CN109588694A - 可快速增加液体粘度的增稠组合物及其制备工艺 - Google Patents
可快速增加液体粘度的增稠组合物及其制备工艺 Download PDFInfo
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- CN109588694A CN109588694A CN201811530667.7A CN201811530667A CN109588694A CN 109588694 A CN109588694 A CN 109588694A CN 201811530667 A CN201811530667 A CN 201811530667A CN 109588694 A CN109588694 A CN 109588694A
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Abstract
本发明涉及可快速增加液体粘度的增稠组合物及其制备工艺,属于保健品、药品和食品技术领域。可快速增加液体粘度的增稠组合物,包括100~250重量份增稠胶体、10~30重量份水溶性小分子有机化合物;将水溶性小分子有机化合物制成质量浓度为5%~30%的溶液,喷涂在增稠胶体表面并干燥。本发明的优点是:通过将溶于含水的液体食品中快速增加液体食品的粘度,改善液体食品的口感,并防止发生吞咽困难患者误吸的意外。
Description
技术领域
本发明涉及可快速增加液体粘度的增稠组合物及其制备工艺,属于保健品、药品和食品技术领域。
背景技术
现有大多数液体食品由于粘度低,导致口感不饱满。为了改善这类产品的口感,使其更丰富厚重,可以加入食品增稠剂,增加其粘度,使之变稠。与粘度低的液体食品相比,被增稠的液体食品不仅口感丰富,增加口服顺应性,还可以使用户心理暗示具有饱腹感,达到心里满足。加入食物增稠剂的液体/半固体产品还可以满足吞咽困难患者的需求,降低被患者误吸的意外。吞咽困难可由中枢神经系统疾病、食管、口咽部疾病引起,亦可由吞咽肌肉的运动运动障碍所致,是常见的健康问题,其影响进食和饮水的安全、效率以及质量。吞咽困难会给患者带来很多危害,比如营养不良、脱水、肺炎;肺炎多是由于误吸导致的,在吞咽过程中食物团块分散成较小碎片,吞咽困难的患者可能会将小碎片食物/液体进入气道,进而进入肺中,造成误吸;如果足够的物质进入肺部,患者可能被肺部集聚的食物/液体窒息;即使小体积的被吸入食物都可以导致支气管肺炎感染,且慢性误吸可以导致支气管扩张症,并可能引发哮喘等疾病。
针对以上问题,目前国内外相关研究人员将吞咽困难患者的食物和饮品增稠,使食品和饮品具有适于患者食用的粘度,改善吞咽困难患者的营养摄入方式。目前具有改善食物粘度的营养产品多是以营养组合物和高分子量的食品级聚合物为主,其中高分子量的食品级聚合物为食品增稠剂,具有能够改善营养产品粘度的作用,使产品的粘度能够利于吞咽困难患者摄入营养成分。虽然,这些营养产品遇水后溶解,通过水合作用而产生初始粘度。但是,这类由于食品级聚合物在溶液中分散性不好,易发生团聚现象,形成“团块”,当患者在食品/饮品中使用该食品级聚合物时,仅食品级聚合物的表面溶解,而“团块”内部仍是非水合状态,因此成团的食品级聚合物没有完全水合,导致食品/饮品的初始粘度低,随着食品级聚合物慢慢进行水合,食品/饮品的粘度不断升高,最终趋于稳定。“成团”的食品级趋于完全水合是一个较长的过程,不利于患者及时使用食物。
发明内容
为了解决上述技术问题,本发明提供了可快速增加液体粘度的增稠组合物,使含水的液体食品能够快速达到所需的粘度,并改善液体食品的口感。
