CN109053280A - A kind of anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof - Google Patents
A kind of anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof Download PDFInfo
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- CN109053280A CN109053280A CN201810926257.8A CN201810926257A CN109053280A CN 109053280 A CN109053280 A CN 109053280A CN 201810926257 A CN201810926257 A CN 201810926257A CN 109053280 A CN109053280 A CN 109053280A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/22—Improving land use; Improving water use or availability; Controlling erosion
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
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Abstract
The present invention relates to a kind of anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof, a kind of anti-ageing Cu Huazhuan fringe compound fertilizer, raw material components ratio by weight includes the following: biological organic Carbon Materials 10-20, feces of livestock and poultry carbide 20-30, microbial bacterial agent 0.01-0.1, humic acid 5-10, magnesium sulfate 0.2-0.8, zinc sulfate 0.4-1.2, ferrimanganic pulvis 0.2-0.5, ammonium molybdate 0.25-0.5, calcium superphosphate 1-5, sodium metasilicate 2-8, urea 10-15, potassium chloride 5-10, binder 10-15.Anti-ageing Cu Huazhuan fringe compound fertilizer preparation method includes biological organic Carbon Materials, the preparation of feces of livestock and poultry carbide, load of microorganisms, compound fertilizer preparation.The preparation process and specified microorganisms bacterium curing method of biological organic Carbon Materials of the invention can hold fertilizer slow-release and excite soil nutrient, effectively improve soil fertility, extend, regulation fertilizer provision from soil phase and crop nutrition content demand match, it plays and improves rice resistance, delays senescence, Accelerate bloom is reduced and is degenerated, fringe, strong fringe are protected, the effect of increasing yield and improving quality is promoted.
Description
Technical field
The present invention relates to a kind of fertilizer, it is specifically related to a kind of anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof.
Background technique
Rice is one of main long-term cropping in China, to ensure that grain ration has made safely significant contribution.For a long time, yield
It is the main target of crop production, leads to that fertilizer is long-term, excessive inappropriate application, promotes soil acidification, hardened, organic matter decline
Equal soil ecologies and problem of environmental pollution become increasingly conspicuous.
In China's Rice Cropping in fertile quantity and structure, not only quantity is big with fertilizer for rice, and fertilization structure it is unreasonable,
Nutrient is unbalanced.In terms of use effect, universal relatively low, the fertilizer efficiency decline of the plant recovery of nutrient of fertilizer, fertilizer nutrient loss cause
Acidification, eutrophication the problems such as be on the rise.And in reality production, agricultural producer generally reflects " the more plant the more gluttonous ",
In other words, the cost of high yield be resource is lost, high investment is realized, the intension with modern agriculture " low-carbon, ecology, sustainable "
Demand for development runs in the opposite direction.Therefore, the inherent law for following soil profit and loss revenue and expenditure and crop nutritional need is turned to by highly energy-consuming, with
" low consumption of resources, low-carbon, sustainable " is starting point, comprehensively, precisely, balance fertilizing, improve utilization rate of fertilizer, reaching yield
Culture fertility is realized while target, subtracts medicine, to promote agricultural sustainable development, is just particularly important.
In rice yield realization of goal, Rice Flowering to heading, the pustulation period, be vegetative growth of rice plants and reproductive growth most
Crucial period.In the growing stage, rice root is energetic, and nitrogen and carbon metabolism is vigorous, and nutrient demand amount is big, nutrients uptake amounts
Typically constitute from time of infertility 50-70% or so.In production, mainly supplemented by forms such as foliage top dressing or foliar fertilizers.Rice this
The upgrowth situation in one stage, such as root system, floret bears amount, number of productive ear, Grain filling, often directly affect rice and finally produce
Amount.Therefore, situation etc. is absorbed and utilized to pass in the soil nurtient supply quantity of this growthdevelopmental stage, nutrient formula and plant nutrition
It is important.In conjunction with soil nutrient status, scientific and reasonable, in due course, suitable ground, it is suitable impose ear manuer, and combine water management, disease anti-
Equal cultivation managements measure is controlled to play a significant role realization high yield target.But in traditional mode of agriculture, the producer
Often using " one Hong head " mode, excessively apply base fertilizer, easily cause effective fertility early period insufficient, rice tillering is few, effective fringe not
Foot, later period fertility is then excessive, and it is late-maturing, easily susceptible that rice is remaining green when it is due to become yellow and ripe, so as to cause the underproduction.Also someone proposes that " tap holder protects tail control successively
It is intermediate ", the fertilization modes such as " preceding light, rear weight, then supply ", but in actual production often due to fertilizer after rice tillering latter stage
Supply is insufficient, and rice phenomena such as chlorisis, early ageing, grain husk flower amount declines, Heading filling is insufficient easily occurs and leads to the underproduction.From application
Effect sees, these technologies have certain effect of increasing production in some areas, but technical operation, in terms of there are also many
Deficiency, region limitation is big, universality is not strong, is unfavorable for large area and gently simplifies popularization and application.
