CN109288687A - A kind of more effect liquid crystal facial mask liquids and preparation method thereof - Google Patents
A kind of more effect liquid crystal facial mask liquids and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
The present invention relates to technical field of skin care, and in particular to a kind of more effect liquid crystal facial mask liquids and preparation method thereof.More effect liquid crystal facial mask liquids include liquid crystal emulsifier, thickener, moisturizer, Sodium Hyaluronate, preservative, various functional components and water.The functional component includes the water-soluble or oil-soluble substance with whitening, crease-resistant, antiallergic, anti-acne and other effects.Facial mask liquid of the invention is crystalline emulsion; the presence of oil-water interfaces layered liquid crystal not only can the various effective components of solubilising; dramatically increase facial mask effect; and it can be with water-soluble substances in effective protection liquid crystal layer and oily phase oil-soluble functional component; its failure is avoided, the performance of functional component performance in facial mask liquid is promoted.The more effect liquid crystal facial mask liquids produced using the method for the present invention, liquid crystal structure is similar with human skin structure, has high cutaneous safety；Liquid crystal structure simulates human skin, has the title of " human body second layer skin ", improves the permeance property of facial mask liquid, is conducive to skin and absorbs.
Description
Technical field
The present invention relates to technical field of skin care, and in particular to a kind of more effect liquid crystal facial mask liquids and preparation method thereof.
Background technique
With economical increasingly developed, social is constantly progressive, and people also never stop to the pursuit of beauty；Allegro life
Living and atmosphere pollution, air-borne dust etc. damage skin and aging of population phenomenon is on the rise, and keep the skin care aobvious
Must be particularly important, skin care item have become necessity for people's lives.Currently, demand not only office of the people for skin care item
It is limited to moisturizing, also not only exclusive product of women, therefore, more effect skin care item come into being, including whitening and anti-aging,
Antiallergic, anti-acne and other effects.Wherein, facial mask is already at a part in for people's lives, either male or women, busy
A facial mask is applied after commonplace life has become a kind of habit.However, the wilderness demand just because of market results in face
The barbarous growth of film industry, many companies utilize consumer for freckle removing and whitening, anti-wrinkle, the eager psychology of anti-acne, with a definite target in view
Be proposed with the various products declared." magical place " of these products be, it can whitening, anti-wrinkle can also nti-freckle,
But this is all only declared.In fact, the most effect of the effect of currently on the market property product is single, unstable and functional component
It is vulnerable.For the technology of current cosmetics company, oil-soluble and water-soluble both effectiveness ingredient tend not to be added simultaneously；
The addition of both effectiveness ingredient may cause the unstable of system, be easy to happen grease lamination, while also will affect skin sense.
In addition, both effectiveness ingredient is mostly relatively active, can not be stable be present in system is easy to oxidize or decompose in light, and general
Logical facial mask liquid can not provide protection for both effectiveness ingredient, and both effectiveness ingredient is caused completely cannot using preceding just no longer valid
Play the performance of its " outstanding ".Such as the effect of whitening ingredient --- vitamin C, its mechanism of action are reduction melanin, suppression
The activity of tyrosinase processed, it is extremely oxidized easily, is illuminated by the light decomposition.So for common facial mask liquid, when facial mask is taken
Out after ingress of air, both effectiveness ingredient cannot play its effect with regard to no longer valid completely.Therefore, a kind of function admirable is developed,
The more effect facial mask liquids for integrating freckle removing and whitening, anti-wrinkle, anti-acne etc., so that both effectiveness ingredient is able to maintain high activity and gos deep into skin
It is the target of the unremitting pursuit of daily chemicals field researcher inside skin.
Summary of the invention
In view of above, the present invention provides a kind of more effect liquid crystal facial mask liquids and preparation method thereof.It is an object of the invention to
3 points.One, heterogeneity, different efficacies ingredient (oil-soluble and it is water-soluble have anti-aging, whitening and antiallergic maintenance function
Can the effect of ingredient) be introduced into liquid crystal emulsified system, premised on liquid crystal emulsified system self performance advantage, make full use of its liquid
Crystal layer (keeps it not volatile the protection for being wrapped in internal oil-soluble active and the water-soluble active object for being distributed in interlayer
Effect), a kind of function admirable is developed, more effect liquid crystal facial mask liquids of freckle removing and whitening, anti-wrinkle, anti-acne etc. are integrated；Two, liquid crystal knot
Structure interlamellar spacing can wrap the combination water of 13%-19%, cause to be easy sliding between liquid crystal layer, and oil-phase component has been wrapped in liquid
Inside crystal layer, so that lotion is easy to sprawl on the skin, the salubrious soft and smooth, non-greasy of skin sense；Three, the layered liquid crystal that the present invention uses
Human keratinous layer is simulated, " human body second layer skin " is equivalent to, the infiltration of active material can be increased according to the similar principle that mixes,
Promote to absorb, skin can also be repaired to a certain extent, delays senescence.
Technical solution of the present invention:
A kind of more effect liquid crystal facial mask liquids, the liquid crystal facial mask liquid include the raw material of following portions by weight:
0.5-2.0 parts of liquid crystal emulsifier
0.5-2.0 parts of grease
2.0-6.0 parts of moisturizer
0.01-0.10 parts of Sodium Hyaluronate
0.1-0.5 parts of thickener
0-8.0 parts of functional component
0.1-1.0 parts of preservative
Add water to 100.0 parts.
