CN109456122A - A kind of water-soluble fertilizer and its preparation process containing amino acid - Google Patents
A kind of water-soluble fertilizer and its preparation process containing amino acid Download PDFInfo
- Publication number
- CN109456122A CN109456122A CN201811455187.9A CN201811455187A CN109456122A CN 109456122 A CN109456122 A CN 109456122A CN 201811455187 A CN201811455187 A CN 201811455187A CN 109456122 A CN109456122 A CN 109456122A
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- Prior art keywords
- amino acid
- water
- soluble fertilizer
- containing amino
- fertilizer containing
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The present invention provides a kind of water-soluble fertilizer containing amino acid, it include: marine algae glycoprotein, compound amino acid, brassin, 4- iodobenzene fluoroacetic acid ethyl ester, plant growth regulator, moderate-element composition and mannitol calcium, the water-soluble fertilizer containing amino acid, it can be improved production capacity, rate of growth 20%, fruit annesl rate reach 98.1%；The present invention also provides the preparation processes of the water-soluble fertilizer containing amino acid, comprising: leaching alcohol, primary activation, re-activation, fermentation and mixing.Water-soluble fertilizer prepared by the present invention containing amino acid can strongly promote root growth, repair impaired root system；Freeze proof ensuing crop, drought resisting, disease-resistant significant effect raising are applied, and nematode, trialeurodes vaporariorum and aphid can be expelled；Also have and promote plant growth, promote Peng fruit, lists ahead of time, 20% can be increased production；Soil can be improved, the gas permeability of soil, retain water and nutrients, fixed nitrogen, phosphorus decomposing, potassium decomposing are increased.
Description
Technical field
The present invention relates to a kind of water-soluble fertilizer and its preparation process containing amino acid belongs to the water-soluble fertilizer technology neck of crops
Domain.
Background technique
Water soluble fertilizer is a kind of quick action fertilizer, good water solubility, without residue, can completely dissolve in water, can be made
The root system of object and blade face are directly absorbed and utilized.Water-soluble fertilizer containing amino acid provides amino in Ministry of Agriculture's NY1429-2010 standard
Acid content is more than or equal to 100g/L.
Application No. is the Chinese patents of CN201810731194 .0, disclose a kind of water-soluble fertilizer containing amino acid, use
25 parts -35 parts of free amino acid containing amino acid 40%, 3-5 parts of the manganese sulfate containing manganese 31%, 3-5 parts of the zinc sulfate containing zinc 35%, water
60-65 parts of technical solution can promote the water-soluble fertilizer containing amino acid of vegetables fast-growth, obvious effect of increasing production.Select trip
Isolated amino acid substitutes the amino acid in traditional proportioning, makes full use of the bioactivity feature of free amino acid, and building, synthesis
The ability of plant cell and tissue sprays the water-soluble fertilizer containing amino acid especially suitable for growth periods such as vegetables, fruit tree, flowers
It applies.
But the existing water-soluble fertilizer containing amino acid, however it remains following insufficient:
(1) for the crop of transplanting, the effect for repairing root system is unobvious；
(2) do not have and improve freeze proof crop, drought resisting, disease-resistant effect and expelling parasite, resistant effect；
(3) effect of increasing production is unobvious, small to the opsonic action of soil；
(4) it does not almost work to the amendment of fruit shape, lacks the effect for promoting annesl yet.
Summary of the invention
The present invention in order to solve the above technical problems, provides a kind of water-soluble fertilizer and its preparation process containing amino acid, with reality
Existing following goal of the invention:
(1) water-soluble fertilizer prepared by the present invention containing amino acid can strongly promote root growth, repair impaired root system；
(2) after applying the water-soluble fertilizer prepared by the present invention containing amino acid, crop is freeze proof, drought resisting, disease-resistant significant effect improve,
And the effect of nematode, trialeurodes vaporariorum and aphid can be expelled；
(3) water-soluble fertilizer prepared by the present invention containing amino acid has and promotes plant growth, promotes Peng fruit, lists ahead of time, can
Volume increase 20%；
(4) water-soluble fertilizer prepared by the present invention containing amino acid, can improve soil, increase the gas permeability of soil, retain water and nutrients, Gu
Nitrogen, phosphorus decomposing, potassium decomposing；
(5) water-soluble fertilizer prepared by the present invention containing amino acid promotees flower, flower and fruit protecting, and the beautiful no deformity of fruit shape increases sugariness,
Promote annesl.
