CN105726365A - Cosmetic containing calophyllum inophyllum kernel oil and preparation method thereof - Google Patents
Cosmetic containing calophyllum inophyllum kernel oil and preparation method thereof Download PDFInfo
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- CN105726365A CN105726365A CN201610187473.6A CN201610187473A CN105726365A CN 105726365 A CN105726365 A CN 105726365A CN 201610187473 A CN201610187473 A CN 201610187473A CN 105726365 A CN105726365 A CN 105726365A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The invention provides cosmetic containing calophyllum inophyllum kernel oil, wherein the calophyllum inophyllum kernel oil accounts for 1-5% (in percentage by mass) of the cosmetic; and the skin cosmetic is skin cream, emulsion or skincare gel. The invention further provides a preparation method for the cosmetic. The calophyllum inophyllum kernel oil adopted by the cosmetic has relatively strong ultraviolet absorption, is relatively wide in absorption range, and has obvious synergistic interaction while co-used with a physical sun-screening agent titanium dioxide. Therefore, the calophyllum inophyllum kernel oil is applied to skin cosmetic as a sunscreen skin-protecting agent; and the finally obtained skin cosmetic is natural and safe, and further has the characteristics of anti-oxidation effect and the like while the sunscreen effect of the skin cosmetic is strengthened.
Description
Technical field
The invention belongs to household chemicals field, relate to a kind of cosmetics, a kind of containing calophyllum inophyllum kernel oil
Cosmetics and preparation method thereof.
Background technology
After skin accepts ultraviolet overexposure, epidermis cell can be damaged；Activated tyrosine enzyme, accelerates pigment synthesis,
Destroy the moisture-keeping functions of skin, make skin become dry, make the elastic fibers in skin corium impaired, make microgroove produce.Strongly
Under irradiation, also can cause skin inflammation, burn.When having abnormal case, then can become pigmentosa skin carcinoma etc..So sun-proof not
Skin melanism may only be prevented, it is possible to prevent the sunburn of skin, be very important so sun-proof for skin protection.
At present, common on market sunscreen has: ultraviolet light screener and UV absorbent.(1) ultraviolet light screener:
Some inorganic particulates are added, as titanium dioxide, zinc oxide etc. make physics sunscreen in sunscreen.These tiny particles
Barrier layer can be formed at skin surface, by reflection, scatters ultraviolet, skin be played a protective role.Advantage be stability high,
Safety is good.Shortcoming is that transparent feel is poor, is easily deposited into white layer at skin surface and comes off, and uses and too much can block pore, shadow
Ring sweat gland secretion, even cause dermatosis etc..Having research report to point out, micronized zinc oxide even nano zine oxide, due to tool
There is the least size so that they have higher chemism, therefore can be absorbed by the body, thus have human body and environment
Potentially hazardous.(2) UV absorbent: this kind of sunscreen is to add a certain amount of ultra-violet absorption thing in sunscreen
Matter and play anti-sunlight function.The molecule of these absorbent can absorb the energy of ultraviolet, then with the form such as heat energy or visible ray
Discharge, thus reduce the injury to skin.The product transparency that advantage is formed into is high, good absorbing effect.Shortcoming is to skin
Skin has certain zest, may cause the side effect such as inflammation, allergy, such as, may induce photosensitivity, and can be a large amount of by skin
Absorb；The characteristic of high oil suction water suction, easily causes xerosis cutis decortication；Water environment is impacted；Even it is exposed under sunlight
Can produce free radical, thus injured skin DNA, have time serious carcinogenic may etc..So the selection of sunscreen is sun-proofization
The core place of cosmetic formula, has conclusive impact to the performance of sunscreen product.
In addition, also a class is the composition with anti-sunlight function extracted from natural plants, can effectively absorb purple
Outside line, scavenging activated oxygen.The extracting solution such as Aloe, Fructus Cucumidis sativi is applied in sunscreen product by China at present.It addition, some medium-height grass
The medicine such as Flos Sophorae Immaturus, Rhizoma Coptidis, Flos Carthami etc. do not only have stronger anti-sunlight function, moreover it is possible to play the effects such as skin protection, whitening, treatment dermatitis, because of
This has higher using value.The sun-proof interval of natural sun-prevention component is big, sensitization rate is low, safe and effective, before having wide application
Scape.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of cosmetics containing calophyllum inophyllum kernel oil and
Preparation method, described this cosmetics containing calophyllum inophyllum kernel oil and preparation method thereof to solve sun-proof skin care of the prior art
Agent is dangerous, and human body easily produces the technical problem of harm.
The invention provides a kind of cosmetics containing calophyllum inophyllum kernel oil, described calophyllum inophyllum kernel oil quality hundred in cosmetics
Proportion by subtraction is 1-5%.
Further, described skin applies some make up as protective skin cream, emulsion or skin protection curry.