According to the present invention to have effects that more liquid crystal facial mask liquids, liquid crystal emulsifier is sucrose ester emulsifier, lecithin
Lipid emulsifiers, glycoside emulsifier, 2 kinds in phytosterol and senior class fatty alcohols or two or more compounding.Compound emulsion
The dosage of agent is 0.5-2.0 parts.
According to the present invention to have effects that more liquid crystal facial mask liquids, the grease is vegetable fat, animal fat, conjunction
At one or more of grease and mineral grease；
The vegetable fat is coconut oil, palm oil, olive oil, apricot kernel oil, grape seed oil, sunflower seed oil, suddenly
Suddenly bar seed oil, camellia seed oil, English walnut seed oil, candlenut tree seed oil, Butyrospermum parkii fruit rouge, mango seed rouge, evening primrose oil, avocado oil, can
It can one or more of seed rouge, Wild soybean oil, Brazil wax, olive oil, shea butter；
The animal fat is one of beeswax, turtle oil, lanolin, lacca wax, saualane, squalene or several
Kind；
The Synthetic Oil be isobutyl palmitate, isopropyl myristate, stearic acid isooctyl, isononyl isononanoate,
Carbonic acid dioctyl ester, diisooctadecanol malate, caprylic/capric glyceryl ester, glycerol three (thylhexoic acid) ester, poly dimethyl silicon
Oxygen alkane, ring five dimethyl silicone polymer, octyl polymethyl siloxane, phenyl trimethicone, PEG-12 poly dimethyl silicon
One or more of oxygen alkane, polymethylsilsesquioxane；
The mineral grease is one or more of atoleine, microwax, ceresine, vaseline.
The grease is further preferred are as follows: jojoba seed oil, olive oil, shea butter, palm oil, olive oil, crocodile
Pear oil, lanolin, saualane, isobutyl palmitate, isopropyl myristate, caprylic/capric glyceryl ester, one in vaseline
Kind is several.
It is according to the present invention to have effects that more liquid crystal facial mask liquids, the moisturizer are natural moisturizer, synthesis moisturizing
It is one or more of in agent；
The natural moisturizer is selected from xylitol, sorbierite, mannitol, hyaluronic acid, Anjidew NL50, panthenol, lactic acid, gathers
One or more of glutamic acid, glycine betaine, trehalose, aloe extract；
The synthesis moisturizer is selected from glycerol, 1,2-PD, diglycerol, 1,3-PD, dipropylene glycol, 1,3- fourth two
One or more of alcohol, Natrulon H-10, poly- ethyl carbamide.
The moisturizer is further preferred are as follows: trehalose, hyaluronic acid, panthenol, glycerol, 1,2-PD, 1,3- fourth two
One or more of alcohol.
According to the present invention to have effects that more liquid crystal facial mask liquids, the thickener is selected from organic water-soluble thickening
It is one or more of in agent, organic semi-synthetic water-soluble thickener, organic synthesis water-soluble thickener and micro mist thickener；
Organic water-soluble thickener be xanthan gum, Scleroglucan, melon bean gum, carragheen, starch, pectin,
One or more of sodium alginate, antler glue (carragheen), gellan gum；
Organic semi-synthetic water-soluble thickener be hydroxypropyl methyl cellulose, hydroxyethyl cellulose, methylcellulose,
One or more of PEG-120 methyl dioleate, sodium carboxymethylcellulose；
The organic synthesis water-soluble thickener be acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked copolymer,
Polyethylene glycol-n, PEG-150 distearate, carbomer (Carbopol 941 (long rheology), Carbopol 934 (it is short stream or
Height is glutinous), Carbopol 940 (short stream or high glutinous), Carbopol 980 (short stream or high glutinous), (the long stream or low of Carbopol 981
It is glutinous), Carbopol Ultrez 10 (short stream or high glutinous), Carbopol Ultrez 30 (in short stream or middle high glutinous)), polypropylene
One or more of sour sodium, acrylic copolymer, polyacrylate cross-linked polymer -6；
The micro mist thickener is that oronain bentonite draws, in microcrystalline cellulose in aluminum magnesium silicate, lithium magnesium silicate, silica, department
It is one or more of.
The thickener is further preferred are as follows: xanthan gum, carragheen, hydroxyethyl cellulose, Carbopol 980, polypropylene
One or more of sour sodium, acrylic copolymer, microcrystalline cellulose.
According to the present invention to have effects that more liquid crystal facial mask liquids, the functional component is whitening class, anti-aging class, resists
One or more of quick class, anti-acne class；
The whitening class is selected from arbutin, ascorbic acid, Vitamin C Ethyl Ether, Sodium Ascorbyl Phosphate, ascorbic acid
Glucoside, kojic acid, kojic dipalmitate, hydroxyacetic acid, malic acid, tartaric acid, citric acid, glabridin, phloretin, daisy
One or more of flower extract, niacinamide, ferulic acid ethylhexyl etc.；
The anti-aging class be selected from tocopherol (vitamin E), tocopherol phosphate sodium, fullerene, ubiquinone (Co-Q10),
Grape seed extract, tea extraction, resveratrol, retinol, retinyl acetate, ginkgo extract, phytosterol, neural acyl
One or more of amine, ginseng root extract；
It is yellow that the antiallergic class is selected from allantoin, Radix Astragali flavone glycosides, bisabolol, bacopa monnieri, radix scutellariae, Paeoniflorin, the leaf of bamboo
One of ketone, Olive leaf P.E, witch hazel, the Portugal OPC mostly peace, Seabuckthorn Oil, dipotassium glycyrrhizinate, Radix Salviae Miltiorrhizae root extract are several
Kind；
The anti-acne class is selected from one or more of riboflavin, azelaic acid, baicalein.