In order to solve the above technical problems, The technical solution adopted by the invention is as follows:
A kind of water-soluble fertilizer containing amino acid, it is characterised in that: including following raw material: marine algae glycoprotein, compound amino acid.
It is further improvement to above-mentioned technical proposal below:
A kind of water-soluble fertilizer containing amino acid, the water-soluble fertilizer containing amino acid, further includes: brassin, 4- iodobenzene
Fluoroacetic acid ethyl ester, plant growth regulator, moderate-element composition and mannitol calcium.
A kind of water-soluble fertilizer containing amino acid, by weight, including following raw material: marine algae glycoprotein 65
Part, 44 parts of compound amino acid, 12 parts of brassin, 5 parts of 4- iodobenzene fluoroacetic acid ethyl ester, 6 parts of plant growth regulator, moderate-element group
Close 25 parts and 12 parts of mannitol calcium of object.
A kind of water-soluble fertilizer containing amino acid, can be improved production capacity, rate of growth 20%, and fruit annesl rate reaches
98.1%。
The present invention also provides a kind of preparation processes of water-soluble fertilizer containing amino acid, comprising: leaching alcohol, primary activation, two
Secondary activation, fermentation and mixing.
The leaching alcohol, propyl alcohol additive amount are 6.5%；
Ethyl alcohol additive amount is 12.5%；
Soaking time is 5-6 hours；
Be ultrasonically treated frequency 55kHZ, 85 DEG C of temperature.
The primary activation, acid are 3:1 with particle mass ratio, are impregnated 2 hours.
The re-activation, zinc chloride: bismuth chloride: hydrochloric acid: the mass ratio of particle is 4:3:7:2；Activation time is 2 small
When, activation temperature is 600 DEG C.
The volume mass ratio 3ml:10g of the fermentation, seed liquor and fermentation medium ferments 12 days, spray-dried, until
Moisture content is 6-7%.
It is raw to weigh marine algae glycoprotein, compound amino acid, brassin, 4- iodobenzene fluoroacetic acid ethyl ester, plant for the mixing
Long regulator, moderate-element composition and the mixing of mannitol calcium；
The marine algae glycoprotein, in terms of weight content, including sugar 12%, protein 77%, molecular weight are 22 kDa；
The antifungal activity enzyme, the molten bacillus OH11 fermentation liquid of protease, producing enzyme, histone deacetylase (HDAC) inhibitor,
Mass ratio is 18:4:1；
The moderate-element composition, by boric acid, benzene peptide amino acid, ammonium molybdate, manganese sulfate, copper sulphate, ferric sulfate, zinc sulfate, sulphur
Sour magnesium and EDTA composition, mass ratio 35:10:15:20:12:7:9:18:22.
Above technical scheme is used, the invention has the benefit that
(1) water-soluble fertilizer prepared by the present invention containing amino acid can strongly promote root growth, repair impaired root system；For
The crop of transplanting, average survival are improved up to 10% or more；
(2) after applying the water-soluble fertilizer prepared by the present invention containing amino acid, crop is freeze proof, drought resisting, disease-resistant significant effect improve,
And the effect of nematode, trialeurodes vaporariorum and aphid can be expelled；
(3) water-soluble fertilizer prepared by the present invention containing amino acid, have promote plant growth, promote Peng fruit, list ahead of time, with kind
For eggplant, Time To Market has done sth. in advance half a month, improves production capacity, rate of growth 20%；
(4) water-soluble fertilizer prepared by the present invention containing amino acid, can improve soil, increase the gas permeability of soil, retain water and nutrients, Gu
Nitrogen, phosphorus decomposing, potassium decomposing；Applied to green cucumber, after one batch of plantation, the gas permeability of soil improves 5.6%.
