooling is 0.2~0.4MPa.
Further, in step S4, cooling rate is 0.4~0.8 DEG C/min.
The present invention has advantages below:
The problem of easily being tanned severely when the 1st, being travelled outdoors instant invention overcomes baby, baby's quilt should be feared by reducing precious mothers
The worry tanned severely and dare not gone out.
2nd, the present invention has the preventing coating protection effect to baby, child skin, it may have certain moist moisture-keeping efficacy.
3rd, the present invention has the physical characteristic of reflection and scattering, system using inorganic particles to ultraviolet, visible ray, infra-red radiation
For going out, baby's physical sunscreen with preventing coating protection effect is newborn.
4th, the no added preservative of the present invention, can also play anti-corrosion function, and protection gentle to having for skin, moist is made
With suitable baby is virgin to be used.
Embodiment
With reference to embodiment, the present invention will be further described, but protection scope of the present invention is not limited to following institute
State.
【Embodiment 1】:
A kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:
A phase components
7.0 parts of water;20.0 parts of glycerine;1.0 parts of carbomer;1.0 parts of arginine;10.0 parts of titanium dioxide;Zinc oxide 10.0
Part;
B phase components
50.0 parts of C12-20 alkyl glucosides;20.0 parts of cetostearyl alcohol;1.0 parts of camellia oil;90.0 parts of jojoba seed oil;
20.0 parts of caprylic/capric triglyceride;
C phase components
0.5 part of decoyl hydroximic acid;0.2 part of Sensiva SC50;1,2- 1.0 parts of hexylene glycol.
A kind of preparation method of baby's physical sunscreen breast, comprises the following steps:
S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, the granularity of titanium dioxide, zinc oxide after grinding is 1000
Mesh, then each material of A phase components is sequentially added in emulsification pot, is heated to 85 DEG C, the concrete operation step of heating is:First
Emulsification pot is heated, when emulsification kettle temperature reaches 60 DEG C, then A phase components is added into emulsification pot, is stirred and is uniformly dissolved,
During stirring, using rotating alternate agitation method, mixing speed 30rpm;
S2, each material of B phase components added in oil phase material pot, be heated to 80 DEG C, be stirred and be uniformly dissolved;
S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, the pre-emulsification that stirs 12min, then carry out
10min homogeneous, insulated and stirred 6min, vacuum defoaming cooling, vacuum 0.2MPa;
S4, when being cooled to 47 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature, cooling rate is
0.8℃/min;
S5, detection are qualified, discharging, obtain finished product.
【Embodiment 2】:
A kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:
A phase components
27.2 parts of water;11.0 parts of glycerine;0.6 part of carbomer;0.5 part of arginine;6.5 parts of titanium dioxide;Zinc oxide 5.2
Part;
B phase components
20.0 parts of C12-20 alkyl glucosides;55.0 parts of cetostearyl alcohol;25.5 parts of camellia oil;Jojoba seed oil 45.5
Part;12.5 parts of caprylic/capric triglyceride;
C phase components
0.7 part of decoyl hydroximic acid;0.15 part of Sensiva SC50;1,2- 1.5 parts of hexylene glycol.
A kind of preparation method of baby's physical sunscreen breast, comprises the following steps:
S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, the granularity of titanium dioxide, zinc oxide after grinding is 900
Mesh, then each material of A phase components is sequentially added in emulsification pot, is heated to 82 DEG C, the concrete operation step of heating is:First
Emulsification pot is heated, when emulsification kettle temperature reaches 50 DEG C, then A phase components is added into emulsification pot, is stirred and is uniformly dissolved,
During stirring, using rotating alternate agitation method, mixing speed 25rpm;
S2, each material of B phase components added in oil phase material pot, be heated to 82 DEG C, be stirred and be uniformly dissolved;
S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, the pre-emulsification that stirs 10min, then carry out
8min homogeneous, insulated and stirred 5min, vacuum defoaming cooling, vacuum 0.3MPa;
S4, when being cooled to 45 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature, cooling rate is
0.6℃/min;
S5, detection are qualified, discharging, obtain finished product.