The functional component is further preferred are as follows: arbutin, kojic dipalmitate, glabridin, ferulic acid ethyl hexyl
Ester, tocopherol (vitamin E), ubiquinone (Co-Q10), tea extraction, retinol, retinyl acetate, phytosterol, neural acyl
One or more of amine, ginseng root extract, allantoin, bisabolol, Radix Salviae Miltiorrhizae root extract, azelaic acid.
According to the present invention to have effects that more liquid crystal facial mask liquids, the preservative is selected from aldehydes, esters, quaternary ammonium salt
Class, acid and its esters, phenols, alcohol ethers, 1,2- di-alcohols, organic acid, fragrant phenol and aromatic alcohol and plant extract species
One or more of；
The aldehydes is selected from formaldehyde, formaldehyde benzylalcohol hemiacetal, imidazolidinyl urea, Bis(hydroxymethyl)imidazolidinyl urea, DMDM
One or more of hydantoins, glutaraldehyde；
The esters are selected from one or more of 4-HBA esters, iodine propilolic alcohol butyl mephenesin Carbamate IPBC；
The quaternary ammonium salt is selected from benzalkonium chloride, benzethonium chloride, cetrimonium chloride, stearyl trimethyl ammonium chloride, behenyl base
One or more of trimethyl ammonium chloride, Chlorhexidine, Hexetidine；
The acid and its esters are selected from one of formic acid, propionic acid, sorbic acid, benzoic acid, salicylic acid, dehydroactic acid or several
Kind；
The phenols is selected from one or more of benzyl chloride phenol, dichloroxylenol, phenylphenol, bromine chlorine sweet smell；
It is sweet that the alcohol ethers are selected from benzyl alcohol, Phenoxyethanol, benzene oxygen isopropanol, dichlorbenzyl alcohol, anesin, chlorobenzene
One or more of ether, triclosan, 2- bromo-2-nitro-1,3-propylene glycol；
1, the 2- di-alcohols is selected from one of 1,2- pentanediol, 1,2- hexylene glycol, pungent glycol, Sensiva SC50
Or it is several；
The organic acid is selected from p- anisic acid, levulic acid, ferulic acid, lichenic acid, glycerol caprylate, the smooth octanoic acid of sorb
One or more of ester；
The fragrance phenol and aromatic alcohol are selected from one or more of peach girder phenol, thymol, benzyl carbinol；
The plant extract species are selected from one or more of azadirachta seed oil, tea tree ethereal oil.
The preservative is further preferred are as follows: Phenoxyethanol, Sensiva SC50, azadirachta seed oil, tea tree ethereal oil, bigcatkin willow
One or more of acid, phenylphenol.
According to the present invention have effects that more liquid crystal facial mask liquids, the thickener if Carbomer thickener,
It then needs that sodium hydroxide solution is added in system, wherein the ratio of carbomer and 10% sodium hydroxide solution is 1:2.
According to the present invention to have effects that more liquid crystal facial mask liquids, effect ingredient, individually or compounding adds
When entering formula described in claim 1, additive amount is 0-8.0 parts.
The present invention also provides a kind of production methods of above-mentioned more effect liquid crystal facial mask liquids, include the following steps:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 70-78 DEG C of thermostat water bath and preheat；
0.5-2.0 parts of liquid crystal emulsifier
0.5-2.0 parts of grease
0-3.0 parts of oiliness functional component
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 70-78 DEG C of thermostat water bath and preheats；
2.0-6.0 parts of moisturizer
0.01-0.10 parts of Sodium Hyaluronate
0.1-0.5 parts of thickener
Water-soluble functional component 0-5.0 parts
Add water to 100.0 parts
(3) when oily phased soln and reach set temperature, homogeneous water phase, and (homogeneous rate is according to the difference of system in homogeneous
Be adjusted in 4000-8000rpm) under the conditions of be directly added into oily phase, homogeneous 5-8min；
(4) lotion is taken out from thermostat water bath, is 25-28 DEG C in ambient temperature, revolving speed is to stir under 300-500rpm
Mix cooling；When temperature is down to 45-50 DEG C, 0.1-1.0 parts of preservative is added into lotion, continues stirring to room temperature, encapsulation
?.
The production method of more effect liquid crystal facial mask liquids according to the present invention, functional component, operating procedure need to be by this
The property of functional component itself determines；If functional component can be stabilized under emulsifying temperature, it is added in warm
Into corresponding water phase or oily phase；If functional component non-refractory, (45 DEG C or more) need to add in due course in stirring temperature-fall period
Enter system.
Heretofore described effect ingredient can be whitening agent, antidotal agent and anti-sensitizer etc., can be effect group
Point one of or it is a variety of.
