CN108836911A - A kind of compact whitening and moistening skin composition and skin care item containing active ingredient of Chinese herbs - Google Patents
A kind of compact whitening and moistening skin composition and skin care item containing active ingredient of Chinese herbs Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The invention discloses a kind of compact whitening and moistening skin composition containing active ingredient of Chinese herbs, includes active ingredient of Chinese herbs, and the active ingredient of Chinese herbs is the extract of the raw material comprising following parts by weight:5~20 parts of safflower, 10~30 parts of almond, 10~20 parts of Rhizoma Chuanxiong, 10~30 parts of Radix Angelicae Sinensis, 15~50 parts of the rhizoma bolbostemmae and 15~40 parts of polygonum cuspidate.Compact whitening and moistening skin composition of the present invention containing active ingredient of Chinese herbs, with stronger tyrosinase activity rejection ability, also there is very strong DPPH free radical scavenging ability, aging and interior free yl are excessive and (or) Scavenging activity decline is closely related, remove free radical excessive in skin, can inhibit skin aging from source, inhibit the formation of wrinkle, the growth of epidermal cell can also be promoted to divide, epidermal cell is made to become full, to restore skin younger state.The skin care item of the present invention also provides a kind of compact whitening and moistening skin composition containing active ingredient of Chinese herbs.
Description
Technical field
The present invention relates to a kind of cosmetic fields, and in particular to a kind of compact whitening and moistening skin group containing active ingredient of Chinese herbs
Close object and skin care item.
Background technique
Skin histology is increasingly flourishing after people's birth, and function is gradually active, will start to degenerate when reaching certain age, this
Degeneration is often unconsciously slowly carried out in people.Wrinkle and pigmentation are the primary outer features of skin aging, with
The growth at age, lipid is also reduced between sebum secretion amount and horn cell, and percutaneous moisture loss rises；Epidermal cell differentiation capability
It reduces, cuticula is thinning, and atrophy of epidermis generates fine wrinkle.Corium generates insoluble collagen, and elasticity reduces, and hyaluronic acid is also with year
Age increases and reduces, and corium moisture is caused to reduce, and generates deeper wrinkle.Furthermore under ultraviolet light irradiation, work is generated in skin
Property oxygen and lipid peroxide, lipid peroxide the substances such as malonaldehyde are resolved into the case where aoxidizing enzyme effect, and albumen qualitative response is formed
Brown element spot, chromogenesis are calm.
The product that currently used wrinkle resistance, whitening produces are various, and effect and effect are variant greatly, and most of product can not usually mention
High skin metabolism promotes skin blood circulation, increases skin-nourishing, can not fundamentally remove the wrinkle and color of skin appearance
Spot.And most products contain heavy metal, safety and the still difficult prediction of sequelae, if improper use, may after cause the damage of skin
Wound.
Skin care item with long-acting compact whitening and moistening skin effect are the hot spots of those skilled in the art's research.Resist in numerous
Wrinkle in whitening and skin-protecting raw material, from the aging ingredient of active ingredient of Chinese herbs, have the characteristics that it is safe and effective and long-acting, as red
Flower, almond, Radix Angelicae Sinensis, Rhizoma Chuanxiong, rhizoma bolbostemmae etc., anti-aging non-defective unit even more since ancient times have skin nutrition, skin whitening, rush
The effects of into skin metabolism.Some active peptides ingredients, such as oligopeptides -1, collagen, silk peptide, then high with concentration,
The strong feature of effect, and side effect very little, or there is no side effect.Therefore, how to be protected with the anti-aging in a variety of sources
Skin ingredient copes with the aging problem of skin, develop it is a kind of it is highly-safe, fundamentally solve color spot and wrinkle, it is existing short-term
Effect, but the product for having long-term effect is skin care field problem in the urgent need to address.
Summary of the invention
One kind is provided and contains active ingredient of Chinese herbs it is an object of the invention to overcome the shortcomings of the prior art place
Compact whitening and moistening skin composition.