【Embodiment 3】:
A kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:
A phase components
14.9 parts of water;20.0 parts of glycerine;0.5 part of carbomer;0.5 part of arginine;7.0 parts of titanium dioxide;Zinc oxide 10.0
Part;
B phase components
1.0 parts of C12-20 alkyl glucosides;50.0 parts of cetostearyl alcohol;15.0 parts of camellia oil;5.0 parts of jojoba seed oil;
5.0 parts of caprylic/capric triglyceride;
C phase components
1.0 parts of decoyl hydroximic acid;0.1 part of Sensiva SC50;1,2- 1.0 parts of hexylene glycol.
A kind of preparation method of baby's physical sunscreen breast, comprises the following steps:
S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, the granularity of titanium dioxide, zinc oxide after grinding is 880
Mesh, then each material of A phase components is sequentially added in emulsification pot, is heated to 81 DEG C, the concrete operation step of heating is:First
Emulsification pot is heated, when emulsification kettle temperature reaches 55 DEG C, then A phase components is added into emulsification pot, is stirred and is uniformly dissolved,
During stirring, using rotating alternate agitation method, mixing speed 23rpm;
S2, each material of B phase components added in oil phase material pot, be heated to 84 DEG C, be stirred and be uniformly dissolved;
S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, the pre-emulsification that stirs 11min, then carry out
8min homogeneous, insulated and stirred 5min, vacuum defoaming cooling, vacuum 0.3MPa;
S4, when being cooled to 46 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature, cooling rate is
0.7℃/min;
S5, detection are qualified, discharging, obtain finished product.
【Embodiment 4】:
A kind of baby's physical sunscreen breast, is formed by the raw material of following parts by weight:
A phase components
70.0 parts of water;1.0 parts of glycerine;0.1 part of carbomer;0.1 part of arginine;1.0 parts of titanium dioxide;0.5 part of zinc oxide;
B phase components
1.0 parts of C12-20 alkyl glucosides;90.0 parts of cetostearyl alcohol;50.0 parts of camellia oil;1.0 parts of jojoba seed oil;
5.0 parts of caprylic/capric triglyceride;
C phase components
1.0 parts of decoyl hydroximic acid;0.1 part of Sensiva SC50;1,2- 2.0 parts of hexylene glycol.
A kind of preparation method of baby's physical sunscreen breast, comprises the following steps:
S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, the granularity of titanium dioxide, zinc oxide after grinding is 800
Mesh, then each material of A phase components is sequentially added in emulsification pot, is heated to 80 DEG C, the concrete operation step of heating is:First
Emulsification pot is heated, when emulsification kettle temperature reaches 40 DEG C, then A phase components is added into emulsification pot, is stirred and is uniformly dissolved,
During stirring, using rotating alternate agitation method, mixing speed 20rpm;
S2, each material of B phase components added in oil phase material pot, be heated to 85 DEG C, be stirred and be uniformly dissolved;
S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, the pre-emulsification that stirs 8min, then carry out
5min homogeneous, insulated and stirred 4min, vacuum defoaming cooling, vacuum 0.4MPa;
S4, when being cooled to 43 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature, cooling rate is
0.4℃/min;
S5, detection are qualified, discharging, obtain finished product.
Measure of merit:
Antitan agent is protected, and moistens moistening effect test:
Clinical trial subjects measures of effectiveness
From double blinding, random, comparative study test;Sunscreen and identical base of the object (n=20) using Application Example 2
The emulsion that matter formula does not add inorganic particles does placebo, twice a day, continuous surrounding.Volunteer is that healthy baby is virgin, year
Age 0-16 year, using the emulsion of Application Example 2 in left face region, using comfort agent emulsion in right face region.
Skin area after being smeared using fixed dosage ultra violet lamp 10 minutes, skin area is observed after four hours
Whether there is erythema situation because ultraviolet irradiates in skin.
Wherein:Test result is scored with 5 points of full marks processed, and preferably 5 points, worst is 0 point, its assessment result such as table
Shown in 1.