Liquid crystal is a kind of state between solid and liquid, therefore liquid crystal is also referred to as mesomorphic state.It not only has picture
Liquid the same mobility and continuity also have the anisotropy as solid crystal.Liquid crystal in the present invention belongs to layer
Shape liquid crystal, the interlayer of such liquid crystal structure, which contains, largely combines water, so being easy mutually sliding, and crystalline emulsion between liquid crystal layer
It more easily sprawls in skin surface and is bonded with skin perfection.The emulsifier molecules layered liquid crystal to be formed that associates is usually multilayer
Network structure, and be present in lotion around single drop, form oil/liquid crystal/water (O/LC/W) special construction.Layered liquid crystal
Structure contains the continuous structure of hydrophilic microcell and oleophylic microcell, this system can not only lock the combination water of a large amount of (13-19%), but also
Hydrophobic continuous phase can be formed, to make liquid crystal facial mask liquid that can wrap up hydrophilic active agents and dissolve lipophilic living
Property ingredient.Meanwhile the layered liquid crystal structure analog human skin that the liquid crystal emulsifier studied of the present invention is formed, it is attached to skin
Surface is equivalent to " second layer skin " of human body, and according to the similar principle that mixes, this structure can promote both effectiveness ingredient in skin table
The infiltration of layer.The special construction of layered liquid crystal makes it be applied to have a clear superiority in facial mask liquid；Such as in combination with water packet
The advantage of oil and water-in-oil emulsion, such lotion have effects that good water lock, inhibit moisture evaporation.Multilayer liquid crystal structure
In the presence of protection effect ingredient and its stability, all kinds of both effectiveness ingredients of solubilising, the certain pungents of reduction are improved (as prevented
Shine agent etc.) injury etc. to skin.
Based on this, the present invention using liquid crystal emulsifier constructed a kind of cutaneous safety it is high and on the skin have it is good
Stability, layered liquid crystal content be high and shape is complete, even-grained liquid crystal emulsified system.Heterogeneity, different efficacies
Ingredient (oil-soluble and water-soluble have the function of the effect of anti-aging, whitening and antiallergic maintenance etc. ingredient) introduces liquid crystal emulsified body
In system, premised on liquid crystal emulsified system self performance advantage, make full use of its liquid crystal layer to the oil-soluble function for being wrapped in inside
The protection (keeping it not vulnerable) of effect ingredient and the water-soluble functional component for being distributed in interlayer.It can according to demand, together in facial mask liquid
When introduce the different ingredient of multiple efficacies, meet the needs of different sexes, different skin crowds are both effectiveness to liquid crystal facial mask liquid.This
Outside, the presence of oil-water interfaces layered liquid crystal structure sprawls lotion easily, shows smooth, salubrious, the good skin such as not sticky
Sense.
The beneficial effects of the present invention are, using more effect liquid crystal facial mask liquids produced by the invention, can by heterogeneity,
The ingredient (oil-soluble and water-soluble have the function of the effect of anti-aging, whitening and antiallergic maintenance ingredient) of different efficacies while drawing
Enter in liquid crystal emulsified system, premised on liquid crystal emulsified system self performance advantage, makes full use of its liquid crystal layer in being wrapped in
The protection of the oil-soluble functional component in portion and the water-soluble functional component for being distributed in interlayer, keeps functional component not vulnerable, sufficiently
It is both effectiveness to play its；Facial mask liquid laminate liquid crystal structure can also effectively facilitate the absorption of functional component, at the same assign facial mask liquid with
Clearly, the skin sense of non-greasy.
Containing water is largely combined in more effect liquid crystal facial mask liquid liquid crystal structures of the invention, there is excellent water lock moisturizing
Performance.In addition, the presence of layered liquid crystal structure sprawls facial mask liquid easily in use, show it is smooth, salubrious, it is not sticky
Etc. good skin sense.According to demand, while the different ingredient of multiple efficacies can be introduced in facial mask liquid, meet different skin crowds couple
The both effectiveness demand of facial mask liquid.
Detailed description of the invention
Fig. 1 is the polarized light microscopy photo of skin whitening, moisturizing liquid crystal facial mask liquid.
Fig. 2 is that the SAXS of skin whitening, moisturizing liquid crystal facial mask liquid schemes.
Fig. 3 is the polarized light microscopy photo of whitening anti-aging moisturizing liquid crystal surface film liquid.
Fig. 4 is the polarized light microscopy photo of antiallergic anti-acne moisturizing liquid crystal surface film liquid.
Fig. 5 is the polarized light microscopy photo of whitening antiallergic moisturizing liquid crystal surface film liquid.
Fig. 6 is the polarized light microscopy photo of anti-aging moisturizing liquid crystal surface film liquid.
Specific embodiment
The invention will be further described with the following Examples.