Currently, the producer is in the actual production process mostly to apply based on chemical fertilizer, but product function is single, and excessive
Using easily causing environmental pollution.In addition, fertilizer nutrient release and the regulation of fertilizer requirement of rice plant also mismatch, cause fertilizer sharp
With rate is low, nutrient loss is serious, rice resistance is poor, environmental pollution is aggravated while improving agriculture production cost, has influenced rice
Yield and quality improves, and is unfavorable for agricultural sustainable development.A kind of anti-ageing Cu Huazhuan fringe compound fertilizer of the invention, it is discarded with agricultural
Object and feces of livestock and poultry are primary raw material, and ecology, environmental protection, safety, nutrient is balanced, comprehensive, and fertilizer is synchronous with plant nutrition absorption, tool
There are Soil building, weight-reducing synergy, postpone leaf senile, promote flower and reduce degeneration, protect the effects of fringe strengthens fringe, increasing yield and improving quality, at present
It yet there are no relevant report.
Biological organic charcoal is the organic matter raw materials such as biomass under completely or partially anoxia condition, by high temperature pyrolysis
The rich carbon organic product of one kind of generation.Biological organic charcoal has apparent improving effect to soil physics and chemical property.Mainly
The reason is that, one has relatively rich microcellular structure, it is light and porous.Soil porosity can be improved after being manured into soil, reduce
The soil weight improves ventilating permeable.Meanwhile good extension space can be provided for root growth.Second, large specific surface area,
Strong adsorption force, rich in a variety of nutrient elements such as nitrogen, phosphorus, potassium.Thus, Exogenous Nutrients can be provided for soil after being manured into soil, together
When can sticking soil nutrient ion, avoid nutrient loss, cause environmental pollution, improve crop nutrition content absorption rate.Third, more
Microporous properties and richness are supported, multilist surface charge and functional group, are conducive to increase soil fertilizer performance, while promoting root growth.Especially
It, multiplies conducive to the existence of edaphon, promotes and improve biological activity of soil.And Soil Probiotics, to improvement soil knot
Structure promotes organic matter decomposition, activates biological activity of soil, increases soil fertility, and promoting root growth, strong sprout etc. also there is important promotion to make
With.The two combines, and will be formed to have complementary advantages and amplified with advantage.The type of probiotics, content are to Different Crop kind, soil types
It is different with crop growth stage effect, it there is no effectively combined charcoal with Soil Probiotics at present, and bloom, fill for heading
The Rice Production demand of slurry phase realizes the anti-ageing method for preparing fertilizer for promoting to spend strong fringe.
Summary of the invention
Regarding to the issue above and conventional fertilizers are insufficient, it is an object of the present invention to provide a kind of anti-ageing Cu Huazhuan fringe compound fertilizer and its
Preparation method, the preparation process and specified microorganisms bacterium curing method of biological organic Carbon Materials can hold fertilizer slow-release and soil excited to support
Point, effectively improve soil fertility, extend, regulation fertilizer provision from soil phase and crop nutrition content demand match, and by in other, it is micro-
Nutrient element coupling is measured, balanced, comprehensive nutrient is provided, rice resistance is improved to play, delays senescence, Accelerate bloom, reduction
It degenerates, protects fringe, strong fringe, promote the effect of increasing yield and improving quality.
The purpose of the present invention is what is be achieved through the following technical solutions, a kind of anti-ageing Cu Huazhuan fringe compound fertilizer and its preparation side
Method is characterized in that:
A kind of anti-ageing Cu Huazhuan fringe compound fertilizer, raw material components ratio by weight include the following: biological organic Carbon Materials 10-
20, feces of livestock and poultry carbide 20-30, microbial bacterial agent 0.01-0.1, humic acid 5-10, magnesium sulfate 0.2-0.8, zinc sulfate 0.4-
1.2, ferrimanganic pulvis 0.2-0.5, ammonium molybdate 0.25-0.5, calcium superphosphate 1-5, sodium metasilicate 2-8, urea 10-15, potassium chloride 5-
10, binder 10-15.
The biological organic Carbon Materials, preparing raw material is stalk biomass, corncob, peanut shell, rice husk, bacterium
Stick, fruit tree branch, coconut husk, one or two of walnut shell or more.
The binder are as follows: bentonite or clay or both mixing, weight ratio is 1:5-5:1 when the two mixes；
The microbial bacterial agent is phosphate solubilizing bacteria, nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3, the bacillus
Mixed Microbes include bacillus amyloliquefaciens, Methylotrophic bacillus, and the two ratio is 2:1-1:2；
The bacillus amyloliquefaciens, depositary institution: China Committee for Culture Collection of Microorganisms's common micro-organisms center is protected
Hiding number is CGMCC No. 11230, and preservation address is Yard 1, BeiChen xi Road, Chaoyang District, Beijing City 3, the micro- life of the Chinese Academy of Sciences
Object research institute, preservation date are as follows: on August 11st, 2015, classification naming is bacillus amyloliquefaciensBacillus amyloliquefaciens；
The Methylotrophic bacillus, depositary institution: in China Committee for Culture Collection of Microorganisms's common micro-organisms
The heart, deposit number are CGMCC No. 11231, and preservation address is Yard 1, BeiChen xi Road, Chaoyang District, Beijing City 3, Chinese science
Institute of microbiology of institute, preservation date are as follows: on August 11st, 2015, classification naming are Methylotrophic bacillusBacillus methylotrophicus；
Preferably, the anti-ageing Cu Huazhuan fringe compound fertilizer, raw material components ratio by weight include the following: biological organic charcoal
Material 18, feces of livestock and poultry 28, humic acid 8, magnesium sulfate 0.5, zinc sulfate 0.8, ferrimanganic pulvis 0.4, ammonium molybdate 0.35, peroxophosphoric acid
Calcium 4, sodium metasilicate 5, urea 12, potassium chloride 8, microbial bacterial agent 0.1, binder 14.