The invention provides a kind of protective skin cream containing calophyllum inophyllum kernel oil, calculate by mass percentage, the content of its raw material and
Form as follows:
Described solid grease is a kind of in fatty acid, fatty alcohol or fatty glyceride or any two or more groups
The mixture become, wherein, described fatty acid is stearic acid, myristic acid, oleic acid or behenic acid, and described fatty alcohol is oil
Alcohol, spermol, cetostearyl alcohol or two Lauryl Alcohols, described fatty glyceride is glyceryl monostearate, distearyl acid
Glyceride or glyceryl tristearate；
Described liquid fat is white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Semen Ricini
Oil, isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree
The mixture of a kind of or any two or more composition in oil, Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent for match Bick 305, polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester,
A kind of or any two or more composition in sorbitan fatty acid ester, glycerine monofatty ester or ethoxylated castor oil
Mixture, wherein, described polyoxyethylene stearyl alcohol ether is polyoxyethylene (2) stearic alcohol ether, polyoxyethylene (21) stearyl alcohol
Ether or the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent is a kind of or any two or more composition in glycerol, 1,3 butylene glycol or hyaluronate sodium
Mixture；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
In described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM second
The mixture of one or more compositions in uride or Kazon, in described preservative, the maximum of phenoxyethanol is used
Amount is 1% (wt) of material gross mass, and the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass,
Imidazolidinyl urea research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described essence is that perfume material mixture commonly used by cosmetics；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E.
Further, described skin applies some make up as protective skin cream, calculates by mass percentage, the content of its raw material and composition
As follows:
Described solid grease is glyceryl monostearate and the mixture of stearic acid composition, calculates in mass ratio, the most singly
Tristerin: stearic acid is 1:4；
Described liquid fat is Semen pruni armeniacae oil and the mixture of iso-octyl palmitate composition, calculates in mass ratio, the sweetest
Almond oil: iso-octyl palmitate is 1:12；
Described emulsifying agent is match Bick 305 and the mixture of polyoxyethylene stearyl alcohol ether composition, calculates in mass ratio, i.e.
Match Bick 305: polyoxyethylene stearyl alcohol ether is 3:5；
Described polyoxyethylene stearyl alcohol ether is the stearic alcohol ether of polyoxyethylene (2) and polyoxyethylene (21) stearic alcohol ether composition
Mixture；Calculate in mass ratio, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 2:3；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, i.e.
Glycerol: butanediol: hyaluronic acid is 1:3:0.05；
Described preservative is hydroxyphenyl methyl ester and the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. oxybenzene
Base methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
Described essence is that perfume material mixture commonly used by cosmetics.
Present invention also offers the preparation method of above-mentioned a kind of protective skin cream containing calophyllum inophyllum kernel oil, comprise the steps:
1) each reacting substance is weighed according to mass percent；
2) solid grease, liquid grease, calophyllum inophyllum kernel oil, emulsifying agent, the oil phase of antioxidant composition are heated to 65-90 DEG C
Stirring and dissolving is incubated standby as A phase；Titanium dioxide is dissolved in portions of de-ionized water standby；
3) wetting agent and the essence of 80%-99% are dissolved in the deionized water of the most dispersed titanium dioxide and are heated to
65-90 DEG C of insulation is as B phase；
4) being dissolved in remaining ionized water by remaining wetting agent and be heated to 45-50 DEG C, insulation is as C phase；
5) controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 3) B of gained is phased
It is that 50-100ml/min adds it to step 2 that system adds speed) in the A phase of gained, and continue homogenizing with homogenizer until A phase
With B phase mix homogeneously；
6) step 5) after A phase and B phase mix homogeneously, it is naturally cooling to 75-80 DEG C, carries out mechanical defoaming；Described machinery
It is that 100-500rpm/min carries out froth breaking that froth breaking i.e. controls speed of agitator；
7) step 6) froth breaking is when being naturally cooling to 40-50 DEG C after completing, and adds step 4) the C phase of gained and preservative, continue
Continuous mechanical agitation stops stirring, discharging to mix homogeneously and after naturally cooling to room temperature, obtains a kind of protecting containing calophyllum inophyllum kernel oil
Skin frost；It is 100-500rpm/min that described mechanical agitation i.e. controls speed of agitator.
The invention provides a kind of emulsion containing calophyllum inophyllum kernel oil, calculate by mass percentage, the content of its raw material and group
Become as follows:
Described solid grease is a kind of in fatty acid, fatty alcohol or fatty glyceride or any two or more groups
The mixture become, wherein, described fatty acid is stearic acid, myristic acid, oleic acid or behenic acid, and described fatty alcohol is oil
Alcohol, spermol, cetostearyl alcohol or two Lauryl Alcohols, described fatty glyceride is glyceryl monostearate, distearyl acid
Glyceride or glyceryl tristearate；
Described liquid fat is white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Semen Ricini
Oil, isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree
The mixture of a kind of or any two or more composition in oil, Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent for match Bick 305, polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester,
A kind of or any two or more composition in sorbitan fatty acid ester, glycerine monofatty ester or ethoxylated castor oil
Mixture, wherein, described polyoxyethylene stearyl alcohol ether is polyoxyethylene (2) stearic alcohol ether, polyoxyethylene (21) stearyl alcohol
Ether or the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent is a kind of or any two or more composition in glycerol, 1,3 butylene glycol or hyaluronate sodium
Mixture；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
In described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM second
The mixture of one or more compositions in uride or Kazon, in described preservative, the maximum of phenoxyethanol is used
Amount is 1% (wt) of material gross mass, and the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass,
Imidazolidinyl urea research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E.