为实现上述目的,本发明采用以下技术方案:
可快速增加液体粘度的增稠组合物,其特征在于,包括100~250重量份增稠胶体、10~30重量份水溶性小分子有机化合物;将水溶性小分子有机化合物制成质量浓度为5%~30%的溶液,喷涂在增稠胶体表面并干燥。
该增稠组合物增稠性强,能够快速分散于食品/饮品中,并完全溶于水中,使食品/饮品成为具有稳定粘度的凝胶。本发明中的增稠胶体(尤其是黄原胶、魔芋胶、卡拉胶、瓜尔胶、刺槐豆胶、秋葵胶、香豆胶、羧甲基纤维素、葫芦巴胶、罗望子胶、肉桂胶、阿拉伯胶、印度胶、黄蓍胶、刺梧桐树胶)可溶于液体食品或饮品中,并使其具有粘度,但是该增稠胶体易团聚,导致其使用功能受限。为了防止增稠胶体团聚,本发明人设计了多种试验思路,进行了大量试验,尝试了稀释增稠胶体、增稠胶体与助分散物质物理混合等方法,但是效果均不理想。发明人创造性的采用表面修饰方法修饰增稠胶体表面,并通过筛选确定修饰剂为水溶性小分子有机化合物,进一步筛选水溶性小分子有机化合物为牛磺酸、甘氨酸、赖氨酸、丙氨酸、谷氨酸、脯氨酸、谷氨酰胺、丝氨酸、精氨酸、苯丙氨酸、苏氨酸、缬氨酸中的一种或多种,将水溶性小分子有机化合物溶液喷射在增稠胶体表面,从而有效地抑制了增稠胶体团聚现象。增稠胶体被水溶性小分子有机化合物结合,进行表面改性,使增稠胶体在含水食品(如液体食品、饮品)中能够快速溶解、最大程度的被分散,迅速形成均匀稳定具有一定粘度的食物,并明显地快速达到峰值粘度的速率。传统的增稠产品溶于液体食品中需要30min~2h才可达到较稳定的所需粘度,本发明所述的增稠组合物在5min内即可达到峰值粘度的95%,用时很短,而且粘度长时间处于稳定状态,所以本发明产品具有很强的实用性。除此之外,被本发明增稠的食品外观美好,增加用户食欲,使食品休闲化。本发明增稠胶体和水溶性小分子有机化合物的用量科学合理,如果水溶性小分子有机化合物用量过少,无法达到本发明快速增稠的目的;水溶性小分子有机化合物用量过多不仅会造成资源浪费,也会由于过多水溶性小分子有机化合物包裹增稠胶体,而稍稍减缓增稠胶体的增稠速度。
本发明可快速增加液体粘度的增稠组合物溶于水中,所述增稠组合物溶于水5min后的溶液粘度≥该溶液峰值粘度的95%。一般增稠组合物溶于水30min后的粘度基本不变,作为该溶液峰值粘度。
所述增稠胶体选自黄原胶、魔芋胶、卡拉胶、瓜尔胶、刺槐豆胶、秋葵胶、香豆胶、羧甲基纤维素、葫芦巴胶、罗望子胶、肉桂胶、阿拉伯胶、印度胶、黄蓍胶、刺梧桐树胶中的一种或多种。
所述水溶性小分子有机化合物选自牛磺酸、甘氨酸、赖氨酸、丙氨酸、谷氨酸、脯氨酸、谷氨酰胺、丝氨酸、精氨酸、苯丙氨酸、苏氨酸、缬氨酸中的一种或多种。
所述的可快速增加液体粘度的增稠组合物,还包括以下一种或多种成分:250~400重量份水溶性稀释剂和10~1000重量份功能性成分。
所述水溶性稀释剂选自麦芽糊精、麦芽糖醇、山梨醇、木糖醇、甘露醇、蔗糖、乳糖、糊精、可溶性淀粉、可压性淀粉、低聚果糖、低聚麦芽糖中的一种或多种。
所述功能性成分选自营养成分、蛋白质、脂肪源、纤维、碳水化合物源、益生元、益生菌、氨基酸、脂肪酸、植物营养素、抗氧化剂中的一种或多种。
所述的可快速增加液体粘度的增稠组合物,还包括以下一种或多种成分:100~200重量份填充剂、30~50重量份崩解剂、15~40重量份润滑剂、30~150重量份矫味剂。