Embodiment 1: a kind of skin whitening, moisturizing liquid crystal facial mask liquid, the raw material including following portions by weight:
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
0.3 part of vitamin E
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
10% 0.24 part of sodium hydroxide
3.0 parts of pneumatically conveying
89.84 parts of water
The implementation steps of above-mentioned formula are as follows:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 75 DEG C of thermostat water bath and preheat；
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
0.3 part of vitamin E
3.0 parts of pneumatically conveying
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 75 DEG C of thermostat water bath and preheats；
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
89.84 parts of water
(3) when oily phased soln and reach set temperature, homogeneous water phase, and oil is directly added under the conditions of homogeneous 7200rpm
Phase, homogeneous 6min；
(4) in homogeneous, 10% sodium hydroxide solution of one third is added into lotion；
(5) the good lotion of homogeneous is taken out from thermostat water bath, is 28 DEG C in ambient temperature, revolving speed is the item of 400rpm
Cooling is stirred under part；When temperature is down to 45-50 DEG C, 1.0 parts of PE-9010 is added and (the limited public affairs of medicine adornment technical concern are won by Lay
Department provide) and residue 2/3rds 10% sodium hydroxide solution.
Products obtained therefrom is milky, sticky lotion, and safety does not stimulate mildly, the skin sense with salubrious non-greasy.Sample
Polarized light microscopy photo (Fig. 1) display, the liquid crystal structure formed in system is than more complete, and granule size is more uniform, and liquid crystal
Particle density is larger.The SAXS figure (Fig. 2) of crystalline emulsion confirms that the liquid crystal in facial mask liquid obtained is typical layered liquid crystal knot
Structure.
Efficacy assessments:
100 20-30 years old women are selected, surface application twice, continues one month weekly.Wherein 15 Genus Homos are in mixed type skin
Skin, skin is more sensitive, feels that skin is very fine and smooth, very moist after use, skin sense is fine；There is acne before use there are also 20 people, makes
It is not red with the skin around rear acne, play the role of anti-inflammatory, acne also has the tendency that cancellation, and these women reflect it is of the invention
Do not stick greasy after on mask sheet, very clearly, skin sense is fine.In addition to this, this 100 application on human skin has different degrees of bleach.
The above experiment shows whitening moisturizing face masque liquid of the invention, equal for the sophistication of increase skin, moisturizing, whitening
There is good effect.
Embodiment 2: a kind of whitening anti-aging moisturizing liquid crystal surface film liquid, the raw material including following portions by weight:
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
10% 0.24 part of sodium hydroxide
3.0 parts of tocopherol (vitamin E)
3.0 parts of ferulic acid ethylhexyl
87.14 parts of water
The implementation steps of above-mentioned formula are as follows:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 75 DEG C of thermostat water bath and preheat；
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
3.0 parts of tocopherol (vitamin E)
3.0 parts of ferulic acid ethylhexyl
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 75 DEG C of thermostat water bath and preheats；
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
87.14 parts of water
(3) when oily phased soln and reach set temperature, homogeneous water phase, and oil is directly added under the conditions of homogeneous 7200rpm
Phase, homogeneous 6min；
(4) in homogeneous, 10% sodium hydroxide solution of one third is added into lotion；
(5) the good lotion of homogeneous is taken out from thermostat water bath, is 28 DEG C in ambient temperature, revolving speed is the item of 400rpm
Cooling is stirred under part；When temperature is down to 45-50 DEG C, 1.0 parts of PE-9010 is added and (the limited public affairs of medicine adornment technical concern are won by Lay
Department provide) and residue 2/3rds 10% sodium hydroxide solution.
Products obtained therefrom is light yellow, sticky lotion, and safety does not stimulate mildly, the skin sense with salubrious non-greasy.Sample
Polarized light microscopy photo show (Fig. 3) that for the liquid crystal structure formed in system than more complete, granule size is more uniform, and liquid crystal
Particle density is larger.The SAXS of crystalline emulsion schemes confirmation, and the liquid crystal in facial mask liquid obtained is typical layered liquid crystal structure.
(attached drawing is similar to the data that 1 attached drawing of embodiment is shown, just repeats no more)
Efficacy assessments:
100 20-30 years old women are selected, surface application twice, continues one month weekly.Wherein 15 Genus Homos are in mixed type skin
Skin, skin is more sensitive, feels that skin is very fine and smooth, very moist after use, skin sense is fine；Have on using preceding skin there are also 15 people
Apparent wrinkle, after use, wrinkle is obviously desalinated.And these women do not sticked after reflecting on mask sheet of the invention it is greasy, very
Clearly, skin sense is fine.In addition to this, this 100 application on human skin has different degrees of bleach.
Embodiment 3: a kind of antiallergic anti-acne moisturizing liquid crystal surface film liquid, the raw material including following portions by weight:
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
10% 0.24 part of sodium hydroxide
1.0 parts of α-bisabolol
3.0 parts of Radix Salviae Miltiorrhizae root extract
2.0 parts of azelaic acid
87.14 parts of water
The implementation steps of above-mentioned formula are as follows:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 75 DEG C of thermostat water bath and preheat；
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
1.0 parts of α-bisabolol
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 75 DEG C of thermostat water bath and preheats；
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
2.0 parts of azelaic acid
3.0 parts of Radix Salviae Miltiorrhizae root extract
87.14 parts of water
(3) when oily phased soln and reach set temperature, homogeneous water phase, and oil is directly added under the conditions of homogeneous 7200rpm
Phase, homogeneous 6min；
(4) in homogeneous, 10% sodium hydroxide solution of one third is added into lotion；
(5) the good lotion of homogeneous is taken out from thermostat water bath, is 28 DEG C in ambient temperature, revolving speed is the item of 400rpm
Cooling is stirred under part；When temperature is down to 45-50 DEG C, 1.0 parts of PE-9010 is added and (the limited public affairs of medicine adornment technical concern are won by Lay
Department provide) and residue 2/3rds 10% sodium hydroxide solution.
