CN109125114A - A kind of tiger spot cuttlefish internal organ polysaccharide hand lotion and preparation method thereof - Google Patents
A kind of tiger spot cuttlefish internal organ polysaccharide hand lotion and preparation method thereof Download PDFInfo
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- CN109125114A CN109125114A CN201811341708.8A CN201811341708A CN109125114A CN 109125114 A CN109125114 A CN 109125114A CN 201811341708 A CN201811341708 A CN 201811341708A CN 109125114 A CN109125114 A CN 109125114A
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- internal organ
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- spot cuttlefish
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Animal Behavior & Ethology (AREA)
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- Gerontology & Geriatric Medicine (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
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Abstract
The invention discloses a kind of hand lotions and preparation method thereof containing tiger spot cuttlefish internal organ polysaccharide, ingredient in parts by weight: 15-30 parts of stearic acid, 2-5 parts of tristerin, 5-8 parts of hexadecanol, 15-30 parts of glycerol, 5-10 parts of white oil, 0.5-2 parts of potassium hydroxide, 1-5 parts of Lavender, 0.1-0.3 parts of sodium benzoate, 2-5 parts of internal organ polysaccharide of tiger spot cuttlefish, 100 parts of deionized water.Hand lotion provided by the invention contains active skull cap components-cuttlefish internal organ polysaccharide, can play moisturizing, repair wound, anti-radiation, anti-oxidant and other effects.In addition, the hand lotion, which has, promotes the skin-protecting functions such as the generation of endogenous natural moisturizing factor, balance skin surface layer fat secretion, supplement skin moisture, freckle removing and whitening, and stability is good, is suitable for saving, can be used for a long time.The preparation method of hand lotion of the present invention is simple to operation, and low in cost, is also suitable for general population's use.
Description
Technical field
The invention belongs to cosmetic technical field, it is related to a kind of skin care item, in particular to a kind of contains tiger spot cuttlefish internal organ
Hand lotion of polysaccharide and preparation method thereof.
Background technique
Tiger spot cuttlefish (Sepiapharaonis) belong to Mollusca, Cephalopoda, Sepiida, Sepiidae, Sepia
Mollusk inhabites extensively in the Indian Ocean-Western Pacific shallow sea warm water domain, is concentrated mainly on east in the distributed areas in China
Sea and South China Sea, figure is larger, reproductive capacity is strong, delicious meat, and meat, blood, bone, ink can be used as medicine.Remember according to Compendium of Material Medica
It carries, cuttlefish meat and cuttlefish blood have the effect of activating blood circulation and dispersing blood clots, tonifying Qi, blood enriching and yin nourishing, often edible to prolong intelligence, delay senescence, mention
High hematopoiesis and immune function；Cuttle bone (cuttlebone) has the effects that dehumidifying, sore, treatment stomach trouble；Cuttlefish Ink has anticancer, anti-spoke
The effects of penetrating, stopping blooding.Therefore, tiger spot cuttlefish is a kind of edible and higher excellent marine product kind of medical value.
Tiger spot cuttlefish internal organ account for about 30% of its weight or so, often throw away as waste during processing of aquatic products,
Environment is polluted, cuttlefish internal organ not only contain a large amount of protein, lipid, but also are rich in active polysaccharide.Polysaccharide is also known as polysaccharide,
Be it is a kind of chain polymer made of glucosides key connection is formed by dehydration as aldose and (or) ketose, have extensive biology living
Property.Such as antitumor, anti-oxidant, reducing blood lipid, hypoglycemic, adjusting immunity, anti-aging, moisture retention.If can be by these internal organ
It is comprehensively utilized, is turned waste into wealth, the economic value added of marine product will be greatly improved.
Skin is the maximum organ of human body, and skin moisture-keeping and antioxidation are most important for skin care.It is protected containing natural
Wet and anti-oxidation function tiger spot cuttlefish internal organ polysaccharide hand lotion can help skin to restore deep moisturizing function, effective stimulus skin
The natural of natural moisturizing factor generating inside skin, returns equilibrium state, moistens moisturizing deeply, plays deep layer water lock and anti-oxidant etc.
Effect.
Summary of the invention
Excessive artificial chemistry ingredient is added for cosmetics in the prior art, causes moistening effect and antioxidant effect not
Ideal, and have the problem of side effect, the present invention prepares a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide, can help skin
Skin restores deep moisturizing function, and the natural generation of natural moisturizing factor, returns equilibrium state inside effective stimulus skin, and depth is grown
Moisten moisturizing, plays deep layer water lock and oxidation resistant effect.