Preferably, biological organic Carbon Materials, feces of livestock and poultry carbide ratio be 1:1-1:2.5.
Preferably, in the anti-ageing Cu Huazhuan fringe compound fertilizer, ammonium molybdate, magnesium sulfate, zinc sulfate, ferrimanganic pulvis,
The weight ratio that its summation accounts for raw material components is 1.8-2.5.
Described anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof, steps are as follows:
(1) preparation of biological organic Carbon Materials: by stalk biomass, corncob, peanut shell, rice husk, bacteria stick, fruit tree branch, coconut palm
Shell, the one or more of of walnut shell carry out natural drying or drying, and water content is made to be down to 18% hereinafter, above-mentioned raw materials are added
Work crushes, length in 3.5cm hereinafter, or may be selected first be crushed and air-dry or dry afterwards, feces of livestock and poultry, by drying or drying, drop
Low water content is to 16% hereinafter, carrying out smashing it through 80-100 mesh；
Using low alternating temperature charring process method, above-mentioned raw materials are weighed by mass fraction, the specific method is as follows:
A. temperature sets 150-300 DEG C, and the residence time is 2.5-3 hours, and heating rate is 20-30 DEG C/min；
B. it heats up 300-450 DEG C, the residence time is 1.5-2 hours, and heating rate is 30-50 DEG C/min, is then dropped at a slow speed
Temperature processing, was down to room temperature in 1.5-2 hours；
In above process, by the plant base wood vinegar condensed and separated, biomass collection thermal cracking is formed, and in carbonization process
In return and be sprayed onto material and solidified, be modified, after cooling down, by Modified Activated Carbon material disintegrating, sieving, 100 purpose of partial size is made
Modified Carbon Materials；
(2) prepared by feces of livestock and poultry carbide: using anoxic dry distillation charring technology, weighs after sunning or drying by mass fraction
Feces of livestock and poultry be put into retort, method particularly includes:
Temperature is set as 150-300 DEG C, and the residence time is 2-2.5 hours, and heating rate is 30-50 DEG C/min；
Cooling processing is carried out after the completion of charing, is down to room temperature in 1-1.5 hours；
By the plant base wood vinegar for condensing and separating, being formed in biomass collection carbonization process, and returns and be sprayed onto carbonization process
Solidified in material, be modified.After cooling down, by Modified Activated Carbon material disintegrating, sieving, the modification livestock and poultry of 100 mesh of partial size are made
Excrement Carbon Materials；
(3) load of microorganisms: the biological organic Carbon Materials and step (2) feces of livestock and poultry Carbon Materials that step (1) is obtained mix equal
It is even, mixing Carbon Materials are mixed well with microbial bacterial agent, moisture control is in 20-30%, and spontaneous fermentation 3-5 days, fermentation was completed
Afterwards, Solid-Liquid Separation is carried out, by remaining solidfied material in saving under room temperature；
The microbial bacterial agent includes: phosphate solubilizing bacteria (phosphorus-solubilizing bacteria), nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3,
The bacillus Mixed Microbes include that both bacillus amyloliquefaciens, Methylotrophic bacillus ratio are 2:1-1:2；
The microbial bacterial agent preparation process is as follows: bacillus amyloliquefaciens, Methylotrophic bacillus using culture medium and
Condition of culture are as follows: culture medium prescription be amino acid powder 2.5%, peptone 2%, xylitol 8%, pH7.0, revolving speed 150-200r/min,
Fermentation time 48 hours；Bacterium number in culture solution is formulated as 2.5 × 109Cfu/ml, and proportionally prepare and obtain gemma bar
Bacterium mixture；The bacterium number of phosphate solubilizing bacteria, nitrogen-fixing bacteria is adjusted to 2.5 × 109Cfu/ml is mixed with above-mentioned bacillus in proportion
Object is mixed to get microbial bacterial agent.
(4) prepared by compound fertilizer: the solidfied material after weighing load of microorganisms by mass fraction, humic acid, magnesium sulfate, sulfuric acid
Zinc, ferrimanganic pulvis, ammonium molybdate, calcium superphosphate, sodium metasilicate, urea, potassium chloride, binder, with blender and organic fertilizer granulator
Pressure granulation is carried out, the blender and pelletizer that other models also can be selected are granulated, and the cylindrical body that partial size is 3-5mm is made
Or spherical compound fertilizer, it then measured, packed.