所述的填充剂选自微晶纤维素、聚乙二醇4000、聚乙二醇6000、甘露醇、山梨醇、糊精、乳糖、可压性淀粉、改性淀粉中的一种或多种;所述的崩解剂选自交联聚维酮、交联羧甲基纤维素钠、低取代羟丙基纤维素、羟基乙酸淀粉钠、羧甲基淀粉钠、羧甲基纤维素钙、海藻酸钠中的一种或多种;所述的润滑剂选自硬脂酸、微粉化泊洛沙姆、富马硬脂酸钠、月桂醇硫酸钠、聚乙二醇、十二烷基硫酸钠、十二烷基硫酸镁、月桂醇硫酸镁、富马酸、富马酸钠中的一种或多种;所述的矫味剂选自酸性调味剂、甜味剂、鲜味剂、香精、天然果蔬汁粉、胶浆剂、奶制品中的一种或多种。
所述的酸性调味剂选自维生素C、苹果酸、柠檬酸中的一种或多种;所述的甜味剂选自糖精钠、甜菊苷、阿斯巴甜、纽甜、蜂蜜、三氯蔗糖、甜蜜素、甘草、安赛蜜、阿沙苏法、塔格糖、甘草酸二钠、葡萄糖、果糖、蔗糖、木糖醇、单糖浆、果汁糖浆中的一种或多种;所述的鲜味剂选自谷氨酸钠、天门冬氨酸、氨基乙酸、L-丙氨酸、琥珀酸二钠、鸟苷酸二钠、肌苷酸二钠、鸡精中的一种或多种;所述的香精选自水溶性天然香精、水溶性合成香精、水溶性天然等同香精、水溶性发酵香精中的一种或多种;所述的天然果蔬汁粉选自蓝莓果汁粉、柠檬汁粉、薄荷汁粉、生姜汁粉、橘子汁粉、菠萝汁粉、水梨汁粉、西瓜汁粉、苹果汁粉、黄瓜汁粉、葡萄汁粉、猕猴桃汁粉、百香果汁粉、草莓汁粉、芒果汁粉、甘蔗汁粉、木瓜汁粉、芦荟汁粉、番茄汁粉、芹菜汁粉、菠菜汁粉、胡萝卜汁粉、甜椒汁粉、青椒汁粉中的一种或多种;所述的胶浆剂选自羧甲基纤维素钠、甲基纤维素、瓜尔豆胶、阿拉伯胶、西黄蓍胶、黄原胶、白芨胶淀粉、卡波姆、聚乙烯醇、聚维酮、明胶中的一种或多种。
所述增稠组合物的剂型为粉剂、颗粒剂。
一种可快速增加液体粘度的增稠组合物的制备工艺,为以下任意一种方法:
方法一:
将水溶性小分子有机化合物溶于水中,制成质量浓度为5%~30%的溶液,喷涂在增稠胶体表面并干燥;按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
或方法二:
1)将水溶性小分子有机化合物溶于水中,制备成质量浓度为5%~30%的水溶性小分子有机化合物溶液;
2)将增稠胶体和水溶性稀释剂加入流化床中,搅拌均匀,并向增稠胶体和水溶性稀释剂混合物表面喷淋步骤1)中的水溶性小分子有机化合物溶液,然后干燥制得增稠胶体组合物;
3)将步骤2)中的增稠胶体组合物与功能性成分、其他辅料混合搅拌30min,按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
或方法三:
1)将水溶性小分子有机化合物溶于水中,制备成质量浓度为5%~30%的水溶性小分子有机化合物溶液;
2)将增稠胶体、水溶性稀释剂和功能成分加入流化床中,搅拌均匀,得到混合物,并向该混合物表面喷淋步骤1)中的水溶性小分子有机化合物溶液,然后干燥制得增稠胶体组合物;
3)将步骤2)中的增稠胶体组合物与其他辅料混合搅拌30min,按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
一种食品或饮品,包括本发明所述的可快速增加液体粘度的增稠组合物。所述食品或饮品包括但不限于口服液、乳品、营养粥、营养糊、果汁、蔬菜汁。
本发明的优点是:通过将溶于含水的液体食品中快速增加液体食品的粘度,改善液体食品的口感,并防止发生吞咽困难患者误吸的意外。该增稠组合物的增稠性强,能够快速溶解、最大程度的分散于食品/饮品中,并完全溶于水中,使食品/饮品迅速形成均匀稳定具有一定粘度的食物,并明显地快速达到峰值粘度的速率。除此之外,被本发明增稠的食品外观美好,增加用户食欲,使食品休闲化。本发明增稠胶体和水溶性小分子有机化合物的用量科学合理,使增稠速度达到最优。