To achieve the goals above, the technical solution adopted by the present invention is that: a kind of shield containing tiger spot cuttlefish internal organ polysaccharide
Hand frost, it is characterised in that: ingredient in parts by weight: 15-30 parts of stearic acid, 2-5 parts of tristerin, 5-8 parts of hexadecanol, sweet
It is 15-30 parts oily, 5-10 parts of white oil, 0.5-2 parts of potassium hydroxide, 1-5 parts of Lavender, 0.1-0.3 parts of sodium benzoate, tiger spot crow
2-5 parts of crafty internal organ polysaccharide, 100 parts of deionized water.
Preferably, each raw material ingredient in parts by weight is as follows: 20 parts of stearic acid, 3 parts of tristerin, and 6 parts of hexadecanol,
20 parts of glycerol, 8 parts of white oil, 1 part of potassium hydroxide, 3 parts of Lavender, 0.2 part of sodium benzoate, 4 parts of polysaccharide of tiger spot cuttlefish internal organ,
100 parts of deionized water.
Further, the preparation method of the tiger spot cuttlefish internal organ polysaccharide is the following steps are included: A: taking fresh tiger spot cuttlefish
Adult takes out after dissection and internal organ and removes gonad, shreds and be placed in high-speed tissue mashing machine, then plus distilled water break into homogenate
Shape, 3 times vol acetone degreasing 3 times, every time 8~10 h, obtain tiger spot cuttlefish internal organ dry powder after 24 h of freeze-drying, crushing, receive
Collection, which is placed at -20 DEG C, to be saved backup.B: freeze-dried powder hot water extraction certain time in the case where setting solid-liquid ratio, centrifuging and taking supernatant are dense
3 times of volume dehydrated alcohols, 4 DEG C of precipitates overnights, centrifuging and taking precipitating 48 h of dialysis, freeze-drying 24 is added in contracting, active carbon decoloring
H obtains tiger spot cuttlefish internal organ polysaccharide.
Preferably, centrifugal condition is 4000 r/min in the step B.
The present invention also provides a kind of preparation methods of hand lotion containing tiger spot cuttlefish internal organ polysaccharide, it is characterised in that: packet
Include following steps:
S1: taking glycerol, white oil and deionized water, uses 30 min of preceding progress ultraviolet sterilization.
S2: by stearic acid, tristerin, hexadecanol, glycerol, white oil in 90-95 DEG C of water-bath uniform stirring 15
Min is configured to oily phase.
S3: being configured to solution for potassium hydroxide and deionized water and be slowly added dropwise in step 2, is vigorously stirred 15 in drop
Min is kept the temperature spare at white emulsified state.
S4: tiger spot cuttlefish internal organ polysaccharide, Lavender, sodium benzoate are sequentially added in the mixed solution of step 3, are protected
90-95 DEG C of temperature is held, 1 min of homogeneous under 10000 r/min stirring obtains high temperature lotion, takes out cooled to room temperature, system
Obtain hand lotion.
The beneficial effects of the present invention are: tiger spot cuttlefish internal organ polysaccharide of the present invention is by degreasing, hot water extraction, concentration alcohol
The processing steps such as heavy, spin dialysis, freeze-drying are prepared, with moisturizing and oxidation resistant activity.The raw material of extraction is
Tiger spot cuttlefish internal organ are turned waste into wealth to alleviate pollution of the waste to environment.The present invention is extracted from tiger spot cuttlefish internal organ
Polysaccharide be pure natural substance, have that moisturizing, to repair wound, bioactivity, the hand lotion color being prepared such as anti-oxidant equal
It is even, it is in rice white；Lotion exquisiteness is soft and smooth, and viscosity is small, has lavender；Heat-resisting cold tolerance is good, under 40 DEG C of high temperature not
Emulsification is not freezed under -20 DEG C of low temperature；Without water-oil separating after 2000 r/min centrifugation, there is corresponding moisturizing and anti-oxidant etc.
Effect.In addition, the Lavender contained in hand lotion, it can be with balance skin surface layer fat secretion, convergence pore, freckle removing and whitening
Equal skin-protecting functions.
Specific embodiment
Embodiment 1: a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide of the present invention, each raw material ingredient in parts by weight:
20 parts of stearic acid, 3 parts of tristerin, 6 parts of hexadecanol, 20 parts of glycerol, 8 parts of white oil, 1 part of stearic acid potash soap, lavender essence
3 parts, 0.2 part of sodium benzoate, 4 parts of polysaccharide of tiger spot cuttlefish internal organ, 100 parts of deionized water of oil.