The application method of the anti-ageing Cu Huazhuan fringe compound fertilizer is applied in the form of top dressing, is applied within 7-9 days before heading stage,
20-30 kgs/acre of amount of application.
Preferably, the application method of the anti-ageing Cu Huazhuan fringe compound fertilizer, dosage are 25 kgs/acre.
Compared with existing fertilizer, the beneficial effects of the present invention are:
(1) using more micropores, high-carbon, the rich organic Carbon Materials of health object as carrier, by loading, coupling microorganism and polynary nutrient member
Element, actively release, decomposition are combined with fixing, sustained release, and multidirectional excitation biological activity of soil, culture fertility improves available nutrient
Supply.It is combined by decomposition, release, slow releasing function, multipath ensures effective, in due course, enough supplies of nutrient.
(2) quick-acting in conjunction with slow, Reasonable Regulation And Control, extension, matching fertilizer phase, psychological need and fertility with plant growth
Phase is synchronous.By promoting, exciting soil microbial activity, actively remaining biologic artifact effectively in the soil such as decomposing straw,
The effects of accelerating decomposition, mineralising process, ensures fertility sustainable supply.The organic Carbon Materials of modification biological and humic acid, releasably
Soluble nutrient ion increases soil directly for utilizing total nutrient content.By sticking, polymerization, sustained release nutrient, regulation extends
The fertilizer provision from soil phase makes soil that can effectively reduce nutrient loss using amount of nutrients is high, sustainable, reserve strength is sufficient, is ensureing crop nutrition content
While being absorbed and utilized, crop nutrition content utilization efficiency is improved, promotes crop growth.
(3) premature senescence resistance, promote to bloom, to protect the strong fringe effect of fringe obvious.It is different from artificial synthesized and other chemicals, modified life
The organic Carbon Materials of object can promote root growth by physics, chemistry, bioelectric detecting approach, adjust root/shoot ratio, increase overground part and support
Divide supply, delay Root and leaf senescence, to be conducive to keep vigorous photosynthesis, increases accumulation of photosynthate, improve
Crop nutrient growth-reproductive growth transformation efficiency, coordinates Resource more, promotes crop flowers, heading and grouting knot
It is real.
(4) nutrition is comprehensive, balanced, enhances physiological resistance, promotes increasing yield and improving quality.In fertilizer of the invention, biological organic charcoal
Material itself is i.e. rich in a large amount of and middle microelement, secondly by science, rationally adds calcium, magnesium, sulphur, zinc, iron, sodium etc.
Meso- and micro-nutrients provide comprehensive, balanced nutrient for Rice Heading, pustulation period.It is coupled by organic with inorganic nutrients, it is real
Now have complementary advantages, fertilizer emergency is mutually helped, and short-term, the long-term needs of vegetative growth of rice plants and reproductive growth are met, and improves Rice Resistance
Property, accelerate protein synthesis, enrich kernel grouting, protect fringe and strengthen fringe, is conducive to improve the yield and quality.
(5) raw material is easy to get, produces simple, reduction pest and disease damage.Raw materials for production are agriculture and forestry waste and feces of livestock and poultry, raw material
It is easy to get, production process is simple, and source is wide, sustainable, at low cost.Solidification, the modification biological for being added to plant base wood vinegar are organic
Carbon Materials can reduce pest and disease damage.Fertilizing soil simultaneously, realization subtracts medicine and carbon fixation and emission reduction, improves agricultural land soil and gives birth to
State environment, increasing yield and improving quality, comprehensive benefit are good.
Specific embodiment
Make in more detail with test data, the technical characteristic above-mentioned and other to the present invention and advantage with reference to embodiments
Explanation.
Embodiment 1
1. anti-ageing Cu Huazhuan fringe compound fertilizer production method
The anti-ageing Cu Huazhuan fringe compound fertilizer, raw material components ratio by weight include the following: biological organic Carbon Materials 10-20,
Feces of livestock and poultry carbide 20-30, microbial bacterial agent 0.01-0.1, humic acid 5-10, magnesium sulfate 0.2-0.8, zinc sulfate 0.4-
1.2, ferrimanganic pulvis 0.2-0.5, ammonium molybdate 0.25-0.5, calcium superphosphate 1-5, sodium metasilicate 2-8, urea 10-15, potassium chloride 5-
10, binder 10-15.
The biological organic Carbon Materials, preparing raw material is stalk biomass, corncob, peanut shell, rice husk, bacterium
Stick, fruit tree branch, coconut husk, one or two of walnut shell or more.
