CN109481371A - A kind of cosmetic face cream and preparation method thereof with antiageing effect - Google Patents
A kind of cosmetic face cream and preparation method thereof with antiageing effect Download PDFInfo
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- CN109481371A CN109481371A CN201910049373.0A CN201910049373A CN109481371A CN 109481371 A CN109481371 A CN 109481371A CN 201910049373 A CN201910049373 A CN 201910049373A CN 109481371 A CN109481371 A CN 109481371A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses a kind of cosmetic face cream and preparation method thereof with antiageing effect.The raw material of the cosmetic face cream is made of Astragalus membranacus root extract, oil tea leaf extract, windproof root extract, isobutyl palmitate, dimethyl silicone polymer, arbutin, first squeezing cocounut oil etc..The preparation method of the cosmetic face cream with antiageing effect is specifically to put into isobutyl palmitate, dimethyl silicone polymer etc. in reaction kettle to carry out high-temperature stirring, then it is added by cetostearyl alcohol, 1,3- butanediol etc. is through primary mix made of homogeneous, sub-mixtures are obtained after stirring homogeneous, Astragalus membranacus root extract isoreactivity ingredient will be added after sub-mixtures again vacuum homogeneous in emulsion pot and obtain ultimate mixture, most obtains finished product cosmetic face cream after cooling, addition auxiliary agent afterwards.The cosmetic face cream with antiageing effect has preferable function of anti-skin aging, there is preferable application prospect in face skin nursing.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of cosmetic face cream and its system with antiageing effect
Preparation Method.
Background technique
Skin is the maximum organ of human body, and the 5%-15% of total weight percentage of liveweight, the gross area is 1.5-2 square metres, thickness
Because people or because of position it is different, be 0.5-4 millimeters.Skin covers whole body, it makes various in vivo organize with organ from physical, machine
Tool, chemically with the invasion of pathogenic microorganism, skin tool there are two aspect barrier action, on the one hand prevent internal water
Point, the loss of electrolyte and other substances, the on the other hand intrusion of tissue external world harmful substance keeps that human internal environment's is steady
It is fixed, important defencive function is physiologically being played, while skin also assists in the metabolic process of human body.Aging be in life process not
The evitable natural law, and first barrier of the skin as human body, skin is at every moment all in aging, aging, elasticity
It slowly reduces, and thins down, more and more fragile and relaxation.Skin aging generally has natural aging and light aging.The former
It refers mainly to age, factor can not be resisted to cause by such as heredity, gravity, endocrine and immune function existing in body
Aging；The latter is mainly the effect due to ultraviolet light, accelerates the process of naturally-aged, and climate change and environmental pollution
Also there is direct influence to the light aging of skin etc. a series of environmental exposures.The approach of anti-aging specifically includes that protection skin
It is stimulated from external environment；Extra free radical in scavenger-cell；Skin Cell is repaired and is supplemented the nutrients.Face cream and cream
Liquid is the most important step of basic skin care, and the effective components such as whitening and anti-aging in face cream, lotion can preferably be inhaled by skin
It receives, dual anti-aging effect is provided, cell neogenesis energy can be stimulated, while promoting collagen synthesis, improve skin surface
Texture and the colour of skin uniformity, keep skin more careful.But common anti-aging face cream some is at present in order to reach anti-ageing well
The industrial components that old effect has used inoxidizability strong, it is quick in short-term, but use for a long time is done great harm to human body；Have
Anti-aging face cream adds vitamins antioxidant, but this kind of antioxidant stability is poor.
Summary of the invention
Based on current cosmetic face cream the problem of not still being able to satisfy consumer demand on anti-aging effects, the present invention provides one
Kind has the cosmetic face cream and preparation method thereof of antiageing effect.
A kind of cosmetic face cream with antiageing effect, by mass percentage, composition is such as the raw material of the cosmetic face cream
Under:
Astragalus membranacus root extract 1.7~2.9%
Oil tea leaf extract 1.2~2.5%
Windproof root extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
1,3 butylene glycol 1.5~5.5%
Glycerol 6.0~10.0%
Isobutyl palmitate 4.0~6.0%
Dimethyl silicone polymer 0.5~7.5%
Liquid paraffin 2.5~3.5%
Arbutin 1.8~2.2%
First squeezing cocounut oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
The above-mentioned cosmetic face cream with antiageing effect contains Astragalus membranacus root extract, oil tea leaf extract, opoponax
The functional components such as extract, arbutin, first squeezing cocounut oil, each functional components except play itself possessed by basic effect with
Outside, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level, from basic
On play the role of skin anti-aging.The cosmetic face cream has preferable using effect, the crowd of aging phenomenon occurs suitable for skin
It uses.