(5) water-soluble fertilizer prepared by the present invention containing amino acid, promotees flower, flower and fruit protecting, and the beautiful no deformity of fruit shape increases sweet tea
Degree promotes annesl；Annesl rate is by pervious 86.5% improve of fertilising to 98.1%, and annesl is uniform.
Specific embodiment
Hereinafter, preferred embodiments of the present invention will be described, it should be understood that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
A kind of water-soluble fertilizer and its preparation process containing amino acid of embodiment 1
(1) material cooking
Feather and waste and old silk are weighed by the mass ratio of 2:3, by feather and the removal of impurities of waste and old silk, is cleaned, at 142 DEG C,
Boiling 25min under the conditions of 0.6MPa, dry, water content is controlled in 12-15%；
(2) alcohol is soaked
6.5% propyl alcohol is added after boiling and 12.5% ethyl alcohol stirs evenly, is impregnated 5-6 hours, is impregnated while being carried out ultrasonic place
It manages, supersonic frequency 55kHZ, 85 DEG C of temperature, then natural air drying or drying are shredded；
(3) primary activation
By after chopping feather and waste and old silk particle acid dip, the acid, comprising: 60% phosphoric acid, malic acid, oxalic acid,
Mass ratio is 10:2:1, and acid is 3:1 with particle mass ratio, is impregnated 2 hours, is washed, dry.
(4) re-activation
Particle after once activating is placed in the mixed liquor of zinc chloride, bismuth chloride, hydrochloric acid, zinc chloride: bismuth chloride: hydrochloric acid:
The mass ratio of particle is to impregnate 2 hours in 4:3:7:2, then in N2Flow is 17ml/min, at 600 DEG C, is activated 2 hours.
(5) seed culture
By bacillus amyloliquefaciens, bacillus thuringiensis, Manny Poole streptomycete s-1 and produce nitrite Actinomycesa lmadurae
It is inoculated into seed culture medium and ferments, fermentation condition: 37 DEG C, humidity 66.5%, oxygen concentration 18.6%, stirring rate
It ferments 10 days under 200rpm；Every liter of seed culture medium contains peptone 15.0g, beef peptone 12.0g, glucose 2.5g, sucrose
1.5g and NaCl 3.0g, surplus are water；
The Manny Poole streptomycete s-1 (streptomyces manipurensis s-1), deposit number is CCTCC No:
M2017261；
The production nitrite Actinomycesa lmadurae (Actinomadura nitritigenes), deposit number is CGMCC No:
4.1178；
The bacillus amyloliquefaciens, bacillus thuringiensis are all from commercially available, and state is powder.
(6) it ferments
Particle after re-activation is added in fermentation medium according to 15% quality additive amount,
Then the hair of the particle after seed liquor being inoculated into according to the inoculum concentration of volume mass ratio 3ml:10g added with re-activation
It ferments, ferments 12 days in ferment culture medium, it is spray-dried, until moisture content is 6-7%, obtain compound amino acid.
(7) it mixes
(a) marine algae glycoprotein, compound amino acid, brassin, 4- iodobenzene fluoroacetic acid ethyl ester, plant are weighed by following parts by weight
Growth regulator, moderate-element composition and mannitol calcium.
Parts by weight are as follows: 65 parts of marine algae glycoprotein, 44 parts of compound amino acid, 12 parts of brassin, 4- iodobenzene fluoroacetic acid second
5 parts of ester, 6 parts of plant growth regulator, 25 parts of moderate-element composition and 12 parts of mannitol calcium,
The marine algae glycoprotein, in terms of weight content, including sugar 12%, protein 77%, molecular weight are 22 kDa；
The antifungal activity enzyme, the molten bacillus OH11 fermentation liquid of protease, producing enzyme, histone deacetylase (HDAC) inhibitor,
Mass ratio is 18:4:1；
The moderate-element composition, by boric acid, benzene peptide amino acid, ammonium molybdate, manganese sulfate, copper sulphate, ferric sulfate, zinc sulfate, sulphur
Sour magnesium and EDTA composition, mass ratio 35:10:15:20:12:7:9:18:22；
The mannitol calcium is purchased from Linyi Wo Meng fertilizer Co., Ltd, and calcic 170g/L, specification 200ml are bottled.