To achieve the above object, the technical scheme adopted by the invention is as follows：A kind of compact whitening containing active ingredient of Chinese herbs
Sin-care composition, includes active ingredient of Chinese herbs, and the active ingredient of Chinese herbs is the extract of the raw material comprising following parts by weight:
5~20 parts of safflower, 10~30 parts of almond, 10~20 parts of Rhizoma Chuanxiong, 10~30 parts of Radix Angelicae Sinensis, 15~50 parts of the rhizoma bolbostemmae and polygonum cuspidate 15~40
Part.
In the present invention, the active ingredient of Chinese herbs select Radix Angelicae Sinensis, the rhizoma bolbostemmae, safflower, almond, Rhizoma Chuanxiong, in polygonum cuspidate Six-element
The effect of medicine compounds, and plays compact whitening and moistening skin.Six-element herbal function is described as follows：
Radix Angelicae Sinensis：Radix Angelicae Sinensis has the function of activating microcirculation and removing stasis medicinal, improves skin microcirculation；It is invigorating blood circulation simultaneously, there is solidification blood capillary
The effect of pipe.Radix Angelicae Sinensis has good SOD sample activity, inhibits the reaction of membrane lipid peroxidatio caused by superoxide radical and free radical anti-
It answers, and the damage with a variety of mechanism antagonism free radicals such as biological film phospholipid join protection membrane lipid to tissue, free radical is hindered
Complexion caused by stagnant is gloomy or gives birth to sore swells, there is special efficacy.It, which has, promotes gloss of having rosy cheeks, and skin nutrition prevents skin thick
It is rough, to acne, chloasma, freckle treatment and black hair, prevents hair loss etc. and to have therapeutic effect.
The rhizoma bolbostemmae：Rhizoma bolbostemmae acrid flavour is bitter, mild-natured slightly cold, have cold dispelling relieve stagnation, relieving restlessness of quenching the thirst, inducing diuresis for treating strangurtia, expedite the emergence of promote lactation,
The effect of mass dissipating and swelling eliminating and removing toxic substances sore.Modern pharmacological research proves, saponin component contained by the rhizoma bolbostemmae has anti-hemolysis, disease-resistant
The effects of poison, the wart that disappears, the bleb that disappears.
Safflower：Safflower have the effects that promoting blood circulation, it is anti-inflammatory, anti-oxidant, by improve skin blood circulation, promote skin it is newly old
Be metabolized, remove free radical, inhibit melanin deposition, accelerate ecchymose removing decoloration, absorption ultraviolet light etc., play whitening, sun-proof, anti-aging
The effect of, and have therapeutic effect to contact dermatitis, seborrheic dermatitis, pruritus, neurodermatitis；It profound can also supplement
The multiple nutritional components of skin.
Almond：Almond volatile oil rich in, vitamin B1、B2Etc. nutritional ingredients, external application keratoderma can be made soft
Change, moisturize the skin, improves skin blood circulation, reduce wrinkle of skin and slowing down skin aging.Modern research shows that almond is to table
Cornu cutaneum cell plastid has proliferation function, has facilitation effect to the generation of ceramide, furthermore to the inhibition of elastoser and can be compared with
The water content for significantly improving cuticula, shows that it has good skin-active, crease-resistant and anti-attenuation；It is also to cathepsin D
Activation shows there is anti-inflammatory, preferably can prevent and inhibit dermatitis；In addition, melanocyte activity can be inhibited, there is whitening skin
The effect of skin.
Rhizoma Chuanxiong：Rhizoma Chuanxiong has the effect of blood-activating and qi-promoting, wind-expelling pain-stopping.Ferulic acid and volatile oil component in Rhizoma Chuanxiong not only have
There is anti-inflammatory, analgesia, eliminate the effects of smooth muscle spasm, moreover it is possible to inhibit the generation of free radical, effective scavenging activated oxygen；Lower
Under concentration, the activity of melanocyte can be effectively suppressed, reduce the generation of melanin；There is hygroscopicity simultaneously, there is moisture-keeping function.