The binder are as follows: bentonite or clay or both mixing, weight ratio is 1:5-5:1 when the two mixes；
The microbial bacterial agent is phosphate solubilizing bacteria, nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3, the bacillus
Mixed Microbes include bacillus amyloliquefaciens, Methylotrophic bacillus, and the two ratio is 2:1-1:2；
Described anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof, steps are as follows:
(1) preparation of biological organic Carbon Materials: by stalk biomass, corncob, peanut shell, rice husk, bacteria stick, fruit tree branch, coconut palm
Shell, the one or more of of walnut shell carry out natural drying or drying, and water content is made to be down to 18% hereinafter, above-mentioned raw materials are added
Work crushes, length in 3.5cm hereinafter, or may be selected first be crushed and air-dry or dry afterwards, feces of livestock and poultry, by drying or drying, drop
Low water content is to 16% hereinafter, carrying out smashing it through 80-100 mesh；
Using low alternating temperature charring process method, above-mentioned raw materials are weighed by mass fraction, the specific method is as follows:
A. temperature sets 150-300 DEG C, and the residence time is 2.5-3 hours, and heating rate is 20-30 DEG C/min；
B. it heats up 300-450 DEG C, the residence time is 1.5-2 hours, and heating rate is 30-50 DEG C/min, is then dropped at a slow speed
Temperature processing, was down to room temperature in 1.5-2 hours；
In above process, by the plant base wood vinegar condensed and separated, biomass collection thermal cracking is formed, and in carbonization process
In return and be sprayed onto material and solidified, be modified, after cooling down, by Modified Activated Carbon material disintegrating, sieving, 100 purpose of partial size is made
Modified Carbon Materials.
(2) prepared by feces of livestock and poultry carbide: using anoxic dry distillation charring technology, weighs by mass fraction by drying or drying
Feces of livestock and poultry after dry is put into retort, method particularly includes:
Temperature is set as 150-300 DEG C, and the residence time is 2-2.5 hours, and heating rate is 30-50 DEG C/min；
Cooling processing is carried out after the completion of charing, is down to room temperature in 1-1.5 hours；
By the plant base wood vinegar for condensing and separating, being formed in biomass collection carbonization process, and returns and be sprayed onto carbonization process
Solidified in material, be modified.After cooling down, by Modified Activated Carbon material disintegrating, sieving, the modification livestock and poultry of 100 mesh of partial size are made
Excrement Carbon Materials.
(3) load of microorganisms: the biological organic Carbon Materials and step (2) feces of livestock and poultry Carbon Materials that step (1) is obtained are mixed
It closes uniformly, mixing Carbon Materials is mixed well with microbial bacterial agent, moisture is controlled in 20-30%, spontaneous fermentation 3-5 days, has been fermented
Cheng Hou carries out Solid-Liquid Separation, by remaining solidfied material in saving under room temperature；
The microbial bacterial agent includes: phosphate solubilizing bacteria (phosphorus-solubilizing bacteria), nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3,
The bacillus Mixed Microbes include that both bacillus amyloliquefaciens, Methylotrophic bacillus ratio are 2:1-1:2；
Phosphate solubilizing bacteria (phosphorus-solubilizing bacteria) is purchased from market from Guangzhou infinitesimal Biotechnology Co., Ltd；
Nitrogen-fixing bacteria are purchased from market from Yangzhou Haicheng Bioisystech Co., Ltd.
The microbial bacterial agent preparation process is as follows: bacillus amyloliquefaciens, Methylotrophic bacillus are using culture
Base and condition of culture are as follows: culture medium prescription is amino acid powder 2.5%, peptone 2%, xylitol 8%, PH7.0, revolving speed 150-200r/
Min, fermentation time 48 hours；Bacterium number in culture solution is formulated as 2.5 × 109cfu/ml, and proportionally prepares and obtains bud
Spore bacillus mixture；The bacterium number of phosphate solubilizing bacteria, nitrogen-fixing bacteria is adjusted to 2.5 × 109Cfu/ml, in proportion with above-mentioned bacillus
Mixture is mixed to get microbial bacterial agent.
(4) prepared by compound fertilizer: the solidfied material after weighing load of microorganisms by mass fraction, humic acid, magnesium sulfate, sulfuric acid
Zinc, ferrimanganic pulvis, ammonium molybdate, calcium superphosphate, sodium metasilicate, urea, potassium chloride, binder, with blender and organic fertilizer granulator
Pressure granulation is carried out, the blender and pelletizer that other models also can be selected are granulated, and the cylindrical body that partial size is 3-5mm is made
Or spherical compound fertilizer, it then measured, packed.
2. Rice Production application test
Test site: Anshan Xiuyan County, Liaoning Province bar man fort, rice varieties are northern round-grained rice 2, are purchased from seed sale market；With conventional fertilizer application
As control, it is set as CK.CF is set as processing is compared with a kind of anti-ageing Cu Huazhuan fringe compound fertilizer (30kg/ mus).Compound fertilizer
Administration time is to be applied in the form of top dressing, uniformly sowed 7-9 days before Rice Heading blooming stage.10 days measurement rice after to top dressing
Plant height, plant above ground portion dry-matter accumulation amount, floret bears, maturity period calculate the percentage of earbearing tiller and measure the indexs such as yield.
Test result shows that the Plant Height of Rice of anti-ageing Cu Huazhuan fringe compound fertilizer processing, dry-matter accumulation amount are above control,
10.78%, 8.36% is improved than control respectively, illustrates that compound fertilizer's processing promotes the growth and development of rice overground part plant.Together
When, floret bears, the percentage of earbearing tiller are also apparently higher than control, show that compound fertilizer's processing plays the role of rush and spends strong fringe, establish for output increased
Basis is determined.And ultimate output measurement shows that compound fertilizer's processing than control volume increase 7.37%, plays growth promoting production-increasing function.