(b) according to the above parts by weight, compound amino acid, moderate-element composition and mannitol calcium are mixed, are added
Suitable water is heated to 54 DEG C, and being slowly stirred rate is 25rad/min, in whipping process, by brassin, 4- iodobenzene oxygen
Mixing is added in ethyl acetate, plant growth regulator, stirs 8min, mixture is made；
(c) vinegar acid for adjusting pH is added into mixture to 5.5-6.0, marine algae glycoprotein is then added, mixing carries out ultrasound
Processing, ultrasonic power 200W, frequency 50kHz ultrasonic temperature are 35 DEG C；Sonication treatment time 1-2min, ultrasonic treatment number are 2
It is secondary, it is dry, it after detection is qualified, is measured, packed, be put in storage, obtain the water-soluble fertilizer of the invention containing amino acid.
Water-soluble fertilizer effectiveness indicator prepared by the present invention containing amino acid:
(1) water-soluble fertilizer prepared by the present invention containing amino acid can strongly promote root growth, repair impaired root system；For
The crop of transplanting, average survival are improved up to 10% or more；
(2) after applying the water-soluble fertilizer prepared by the present invention containing amino acid, crop is freeze proof, drought resisting, disease-resistant significant effect improve,
And the effect of nematode, trialeurodes vaporariorum and aphid can be expelled；
(3) water-soluble fertilizer prepared by the present invention containing amino acid, have promote plant growth, promote Peng fruit, list ahead of time, with kind
For eggplant, Time To Market has done sth. in advance half a month, improves production capacity, rate of growth 20%；
(4) water-soluble fertilizer prepared by the present invention containing amino acid, can improve soil, increase the gas permeability of soil, retain water and nutrients, Gu
Nitrogen, phosphorus decomposing, potassium decomposing；Applied to green cucumber, after one batch of plantation, the gas permeability of soil improves 5.6%.
(5) water-soluble fertilizer prepared by the present invention containing amino acid, promotees flower, flower and fruit protecting, and the beautiful no deformity of fruit shape increases sweet tea
Degree promotes annesl；Annesl rate is improved by fertilising pervious 86.5% to 98.1%.
The water-soluble fertilizer containing amino acid of preparation of the invention complies fully in the Ministry of Agriculture's NY1429-2010 standard
All mandatory term and most of recommendatory clause, proportion science, nutrition is balanced, and absorptivity is high, has wide economy
Value and social value.
Unless otherwise indicated, percentage employed in the present invention is weight percent, ratio of the present invention,
For mass ratio.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features.
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (10)
1. a kind of water-soluble fertilizer containing amino acid, it is characterised in that: including marine algae glycoprotein, compound amino acid.
2. a kind of water-soluble fertilizer containing amino acid according to claim 1, it is characterised in that: described containing the water-soluble of amino acid
Fertilizer, further includes: brassin, 4- iodobenzene fluoroacetic acid ethyl ester, plant growth regulator, moderate-element composition and mannitol
Calcium.
3. a kind of water-soluble fertilizer containing amino acid according to claim 1, it is characterised in that: by weight, including it is following
Raw material: 65 parts of marine algae glycoprotein, 44 parts of compound amino acid, 12 parts of brassin, 5 parts of 4- iodobenzene fluoroacetic acid ethyl ester, plant are raw
6 parts of long regulator, 25 parts of moderate-element composition and 12 parts of mannitol calcium.
4. a kind of water-soluble fertilizer containing amino acid according to claim 3, it is characterised in that: can be improved production capacity, increase production
Rate 20%, fruit annesl rate reach 98.1%.
5. a kind of preparation process of the water-soluble fertilizer containing amino acid, it is characterised in that: include: leaching alcohol, primary activation, secondary work
Change, ferment and mixes.