具体实施方式
实施例1
一.配方:
100g魔芋胶,20g牛磺酸
二.工艺:
将牛磺酸溶于水中,制备成质量浓度为15%的牛磺酸溶液;并向魔芋胶表面喷淋牛磺酸溶液,然后干燥制得魔芋胶组合物;将魔芋胶组合物研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
实施例2
一.配方:
200g黄原胶,30g甘氨酸,250g麦芽糖醇
二.工艺:
将甘氨酸溶于水中,制备成质量浓度为30%的甘氨酸溶液;将黄原胶和麦芽糖醇加入流化床中,搅拌均匀,并向黄原胶和麦芽糖醇混合物表面喷淋甘氨酸溶液,然后干燥制得黄原胶组合物;将增稠胶体组合物加入到制粒机中制成颗粒剂,得到可快速增加液体粘度的增稠组合物。
实施例3
一.配方:
250g卡拉胶,10g丝氨酸,350g可溶性淀粉
二.工艺:
将丝氨酸溶于水中,制备成质量浓度为5%的丝氨酸溶液;将卡拉胶和可溶性淀粉加入流化床中,搅拌均匀,得到混合物,并向该混合物表面喷淋丝氨酸溶液,然后干燥制得卡拉胶组合物;将卡拉胶组合物研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
实施例4
一.配方:
150g羧甲基纤维素,10g丙氨酸,400g麦芽糊精,45g羟基乙酸淀粉钠
二.工艺:
将丙氨酸溶于水中,制备成质量浓度为25%的丙氨酸溶液;将羧甲基纤维素和麦芽糊精加入流化床中,搅拌均匀,并向羧甲基纤维素和麦芽糊精混合物表面喷淋丙氨酸溶液,然后干燥制得羧甲基纤维素组合物;将羧甲基纤维素组合物与羟基乙酸淀粉钠混合搅拌30min,然后加入到制粒机中制成颗粒剂,得到可快速增加液体粘度的增稠组合物。
实施例5
一.配方:
250g黄蓍胶,20g谷氨酸,300g乳糖,150g聚乙二醇4000,30g交联羧甲基纤维素钠,25g硬脂酸,100g橘子汁粉,50g果糖,10g抗氧化剂
二.工艺:
将谷氨酸溶于水中,制备成质量浓度为30%的谷氨酸溶液;将黄蓍胶、乳糖和抗氧化剂加入流化床中,搅拌均匀,得到混合物,并向该混合物表面喷淋谷氨酸溶液,然后干燥制得黄蓍胶组合物;将黄蓍胶组合物与聚乙二醇4000、交联羧甲基纤维素钠、硬脂酸、橘子汁粉、果糖混合搅拌30min,然后研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
实施例6
一.配方:
200g黄原胶,30g赖氨酸,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将赖氨酸溶于水中,制备成质量浓度为20%的赖氨酸溶液;将黄原胶和木糖醇加入流化床中,搅拌均匀,并向黄原胶和木糖醇混合物表面喷淋赖氨酸溶液,然后干燥制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
实施例7
一.配方:
100g刺槐豆胶,25g丝氨酸,400g低聚果糖,130g聚乙二醇6000,50g羧甲基淀粉钠,15g十二烷基硫酸镁,30g甜菊苷,1000g蛋白质
二.工艺:
将丝氨酸溶于水中,制备成质量浓度为5%的丝氨酸溶液;将刺槐豆胶和低聚果糖加入流化床中,搅拌均匀,并向刺槐豆胶和低聚果糖混合物表面喷淋丝氨酸溶液,然后干燥制得刺槐豆胶组合物;将刺槐豆胶组合物与蛋白质、聚乙二醇6000、羧甲基淀粉钠、十二烷基硫酸镁、甜菊苷混合搅拌30min,然后加入到制粒机中制成颗粒剂,得到可快速增加液体粘度的增稠组合物。
实施例8
一.配方:
220g魔芋胶,10g甘氨酸,330g低聚麦芽糖,200g微晶纤维素,35g交联聚维酮,40g富马硬脂酸钠,60g维生素C,40g葡萄糖,250g植物营养素
二.工艺:
将甘氨酸溶于水中,制备成质量质量浓度为10%的甘氨酸溶液;将魔芋胶、低聚麦芽糖和植物营养素加入流化床中,搅拌均匀,得到混合物,并向该混合物表面喷淋甘氨酸溶液,然后干燥制得魔芋胶组合物;将魔芋胶组合物与微晶纤维素、交联聚维酮、富马硬脂酸钠、维生素C、葡萄糖混合搅拌30min,然后加入到制粒机中制成颗粒剂,得到可快速增加液体粘度的增稠组合物
对照例1
一.配方:
200g黄原胶,100g赖氨酸,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将赖氨酸溶于水中,制备成质量浓度为20%的赖氨酸溶液;将黄原胶和木糖醇加入流化床中,搅拌均匀,并向黄原胶和木糖醇混合物表面喷淋赖氨酸溶液,然后干燥制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到产品。
对照例2
一.配方:
200g黄原胶,5g赖氨酸,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将赖氨酸溶于水中,制备成质量浓度为20%的赖氨酸溶液;将黄原胶和木糖醇加入流化床中,搅拌均匀,并向黄原胶和木糖醇混合物表面喷淋赖氨酸溶液,然后干燥制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到产品。
对照例3
一.配方:
200g黄原胶,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将黄原胶和木糖醇加入流化床中,搅拌均匀制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到产品。
对照例4
一.配方:
200g黄原胶,30g赖氨酸,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将赖氨酸溶于水中,制备成质量浓度为20%的赖氨酸溶液;将黄原胶和木糖醇溶于赖氨酸溶液中并混合搅拌均匀,然后干燥制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
对照例5
一.配方:
200g黄原胶,30g赖氨酸,250g木糖醇,100g微晶纤维素,40g低取代羟丙基纤维素,30g微粉化泊洛沙姆,55g苹果酸,15g糖精钠,700g益生菌
二.工艺:
将赖氨酸、黄原胶和木糖醇混合搅拌均匀制得黄原胶组合物;将黄原胶组合物与益生菌、微晶纤维素、低取代羟丙基纤维素、微粉化泊洛沙姆、苹果酸、糖精钠混合搅拌30min,然后研磨粉碎制成粉剂,得到可快速增加液体粘度的增稠组合物。
实施例9.检测内容
一.方法
1.粘度检测
在20℃下,分别将1g被测实施例和对照例样品均加入到99g水中制备成液体,使用低转速搅拌器,在600rpm搅拌30秒。将液体静置2分钟、5分钟、10分钟和30分钟,并用B型粘度计(南京骏河机电有限公司生产,转速12rpm,30秒后第3号转子)确定每个时间点的粘度。用粘度百分率评价粘度性能,其中30分钟时达到的粘度视为100%,其他时间点的粘度百分率=相应的粘度测定值÷30分钟之后的粘度×100%。
2.分散性检测
将被测实施例和对照例样品溶于水中制备成浓度为1%的液体,取100ml被测液体于无色透明的容器中,在光亮处肉眼观察未分散团块的数目。
二.结果
1.粘度检测
各实施例和对照例样品液体的粘度百分率测定结果列于表1中。