Further, calculating by mass percentage, content and the composition of its raw material are as follows:
Described solid grease is cetostearyl alcohol and stearic acid calculates in mass ratio, i.e. cetostearyl alcohol: stearic acid is
The mixture of 3:1 composition；
Described liquid fat is isopropyl palmitate, dimethicone and the mixture of Jojoba oil composition, by quality
Than calculating, i.e. isopropyl palmitate: dimethicone: Jojoba oil is 5:3:2；
Described emulsifying agent is the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition,
Calculate in mass ratio, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 1.5:2；
Described wetting agent is hyaluronate sodium；
Described rheology control agent is hydroxyethyl cellulose；
Described preservative is hydroxyphenyl methyl ester and the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. oxybenzene
Base methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
Present invention also offers the preparation method of the above-mentioned emulsion containing calophyllum inophyllum kernel oil, comprise the steps:
1) each reacting substance is weighed according to mass percent；
2) solid grease, liquid grease, calophyllum inophyllum kernel oil, emulsifying agent, the oil phase of antioxidant composition are heated to 65-90 DEG C
Stirring and dissolving is incubated standby as A phase；
3) rheology control agent it is dissolved in portions of de-ionized water and is heated to 65-90 DEG C of insulation as B phase；
4) being dissolved in remaining deionized water by wetting agent and be heated to 45-50 DEG C, insulation is as C phase；
5) controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 3) B of gained is phased
It is that 50-100ml/min adds it to step 2 that system adds speed) in the A phase of gained, and continue homogenizing with homogenizer until A phase
With B phase mix homogeneously；
6) step 5) after A phase and B phase mix homogeneously, it is naturally cooling to 75-80 DEG C, carries out mechanical defoaming；Described machinery
It is that 100-500rpm/min carries out froth breaking that froth breaking i.e. controls speed of agitator；
7) step 6) froth breaking is when being naturally cooling to 45 DEG C after completing, and adds step 4) the C phase of gained and preservative, continue machine
Tool stirring is to mix homogeneously and stops stirring, discharging after naturally cooling to room temperature, obtains a kind of protective skin cream containing calophyllum inophyllum kernel oil
Or emulsion；It is 100-500rpm/min that described mechanical agitation i.e. controls speed of agitator.
The invention provides a kind of skin protection curry containing calophyllum inophyllum kernel oil, it is characterised in that the content of its raw material and composition
As follows:
Described liquid fat is white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Semen Ricini
Oil, isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree
The mixture of one or more compositions in oil, Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent is polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester, anhydrous sorbitol
The mixture of one or more compositions in fatty acid ester, glycerine monofatty ester or ethoxylated castor oil；
Wherein said polyoxyethylene stearyl alcohol ether be the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21),
Or the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent be the one in glycerol, 1,3 butylene glycol, hyaluronic acid, hyaluronate sodium or nicotiamide or
The mixture of two or more compositions；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
In described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM second
The mixture of one or more compositions in uride or Kazon, in described preservative, the maximum of phenoxyethanol is used
Amount is 1% (wt) of material gross mass, and the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass,
Imidazolidinyl urea research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E；
Described essence is that perfume material mixture commonly used by cosmetics；
Described alkaline agent is triethanolamine, sodium hydroxide or potassium hydroxide.
Further, calculating by mass percentage, content and the composition of its raw material are as follows:
Described liquid fat is the mixture of dimethicone and Cyclomethicone composition, counts in mass ratio
Calculate, i.e. dimethicone: Cyclomethicone is 2:1；
Described emulsifying agent is polyoxyethylene sorbitan fatty acid ester-80；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, i.e.
Glycerol: 1,3 butylene glycol: hyaluronate sodium is 1:2:0.05；
Described rheology control agent is carbomer；
Described preservative is the mixture of hydroxyphenyl methyl ester and hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. oxybenzene
Base methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT)；
Described alkaline agent is triethanolamine.
Present invention also offers the preparation method of above-mentioned a kind of skin protection curry containing calophyllum inophyllum kernel oil, including walking as follows
Rapid:
1) each reacting substance is weighed according to mass percent；
2) take portions of de-ionized water in a container, start agitator, rheology control agent is slowly poured into above-mentioned appearance
In device, it is standby that rheology control agent adds complete continuation stirring 15-20min；
3) liquid fat, calophyllum inophyllum kernel oil, antioxidant and emulsifying agent Hybrid Heating are heated to 45-55 DEG C as oil phase
Obtain oil phase；
4) wetting agent and essence are joined step 2) solution in be heated uniformly to 45-55 DEG C as Aqueous dispersions and obtain
Aqueous phase；
5) by step 3) oil phase of gained joins step 4) in the aqueous phase of gained, open homogenizer, mixing speed simultaneously
For 10000-20000rpm/min, carrying out emulsifying, it is 6-7 that emulsifying regulates pH value with alkaline agent after terminating, and continues stirring, controls stirring
Rotating speed is 100-500rpm/min, when being naturally cooling to 40-50 DEG C, adds preservative, continues mechanical agitation to mix homogeneously also
Stop stirring, discharging after naturally cooling to room temperature, obtain a kind of skin protection curry containing calophyllum inophyllum kernel oil.
Calophyllum inophyllum kernel oil is to extract from the nut of Indonesian cherry-apple tree to obtain, and through ECOCERT certification be organic planting
Thing oil.This protophyte oil is rich in biological activity, has skin protection, the feature of high uv absorption, can prevent ultraviolet from causing
The oldest and the most feeble problem, by calophyllum inophyllum kernel oil Substitute For Partial Orangic sunscreen, it is possible to decrease the probability of the problem such as allergy, stimulation, simultaneously
Utilize calophyllum inophyllum kernel oil to have stronger ultraviolet absorption ability, together with inorganic UV shield agent, sun-proof result can be played
The effect of Synergistic.