6. a kind of preparation process of water-soluble fertilizer containing amino acid according to claim 5, it is characterised in that:
The leaching alcohol, propyl alcohol additive amount are 6.5%；
Ethyl alcohol additive amount is 12.5%；
Soaking time is 5-6 hours；
Be ultrasonically treated frequency 55kHZ, 85 DEG C of temperature.
7. a kind of preparation process of water-soluble fertilizer containing amino acid according to claim 5, it is characterised in that:
The primary activation, acid are 3:1 with particle mass ratio, are impregnated 2 hours.
8. a kind of preparation process of water-soluble fertilizer containing amino acid according to claim 5, it is characterised in that:
The re-activation, zinc chloride: bismuth chloride: hydrochloric acid: the mass ratio of particle is 4:3:7:2；Activation time is 2 hours, living
Changing temperature is 600 DEG C.
9. a kind of preparation process of water-soluble fertilizer containing amino acid according to claim 8, it is characterised in that:
The volume mass ratio 3ml:10g of the fermentation, seed liquor and fermentation medium ferments 12 days, spray-dried, until aqueous
Rate is 6-7%.
10. a kind of preparation process of the water-soluble fertilizer containing amino acid according to claim 1 or 5, it is characterised in that:
The mixing weighs marine algae glycoprotein, compound amino acid, brassin, 4- iodobenzene fluoroacetic acid ethyl ester, plant growth tune
Save agent, moderate-element composition and the mixing of mannitol calcium；
The marine algae glycoprotein, in terms of weight content, including sugar 12%, protein 77%, molecular weight are 22 kDa；
The antifungal activity enzyme, the molten bacillus OH11 fermentation liquid of protease, producing enzyme, histone deacetylase (HDAC) inhibitor,
Mass ratio is 18:4:1；
The moderate-element composition, by boric acid, benzene peptide amino acid, ammonium molybdate, manganese sulfate, copper sulphate, ferric sulfate, zinc sulfate, sulphur
Sour magnesium and EDTA composition, mass ratio 35:10:15:20:12:7:9:18:22.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811455187.9A CN109456122A (en) | 2018-11-30 | 2018-11-30 | A kind of water-soluble fertilizer and its preparation process containing amino acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811455187.9A CN109456122A (en) | 2018-11-30 | 2018-11-30 | A kind of water-soluble fertilizer and its preparation process containing amino acid |
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| Publication Number | Publication Date |
|---|---|
| CN109456122A true CN109456122A (en) | 2019-03-12 |
Family
ID=65612195
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811455187.9A Withdrawn CN109456122A (en) | 2018-11-30 | 2018-11-30 | A kind of water-soluble fertilizer and its preparation process containing amino acid |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111592429A (en) * | 2020-06-04 | 2020-08-28 | 漳州三炬生物技术有限公司 | Vegetable water culture nutrient solution containing amino acids as well as preparation method and application of vegetable water culture nutrient solution |
| CN113185351A (en) * | 2021-04-26 | 2021-07-30 | 绿地集团森茂园林有限公司 | Soil conditioner and seedling planting method adopting same |
| CN115380922A (en) * | 2022-10-28 | 2022-11-25 | 中国热带农业科学院南亚热带作物研究所 | Microbial plant growth regulator with growth promoting effect and application thereof |
-
2018
- 2018-11-30 CN CN201811455187.9A patent/CN109456122A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111592429A (en) * | 2020-06-04 | 2020-08-28 | 漳州三炬生物技术有限公司 | Vegetable water culture nutrient solution containing amino acids as well as preparation method and application of vegetable water culture nutrient solution |
| CN113185351A (en) * | 2021-04-26 | 2021-07-30 | 绿地集团森茂园林有限公司 | Soil conditioner and seedling planting method adopting same |
| CN115380922A (en) * | 2022-10-28 | 2022-11-25 | 中国热带农业科学院南亚热带作物研究所 | Microbial plant growth regulator with growth promoting effect and application thereof |
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Application publication date: 20190312 |