表1实施例和对照例样品液体的粘度百分率
时间(分钟) | 0 | 2 | 5 | 10 | 30 |
实施例1 | 0% | 90.6 | 95.2 | 97.1 | 100% |
实施例2 | 0% | 91.3 | 95.7 | 97.6 | 100% |
实施例3 | 0% | 91.8 | 95.5 | 98.3 | 100% |
实施例4 | 0% | 92.9 | 96.4 | 98.0 | 100% |
实施例5 | 0% | 92.5 | 96.1 | 98.5 | 100% |
实施例6 | 0% | 93.7 | 97.2 | 99.2 | 100% |
实施例7 | 0% | 93.1 | 96.5 | 98.8 | 100% |
实施例8 | 0% | 93.4 | 96.3 | 98.4 | 100% |
对照例1 | 0% | 77.8 | 88.5 | 93.7 | 100% |
对照例2 | 0% | 46.7 | 65.8 | 77.2 | 100% |
对照例3 | 0% | 40.8 | 57.9 | 68.5 | 100% |
对照例4 | 0% | 50.2 | 66.8 | 78.9 | 100% |
对照例5 | 0% | 42.1 | 60.5 | 71.7 | 100% |
将8个实施例样品和5个对照例样品溶于水,制备成液体。表1中记录了各样品液体分别在0分钟、2分钟、5分钟、10分钟和30分钟时的粘度百分率,其中各被测样品液体静止30分钟时的粘度百分率均记为100%,0分钟时的粘度百分率为0%。2分钟、5分钟、10分钟时,实施例和对照例样品液体的粘度百分率相差较大;2分钟时,8个实施例的粘度百分率均大于90%,而对照1的粘度百分率为77.8%,对照例2-对照例5的粘度百分率为40%~51%;5分钟时,实施例的粘度百分率都已经达到95%,而对照1的粘度百分率为88.5%,对照例2-对照例5的粘度百分率为57%~67%;10分钟时,8个实施例的粘度百分率均高于97%,实施例6甚至达到99.2%,而对照1的粘度百分率为93.7%,对照例2-对照例5的粘度百分率只有68%~80%。综上所述,实施例样品溶于水中能快速增加液体的粘度,5分钟即可达到峰值粘度的95%以上,具有快速增稠的作用;虽然,对照例1中的水溶性小分子有机化合物与增稠组合物的用量比例很高,但是快速增稠效果却稍差于实施例;对照例2中水溶性小分子有机化合物用量较少,对照例3中不含水溶性小分子有机化合物,两者的快速增稠效果很差。对照例4和对照例5中的水溶性小分子有机化合物没有易喷淋的方式结合在增稠胶体表面,增稠效果也很差。
2.分散性检测
表2实施例和对照例样品液体的分散性
被测样品 | 未分散团块数目 |
实施例1 | 19 |
实施例2 | 16 |
实施例3 | 15 |
实施例4 | 18 |
实施例5 | 13 |
实施例6 | 8 |
实施例7 | 12 |
实施例8 | 11 |
对照例1 | 17 |
对照例2 | 35 |
对照例3 | 41 |
对照例4 | 40 |
对照例5 | 45 |
表2通过记录被测样品液体中未分散团块的数目来判断实施例和对照例样品的分散性,取100mL、浓度为1%的被测样品液体,在光亮处肉眼观察为分散团块的数目,并记录。表中数据显示8个实施例样品液体中未分散团块为8~19个;对照例1样品液体中未分散团块数目为17个,与实施例相似;对照例3和对照例3样品液体未分散团块分别为35个和41个。以上数据表明,本发明的实施例在水中的分散性更好,对照例1的水中分散性虽好,但是水溶性小分子有机化合物用量多,对照例2-对照例5在水中的分散性效果差,所以本发明实施例的效果最佳。