The Astragalus membranacus root extract, oil tea leaf extract and windproof root extract in one of the embodiments,
The preparation method comprises the following steps:
Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, are sieved, being added to weight is 30 times, and volumetric concentration is
In 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W, supernatant is then taken to be centrifuged,
Filtering, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last chilled dry
It is dry to obtain Astragalus membranacus root extract, oil tea leaf extract and windproof root extract.
The raw material of the cosmetic face cream by mass percentage, forms as follows in one of the embodiments:
Astragalus membranacus root extract 2.3%
Oil tea leaf extract 1.8%
Windproof root extract 0.7%
Cetostearyl alcohol 5.8%
1,3 butylene glycol 3.5%
Glycerol 8.0%
Isobutyl palmitate 5.0%
Dimethyl silicone polymer 4.0%
Liquid paraffin 3.0%
Arbutin 2.0%
First squeezing cocounut oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
The essence is any one in ginger extrait, flavoring rose essence, lavender oil in one of the embodiments,
Kind.
The antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro pyrrole in one of the embodiments,
Any one muttered in triol.
Any one of the preservative in Nipasol, sorbic acid, triclosan in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned cosmetic face cream with antiageing effect, comprise the steps of:
(1) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1200~1800
Rev/min rate homogenous disperse 30~40 minutes, obtain primary mix；
(2) it by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, improves anti-
It answers kettle temperature degree to 88~92 DEG C, is stirred 15~25 minutes under 300~500 revs/min of rate, then to being added in reaction kettle
Step (1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary
Grade mixture；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, inside subsequent pot to be emulsified
When temperature is down to 55 DEG C or less, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot,
According still further to rate homogeneous 18~20 minutes of 2400~2600 revs/min, ultimate mixture is obtained；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, arbutin, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 120~160 revs/min of rate, obtain finished product face cream.
The preparation method of the above-mentioned cosmetic face cream with antiageing effect, process conditions are mild, controllability is strong, product quality
Stablize, production cost economy, is suitable for large-scale production.
Emulsion pot is evacuated to -0.06~-0.1MPa in the step (3) in one of the embodiments,.
The present invention also provides application of the cosmetic face cream with antiageing effect in face skin nursing.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment,
The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair
It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of cosmetic face cream with antiageing effect, by mass percentage, composition is such as the raw material of the cosmetic face cream
Under:
Astragalus membranacus root extract 1.7~2.9%
Oil tea leaf extract 1.2~2.5%
Windproof root extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
1,3 butylene glycol 1.5~5.5%
Glycerol 6.0~10.0%
Isobutyl palmitate 4.0~6.0%
Dimethyl silicone polymer 0.5~7.5%
Liquid paraffin 2.5~3.5%
Arbutin 1.8~2.2%
First squeezing cocounut oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
Wherein, Astragalus membranacus originates in the ground such as the Inner Mongol, Shanxi, Gansu, Heilungkiang, is state three level protecting plant.Containing soap
The various trace elements such as glucoside, sucrose, polysaccharide, a variety of amino acid, folic acid and selenium, zinc, copper.Astragalus membranacus root extract can promote
The effect of skin permeability, toxin expelling, raising skin whiteness.
Wherein, Camellia Leaves are the leaf of tea oil tree, and Camellia Leaves contain tea polyphenols, protein, reduced sugar, amino acid, tea soap
The ingredients such as element, chlorophyll and flavone compound, active constituent have anti-oxidant, free radical resisting, bacteriostasis, preservation and anticancer,
Anti-cancer and other effects.Oil tea leaf extract be applied to skin-protection product on, can give full play of oil tea component it is anti-oxidant, remove from
By base, enhancing epidermal cell vigor, promote skin metabolism, the outstanding advantage of delay skin aging.
Wherein, radix saposhnikoviae is the dry root that umbelliferae Saposhnikovia divaricata does not take out scape plant.Radix saposhnikoviae containing volatile oil, chromone,
A variety of chemical components such as cumarin, organic acid, heteroglycan and polyacetylene, windproof root extract can be used as antioxidant, receive sword agent,
Certain inhibiting effect is known as to black simultaneously and while having the function of antibacterial anti-inflammatory.