The one of the present invention contains calophyllum inophyllum kernel oil cosmetics, can be protective skin cream, cream, emulsion or skin protection curry, this sea
Chinese bush cherry fruit oil pure natural, safety, ultraviolet absorption effect are good, and have certain antioxidant effect.
The present invention compares with prior art, and its technological progress is significant.The calophyllum inophyllum kernel oil that the present invention uses is owing to having
Stronger uv absorption, and absorption region is wider, when being used in conjunction with physical sunscreen agent titanium dioxide, has the most collaborative increasing
Effect effect.Therefore applying calophyllum inophyllum kernel oil in skin applies some make up as a kind of sun-proof skin care agent, the skin of final gained is made up
The natural safety of product, while enhancing skin applies some make up sun-proof result, also has the features such as antioxidation.It addition, the present invention
The skin containing this calophyllum inophyllum kernel oil apply some make up, its preparation technology simple possible, be suitable to industrialized production.
Accompanying drawing explanation
Fig. 1 is the ultra-violet absorption comparison diagram of ethylhexyl salicylate.
Fig. 2 is the ultra-violet absorption comparison diagram of calophyllum inophyllum kernel oil.
Detailed description of the invention
Below by embodiment and combine accompanying drawing the present invention is expanded on further, but it is not limiting as the present invention.
Embodiment 1
Using calophyllum inophyllum kernel oil as ultraviolet protection skin protectant, the application in preparing protective skin cream, i.e. one is containing calophyllum inophyllum kernel oil
Protective skin cream, calculate by mass percentage, content and the composition of its raw material are as follows:
Described solid grease is glyceryl monostearate and the mixture of stearic acid composition, calculates in mass ratio, the most singly
Tristerin: stearic acid is 1:4；
Described liquid fat is Semen pruni armeniacae oil and the mixture of iso-octyl palmitate composition, calculates in mass ratio, the sweetest
Almond oil: iso-octyl palmitate is 1:12；
Described emulsifying agent is match Bick 305 and the mixture of polyoxyethylene stearyl alcohol ether composition, calculates in mass ratio, i.e.
Match Bick 305: polyoxyethylene stearyl alcohol ether is 3:5；
Described polyoxyethylene stearyl alcohol ether is the stearic alcohol ether of polyoxyethylene (2) and polyoxyethylene (21) stearic alcohol ether composition
Mixture；Calculate in mass ratio, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 2:3；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, i.e.
Glycerol: butanediol: hyaluronic acid is 1:3:0.05；
Described preservative is hydroxyphenyl methyl ester and the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. oxybenzene
Base methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
The preparation method of above-mentioned a kind of protective skin cream containing calophyllum inophyllum kernel oil, specifically includes following steps:
1), by 3.0g calophyllum inophyllum kernel oil, the stearic acid of the 2.5g i.e. 2.0g of solid grease and the glyceryl monostearate of 0.5g,
The Semen pruni armeniacae oil of the 6.5g i.e. 0.5g of liquid grease and the iso-octyl palmitate of 6.0g, the match Bick 305 of the i.e. 1.5g of 4.0g emulsifying agent
Polyoxyethylene (21) stearic alcohol ether, the 0.05g antioxidant 2 of stearic alcohol ether and 1.5g, 6-bis-uncle with the polyoxyethylene (2) of 1.0g
The oil phase of butylated hydroxytoluene composition is heated to 65-90 DEG C of stirring and dissolving and is incubated standby as A phase；2.0g titanium dioxide is dissolved in
In 37.6g deionized water standby；
2), the 1,3 butylene glycol of the 4.0g wetting agent i.e. glycerol of 1.0g and 3.0g is dissolved in the most dispersed titanium dioxide
In deionized water and be heated to 65-90 DEG C insulation as B phase；
3), by 0.05g hyaluronate sodium being dissolved in 40.0g deionized water and be heated to 45-50 DEG C, insulation is as C phase；
4), controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 2) B of gained is phased
Drop rate processed is that 50-100ml/min adds it to step 1) in the A phase of gained, continue homogenizing 3min with homogenizer simultaneously；
5), step 4) after homogenizing 3min terminates, be cooled to 75-80 DEG C, use agitator instead controlling speed of agitator is 100-
500rpm/min carries out mechanical defoaming；
6), step 5) mechanical defoaming is when being cooled to 45 DEG C after completing, and adds step 3) the C phase of gained and 0.3g preservative are i.e.
0.2g hydroxyphenyl methyl ester and 0.1g hydroxyphenyl propyl ester, continuing to control agitator speed is that 100-500rpm/min is stirred, and treats
Cool to room temperature stopping stirring, and discharging obtains a kind of protective skin cream containing calophyllum inophyllum kernel oil.