Polygonum cuspidate：Its is bitter in taste, flat, there is the function of wind-dispelling, dampness removing, broken silt, promoting menstruation.Its extract is to B-16 melanocyte
Activity have a good inhibiting effect, in addition have facilitation to macrophage activity, reduce black by the two aspects
Cellulose content can be used for whitening class cosmetics；There is inhibiting effect to elastoser, in conjunction with inoxidizability, is suitable for crease-resistant skin-active
Class skin care item；Antibacterial agent, hair restorer and anoretic are also acted as simultaneously.
Tyrosinase is widely present in organism, and tyrosinase is the major rate-limiting enzyme in melanin forming process, is led to
Cross and inhibit tyrosinase activity, it is possible to reduce the formation of melanin and the effect of reach skin whitening.It is of the present invention containing in
The compact whitening and moistening skin composition of medicine active constituent has stronger tyrosinase activity rejection ability, also has very strong
DPPH free radical scavenging ability, aging and interior free yl are excessive and (or) Scavenging activity decline is closely related, remove in skin
Excessive free radical can inhibit skin aging from source, inhibit the formation of wrinkle, moreover it is possible to and promote the growth of epidermal cell to divide,
Epidermal cell is set to become full, to restore skin younger state.
Preferably, the compact whitening and moistening skin composition also includes active peptides, and the active peptides include oligopeptides -1, glue
At least one of former albumen and silk peptide.
Oligopeptides -1：Also known as epithelical cell growth factor, it is a kind of intracorporal active material of people, the work being made of 53 amino
Property polypeptide, stability is fabulous, is not easy flowing of scattering at normal temperature, and good coordination effect can be formed with enzymes various in human body
It answers.Oligopeptides -1 promotes the Proliferation, Differentiation of cell by the tyrosine phosphorylation of stimulation epidermal growth factor receptor, thus with
The effect of newborn cell replaces aging and dead cell, reaches repairing hyperplasia skin surface cell, promotes epidermal cell to become
Obtain full, recovery younger state.It can also promote collagen growth ability, repair the collagen elastomer of aging fracture,
So being described as " the beautiful factor " by numerous scientists.
Collagen：Collagen is similar to the structure of human skin collagen, contains glycoprotein for non-soluble fiber shape,
It is rich in a large amount of amino acid and hydrophilic group in molecule, there is certain surface-active and good compatibility, simultaneously because its molecule
In contain a large amount of hydroxyl, therefore have fairly good moisture-keeping function；In addition, there are also the tyrosine prevented in skin for collagen
It is converted into the effect of melanin；Therefore it has the effects that pure natural moisturizing, whitening, wrinkle resistant, nti-freckle, can be widely applied to cosmetically
In product.
Silk peptide：It is the catabolite of fibroin, is that natural silk is obtained through hydrolyzing under felicity condition, molecular weight about exists
Between 300~5000.Silk beauty has long history in China, and early in the Ming Dynasty of China, silk has been used as imperial palace highest-ranking imperial concubine's
Beautifying secret recipe, according to《Compendium of Materia Medica》It records:Silk powder can eliminate skin blackspot, treat suppurative dermatitis.Modern study table
It is bright, silk peptide have potent lasting moisture-retaining capacity, secretion that is naturally crease-resistant and promoting collagen, it is potent brighten, anti-UV, anti-hair
Scorching and pock improves the effect of inflammatory wound.
Preferably, the active peptides include the component of following parts by weight：0.00001~0.001 part of oligopeptides -1, glue
0.1~2 part and 0.1~2 part of silk peptide of former albumen.
The skin elasticity that the present invention occurs for skin aging reduces, roughness increases, moisten remitted its fury, wrinkle increases
Situations such as more, pigmentation, color spot increase is guidance, through scientific and reasonable formula with basic theory of tcm, will extract the tight of Chinese medicine
Cause whitening and moistening skin ingredient, with can stimulate skin surface Porcine HGF, repair skin surface cell active peptides at
Point equal science organically combines, and adds basic moisturizing moisturizing ingredient and keep the skin wet and enhance skin moisturizing energy to skin
Power, be made with tender white muscle skin, promote skin growth metabolism, compact anti-wrinkle, senile-resistant efficacy skin care item.