Wherein, arbutin, that is, 4- hydroxy phenyl-β-D- glucopyranoside, is the glucose of quinhydrones (Isosorbide-5-Nitrae hydroquinone)
Glycosides.The existing beauty and skin care function of arbutin, and can anti-inflammatory, anti-irritation.It can inhibit the tyrosinase in skin, thus significantly
Improve Skin pigmentation, dispel color spot and freckle, can eliminate tanned caused by 90%UV.Realize whitening, nti-freckle, moisturizing, softness,
Anti-wrinkle, anti-inflammatory effect.
Wherein, first squeezing cocounut oil can alleviate wrinkle, cutis laxa and senile plaque, can also prevent and treat skin infection, psoriasis,
Eczema, dermatitis etc..
The above-mentioned cosmetic face cream with antiageing effect contains Astragalus membranacus root extract, oil tea leaf extract, opoponax
The functional components such as extract, arbutin, first squeezing cocounut oil, each functional components except play itself possessed by basic effect with
Outside, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level, from basic
On play the role of skin anti-aging.The cosmetic face cream has preferable using effect, the crowd of aging phenomenon occurs suitable for skin
It uses.
In a preferred embodiment, the Astragalus membranacus root extract, oil tea leaf extract and windproof root extract
The preparation method comprises the following steps:
Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, are sieved, being added to weight is 30 times, and volumetric concentration is
In 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W, supernatant is then taken to be centrifuged,
Filtering, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last chilled dry
It is dry to obtain Astragalus membranacus root extract, oil tea leaf extract and windproof root extract.
In a preferred embodiment, the raw material of the cosmetic face cream by mass percentage, forms as follows:
Astragalus membranacus root extract 2.3%
Oil tea leaf extract 1.8%
Windproof root extract 0.7%
Cetostearyl alcohol 5.8%
1,3 butylene glycol 3.5%
Glycerol 8.0%
Isobutyl palmitate 5.0%
Dimethyl silicone polymer 4.0%
Liquid paraffin 3.0%
Arbutin 2.0%
First squeezing cocounut oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
In a preferred embodiment, the essence is any in ginger extrait, flavoring rose essence, lavender oil
It is a kind of.
In a preferred embodiment, the antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro
Any one in pyrans triol.
In a preferred embodiment, the preservative is any one in Nipasol, sorbic acid, triclosan
Kind.
The present invention also provides the preparation methods of the above-mentioned cosmetic face cream with antiageing effect, comprise the steps of:
(1) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1200~1800
Rev/min rate homogenous disperse 30~40 minutes, obtain primary mix；
(2) it by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, improves anti-
It answers kettle temperature degree to 88~92 DEG C, is stirred 15~25 minutes under 300~500 revs/min of rate, then to being added in reaction kettle
Step (1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary
Grade mixture；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, inside subsequent pot to be emulsified
When temperature is down to 55 DEG C or less, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot,
According still further to rate homogeneous 18~20 minutes of 2400~2600 revs/min, ultimate mixture is obtained；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, arbutin, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 120~160 revs/min of rate, obtain finished product face cream.
In a preferred embodiment, emulsion pot is evacuated to -0.06~-0.1MPa in the step (3).
The present invention also provides application of the above-mentioned cosmetic face cream with antiageing effect in face skin nursing.
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality
Apply example.
Embodiment 1
The cosmetic face cream formula with antiageing effect of the present embodiment is as follows:
Astragalus membranacus root extract 1.7%
Oil tea leaf extract 1.2%
Windproof root extract 0.6%
Cetostearyl alcohol 5.5%
1,3 butylene glycol 1.5%
Glycerol 6.0%
Isobutyl palmitate 4.0%
Dimethyl silicone polymer 0.5%
Liquid paraffin 2.5%
Arbutin 1.8%
First squeezing cocounut oil 0.05%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The cosmetic face cream with antiageing effect of the present embodiment is prepared as follows:
(1) Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, is sieved, being added to weight is 30 times, and volume is dense
Degree is in 70% ethanol solution, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Astragalus membranacus root extract, oil tea leaf extract and windproof root extract
(2) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1200 revs/min
Rate homogenous disperse 30 minutes, obtain primary mix；
(3) it by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, improves anti-
It answers kettle temperature degree to 88 DEG C, is stirred 15 minutes under 300 revs/min of rate, it is resulting then to step (2) are added in reaction kettle
Primary mix stirs homogeneous 30 minutes under 1800 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65 DEG C, according to rate homogeneous 8 minutes of 2000 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot, according still further to 2400 revs/min
The rate homogeneous of clock 18 minutes, obtains ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, arbutin, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 120 revs/min of rate, are obtained finished product face cream, are denoted as S1.