Products obtained therefrom is sticky lotion, and safety does not stimulate mildly, the skin sense with salubrious non-greasy.The polarisation of sample
Microphoto shows (Fig. 4) that for the liquid crystal structure formed in system than more complete, granule size is more uniform, and liquid crystal particle is close
It spends larger.The SAXS of crystalline emulsion schemes confirmation, and the liquid crystal in facial mask liquid obtained is typical layered liquid crystal structure.(attached drawing with
The data that 1 attached drawing of embodiment is shown are similar, just repeat no more)
Efficacy assessments:
100 20-30 years old women are selected, surface application twice, continues one month weekly.Wherein 25 Genus Homos are in mixed type skin
Skin, skin is more sensitive, feels that skin is very fine and smooth, very moist after use, skin sense is fine, without irritation；Make there are also 50 people
It is not red using the skin around rear acne with preceding there is acne, there is anti-inflammatory, acne also has the tendency that obviously eliminating, and these
Women does not stick greasy after reflecting on mask sheet of the invention, very clearly, skin sense is fine.
Embodiment 4: a kind of whitening antiallergic moisturizing liquid crystal surface film liquid, the raw material including following portions by weight:
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
10% 0.24 part of sodium hydroxide
2.0 parts of allantoin
3.0 parts of alpha-arbutin
2.0 parts of α-bisabolol
86.14 parts of water
The implementation steps of above-mentioned formula are as follows:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 75 DEG C of thermostat water bath and preheat；
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
2.0 parts of α-bisabolol
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 75 DEG C of thermostat water bath and preheats；
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
2.0 parts of allantoin
3.0 parts of alpha-arbutin
86.14 parts of water
(3) when oily phased soln and reach set temperature, homogeneous water phase, and oil is directly added under the conditions of homogeneous 7200rpm
Phase, homogeneous 6min；
(4) in homogeneous, 10% sodium hydroxide solution of one third is added into lotion；
(5) the good lotion of homogeneous is taken out from thermostat water bath, is 28 DEG C in ambient temperature, revolving speed is the item of 400rpm
Cooling is stirred under part；When temperature is down to 45-50 DEG C, 1.0 parts of PE-9010 is added and (the limited public affairs of medicine adornment technical concern are won by Lay
Department provide) and residue 2/3rds 10% sodium hydroxide solution.
Products obtained therefrom is sticky lotion, and safety does not stimulate mildly, the skin sense with salubrious non-greasy.The polarisation of sample
Microphoto shows (Fig. 5) that for the liquid crystal structure formed in system than more complete, granule size is more uniform, and liquid crystal particle is close
It spends larger.The SAXS of crystalline emulsion schemes confirmation, and the liquid crystal in facial mask liquid obtained is typical layered liquid crystal structure.(attached drawing with
The data that 1 attached drawing of embodiment is shown are similar, just repeat no more)
Efficacy assessments:
100 20-30 years old women are selected, surface application twice, continues one month weekly.Wherein 15 Genus Homos are in mixed type skin
Skin, skin is more sensitive, feels that skin is very fine and smooth, very moist after use, skin sense is fine；Have not there are also 35 people using preceding skin
It is not red using rear skin with the redness of degree, there is anti-inflammatory, and after these women reflect on mask sheet of the invention
Do not stick greasy, very clearly, skin sense is fine.In addition to this, this 100 application on human skin has different degrees of bleach.
Embodiment 5: a kind of anti-aging moisturizing liquid crystal surface film liquid, the raw material including following portions by weight:
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
10% 0.24 part of sodium hydroxide
1.0 parts of Co-Q10
3.0 parts of tea extraction
1.0 parts of retinyl acetate
88.14 parts of water
The implementation steps of above-mentioned formula are as follows:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 75 DEG C of thermostat water bath and preheat；
1.2 parts of liquid crystal emulsifier
0.3 part of olive oil
0.3 part of saualane
0.2 part of vaseline
0.2 part of shea butter
0.2 part of isobutyl palmitate
1.0 parts of Co-Q10
1.0 parts of retinyl acetate
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 75 DEG C of thermostat water bath and preheats；
4.0 parts of glycerol
0.1 part of Sodium Hyaluronate
9800.12 parts of card wave
86.14 parts of water
(3) when oily phased soln and reach set temperature, homogeneous water phase, and oil is directly added under the conditions of homogeneous 7200rpm
Phase, homogeneous 6min；
(4) in homogeneous, 10% sodium hydroxide solution of one third is added into lotion；
(5) the good lotion of homogeneous is taken out from thermostat water bath, is 28 DEG C in ambient temperature, revolving speed is the item of 400rpm
Cooling is stirred under part；When temperature is down to 45-50 DEG C, 3.0 parts of tea extraction is added, 1.0 parts of PE-9010 (wins medicine by Lay
Adornment technical concern Co., Ltd provide) and residue 2/3rds 10% sodium hydroxide solution.