Table 1:
Group | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | Average value |
Left face | 5 | 4 | 4 | 5 | 4 | 4 | 3 | 5 | 3 | 5 | |
Right face | 1 | 0 | 0 | 2 | 1 | 1 | 2 | 0 | 0 | 1 | |
Group | 11 | 12 | 13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 | |
Left face | 4 | 5 | 4 | 5 | 3 | 5 | 4 | 5 | 2 | 5 | 4.2 |
Right face | 2 | 1 | 1 | 2 | 0 | 1 | 2 | 1 | 0 | 1 | 0.9 |
It can to sum up show that this product is better than ordinary emulsion effect using rear sun-proof protecting effect, and be adapted to baby child to make
With.
Claims (7)
- A kind of 1. baby's physical sunscreen breast, it is characterised in that:Formed by the raw material of following parts by weight:A phase components7.0~70.0 parts of water;1.0~20.0 parts of glycerine;0.1~1.0 part of carbomer;0.1~1.0 part of arginine;Titanium dioxide 1.0~10.0 parts;0.5~10.0 part of zinc oxide;B phase components1.0~50.0 parts of C12-20 alkyl glucosides;20.0~90.0 parts of cetostearyl alcohol;1.0~50.0 parts of camellia oil;Flash Bar 1.0~90.0 parts of seed oil;5.0~20.0 parts of caprylic/capric triglyceride;C phase components0.5~1.0 part of decoyl hydroximic acid;0.1~0.2 part of Sensiva SC50;1,2- 1.0~2.0 parts of hexylene glycol.
- A kind of 2. baby's physical sunscreen breast according to claim 1, it is characterised in that:Formed by the raw material of following parts by weight:A phase components27.2 parts of water;11.0 parts of glycerine;0.6 part of carbomer;0.5 part of arginine;6.5 parts of titanium dioxide;5.2 parts of zinc oxide;B phase components20.0 parts of C12-20 alkyl glucosides;55.0 parts of cetostearyl alcohol;25.5 parts of camellia oil;45.5 parts of jojoba seed oil;It is pungent 12.5 parts of acid/Triglyceride DDD;C phase components0.7 part of decoyl hydroximic acid;0.15 part of Sensiva SC50;1,2- 1.5 parts of hexylene glycol.
- A kind of 3. preparation method of baby's physical sunscreen breast as claimed in claim 1, it is characterised in that:Comprise the following steps:S1, titanium dioxide, zinc oxide ground into exquisiteness respectively, then sequentially added each material of A phase components in emulsification pot, heating 80~85 DEG C are warming up to, is stirred and is uniformly dissolved;S2, each material of B phase components added in oil phase material pot, be heated to 80~85 DEG C, be stirred and be uniformly dissolved;S3, by the B phases component obtained in step S2 be pumped into emulsification pot in, 8~12min of the pre-emulsification that stirs, then carry out 5~ 10min homogeneous, 4~6min of insulated and stirred, vacuum defoaming cooling;S4, when being cooled to 43~47 DEG C, C phase components are added into emulsification pot, stirs, is cooled to normal temperature;S5, detection are qualified, discharging, obtain finished product.
- A kind of 4. preparation method of baby's physical sunscreen breast according to claim 3, it is characterised in that:In step S1, grinding Titanium dioxide afterwards, the granularity of zinc oxide are 800~1000 mesh.
- A kind of 5. preparation method of baby's physical sunscreen breast according to claim 3, it is characterised in that:In step S1, heating Concrete operation step be:First emulsification pot is heated, when emulsification kettle temperature reaches 40~60 DEG C, then A is added into emulsification pot Phase component, during stirring, using rotating alternate agitation method, mixing speed is 20~30rpm.
- A kind of 6. preparation method of baby's physical sunscreen breast according to claim 3, it is characterised in that:In step S3, vacuum The vacuum of defoaming cooling is 0.2~0.4MPa.
- A kind of 7. preparation method of baby's physical sunscreen breast according to claim 3, it is characterised in that:In step S4, cooling Speed is 0.4~0.8 DEG C/min.
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CN109758394A (en) * | 2019-02-28 | 2019-05-17 | 王文概 | A kind of multiple-effect milky lotion and preparation method thereof containing camellia seed oil |
CN110115696A (en) * | 2019-06-10 | 2019-08-13 | 王文概 | A kind of dedicated sunscreen of baby child and preparation method thereof containing camellia seed oil |
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