Embodiment 2: a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide of the present invention, each raw material ingredient in parts by weight:
15 parts of stearic acid, 2 parts of tristerin, 5 parts of hexadecanol, 15 parts of glycerol, 5 parts of white oil, 0.5 part of potassium hydroxide, lavender essence
1 part, 0.1 part of sodium benzoate, 2 parts of polysaccharide of tiger spot cuttlefish internal organ, 100 parts of deionized water of oil.
Embodiment 3: a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide of the present invention, each raw material ingredient in parts by weight:
30 parts of stearic acid, 5 parts of tristerin, 8 parts of hexadecanol, 30 parts of glycerol, 10 parts of white oil, 2 parts of potassium hydroxide, Lavender
5 parts, 0.3 part of sodium benzoate, 5 parts of polysaccharide of tiger spot cuttlefish internal organ, 100 parts of deionized water.
Embodiment 4: a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide of the present invention, each raw material ingredient in parts by weight:
25 parts of stearic acid, 4 parts of tristerin, 7 parts of hexadecanol, 25 parts of glycerol, 9 parts of white oil, 1.5 parts of potassium hydroxide, lavender essence
4 parts, 0.25 part of sodium benzoate, 3 parts of polysaccharide of tiger spot cuttlefish internal organ, 100 parts of deionized water of oil.
Specifically, tiger spot cuttlefish internal organ polysaccharide described in embodiment 1-4 is prepared by following steps.
A: taking fresh tiger spot cuttlefish adult 5 (about 10 kg of weight), and internal organ (removing gonad) is taken out after dissection, is shredded
Be placed in high-speed tissue mashing machine, then plus 2500 mL distilled water break into homogenate shape, 3 times vol acetone degreasing 3 times, every time 8~
Filtered homogenate is placed on freeze drier and is freeze-dried 24 h, crushed again with crusher for Chinese herbal medicine, finally by 10 h
Tiger spot cuttlefish internal organ dry powder is obtained, collection, which is placed at -20 DEG C, to be saved backup.
B: freeze-dried powder is 1:30 g/mL in solid-liquid ratio, and Extracting temperature is that 1 h is extracted in 90 DEG C of hot water, in centrifuging and taking
Clearly, be concentrated into the 1/5 of original volume, be added 2% active carbon (w/v), decolourize under the conditions of 50 DEG C 1 h, it is anhydrous to add 3 times of volumes
4 DEG C of precipitates overnights of ethyl alcohol, centrifuging and taking precipitating, bag filter 48 h of dialysis for being 8000-12000 with molecular cut off, every 4 h
A water is changed, finally pours into the liquid in bag filter in culture dish, is placed on freeze drier and is freeze-dried 24 h, obtain tiger spot
Cuttlefish internal organ polysaccharide.
For hand lotion described in embodiment 1-4 using being made following preparation method, the preparation method is the following steps are included: S1: taking
Glycerol, white oil and deionized water use 30 min of preceding progress ultraviolet sterilization.S2: by stearic acid, tristerin, hexadecanol,
Glycerol, white oil 15 min of uniform stirring in 90-95 DEG C of water-bath, are configured to oily phase.S3: by potassium hydroxide and deionized water
It is configured to solution to be slowly added dropwise in step 2,15 min is vigorously stirred in drop into white emulsified state, are kept the temperature spare.S4: will
Tiger spot cuttlefish internal organ polysaccharide, Lavender, sodium benzoate sequentially add in the mixed solution of step 3, keep temperature 90-95
DEG C, 1 min of homogeneous under 10000 r/min stirring obtains high temperature lotion, takes out cooled to room temperature, hand lotion is made.
Embodiment 1-4 is used into the hand lotion product that is prepared of the above method, through external moisturizing experiment show 24 h and
The moisturizing rate of 48 h is respectively 94.55% and 92.72%, and anti-oxidant experiment shows under the conditions of concentration is 25 mg/mL, to 1,1-
Diphenyl -2- trinitrophenyl-hydrazine (DPPH) free radical scavenging activity is 56.79%, (3- ethyl-benzothiazole bis- to 2,2 '-hydrazines -
Quinoline -6- sulfonic acid) diamine salts (ABTS) free radical scavenging activity be 83.08%.
The above is merely to illustrate the contents of the present invention, and in addition to this, there are also other embodiments by the present invention, in every case
Those skilled in the art are because of technical inspiration involved in the present invention, and the technology for using equivalent replacement or equivalent deformation mode to be formed
Scheme is fallen within the scope of protection of the present invention.