Products obtained therefrom is sticky lotion, and safety does not stimulate mildly, the skin sense with salubrious non-greasy.The polarisation of sample
Microphoto shows (Fig. 6) that for the liquid crystal structure formed in system than more complete, granule size is more uniform, and liquid crystal particle is close
It spends larger.The SAXS of crystalline emulsion schemes confirmation, and the liquid crystal in facial mask liquid obtained is typical layered liquid crystal structure.(attached drawing with
The data that 1 attached drawing of embodiment is shown are similar, just repeat no more)
Efficacy assessments:
100 20-30 years old women are selected, surface application twice, continues one month weekly.Wherein 35 Genus Homos are in mixed type skin
Skin, skin is more sensitive, feels that skin is very fine and smooth, very moist after use, skin sense is fine；Have before use significantly there are also 65 people
Wrinkle is obviously desalinated using rear wrinkle, and these women reflect on mask sheet of the invention after do not stick it is greasy, very clearly, skin sense
Very well.In addition to this, it is good to react the product performance of keeping humidity by this 100 women.
Above-mentioned fact Example is the specific embodiment of the more effect liquid crystal facial mask liquids of the present invention, but embodiments of the present invention are simultaneously
It is not restricted to the described embodiments, other any changes made without departing from the spirit and principles of the present invention are modified, replaced
In generation, simplifies combination, should be equivalent substitute mode, is included in protection scope of the present invention.
Claims (10)
1. a kind of more effect liquid crystal facial mask liquids, which is characterized in that the liquid crystal facial mask liquid includes the raw material of following portions by weight:
0.5-2.0 parts of liquid crystal emulsifier
0.5-2.0 parts of grease
2.0-6.0 parts of moisturizer
0.01-0.10 parts of Sodium Hyaluronate
0.1-0.5 parts of thickener
0-8.0 parts of functional component
0.1-1.0 parts of preservative
Add water to 100.0 parts.
2. having effects that more liquid crystal facial mask liquids as described in claim 1, which is characterized in that liquid crystal emulsifier is sucrose ester cream
Agent, lecithin lipid emulsifiers, glycoside emulsifier, 2 kinds in phytosterol and senior class fatty alcohols or two or more is multiple
Match.
3. having effects that more liquid crystal facial mask liquids as described in claim 1, which is characterized in that the grease be vegetable fat,
One or more of animal fat, Synthetic Oil and mineral grease；
The vegetable fat is coconut oil, palm oil, olive oil, apricot kernel oil, grape seed oil, sunflower seed oil, Jojoba
Seed oil, camellia seed oil, English walnut seed oil, candlenut tree seed oil, Butyrospermum parkii fruit rouge, mango seed rouge, evening primrose oil, avocado oil, cocoa seed
One or more of rouge, Wild soybean oil, Brazil wax, olive oil, shea butter；
The animal fat is one or more of beeswax, turtle oil, lanolin, lacca wax, saualane, squalene；
The Synthetic Oil is isobutyl palmitate, isopropyl myristate, stearic acid isooctyl, isononyl isononanoate, carbonic acid
Dioctyl ester, diisooctadecanol malate, caprylic/capric glyceryl ester, glycerol three (thylhexoic acid) ester, polydimethylsiloxanes
Alkane, ring five dimethyl silicone polymer, octyl polymethyl siloxane, phenyl trimethicone, PEG-12 polydimethylsiloxanes
One or more of alkane, polymethylsilsesquioxane；
The mineral grease is one or more of atoleine, microwax, ceresine, vaseline.
4. having effects that more liquid crystal facial mask liquids as described in claim 1, which is characterized in that the moisturizer is natural moisture preserving
It is one or more of in agent, synthesis moisturizer；
The natural moisturizer is selected from xylitol, sorbierite, mannitol, hyaluronic acid, Anjidew NL50, panthenol, lactic acid, polyglutamic
One or more of acid, glycine betaine, trehalose, aloe extract；
The synthesis moisturizer be selected from glycerol, 1,2-PD, diglycerol, 1,3-PD, dipropylene glycol, 1,3-BDO,
One or more of Natrulon H-10, poly- ethyl carbamide.
5. in more effect liquid crystal facial mask liquids as described in claim 1, which is characterized in that the thickener is selected from organic natural water
It is a kind of or several in soluble surfactant, organic semi-synthetic water-soluble thickener, organic synthesis water-soluble thickener and micro mist thickener
Kind；
Organic water-soluble thickener is xanthan gum, Scleroglucan, melon bean gum, carragheen, starch, pectin, brown alga
One or more of sour sodium, antler glue (carragheen), gellan gum；
Organic semi-synthetic water-soluble thickener is hydroxypropyl methyl cellulose, hydroxyethyl cellulose, methylcellulose, PEG-
One or more of 120 methyl dioleates, sodium carboxymethylcellulose；
The organic synthesis water-soluble thickener is acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked copolymer, poly- second
Glycol-n, PEG-150 distearate, carbomer (Carbopol941 (long rheology), Carbopol934 (short stream or high glutinous),
Carbopol940 (short stream or high glutinous), Carbopol980 (short stream or high glutinous), Carbopol981 (long stream or low glutinous),
CarbopolUltrez 10 (short stream or high glutinous), CarbopolUltrez30 (in short stream or middle high glutinous)), Sodium Polyacrylate, third
One or more of olefin(e) acid copolymer, polyacrylate cross-linked polymer -6；
The micro mist thickener is one of aluminum magnesium silicate, lithium magnesium silicate, silica, department's drawing oronain bentonite, microcrystalline cellulose
Or it is several.