The active peptides ingredient selects three kinds of oligopeptides -1, collagen, silk peptide ingredients to cooperate by said ratio, reaches
To the effect of promoting skin growth, inhibition wrinkle.
Preferably, the compact whitening and moistening skin composition includes the component of following weight percentage：Active ingredient of Chinese herbs
0.2~5%, active peptides ingredient 0.2~4.1%, antioxidant 0.05~1%, emollients 1~25%, moisturizer 5~20%
With emulsifier 0.5~4%.
Preferably, the preparation method of the active ingredient of Chinese herbs is：The raw material of active ingredient of Chinese herbs is used into Extraction solvent
It extracts to get the active ingredient of Chinese herbs；The weight ratio of the raw material and Extraction solvent is：Raw material：Extraction solvent=
1:3~10.
Preferably, the preparation method of the active ingredient of Chinese herbs is：
(a), the raw material of active ingredient of Chinese herbs is added in Extraction solvent, is impregnated 36~72 hours in 25~50 DEG C, filtering,
Up to the active ingredient of Chinese herbs；The weight ratio of the raw material and Extraction solvent is：Raw material：Extraction solvent=1:3~8；
Or (b), by the raw material of active ingredient of Chinese herbs be added in Extraction solvent, 90~105 DEG C are heated to, heat preservation 1.5~3 is small
When, 20~50 DEG C are cooled to, is filtered to get the active ingredient of Chinese herbs；The weight ratio of the raw material and Extraction solvent is：It is former
Material：Extraction solvent=1:5~10；
(a) or (b) in, Extraction solvent be water, glycerol, polyethylene glycol 400, Macrogol 600, n-butanol, acetic acid
At least two in ethyl ester, camellia oil and sesame oil.
Preferably, the Extraction solvent is grouped as by least two groups of following weight percentage：It is water 10~50%, sweet
Oily 30~50%, polyethylene glycol 400 10~50%, Macrogol 600 10~50%, ethyl acetate 1~15%, n-butanol 1
~15%, camellia oil 10~40% and sesame oil 10~40%.
Preferably, the emollients include carbonic acid dioctyl ester, saualane, white oil, cetanol, myristyl myristate,
Shea butter, beeswax, jojoba oil, Sweet Almond Oil, olive oil, Glycerin, mixed triester with caprylic acid capric acid, cetostearyl alcohol, stearyl alcohol, ring-type two
At least one of methyl polysiloxane.
Preferably, the antioxidant includes vitamin E；The moisturizer include glycerol, butanediol, 1,2- propylene glycol,
One of Sodium Hyaluronate, Sensiva SC50,1,2- hexylene glycol and trehalose；The emulsifier includes emulsification monostearate
At least one of the stearic alcohol ether of the stearic alcohol ether/polyoxyethylene (21) of glyceride, polyoxyethylene (2), match Bick 305.
Preferably, the compact whitening and moistening skin composition also includes thickener and preservative；The thickener is described tight
The weight percentage for causing whitening and moistening skin composition is 0.05~2%；The preservative is in the compact whitening and moistening skin composition
Weight percentage be 0.05~0.5%；The thickener includes xanthan gum, ammonium acryloyldime-thyltaurate/VP copolymerization
At least one of object.
It is white and moist comprising the firming skin toner described above containing active ingredient of Chinese herbs that another object of the present invention is to provide a kind of
The skin care item of skin composition, the skin care item are cream, lotion, face cream, Essence or facial mask.
The skin care item are in addition to said components clearly require, in the range of lossless effect of the invention, this field
Technical staff can be added or used to other adjunct ingredients according to specific skin care item dosage form.