通过以上分析可知,本发明的增稠组合物增稠性强,能够快速分散于食品/饮品中,并完全溶于水中,使食品/饮品成为具有稳定粘度的凝胶。本发明的可快速增加液体粘度的增稠组合物包括100~250重量份增稠胶体和10~30重量份水溶性小分子有机化合物。增稠胶体(尤其是黄原胶、魔芋胶、卡拉胶、瓜尔胶、刺槐豆胶、秋葵胶、香豆胶、羧甲基纤维素、葫芦巴胶、罗望子胶、肉桂胶、阿拉伯胶、印度胶、黄蓍胶、刺梧桐树胶)可溶于液体食品或饮品中,并使其具有粘度,但是该增稠胶体易团聚,导致其使用功能受限。为了防止增稠胶体团聚,本发明使用了水溶性小分子有机化合物,水溶性小分子有机化合物为牛磺酸、甘氨酸、赖氨酸、丙氨酸、谷氨酸、脯氨酸、谷氨酰胺、丝氨酸、精氨酸、苯丙氨酸、苏氨酸、缬氨酸中的一种或多种,将水溶性小分子有机化合物溶液喷射在增稠胶体表面。增稠胶体被水溶性小分子有机化合物结合,进行表面改性,使增稠胶体在含水食品(如液体食品、饮品)中能够快速溶解、最大程度的被分散,迅速形成均匀稳定具有一定粘度的食物,并明显地加快达到峰值粘度的速率,而且粘度长时间处于稳定状态,所以本发明产品具有很强的实用性。除此之外,被本发明增稠的食品外观美好,增加用户食欲,使食品休闲化。本发明增稠胶体和水溶性小分子有机化合物的用量科学合理,水溶性小分子有机化合物用量过少,无法达到本发明快速增稠的目的;水溶性小分子有机化合物用量过多会造成资源浪费。
以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (13)
1.可快速增加液体粘度的增稠组合物,其特征在于,包括100~250重量份增稠胶体、10~30重量份水溶性小分子有机化合物;将水溶性小分子有机化合物制成质量浓度为5%~30%的溶液,喷涂在增稠胶体表面并干燥。
2.根据权利要求1所述的可快速增加液体粘度的增稠组合物,其特征在于:所述增稠组合物溶于水中,5min后的溶液粘度≥该溶液峰值粘度的95%。
3.根据权利要求1所述的可快速增加液体粘度的增稠组合物,其特征在于,所述增稠胶体选自黄原胶、魔芋胶、卡拉胶、瓜尔胶、刺槐豆胶、秋葵胶、香豆胶、羧甲基纤维素、葫芦巴胶、罗望子胶、肉桂胶、阿拉伯胶、印度胶、黄蓍胶、刺梧桐树胶中的一种或多种。
4.根据权利要求1所述的可快速增加液体粘度的增稠组合物,其特征在于,所述水溶性小分子有机化合物选自牛磺酸、甘氨酸、赖氨酸、丙氨酸、谷氨酸、脯氨酸、谷氨酰胺、丝氨酸、精氨酸、苯丙氨酸、苏氨酸、缬氨酸中的一种或多种。
5.根据权利要求1所述的可快速增加液体粘度的增稠组合物,其特征在于还包括以下一种或多种成分:250~400重量份水溶性稀释剂和10~1000重量份功能性成分。
6.根据权利要求5所述的可快速增加液体粘度的增稠组合物,其特征在于:所述水溶性稀释剂选自麦芽糊精、麦芽糖醇、山梨醇、木糖醇、甘露醇、蔗糖、乳糖、糊精、可溶性淀粉、可压性淀粉、低聚果糖、低聚麦芽糖中的一种或多种。
7.根据权利要求5所述的可快速增加液体粘度的增稠组合物,其特征在于:所述功能性成分选自营养成分、蛋白质、脂肪源、纤维、碳水化合物源、益生元、益生菌、氨基酸、脂肪酸、植物营养素、抗氧化剂中的一种或多种。
8.根据权利要求1所述的可快速增加液体粘度的增稠组合物,其特征在于:还包括以下一种或多种成分:100~200重量份填充剂、30~50重量份崩解剂、15~40重量份润滑剂、30~150重量份矫味剂。