Embodiment 2
The cosmetic face cream formula with antiageing effect of the present embodiment is as follows:
Astragalus membranacus root extract 2.3%
Oil tea leaf extract 1.8%
Windproof root extract 0.7%
Cetostearyl alcohol 5.8%
1,3 butylene glycol 3.5%
Glycerol 8.0%
Isobutyl palmitate 5.0%
Dimethyl silicone polymer 4.0%
Liquid paraffin 3.0%
Arbutin 2.0%
First squeezing cocounut oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
The cosmetic face cream with antiageing effect of the present embodiment is prepared as follows:
(1) Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, is sieved, being added to weight is 30 times, and volume is dense
Degree is in 75% ethanol solution, ultrasonic extraction 5 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Astragalus membranacus root extract, oil tea leaf extract and windproof root extract
(2) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1500 revs/min
Rate homogenous disperse 35 minutes, obtain primary mix；
(3) it by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, improves anti-
It answers kettle temperature degree to 90 DEG C, is stirred 20 minutes under 400 revs/min of rate, it is resulting then to step (2) are added in reaction kettle
Primary mix stirs homogeneous 40 minutes under 1900 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 70 DEG C, according to rate homogeneous 9 minutes of 2100 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot, according still further to 2500 revs/min
The rate homogeneous of clock 19 minutes, obtains ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, arbutin, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 140 revs/min of rate, are obtained finished product face cream, are denoted as S2.
Embodiment 3
The cosmetic face cream formula with antiageing effect of the present embodiment is as follows:
Astragalus membranacus root extract 2.9%
Oil tea leaf extract 2.5%
Windproof root extract 0.8%
Cetostearyl alcohol 6.0%
1,3 butylene glycol 5.5%
Glycerol 10.0%
Isobutyl palmitate 6.0%
Dimethyl silicone polymer 7.5%
Liquid paraffin 3.5%
Arbutin 2.2%
First squeezing cocounut oil 0.15%
Essence 0.03%
Antioxidant 0.05%
Preservative 0.2%
Deionized water surplus.
The cosmetic face cream with antiageing effect of the present embodiment is prepared as follows:
(1) Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, is sieved, being added to weight is 30 times, and volume is dense
Degree is in 80% ethanol solution, ultrasonic extraction 6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Astragalus membranacus root extract, oil tea leaf extract and windproof root extract
(2) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1800 revs/min
Rate homogenous disperse 40 minutes, obtain primary mix；
(3) it by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, improves anti-
It answers kettle temperature degree to 92 DEG C, is stirred 25 minutes under 500 revs/min of rate, it is resulting then to step (2) are added in reaction kettle
Primary mix stirs homogeneous 50 minutes under 2000 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 75 DEG C, according to rate homogeneous 10 minutes of 2200 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot, according still further to 2600 revs/min
The rate homogeneous of clock 20 minutes, obtains ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, arbutin, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 160 revs/min of rate, are obtained finished product face cream, are denoted as S3.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add film pod
Radix Astragali root extract, final cosmetic face cream obtained are denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add oil tea
Leaf extract, final cosmetic face cream obtained are denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add radix saposhnikoviae
Root extract, final cosmetic face cream obtained are denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add black bearberry
Glycosides, final cosmetic face cream obtained are denoted as C4.
Comparative example 5
Substantially with embodiment 1, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add first squeezing
Cocounut oil, final cosmetic face cream obtained are denoted as C5.
Performance test
Cosmetic face cream prepared by Examples 1 to 3 and comparative example 1~5 is subjected to using effect performance test.
Select the age at 35~45 years old, skin the crowd of aging phenomenon occurs as test object, is randomly divided into 8 groups, often
15 people of group, each group skin of face situation, in terms of the difference that there are no significant, 1~8 group respectively it is daily it is early,
Two periods of evening smear cosmetic face cream S1~S3 that the embodiment of the present invention 1~3 is prepared and comparative example 1~5 is prepared
Cosmetic face cream C1~C5 it is each primary, after being used continuously one month, effect assessment is carried out using the method for marking.Full marks are 5
Point, 4~5 points of expression improvements are splendid；3~4 points of expression improvements are good；2~3 points of expression improvements are general；2 points with
Lower expression is not affected significantly effect, and last each group is made even respectively, and the specific situation that scores is as shown in table 1:
Table 1
Test result is as shown above, the cosmetic face cream of embodiment S1~S3 group and the cosmetic face cream of comparative example C1~C5 group
It compares, more excellent skin aging situation improvement, and the cosmetic face cream tool of embodiment S2 is all had for user
There is most excellent using effect.It can be seen that from the case where embodiment and comparative example of the invention with antiageing effect
Astragalus membranacus root extract, oil tea leaf extract, windproof root extract, arbutin, first squeezing cocounut oil in cosmetic face cream ingredient is equal
Using effect is produced and is significantly affected, and in the case that mentioned component is used in conjunction with, using effect is any compared to lacking
A kind of ingredient, which has, to be extremely obviously improved, it is seen that produces synergistic effect between above-mentioned several ingredients, has good
Good application prospect.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.