The beneficial effects of the present invention are：The compact whitening and moistening skin group containing active ingredient of Chinese herbs that the present invention provides a kind of
Object is closed, the compact whitening and moistening skin composition of the present invention containing active ingredient of Chinese herbs has the suppression of stronger tyrosinase activity
Ability processed also has very strong DPPH free radical scavenging ability, and aging and interior free yl are excessively and (or) under Scavenging activity
Closely related, excessive free radical in removing skin is dropped, the formation of wrinkle can be inhibited, moreover it is possible to promote from source inhibition skin aging
Growth into epidermal cell is divided, and so that epidermal cell is become full, to restore skin younger state.The present invention also provides one
The skin care item of compact whitening and moistening skin composition of the kind containing active ingredient of Chinese herbs.
Specific embodiment
The source of the test material of embodiment：Medicinal material used derives from Hebei along prestige pharmaceutcal corporation, Ltd；Oligopeptides -1
Derived from Guangzhou Guangzhou Ritz-Carlton cosmetics Co., Ltd；Collagen, silk peptide, Sodium Hyaluronate derive from Xi'an rhythm standing grain biology section
Skill Co., Ltd；Vitamin E, shea butter, carbonic acid dioctyl ester derive from German BASF group；Cetanol, oxybenzene third
Ester, methyl hydroxybenzoate, Phenoxyethanol derive from Zhejiang Shengxiao Chemicals Co., Ltd.；Saualane derives from Japanese grease strain formula meeting
Society；White oil comes from Qingdao Sheng En Science and Technology Ltd.；Myristyl myristate, Glycerin, mixed triester with caprylic acid capric acid, Sensiva SC50,1,
2- propylene glycol derives from Linyi Lv Sen Chemical Co., Ltd.；Beeswax derives from Henan Province Changxing apiculture Co., Ltd；Jojoba
Oil derives from He Heba Industrial Co., Ltd；Sweet Almond Oil derives from Germany Henry；Olive oil derives from Spain's bud Linne；Whale
Wax stearyl alcohol derives from Liaoning Huaxing Group Chemical Co., Ltd.；Cyclic dimethyl polysiloxane is public from Dow corning
Department；Glycerol source is in Linyi Lv Sen Chemical Co., Ltd.；Butanediol derives from U.S. OXEA；Trehalose derives from Japanese woods original strain
Formula commercial firm；1,2- hexylene glycol derives from Shantou City Xun Nuo Chemical Industry Science Co., Ltd；Self-emulsifying glycerin monostearate, polyoxy second
The stearic alcohol ether of alkene (2) tristearin alcohol ether/polyoxyethylene (21) derives from He great chemical company of Britain；Acryloyldimethyl taurine
Ammonium/VP copolymer derives from U.S. Ke Laien Co., Ltd；Xanthan gum derives from Shandong You Suo Chemical Industry Science Co., Ltd；It is stearic
Alcohol derives from Thailand cocoanut tree；Bick 305 is matched from France's match Bick；Essence derives from daily chemical essence Co., Ltd.
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
The raw material of a kind of embodiment of active ingredient of Chinese herbs, active ingredient of Chinese herbs described in the present embodiment is as follows：Radix Angelicae Sinensis 25g,
Rhizoma bolbostemmae 35g, safflower 15g, almond 20g, Rhizoma Chuanxiong 10g and polygonum cuspidate 30g.
The preparation method of active ingredient of Chinese herbs described in the present embodiment is as follows：Raw material is mixed, addition is by weight ratio：It is sweet
Oil:Polyethylene glycol 400:Ethyl acetate=50:40:In the Extraction solvent of 10 compositions, impregnated 72 hours at 25~35 DEG C；It is described
The weight ratio of raw material and Extraction solvent is：Raw material：Extraction solvent=1:4, with 200 mesh filter-cloth filterings, obtain active ingredient of Chinese herbs.
Embodiment 2
The raw material of a kind of embodiment of active ingredient of Chinese herbs, active ingredient of Chinese herbs described in the present embodiment is as follows：Radix Angelicae Sinensis 30g,
Rhizoma bolbostemmae 15g, safflower 20g, almond 20g, Rhizoma Chuanxiong 20g and polygonum cuspidate 20g.