Embodiment 2
Using calophyllum inophyllum kernel oil as ultraviolet protection skin protectant, the application in preparation emulsion, a kind of containing calophyllum inophyllum kernel oil
Emulsion, calculates by mass percentage, and content and the composition of its raw material are as follows:
Described solid grease is cetostearyl alcohol and the mixture of stearic acid composition, calculates in mass ratio, i.e. 16
Eight alcohol: stearic acid is 3:1；
Described liquid fat is isopropyl palmitate, dimethicone and the mixture of Jojoba oil composition, by quality
Than calculating, i.e. isopropyl palmitate: dimethicone: Jojoba oil is 5:3:2；
Described emulsifying agent is the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition,
Calculate in mass ratio, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 1.5:2；
Described wetting agent is hyaluronate sodium；
Described rheology control agent is hydroxyethyl cellulose；
Described preservative is hydroxyphenyl methyl ester, the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. hydroxyphenyl
Methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
The preparation method of above-mentioned a kind of emulsion containing calophyllum inophyllum kernel oil, specifically includes following steps:
1), by 1.0g calophyllum inophyllum kernel oil, the cetostearyl alcohol of the 4.0g i.e. 3.0g of solid grease and the stearic acid of 1.0g, 10.0g
The dimethicone of the liquid grease i.e. isopropyl palmitate of 5.0g and 3.0g is with the Jojoba oil of 2.0g, 3.5g emulsifying agent i.e.
The stearic alcohol ether of the polyoxyethylene (2) of 1.5g is stearic alcohol ether, 0.05g antioxidant 2, the tertiary fourth of 6-bis-with the polyoxyethylene (21) of 2.0g
The oil phase of base hydroxy-methylbenzene composition is heated to 65-90 DEG C of stirring and dissolving and is incubated standby as A phase；
2), 0.2g rheology control agent hydroxyethyl cellulose it is dissolved in the deionized water of 40.9g and is heated to 65-90 DEG C of guarantor
Temperature is standby as B phase；
3), by 0.05g hyaluronate sodium being dissolved in 40.0g deionized water and be heated to 45-50 DEG C, insulation is as C phase；
4), controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 2) B of gained is phased
Drop rate processed is that 50-100ml/min adds it to step 1) in the A phase of gained, continue homogenizing 3min with homogenizer simultaneously；
5), step 4) after homogenizing 3min, be cooled to 75-80 DEG C, use agitator instead controlling speed of agitator is 100-500rpm/
Min carries out mechanical defoaming；
6), step 5) froth breaking is when being cooled to 45 DEG C after completing, and adds step 3) the C phase of gained and 0.3g preservative i.e. 0.2g
Hydroxyphenyl methyl ester and the hydroxyphenyl propyl ester of 0.1g, continue control agitator speed be that 100-500rpm/min is stirred, treat
Cool to room temperature stopping stirring, and discharging obtains a kind of emulsion containing calophyllum inophyllum kernel oil.
Embodiment 3
Using calophyllum inophyllum kernel oil as UV resistance skin protectant, the application in preparation skin protection curry, i.e. one is containing calophyllum inophyllum kernel oil
Skin protection curry, calculate by mass percentage, content and the composition of its raw material are as follows:
Described liquid fat is dimethicone, the mixture of Cyclomethicone composition, calculates in mass ratio,
I.e. dimethicone: Cyclomethicone is 2:1；
Described emulsifying agent is polyoxyethylene sorbitan fatty acid ester-80；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, i.e.
Glycerol: 1,3 butylene glycol: hyaluronate sodium is 1:2:0.05；
Described rheology control agent is carbomer；
Described preservative is hydroxyphenyl methyl ester, the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. hydroxyphenyl
Methyl ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT)；
Described alkaline agent is triethanolamine.
The preparation method of above-mentioned a kind of skin protection curry containing calophyllum inophyllum kernel oil, specifically includes following steps:
1), the deionized water of corresponding amount is added in beaker, start agitator, then by 0.5g rheology control agent i.e. card ripple
Nurse is slowly poured in beaker, and it is standby that rheology control agent adds complete continuation stirring 15-20min；
2), by 3.0g liquid fat i.e. 2.0g dimethicone and 1.0g Cyclomethicone, 1.0g calophyllum inophyllum kernel oil,
0.05g antioxidant 2,6-di-tert-butyl hydroxy toluene and 1.0g emulsifying agent i.e. polyoxyethylene sorbitan fatty acid ester-
80 Hybrid Heating are heated to 50 DEG C as oil phase and obtain oil phase；
3), 3.05g wetting agent i.e. 1.0g glycerol, the 1,3 butylene glycol of 2.0g and 0.05g hyaluronate sodium are joined step
Rapid 1) deionized water after adding rheology control agent in is heated to 50 DEG C of mix homogeneously and obtains aqueous phase；
4), by step 2) oil phase of gained joins step 3) in the aqueous phase of gained, open homogenizer, mixing speed simultaneously
For 10000-20000rpm/min, carry out emulsifying 3min, emulsifying terminate after with triethanolamine regulation pH value be 6-7, continue stirring,
Control speed of agitator is 100-500rpm/min, when being naturally cooling to 45 DEG C, adds 0.3g preservative i.e. 0.2g hydroxyphenyl methyl ester
With 0.1g hydroxyphenyl propyl ester, continue mechanical agitation and to mix homogeneously and stop stirring, discharging after naturally cooling to room temperature, obtain one
Plant the skin protection curry containing calophyllum inophyllum kernel oil.