Claims (9)
1. a kind of cosmetic face cream with antiageing effect, which is characterized in that the raw material of the cosmetic face cream is by weight percent
Meter forms as follows:
Astragalus membranacus root extract 1.7~2.9%
Oil tea leaf extract 1.2~2.5%
Windproof root extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
1,3 butylene glycol 1.5~5.5%
Glycerol 6.0~10.0%
Isobutyl palmitate 4.0~6.0%
Dimethyl silicone polymer 0.5~7.5%
Liquid paraffin 2.5~3.5%
Arbutin 1.8~2.2%
First squeezing cocounut oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
2. the cosmetic face cream according to claim 1 with antiageing effect, which is characterized in that the Astragalus membranacus root mentions
Take object, oil tea leaf extract and windproof root extract the preparation method comprises the following steps:
Astragalus membranacus root, Camellia Leaves and opoponax are crushed respectively, be sieved, be added to weight be 30 times, volumetric concentration be 70~
In 80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, filtering,
Again by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
To Astragalus membranacus root extract, oil tea leaf extract and windproof root extract.
3. the cosmetic face cream according to claim 1 with antiageing effect, which is characterized in that the original of the cosmetic face cream
Material by mass percentage, forms as follows:
Astragalus membranacus root extract 2.3%
Oil tea leaf extract 1.8%
Windproof root extract 0.7%
Cetostearyl alcohol 5.8%
1,3 butylene glycol 3.5%
Glycerol 8.0%
Isobutyl palmitate 5.0%
Dimethyl silicone polymer 4.0%
Liquid paraffin 3.0%
Arbutin 2.0%
First squeezing cocounut oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
4. described in any item cosmetic face creams with antiageing effect according to claim 1~3, which is characterized in that the perfume (or spice)
Any one selected from ginger extrait, flavoring rose essence, lavender oil.
5. described in any item cosmetic face creams with antiageing effect according to claim 1~3, which is characterized in that described anti-
Any one of oxidant in butylated hydroxy anisole, allantoin, hydroxypropyl oxinane triol.
6. described in any item cosmetic face creams with antiageing effect according to claim 1~3, which is characterized in that described anti-
Any one of rotten agent in Nipasol, sorbic acid, triclosan.
7. a kind of preparation method of the cosmetic face cream as described in any one of claims 1 to 6 with antiageing effect, feature
It is, comprises the steps of:
(1) cetostearyl alcohol, 1,3-BDO, glycerol, deionized water are put into homogenizer, according to 1200~1800 revs/min
The rate homogenous disperse of clock 30~40 minutes, obtains primary mix；
(2) by isobutyl palmitate, dimethyl silicone polymer, liquid paraffin, first squeezing cocounut oil investment reaction kettle, reaction kettle is improved
Temperature stirs 15~25 minutes under 300~500 revs/min of rate to 88~92 DEG C, then to step is added in reaction kettle
(1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary mixed
Close object；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, kept inside emulsion pot
Temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, subsequent pot internal temperature to be emulsified
When being down to 55 DEG C or less, Astragalus membranacus root extract, oil tea leaf extract, windproof root extract are added into emulsion pot, then press
According to rate homogeneous 18~20 minutes of 2400~2600 revs/min, ultimate mixture is obtained；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, thereto be added arbutin, essence, antioxidant,
Preservative is stirred evenly according to 120~160 revs/min of rate, obtains finished product face cream.
8. the preparation method of the cosmetic face cream according to claim 7 with antiageing effect, which is characterized in that the step
Suddenly emulsion pot is evacuated to -0.06~-0.1MPa in (3).
9. described in any item cosmetic face creams with antiageing effect are in face skin nursing according to claim 1~6
Using.
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Application publication date: 20190319 |