The preparation method of active ingredient of Chinese herbs described in the present embodiment is as follows：Raw material is mixed, addition is by weight ratio：It is sweet
Oil:Macrogol 600:N-butanol=60:30:In the Extraction solvent of 10 compositions, impregnated 24 hours at 40~50 DEG C；The original
Material and the weight ratio of Extraction solvent are：Raw material：Extraction solvent=1:8, with 200 mesh filter-cloth filterings, obtain active ingredient of Chinese herbs.
Embodiment 3
The raw material of a kind of embodiment of active ingredient of Chinese herbs, active ingredient of Chinese herbs described in the present embodiment is as follows：Radix Angelicae Sinensis 10g,
Rhizoma bolbostemmae 50g, safflower 5g, almond 10g, Rhizoma Chuanxiong 10g and polygonum cuspidate 15g.
The preparation method of active ingredient of Chinese herbs described in the present embodiment is as follows：Raw material is mixed, addition is by weight ratio：It is sweet
Oil:Camellia oil:Water:Ethyl acetate=50:30:16:In the Extraction solvent of 4 compositions, impregnated 36 hours at 30~40 DEG C；It is described
The weight ratio of raw material and Extraction solvent is：Raw material：Extraction solvent=1:5, with 200 mesh filter-cloth filterings, obtain active ingredient of Chinese herbs.
Embodiment 4
The raw material of a kind of embodiment of active ingredient of Chinese herbs, active ingredient of Chinese herbs described in the present embodiment is as follows：Radix Angelicae Sinensis 20g,
Rhizoma bolbostemmae 25g, safflower 10g, almond 20g, Rhizoma Chuanxiong 10g and polygonum cuspidate 40g.
The preparation method of active ingredient of Chinese herbs described in the present embodiment is as follows：Raw material is mixed, addition is by weight ratio：Water:
Polyethylene glycol 400:Glycerol=45:15:In the Extraction solvent of 40 compositions, 90~105 DEG C are heated to, 2 hours is kept the temperature, is cooled to 30
~40 DEG C, the weight ratio of the raw material and Extraction solvent is：Raw material：Extraction solvent=1:5, with 200 mesh filter-cloth filterings, obtain Chinese medicine
Active constituent.
Embodiment 5
A kind of skin care item embodiment of the compact whitening and moistening skin composition comprising described containing active ingredient of Chinese herbs, the present embodiment
The skin care item are face cream, and face cream described in the present embodiment includes the component of following weight percentage：
A phase component：Carbonic acid dioctyl ester 2.0%, saualane 3.0%, white oil 3.0%, cetanol 3.0%, myristic acid meat
Cardamom ester 4.0%, shea butter 3.0%, vitamin E 0.1%, self-emulsifying glycerin monostearate 3.0% and Nipasol
0.1%；
B phase component：Active ingredient of Chinese herbs 1.5%, the glycerol 5.0%, butanediol 5.0%, hyaluronic acid of the preparation of embodiment 1
Sodium 0.5% and methyl hydroxybenzoate 0.1%；
C phase component：Oligopeptides -1 0.0001%, collagen 0.5% and silk peptide 0.5%；
Essence 0.02%；
Surplus is water.
The preparation method of face cream described in the present embodiment includes the following steps：
(1) B phase component is added into appropriate purified water, is dissolved by heating respectively with A phase component completely, and respectively at 80~85 DEG C
Constant temperature disinfection 30 minutes；
(2) appropriate purified water stirring and dissolving is added in C phase component, using 0.22 μm of sterilised membrane filter filtration sterilization；
(3) the A phase and B phase are stirred, speed of agitator 960rpm in emulsion pot, is uniformly mixed, at 80 DEG C
Emulsifying 10 minutes, homogeneous revolving speed was 3000rpm, started to cool down after the completion of homogeneous, be added when temperature is down to 40 DEG C C phase,
Essence is uniformly mixed, is cooled to 35 DEG C to get the face cream.