Compare with one of organic uv absorbers commonly used in the prior art ethylhexyl salicylate, take 0.05g water
Poplar acid Octyl Nitrite and 0.05g calophyllum inophyllum kernel oil with after 50ml ethanol dilution, are analyzed with ultraviolet spectrophotometer respectively, both
As depicted in figs. 1 and 2, contrast is it can be seen that under same concentrations, calophyllum inophyllum kernel oil is at 250-for the uv absorption spectra of gained
Having obvious ultraviolet absorption ability in the range of 340nm, absorption intensity is 2.7；And the uv absorption of ethylhexyl salicylate
Peak wave-length coverage is between 280-340nm, and absorption intensity is 2.6, it is seen that the uv absorption intensity of calophyllum inophyllum kernel oil and salicylic acid second
The own ester of base is close, and uv absorption wave-length coverage is more wider than ethylhexyl salicylate, be a kind of efficiently, the natural of safety, wide spectrum plant
Thing sun-prevention component, may be used in sun care preparations.
Under the same terms of embodiment 1, replace the calophyllum inophyllum kernel oil of isoconcentration (mg/ml) with ethylhexyl salicylate, utilize
The SPF-290AS SPF (sun protection factor) test system that Optometrics (U.S.) manufactures carries out ultraviolet protection level investigation, the former
(ethylhexyl salicylate) SPF numerical value is 6.617, and the latter's (calophyllum inophyllum kernel oil) SPF numerical value is 4.453.
In sum, it can be deduced that under same concentrations consumption, its effect is lower slightly with ethylhexyl salicylate ratio, can portion
Dividing and substitute chemical sun, the most above-mentioned calophyllum inophyllum kernel oil is a kind of safe and effective natural plant sunscreen component, can conduct
UV resistance skin protectant is in skin protection cosmetics.
Foregoing is only the basic explanation under present inventive concept, and according to technical scheme made any etc.
Effect conversion, all should belong to protection scope of the present invention.
Claims (11)
1. the skin containing calophyllum inophyllum kernel oil applies some make up, it is characterised in that described calophyllum inophyllum kernel oil is in skin applies some make up
Mass percent is 1-5%.
A kind of skin containing calophyllum inophyllum kernel oil applies some make up, it is characterised in that described skin is made up
Product are protective skin cream, emulsion or skin protection curry.
3. the protective skin cream containing calophyllum inophyllum kernel oil, it is characterised in that calculate by mass percentage, the content of its raw material and composition
As follows:
Described solid grease is a kind of or any two or more composition in fatty acid, fatty alcohol or fatty glyceride
Mixture, wherein, described fatty acid is stearic acid, myristic acid, oleic acid or behenic acid, and described fatty alcohol is oleyl alcohol, whale
Ceryl alcohol, cetostearyl alcohol or two Lauryl Alcohols, described fatty glyceride is glyceryl monostearate, distearin
Or glyceryl tristearate；
Described liquid fat be white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Oleum Ricini,
Isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree oil,
The mixture of a kind of or any two or more composition in Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent is match Bick 305, polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester, dehydration
Mixing of a kind of or any two or more composition in Span, glycerine monofatty ester or ethoxylated castor oil
Compound, wherein, described polyoxyethylene stearyl alcohol ether be the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21) or
The mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent is mixing of a kind of or any two or more composition in glycerol, 1,3 butylene glycol or hyaluronate sodium
Compound；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
Described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM Hydantoin
Or the mixture of one or more compositions in Kazon, in described preservative, the research on maximum utilized quantity of phenoxyethanol is
1% (wt) of material gross mass, the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass, imidazoles
Ureine research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E.
A kind of protective skin cream containing calophyllum inophyllum kernel oil, it is characterised in that calculate by mass percentage,
Content and the composition of its raw material are as follows:
Described solid grease is glyceryl monostearate and the mixture of stearic acid composition, calculates in mass ratio, i.e. single stearic
Acid glyceride: stearic acid is 1:4；
Described liquid fat is Semen pruni armeniacae oil and the mixture of iso-octyl palmitate composition, calculates in mass ratio, i.e. Semen pruni armeniacae
Oil: iso-octyl palmitate is 1:12；
Described emulsifying agent is match Bick 305 and the mixture of polyoxyethylene stearyl alcohol ether composition, calculates in mass ratio, i.e. matches ratio
Grams 305: polyoxyethylene stearyl alcohol ether is 3:5；
Described polyoxyethylene stearyl alcohol ether is the mixed of the stearic alcohol ether of polyoxyethylene (2) and polyoxyethylene (21) stearic alcohol ether composition
Compound；Calculate in mass ratio, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 2:3；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, the sweetest
Oil: butanediol: hyaluronic acid is 1:3:0.05；
Described preservative is hydroxyphenyl methyl ester and the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. hydroxyphenyl first
Ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
5. the preparation method of a kind of protective skin cream containing calophyllum inophyllum kernel oil described in claim 3, it is characterised in that include walking as follows
Rapid:
1) each reacting substance is weighed according to mass percent；
2) solid grease, liquid grease, calophyllum inophyllum kernel oil, emulsifying agent, the oil phase of antioxidant composition are heated to 65-90 DEG C of stirring
Dissolving is incubated standby as A phase；Titanium dioxide is dissolved in portions of de-ionized water standby；
3) wetting agent and the essence of 80%-99% are dissolved in the deionized water of the most dispersed titanium dioxide and are heated to 65-
90 DEG C of insulations are as B phase；
4) being dissolved in remaining ionized water by remaining wetting agent and be heated to 45-50 DEG C, insulation is as C phase；
5) controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 3) the B phase control of gained adds
Entering speed is that 50-100ml/min adds it to step 2) in the A phase of gained, and continue homogenizing with homogenizer until A phase and B
Phase mix homogeneously；
6) step 5) after A phase and B phase mix homogeneously, it is naturally cooling to 75-80 DEG C, carries out mechanical defoaming；Described mechanical defoaming
I.e. controlling speed of agitator is that 100-500rpm/min carries out froth breaking；
7) step 6) froth breaking is when being naturally cooling to 40-50 DEG C after completing, and adds step 4) the C phase of gained and preservative, continue machine
Tool stirring is to mix homogeneously and stops stirring, discharging after naturally cooling to room temperature, obtains a kind of protective skin cream containing calophyllum inophyllum kernel oil；
It is 100-500rpm/min that described mechanical agitation i.e. controls speed of agitator.