Influence of 1 compound fertilizer of table to rice growth and yield traits
Embodiment 2
A kind of anti-ageing Cu Huazhuan fringe compound fertilizer, raw material components ratio by weight include the following: biological organic Carbon Materials 18, animal dung
Just 28, humic acid 8, magnesium sulfate 0.5, zinc sulfate 0.8, ferrimanganic pulvis 0.4, ammonium molybdate 0.35, calcium superphosphate 4, sodium metasilicate 5,
Urea 12, potassium chloride 8, microbial bacterial agent 0.1, binder 14.
The biological organic Carbon Materials, preparing raw material is corncob, peanut shell, rice husk, and three's weight ratio is 1:
1:1。
The binder are as follows: bentonite and clay, weight ratio is 5:3 when the two mixes；
The microbial bacterial agent is phosphate solubilizing bacteria, nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3, the bacillus
Mixed Microbes include bacillus amyloliquefaciens, Methylotrophic bacillus, and the two ratio is 1:1；
Described anti-ageing Cu Huazhuan fringe compound fertilizer and preparation method thereof, steps are as follows:
(1) preparation of biological organic Carbon Materials: by stalk biomass, corncob, peanut shell, rice husk, bacteria stick, fruit tree branch, coconut palm
Shell, the one or more of of walnut shell carry out natural drying or drying, and water content is made to be down to 18% hereinafter, above-mentioned raw materials are added
Work crushes, length in 3.5cm hereinafter, or may be selected first be crushed and air-dry or dry afterwards, feces of livestock and poultry, by drying or drying, drop
Low water content is to 16% hereinafter, carrying out smashing it through 80-100 mesh；
Using low alternating temperature charring process method, above-mentioned raw materials are weighed by mass fraction, the specific method is as follows:
A. temperature sets 150-300 DEG C, and the residence time is 3 hours, and heating rate is 20-30 DEG C/min；
B. it heats up 300-450 DEG C, the residence time is 2 hours, and heating rate is 30-50 DEG C/min, is then carried out at cooling at a slow speed
Reason, was down to room temperature in 2 hours；
In above process, by the plant base wood vinegar condensed and separated, biomass collection thermal cracking is formed, and in carbonization process
In return and be sprayed onto material and solidified, be modified, after cooling down, by Modified Activated Carbon material disintegrating, sieving, 100 purpose of partial size is made
Modified Carbon Materials.
(2) prepared by feces of livestock and poultry carbide: using anoxic dry distillation charring technology, weighs by mass fraction by drying or drying
Feces of livestock and poultry after dry is put into retort, method particularly includes:
Temperature is set as 150-300 DEG C, and the residence time is 2.5 hours, and heating rate is 30-50 DEG C/min；
Cooling processing is carried out after the completion of charing, is down to room temperature in 1.5 hours；
By the plant base wood vinegar for condensing and separating, being formed in biomass collection carbonization process, and returns and be sprayed onto carbonization process
Solidified in material, be modified.After cooling down, by Modified Activated Carbon material disintegrating, sieving, the modification livestock and poultry of 100 mesh of partial size are made
Excrement Carbon Materials.
(3) load of microorganisms: the biological organic Carbon Materials and step (2) feces of livestock and poultry Carbon Materials that step (1) is obtained are mixed
It closes uniformly, mixing Carbon Materials is mixed well with microbial bacterial agent, moisture is controlled in 20-30%, spontaneous fermentation 3-5 days, has been fermented
Cheng Hou carries out Solid-Liquid Separation, by remaining solidfied material in saving under room temperature；
The microbial bacterial agent includes: phosphate solubilizing bacteria (phosphorus-solubilizing bacteria), nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3,
The bacillus Mixed Microbes include that both bacillus amyloliquefaciens, Methylotrophic bacillus ratio are 1:1；
Phosphate solubilizing bacteria (phosphorus-solubilizing bacteria) is purchased from market from Guangzhou infinitesimal Biotechnology Co., Ltd；
Nitrogen-fixing bacteria are purchased from market from Yangzhou Haicheng Bioisystech Co., Ltd.
The microbial bacterial agent preparation process is as follows: bacillus amyloliquefaciens, Methylotrophic bacillus are using culture
Base and condition of culture are as follows: culture medium prescription is amino acid powder 2.5%, peptone 2%, xylitol 8%, PH7.0, revolving speed 150-200r/
Min, fermentation time 48 hours；Bacterium number in culture solution is formulated as 2.5 × 109Cfu/ml, and proportionally (solution starch gemma
Bacillus and Methylotrophic bacillus ratio are prepared for 1:1) obtains bacillus mixture；By the bacterium of phosphate solubilizing bacteria, potassium solubilizing bacteria
Number is adjusted to 2.5 × 109Cfu/ml, (1:2:3) and above-mentioned bacillus mixture are mixed to get microbial bacterial agent in proportion.