Embodiment 6
A kind of skin care item embodiment of the compact whitening and moistening skin composition comprising described containing active ingredient of Chinese herbs, the present embodiment
The skin care item are eye cream, and eye cream described in the present embodiment includes the component of following weight percentage：
A phase component：Carbonic acid dioctyl ester 2.0%, olive oil 3.0%, beeswax 2.5%, jojoba oil 1.0%, cetearyl alcohol
Alcohol 3.0%, myristyl myristate 2.0%, vitamin E 0.5%, ammonium acryloyl taurate/VP copolymer
1.0% and self-emulsifying glycerin monostearate 3.0%；
B phase component：Active ingredient of Chinese herbs 1.0%, the butanediol 5.0%, Sodium Hyaluronate 0.5%, second of the preparation of embodiment 1
Base hexyl glycerol 0.3%, 1,2- hexylene glycol 0.5% and Phenoxyethanol 0.2%；
C phase component：Oligopeptides -1 0.0005%, collagen 1.0% and silk peptide 1.0%；
Essence 0.01%；
Surplus is water.
The preparation method of eye cream described in the present embodiment comprises the steps of：
(1) B phase component is added into appropriate purified water, is dissolved by heating respectively with A phase component completely, and the constant temperature at 85 DEG C respectively
Disinfection 30 minutes；
(2) appropriate purified water stirring and dissolving is added in C phase component, using 0.22 μm of sterilised membrane filter filtration sterilization；
(3) the A phase and B phase are stirred, speed of agitator 960rpm in emulsion pot, is uniformly mixed, at 80 DEG C
Emulsifying 10 minutes, homogeneous revolving speed was 3000rpm, starts to cool down after the completion of homogeneous, starts to cool down, when temperature is down to 40 DEG C
C phase, essence is added, is uniformly mixed, is cooled to 35 DEG C to get the eye cream.
Embodiment 7
A kind of skin care item embodiment of the compact whitening and moistening skin composition comprising described containing active ingredient of Chinese herbs, the present embodiment
The skin care item are lotion, and lotion described in the present embodiment includes the component of following weight percentage：
A phase component：Sweet Almond Oil 5.0%, jojoba oil 2.0%, Glycerin, mixed triester with caprylic acid capric acid 3%, stearyl alcohol 1.0%, ring-type
Dimethyl polysiloxane 1.0%, vitamin E 0.1%, ammonium acryloyl taurate/VP copolymer 0.2%, polyoxyethylene
(2) the stearic alcohol ether 2.0% of stearic alcohol ether/polyoxyethylene (21), match Bick 305 0.5% and Nipasol 0.1%；
B phase component：The active ingredient of Chinese herbs 0.5% of the preparation of embodiment 1,1,2- propylene glycol 5.0%, glycerol 5.0%, seaweed
Sugar 3.0%, Sodium Hyaluronate 0.2% and methyl hydroxybenzoate 0.1%；
C phase component：Oligopeptides -1 0.00005%, collagen 0.1% and silk peptide 0.1%；
Essence 0.02%；
Surplus is water.
The preparation method of lotion described in the present embodiment comprises the steps of：
(1) B phase component is added into appropriate purified water, is dissolved by heating respectively with A phase component completely, and the constant temperature at 85 DEG C respectively
Disinfection 30 minutes；
(2) appropriate purified water stirring and dissolving is added in C phase component, using 0.22 μm of sterilised membrane filter filtration sterilization；
(3) the A phase and B phase are stirred, speed of agitator 960rpm in emulsion pot, is uniformly mixed, at 80 DEG C
Emulsifying 15 minutes, homogeneous revolving speed was 3000rpm, starts to cool down after the completion of homogeneous, starts to cool down, when temperature is down to 40 DEG C
C phase, essence is added, is uniformly mixed, is cooled to 35 DEG C to get the lotion.