6. the emulsion containing calophyllum inophyllum kernel oil, it is characterised in that calculating by mass percentage, the content of its raw material and composition are such as
Under:
Described solid grease is a kind of or any two or more composition in fatty acid, fatty alcohol or fatty glyceride
Mixture, wherein, described fatty acid is stearic acid, myristic acid, oleic acid or behenic acid, and described fatty alcohol is oleyl alcohol, whale
Ceryl alcohol, cetostearyl alcohol or two Lauryl Alcohols, described fatty glyceride is glyceryl monostearate, distearin
Or glyceryl tristearate；
Described liquid fat be white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Oleum Ricini,
Isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree oil,
The mixture of a kind of or any two or more composition in Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent is match Bick 305, polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester, dehydration
Mixing of a kind of or any two or more composition in Span, glycerine monofatty ester or ethoxylated castor oil
Compound, wherein, described polyoxyethylene stearyl alcohol ether be the stearic alcohol ether of polyoxyethylene (2), the stearic alcohol ether of polyoxyethylene (21) or
The mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent is mixing of a kind of or any two or more composition in glycerol, 1,3 butylene glycol or hyaluronate sodium
Compound；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
Described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM Hydantoin
Or the mixture of one or more compositions in Kazon, in described preservative, the research on maximum utilized quantity of phenoxyethanol is
1% (wt) of material gross mass, the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass, imidazoles
Ureine research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E.
A kind of emulsion containing calophyllum inophyllum kernel oil, it is characterised in that calculate by mass percentage, its
Content and the composition of raw material are as follows:
Described solid grease is cetostearyl alcohol and stearic acid calculates in mass ratio, i.e. cetostearyl alcohol: stearic acid is 3:1 group
The mixture become；
Described liquid fat is isopropyl palmitate, dimethicone and the mixture of Jojoba oil composition, counts in mass ratio
Calculate, i.e. isopropyl palmitate: dimethicone: Jojoba oil is 5:3:2；
Described emulsifying agent is the mixture of the stearic alcohol ether of polyoxyethylene (2) alcohol ether stearic with polyoxyethylene (21) composition, by matter
Amount ratio calculates, i.e. the stearic alcohol ether of polyoxyethylene (2): the stearic alcohol ether of polyoxyethylene (21) is 1.5:2；
Described wetting agent is hyaluronate sodium；
Described rheology control agent is hydroxyethyl cellulose；
Described preservative is hydroxyphenyl methyl ester and the mixture of hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. hydroxyphenyl first
Ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT).
8. the preparation method of a kind of emulsion containing calophyllum inophyllum kernel oil described in claim 6, it is characterised in that include walking as follows
Rapid:
1) each reacting substance is weighed according to mass percent；
2) solid grease, liquid grease, calophyllum inophyllum kernel oil, emulsifying agent, the oil phase of antioxidant composition are heated to 65-90 DEG C of stirring
Dissolving is incubated standby as A phase；
3) rheology control agent it is dissolved in portions of de-ionized water and is heated to 65-90 DEG C of insulation as B phase；
4) being dissolved in remaining deionized water by wetting agent and be heated to 45-50 DEG C, insulation is as C phase；
5) controlling under the conditions of homogenizer rotating speed is 10000-20000rpm/min, by step 3) the B phase control of gained adds
Entering speed is that 50-100ml/min adds it to step 2) in the A phase of gained, and continue homogenizing with homogenizer until A phase and B
Phase mix homogeneously；
6) step 5) after A phase and B phase mix homogeneously, it is naturally cooling to 75-80 DEG C, carries out mechanical defoaming；Described mechanical defoaming
I.e. controlling speed of agitator is that 100-500rpm/min carries out froth breaking；
7) step 6) froth breaking is when being naturally cooling to 45 DEG C after completing, and adds step 4) the C phase of gained and preservative, continue machinery and stir
Mix to mix homogeneously and stop stirring, discharging after naturally cooling to room temperature, obtaining a kind of protective skin cream containing calophyllum inophyllum kernel oil or breast
Liquid；It is 100-500rpm/min that described mechanical agitation i.e. controls speed of agitator.