(4) prepared by compound fertilizer: the solidfied material after weighing load of microorganisms by mass fraction, humic acid, magnesium sulfate, sulfuric acid
Zinc, ferrimanganic pulvis, ammonium molybdate, calcium superphosphate, sodium metasilicate, urea, potassium chloride, binder, with blender and organic fertilizer granulator
Pressure granulation is carried out, cylindrical body or spherical compound fertilizer that partial size is 3-5mm is made, then measured, packed.
2. rice application test
Test site: Tieling Yinzhou District ox mound, rice varieties are northern round-grained rice 2, are purchased from seed sale market.
Using local conventional fertilizer application as control, it is set as CK；The processing of anti-ageing Cu Huazhuan fringe compound fertilizer is set as processing is compared
CF, compound fertilizer's amount of application are 25kg per acre, apply within 9 days before heading stage, are manured into soil in the form of top dressing, other cultivation managements are arranged
Apply routinely rice field producting rule management.At heading stage, overground part stem, leaf, fringe dry weight, floret bears, SPAD is measured by sampling
Value.The indexs of correlation such as panicled characters and setting percentage, yield are measured in the maturity period.
As can be seen from the test results, Rice Leaf, stem after applying compound fertilizer, fringe dry weight are above control, compare respectively
According to improving 7.01%, 11.72%, 12.60%, show that compound fertilizer promotes rice overground part growth and development, especially to fringe formed and
Dry-matter accumulation is obviously promoted effect.Floret bears, compound fertilizer's processing improve 15.31% than control, show that compound fertilizer is conducive to
Promote clever flower-shape at laying the foundation for later period yield.SPAD value and photosynthetic rate, compound fertilizer's processing are improved than control respectively
8.91%, 2.29%, show that the blade of compound fertilizer's processing maintains relatively high chlorophyll content and stronger photosynthesis energy
Power plays certain anti-aging effects to rice, advantageously forms more photosynthates, promotes source-library accumulation, produces for the later period
Amount is promoted and establishes material base (table 2).
And from the point of view of maturity period Rice Panicle Traits, either spike length, grain number per spike or setting percentage, number of productive ear are compound
Fertilizer processing is above control, shows that compound fertilizer's processing plays the role of preferable " strong fringe ".Ultimate output statistics indicate that, compound fertilizer
Processing improves 6.98% than control, and production-increasing function is obvious (table 3).
To sum up, preferable anti-ageing rush Hua Zhuansui, growth promoting production-increasing function are played using the compound fertilizer in Rice Production.
2 compound fertilizer of table is on rice growth and photosynthetic influence
Influence of 3 compound fertilizer of table to Rice Panicle Traits and yield
Claims (6)
1. a kind of anti-ageing Cu Huazhuan fringe compound fertilizer, it is characterized in that: the raw material components of the anti-ageing Cu Huazhuan fringe compound fertilizer are by weight
Ratio includes the following: biological organic Carbon Materials 10-20, feces of livestock and poultry carbide 20-30, microbial bacterial agent 0.01-0.1, and corruption is planted
Sour 5-10, magnesium sulfate 0.2-0.8, zinc sulfate 0.4-1.2, ferrimanganic pulvis 0.2-0.5, ammonium molybdate 0.25-0.5, calcium superphosphate 1-
5, sodium metasilicate 2-8, urea 10-15, potassium chloride 5-10, binder 10-15；
The biological organic Carbon Materials, prepare raw material be stalk biomass, corncob, peanut shell, rice husk, bacteria stick,
Fruit tree branch, coconut husk, one or two of walnut shell or more；
The binder are as follows: bentonite or clay or both mixing, weight ratio is 1:5-5:1 when the two mixes；
The microbial bacterial agent is phosphate solubilizing bacteria, nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3, the bacillus
Mixed Microbes include bacillus amyloliquefaciens, Methylotrophic bacillus, and the two ratio is 2:1-1:2；
The bacillus amyloliquefaciens, depositary institution: China Committee for Culture Collection of Microorganisms's common micro-organisms center is protected
Hiding number is CGMCC No. 11230, and preservation address is Yard 1, BeiChen xi Road, Chaoyang District, Beijing City 3, the micro- life of the Chinese Academy of Sciences
Object research institute, preservation date are as follows: on August 11st, 2015, classification naming is bacillus amyloliquefaciensBacillus amyloliquefaciens；
The Methylotrophic bacillus, depositary institution: in China Committee for Culture Collection of Microorganisms's common micro-organisms
The heart, deposit number are CGMCC No. 11231, and preservation address is Yard 1, BeiChen xi Road, Chaoyang District, Beijing City 3, Chinese science
Institute of microbiology of institute, preservation date are as follows: on August 11st, 2015, classification naming are Methylotrophic bacillusBacillus methylotrophicus。
2. a kind of anti-ageing Cu Huazhuan fringe compound fertilizer according to claim 1, it is characterized in that: the anti-ageing rush spends strong fringe compound
The raw material components ratio by weight of fertilizer includes the following: biological organic Carbon Materials 18, feces of livestock and poultry 28, humic acid 8, and magnesium sulfate is
0.5, zinc sulfate 0.8, ferrimanganic pulvis 0.4, ammonium molybdate 0.35, calcium superphosphate 4, sodium metasilicate 5, urea 12, potassium chloride 8, microorganism
Microbial inoculum 0.1, binder 14.