9.根据权利要求8所述的可快速增加液体粘度的增稠组合物,其特征在于:所述的填充剂选自微晶纤维素、聚乙二醇4000、聚乙二醇6000、甘露醇、山梨醇、糊精、乳糖、可压性淀粉、改性淀粉中的一种或多种;所述的崩解剂选自交联聚维酮、交联羧甲基纤维素钠、低取代羟丙基纤维素、羟基乙酸淀粉钠、羧甲基淀粉钠、羧甲基纤维素钙、海藻酸钠中的一种或多种;所述的润滑剂选自硬脂酸、微粉化泊洛沙姆、富马硬脂酸钠、月桂醇硫酸钠、聚乙二醇、十二烷基硫酸钠、十二烷基硫酸镁、月桂醇硫酸镁、富马酸、富马酸钠中的一种或多种;所述的矫味剂选自酸性调味剂、甜味剂、鲜味剂、香精、天然果蔬汁粉、胶浆剂、奶制品中的一种或多种。
10.根据权利要求9所述的可快速增加液体粘度的增稠组合物,其特征在于:所述的酸性调味剂选自维生素C、苹果酸、柠檬酸中的一种或多种;所述的甜味剂选自糖精钠、甜菊苷、阿斯巴甜、纽甜、蜂蜜、三氯蔗糖、甜蜜素、甘草、安赛蜜、阿沙苏法、塔格糖、甘草酸二钠、葡萄糖、果糖、蔗糖、木糖醇、单糖浆、果汁糖浆中的一种或多种;所述的鲜味剂选自谷氨酸钠、天门冬氨酸、氨基乙酸、L-丙氨酸、琥珀酸二钠、鸟苷酸二钠、肌苷酸二钠、鸡精中的一种或多种;所述的香精选自水溶性天然香精、水溶性合成香精、水溶性天然等同香精、水溶性发酵香精中的一种或多种;所述的天然果蔬汁粉选自蓝莓果汁粉、柠檬汁粉、薄荷汁粉、生姜汁粉、橘子汁粉、菠萝汁粉、水梨汁粉、西瓜汁粉、苹果汁粉、黄瓜汁粉、葡萄汁粉、猕猴桃汁粉、百香果汁粉、草莓汁粉、芒果汁粉、甘蔗汁粉、木瓜汁粉、芦荟汁粉、番茄汁粉、芹菜汁粉、菠菜汁粉、胡萝卜汁粉、甜椒汁粉、青椒汁粉中的一种或多种;所述的胶浆剂选自羧甲基纤维素钠、甲基纤维素、瓜尔豆胶、阿拉伯胶、西黄蓍胶、黄原胶、白芨胶淀粉、卡波姆、聚乙烯醇、聚维酮、明胶中的一种或多种。
11.根据权利要求1-10中任何一项所述的可快速增加液体粘度的增稠组合物,其特征在于:所述增稠组合物的剂型为粉剂、颗粒剂。
12.权利要求11所述的一种可快速增加液体粘度的增稠组合物的制备工艺,其特征在于所述制备工艺为以下任意一种方法:
方法一:
将水溶性小分子有机化合物溶于水中,制成质量浓度为5%~30%的溶液,喷涂在增稠胶体表面并干燥;按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
方法二:
1)将水溶性小分子有机化合物溶于水中,制备成质量浓度为5%~30%的水溶性小分子有机化合物溶液;
2)将增稠胶体和水溶性稀释剂加入流化床中,搅拌均匀,并向增稠胶体和水溶性稀释剂混合物表面喷淋步骤1)中的水溶性小分子有机化合物溶液,然后干燥制得增稠胶体组合物;
3)将步骤2)中的增稠胶体组合物与功能性成分、其他辅料混合搅拌30min,按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
或方法三:
1)将水溶性小分子有机化合物溶于水中,制备成质量浓度为5%~30%的水溶性小分子有机化合物溶液;
2)将增稠胶体、水溶性稀释剂和功能成分加入流化床中,搅拌均匀,得到混合物,并向该混合物表面喷淋步骤1)中的水溶性小分子有机化合物溶液,然后干燥制得增稠胶体组合物;
3)将步骤2)中的增稠胶体组合物与其他辅料混合搅拌30min,按照需求制备成所需剂型,得到可快速增加液体粘度的增稠组合物。
13.一种食品或饮品,其特征在于:包括权利要求1~12中任何一项所述的可快速增加液体粘度的增稠组合物。
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