Claims (5)
1. a kind of hand lotion containing tiger spot cuttlefish internal organ polysaccharide, it is characterised in that: ingredient in parts by weight: stearic acid 15-30
Part, 2-5 parts of tristerin, 5-8 parts of hexadecanol, 15-30 parts of glycerol, 5-10 parts of white oil, 0.5-2 parts of potassium hydroxide, smoke clothing
Careless essential oil 1-5 parts, 0.1-0.3 parts of sodium benzoate, 2-5 parts of internal organ polysaccharide of tiger spot cuttlefish, 100 parts of deionized water.
2. the hand lotion according to claim 1 containing tiger spot cuttlefish internal organ polysaccharide, which is characterized in that match in parts by weight
Material: 20 parts of stearic acid, 3 parts of tristerin, 6 parts of hexadecanol, 20 parts of glycerol, 8 parts of white oil, 1 part of potassium hydroxide, lavender essence
3 parts, 0.2 part of sodium benzoate, 4 parts of polysaccharide of tiger spot cuttlefish internal organ, 100 parts of deionized water of oil.
3. the hand lotion according to claim 1 containing tiger spot cuttlefish internal organ polysaccharide, it is characterised in that: the tiger spot cuttlefish
The preparation method of internal organ polysaccharide the following steps are included:
A: taking fresh tiger spot cuttlefish adult, and internal organ are taken out after dissection and remove gonad, shreds and is placed on high-speed tissue mashing machine
In, then plus distilled water break into homogenate shape, 3 times vol acetone degreasing 3 times, every time 8~10 h, after 24 h of freeze-drying, crushing
To tiger spot cuttlefish internal organ dry powder, collection, which is placed at -20 DEG C, to be saved backup；
B: freeze-dried powder hot water extraction certain time in the case where setting solid-liquid ratio, centrifuging and taking supernatant, concentration, active carbon decoloring are added 3 times
4 DEG C of precipitates overnights of volume dehydrated alcohol, centrifuging and taking precipitating 48 h of dialysis, are freeze-dried 24 h, obtain tiger spot cuttlefish internal organ polysaccharide.
4. the hand lotion according to claim 1 containing tiger spot cuttlefish internal organ polysaccharide, it is characterised in that: in the step B
Centrifugal condition is 4000 r/min.
5. a kind of preparation method of the hand lotion containing tiger spot cuttlefish internal organ polysaccharide, it is characterised in that: the following steps are included:
S1: taking glycerol, white oil and deionized water, uses 30 min of preceding progress ultraviolet sterilization；
S2: by stearic acid, tristerin, hexadecanol, glycerol, white oil in 90-95 DEG C of water-bath uniform stirring 15
Min is configured to oily phase；
S3: being configured to solution for potassium hydroxide and deionized water and be slowly added dropwise in step 2, while drop while be vigorously stirred 15 min at
White emulsified state is kept the temperature spare；
S4: tiger spot cuttlefish internal organ polysaccharide, Lavender, sodium benzoate are sequentially added in the mixed solution of step 3, keep temperature
90-95 DEG C of degree, 1 min of homogeneous under 10000 r/min stirring, obtains high temperature lotion, takes out cooled to room temperature, and shield is made
Hand frost.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811341708.8A CN109125114A (en) | 2018-11-12 | 2018-11-12 | A kind of tiger spot cuttlefish internal organ polysaccharide hand lotion and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811341708.8A CN109125114A (en) | 2018-11-12 | 2018-11-12 | A kind of tiger spot cuttlefish internal organ polysaccharide hand lotion and preparation method thereof |
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| CN201811341708.8A Pending CN109125114A (en) | 2018-11-12 | 2018-11-12 | A kind of tiger spot cuttlefish internal organ polysaccharide hand lotion and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117777316A (en) * | 2023-12-29 | 2024-03-29 | 岭南师范学院 | Preparation method and application of squid visceral polysaccharide |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104739736A (en) * | 2013-12-28 | 2015-07-01 | 大连美乐生物技术开发有限公司 | Hand cream and preparation method thereof |
-
2018
- 2018-11-12 CN CN201811341708.8A patent/CN109125114A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104739736A (en) * | 2013-12-28 | 2015-07-01 | 大连美乐生物技术开发有限公司 | Hand cream and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 孙玉林等: "响应面法优化虎斑乌贼内脏多糖提取工艺及抗氧化活性、吸湿保湿性能研究", 《食品工业科技》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117777316A (en) * | 2023-12-29 | 2024-03-29 | 岭南师范学院 | Preparation method and application of squid visceral polysaccharide |
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