3. a kind of anti-ageing Cu Huazhuan fringe compound fertilizer according to claim 1, it is characterized in that: the biological organic Carbon Materials,
The ratio of feces of livestock and poultry carbide is 1:1-1:2.5.
4. a kind of anti-ageing Cu Huazhuan fringe compound fertilizer according to claim 1, it is characterized in that: the anti-ageing rush spends strong fringe compound
In fertilizer, ammonium molybdate, magnesium sulfate, zinc sulfate, ferrimanganic pulvis, the weight ratio that summation accounts for raw material components is 1.8-2.5.
5. a kind of anti-ageing Cu Huazhuan fringe compound fertilizer according to claim 1, it is characterized in that: the anti-ageing rush spends strong fringe compound
The application method of fertilizer is applied in the form of top dressing, is applied within 7-9 days before heading stage, 20-30 kgs/acre of amount of application.
6. a kind of preparation method of anti-ageing Cu Huazhuan fringe compound fertilizer, it is characterized in that: the following steps are included:
(1) preparation of biological organic Carbon Materials: by stalk biomass, corncob, peanut shell, rice husk, bacteria stick, fruit tree branch, coconut palm
Shell, the one or more of of walnut shell carry out natural drying or drying, and water content is made to be down to 18% hereinafter, above-mentioned raw materials are added
Work crushes, length in 3.5cm hereinafter, or may be selected first be crushed and air-dry or dry afterwards, feces of livestock and poultry, by drying or drying, drop
Low water content is to 16% hereinafter, carrying out smashing it through 80-100 mesh；
Using low alternating temperature charring process method, above-mentioned raw materials are weighed by mass fraction, the specific method is as follows:
A. temperature sets 150-300 DEG C, and the residence time is 2.5-3 hours, and heating rate is 20-30 DEG C/min；
B. it heats up 300-450 DEG C, the residence time is 1.5-2 hours, and heating rate is 30-50 DEG C/min, is then dropped at a slow speed
Temperature processing, was down to room temperature in 1.5-2 hours；
In above process, by the plant base wood vinegar condensed and separated, biomass collection thermal cracking is formed, and in carbonization process
In return and be sprayed onto material and solidified, be modified, after cooling down, by Modified Activated Carbon material disintegrating, sieving, 100 purpose of partial size is made
Modified Carbon Materials；
(2) prepared by feces of livestock and poultry carbide: using anoxic dry distillation charring technology, weighs after sunning or drying by mass fraction
Feces of livestock and poultry be put into retort, method particularly includes:
Temperature is set as 150-300 DEG C, and the residence time is 2-2.5 hours, and heating rate is 30-50 DEG C/min；
Cooling processing is carried out after the completion of charing, is down to room temperature in 1-1.5 hours；
By the plant base wood vinegar for condensing and separating, being formed in biomass collection carbonization process, and returns and be sprayed onto carbonization process
Solidified in material, be modified；
After cooling down, by Modified Activated Carbon material disintegrating, sieving, the modification feces of livestock and poultry Carbon Materials of 100 mesh of partial size are made；
(3) load of microorganisms: the biological organic Carbon Materials and step (2) feces of livestock and poultry Carbon Materials that step (1) is obtained mix equal
It is even, mixing Carbon Materials are mixed well with microbial bacterial agent, moisture control is in 20-30%, and spontaneous fermentation 3-5 days, fermentation was completed
Afterwards, Solid-Liquid Separation is carried out, by remaining solidfied material in saving under room temperature；
The microbial bacterial agent includes: phosphate solubilizing bacteria (phosphorus-solubilizing bacteria), nitrogen-fixing bacteria, bacillus Mixed Microbes, proportions 1:2:3,
The bacillus Mixed Microbes include that both bacillus amyloliquefaciens, Methylotrophic bacillus ratio are 2:1-1:2；
The microbial bacterial agent preparation process is as follows: bacillus amyloliquefaciens, Methylotrophic bacillus using culture medium and
Condition of culture are as follows: culture medium prescription be amino acid powder 2.5%, peptone 2%, xylitol 8%, pH7.0, revolving speed 150-200r/min,
Fermentation time 48 hours；Bacterium number in culture solution is formulated as 2.5 × 109Cfu/ml, and proportionally prepare and obtain gemma bar
Bacterium mixture；The bacterium number of phosphate solubilizing bacteria, nitrogen-fixing bacteria is adjusted to 2.5 × 109Cfu/ml is mixed with above-mentioned bacillus in proportion
Object is mixed to get microbial bacterial agent；
(4) compound fertilizer prepare: the solidfied material after weighing load of microorganisms by mass fraction, humic acid, magnesium sulfate, zinc sulfate,
Ferrimanganic pulvis, ammonium molybdate, calcium superphosphate, sodium metasilicate, urea, potassium chloride, binder are carried out with blender and organic fertilizer granulator
Pressure is granulated, and the blender and pelletizer that other models also can be selected are granulated, and cylindrical body or ball that partial size is 3-5mm is made
Then shape compound fertilizer is measured, is packed.
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