9. the skin protection curry containing calophyllum inophyllum kernel oil, it is characterised in that calculate by mass percentage, the content of its raw material and group
Become as follows:
Described liquid fat be white oil, dimethicone, Jojoba oil, Cyclomethicone, olive oil, Oleum Ricini,
Isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, caprylic capric triglyceride, Semen Tritici aestivi germ oil, American Avocado Tree oil,
The mixture of one or more compositions in Semen pruni armeniacae oil, Oleum Cocois or Petiolus Trachycarpi oil；
Described emulsifying agent is polyoxyethylene stearyl alcohol ether, polyoxyethylene sorbitan fatty acid ester, sorbitan fatty
The mixture of one or more compositions in acid esters, glycerine monofatty ester or ethoxylated castor oil；
Wherein said polyoxyethylene stearyl alcohol ether is the stearic alcohol ether of polyoxyethylene (2), polyoxyethylene (21) stearic alcohol ether or poly-
The mixture of the stearic alcohol ether of oxygen ethylene (2) alcohol ether stearic with polyoxyethylene (21) composition；
Described wetting agent is one or both in glycerol, 1,3 butylene glycol, hyaluronic acid, hyaluronate sodium or nicotiamide
The mixture of composition described above；
Described rheology control agent is hydroxyethyl cellulose or carbomer；
Described preservative is phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, imidazolidinyl urea, chlorphenesin, DMDM Hydantoin
Or the mixture of one or more compositions in Kazon, in described preservative, the research on maximum utilized quantity of phenoxyethanol is
1% (wt) of material gross mass, the maximum single consumption of methyl hydroxybenzoate, propyl hydroxybenzoate is 0.4% (wt) of material gross mass, imidazoles
Ureine research on maximum utilized quantity is 0.6% (wt) of material gross mass, and chlorphenesin research on maximum utilized quantity is the 0.3% of material gross mass
(wt), DMDM Hydantoin research on maximum utilized quantity is 0.6% (wt) of material gross mass, and Kazon research on maximum utilized quantity is material gross mass
0.0015% (wt)；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT) or vitamin E；
Described essence is that perfume material mixture commonly used by cosmetics；
Described alkaline agent is triethanolamine, sodium hydroxide or potassium hydroxide.
A kind of skin protection curry containing calophyllum inophyllum kernel oil, it is characterised in that by mass percentage
Calculating, content and the composition of its raw material are as follows:
Described liquid fat is the mixture of dimethicone and Cyclomethicone composition, calculates in mass ratio, i.e.
Dimethicone: Cyclomethicone is 2:1；
Described emulsifying agent is polyoxyethylene sorbitan fatty acid ester-80；
Described wetting agent is glycerol, 1,3 butylene glycol and the mixture of hyaluronate sodium composition, calculates in mass ratio, the sweetest
Oil: 1,3 butylene glycol: hyaluronate sodium is 1:2:0.05；
Described rheology control agent is carbomer；
Described preservative is the mixture of hydroxyphenyl methyl ester and hydroxyphenyl propyl ester composition, calculates in mass ratio, i.e. hydroxyphenyl first
Ester: hydroxyphenyl propyl ester is 2:1；
Described antioxidant is 2,6-di-tert-butyl hydroxy toluene (BHT)；
Described alkaline agent is triethanolamine.
The preparation method of 11. a kind of skin protection currys containing calophyllum inophyllum kernel oil, it is characterised in that include
Following steps:
1) each reacting substance is weighed according to mass percent；
2) take portions of de-ionized water in a container, start agitator, rheology control agent is slowly poured in above-mentioned container,
It is standby that rheology control agent adds complete continuation stirring 15-20min；
3) as oil phase, liquid fat, calophyllum inophyllum kernel oil, antioxidant and emulsifying agent Hybrid Heating are heated to 45-55 DEG C to obtain
Oil phase；
4) wetting agent and essence are joined step 2) solution in be heated uniformly to 45-55 DEG C as Aqueous dispersions and obtain water
Phase；
5) by step 3) oil phase of gained joins step 4) in the aqueous phase of gained, open homogenizer simultaneously, mixing speed is
10000-20000rpm/min, carries out emulsifying, and it is 6-7 that emulsifying regulates pH value with alkaline agent after terminating, and continues stirring, controls stirring turn
Speed is 100-500rpm/min, when being naturally cooling to 40-50 DEG C, adds preservative, continues mechanical agitation to mix homogeneously the most certainly
Stop stirring, discharging after being so cooled to room temperature, obtain a kind of skin protection curry containing calophyllum inophyllum kernel oil.
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| CN106619227A (en) * | 2017-01-10 | 2017-05-10 | 韩后化妆品股份有限公司 | Compound grease, sunscreen cream applying compound grease, and preparation method of sunscreen cream |
| CN107242980A (en) * | 2017-06-27 | 2017-10-13 | 江苏天芳健康科技有限公司 | A kind of cream of containing gingko extract |
| CN108158868A (en) * | 2018-03-16 | 2018-06-15 | 广州欧盛化妆品有限公司 | A kind of cleawhite over-night essences and preparation method thereof |
| CN108524392A (en) * | 2018-05-28 | 2018-09-14 | 上海应用技术大学 | A kind of sunscreen composition and suncream containing barley young leaf powder and calophyllum inophyllum kernel oil |
| CN109481371A (en) * | 2019-01-18 | 2019-03-19 | 陈伟伟 | A kind of cosmetic face cream and preparation method thereof with antiageing effect |
| CN113952250A (en) * | 2021-11-02 | 2022-01-21 | 上海忱扬生物科技有限公司 | Stable anti-photoaging composition and preparation method thereof |
| CN113952250B (en) * | 2021-11-02 | 2023-11-21 | 上海忱扬生物科技有限公司 | Stable photo-aging resistant composition and preparation method thereof |
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