6. having effects that more liquid crystal facial mask liquids as described in claim 1, which is characterized in that the functional component be whitening class,
One or more of anti-aging class, antiallergic class, anti-acne class；
The whitening class is selected from arbutin, ascorbic acid, Vitamin C Ethyl Ether, Sodium Ascorbyl Phosphate, ascorbic acid glucose
Glycosides, kojic acid, kojic dipalmitate, hydroxyacetic acid, malic acid, tartaric acid, citric acid, glabridin, phloretin, Daisy mention
Take one or more of object, niacinamide, ferulic acid ethylhexyl etc.；
The anti-aging class is selected from tocopherol (vitamin E), tocopherol phosphate sodium, fullerene, ubiquinone (Co-Q10), grape
Seed extract, tea extraction, resveratrol, retinol, retinyl acetate, ginkgo extract, phytosterol, ceramide,
One or more of ginseng root extract；
The antiallergic class is selected from allantoin, Radix Astragali flavone glycosides, bisabolol, bacopa monnieri, radix scutellariae, Paeoniflorin, bamboo-leaves flavones, olive
One or more of olive leaf extract, witch hazel, the Portugal OPC mostly peace, Seabuckthorn Oil, dipotassium glycyrrhizinate, Radix Salviae Miltiorrhizae root extract；
The anti-acne class is selected from one or more of riboflavin, azelaic acid, baicalein.
7. having effects that more liquid crystal facial mask liquids as described in claim 1, which is characterized in that the preservative is selected from aldehydes, ester
Class, quaternary ammonium salt, acid and its esters, phenols, alcohol ethers, 1,2- di-alcohols, organic acid, fragrant phenol and aromatic alcohol and plant
Extract one or more of species；
The aldehydes is in formaldehyde, formaldehyde benzylalcohol hemiacetal, imidazolidinyl urea, Bis(hydroxymethyl)imidazolidinyl urea, DMDM second
One or more of uride, glutaraldehyde；
The esters are selected from one or more of 4-HBA esters, iodine propilolic alcohol butyl mephenesin Carbamate IPBC；
The quaternary ammonium salt is selected from benzalkonium chloride, benzethonium chloride, cetrimonium chloride, stearyl trimethyl ammonium chloride, behenyl base front three
One or more of ammonium chloride, Chlorhexidine, Hexetidine；
The acid and its esters are selected from one or more of formic acid, propionic acid, sorbic acid, benzoic acid, salicylic acid, dehydroactic acid；
The phenols is selected from one or more of benzyl chloride phenol, dichloroxylenol, phenylphenol, bromine chlorine sweet smell；
The alcohol ethers be selected from benzyl alcohol, Phenoxyethanol, benzene oxygen isopropanol, dichlorbenzyl alcohol, anesin, Chlorphenesin,
One or more of triclosan, 2- bromo-2-nitro-1,3-propylene glycol；
1, the 2- di-alcohols is selected from one of 1,2- pentanediol, 1,2- hexylene glycol, pungent glycol, Sensiva SC50 or several
Kind；
The organic acid is in p- anisic acid, levulic acid, ferulic acid, lichenic acid, glycerol caprylate, the smooth caprylate of sorb
One or more；
The fragrance phenol and aromatic alcohol are selected from one or more of peach girder phenol, thymol, benzyl carbinol；
The plant extract species are selected from one or more of azadirachta seed oil, tea tree ethereal oil.
8. having effects that more liquid crystal facial mask liquids as claimed in claim 5, which is characterized in that the thickener is if carbomer
Class thickener then needs that sodium hydroxide solution is added in system, and wherein the ratio of carbomer and 10% sodium hydroxide solution is
1:2.
9. the production method of more effect liquid crystal facial mask liquids as described in claim 1, includes the following steps:
(1) weigh the raw material of following portions by weight, i.e., oily phase, and put it into 70-78 DEG C of thermostat water bath and preheat；
0.5-2.0 parts of liquid crystal emulsifier
0.5-2.0 parts of grease
0-3.0 parts of oiliness functional component
(2) raw material of following portions by weight, i.e. water phase are weighed, and puts it into 70-78 DEG C of thermostat water bath and preheats；
2.0-6.0 parts of moisturizer
0.01-0.10 parts of Sodium Hyaluronate
0.1-0.5 parts of thickener
Water-soluble functional component 0-5.0 parts
Add water to 100.0 parts
(3) when oily phased soln and reach set temperature, homogeneous water phase, and in homogeneous, homogeneous rate is carried out according to the difference of system
Adjusting is directly added into oily phase, homogeneous 5-8min under the conditions of 4000-8000rpm；
(4) lotion is taken out from thermostat water bath, is 25-28 DEG C in ambient temperature, revolving speed is to stir drop under 300-500rpm
Temperature；When temperature is down to 45-50 DEG C, 0.1-1.0 parts of preservative is added into lotion, continues stirring to room temperature, encapsulation.
10. the production method of more effect liquid crystal facial mask liquids as described in claim 9, which is characterized in that functional component, behaviour
Making step need to be determined by the property of the functional component itself；If functional component can be stabilized under emulsifying temperature, pre-
It is added in thermal process in corresponding water phase or oily phase；It, need to be in stirring temperature-fall period in due course if functional component non-refractory
Addition system.
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