Embodiment 8
A kind of skin care item embodiment of the compact whitening and moistening skin composition comprising described containing active ingredient of Chinese herbs, the present embodiment
The skin care item are Essence, and Essence described in the present embodiment includes the component of following weight percentage：
A phase component：Saualane 1.0%, vitamin E 0.2%, self-emulsifying glycerin monostearate 0.5% and Nipasol
0.1%；
B phase component：Active ingredient of Chinese herbs 2.0%, the butanediol 5.0%, glycerol 5.0%, trehalose of the preparation of embodiment 1
4.0%, Sodium Hyaluronate 1.0%, xanthan gum 0.2%, Phenoxyethanol 0.2% and methyl hydroxybenzoate 0.1%；
C phase component：Oligopeptides -1 0.001%, collagen 2% and silk peptide 2%；
Essence 0.01%；
Surplus is water.
The preparation method of Essence described in the present embodiment comprises the steps of：
(1) B phase component is added into appropriate purified water, is dissolved by heating respectively with A phase component completely, and the constant temperature disinfection at 85 DEG C
30 minutes；
(2) appropriate purified water stirring and dissolving is added in C phase component, using 0.22 μm of sterilised membrane filter filtration sterilization；
(3) the A phase and B phase are stirred, speed of agitator 960rpm in emulsion pot, is uniformly mixed, at 80 DEG C
Emulsifying 5 minutes, homogeneous revolving speed was 2500rpm, starts to cool down after the completion of homogeneous, and C phase, perfume (or spice) are added when temperature is down to 40 DEG C
Essence is uniformly mixed, is cooled to 35 DEG C to get the Essence.
Embodiment 9
A kind of skin care item embodiment of the compact whitening and moistening skin composition comprising described containing active ingredient of Chinese herbs, the present embodiment
The skin care item are facial mask, and the component of facial mask described in the present embodiment is same as Example 8, and preparation method is to be immersed in face paper
In Essence described in 25~30mL embodiment 8 to get.
Comparative example 1
The raw material of active ingredient of Chinese herbs described in this comparative example is the same as embodiment 1.
The preparation method of active ingredient of Chinese herbs described in this comparative example is as follows：Raw material is mixed, purified water is added, it is small to decoct 2
When；The weight ratio of the raw material and purified water is：Raw material：Purified water=1:4, stop heating, is cooled to 30-40 DEG C, the filter of 200 mesh
Cloth filtering, obtains the active ingredient of Chinese herbs.
Comparative example 2
The difference that the difference is that only B phase component of face cream described in this comparative example and embodiment 5, in this comparative example, B phase
Group is divided into：Active ingredient of Chinese herbs 1.5%, the glycerol 5.0%, butanediol 5.0%, 0.5% and of Sodium Hyaluronate of the preparation of comparative example 1
Methyl hydroxybenzoate 0.1%.
The preparation method of face cream described in this comparative example is the same as embodiment 5.
Comparative example 3
The difference that the difference is that only B phase component of face cream described in this comparative example and embodiment 5, in this comparative example, B phase
Group is divided into：Glycerol 5.0%, butanediol 5.0%, Sodium Hyaluronate 0.5% and methyl hydroxybenzoate 0.1%.
The preparation method of face cream described in this comparative example is the same as embodiment 5.
Embodiment 10
The detection of physical and chemical index is tested：
1, sample
Using sample obtained by the embodiment of the present invention 5~8, comparative example 2,3 as test specimen.
2, test method
(1) pH value measures：According to GB/T13531.1, sample 1g is taken, 9g ultrapure water is added, is heated to 40 DEG C, stirring is equal
It is even, it is cooled to room temperature, pH meter measures pH.
(2) heat-resistant stability：By sample be placed in 40 ± 1 DEG C keep 24 hours, restore room temperature after visual observations character whether there is or not
It is obvious abnormal.
(3) resist cold stability：Sample is placed in -10~-5 DEG C to be kept for 24 hours, there is visual observations character after restoring room temperature
Non Apparent Abnormality.
3, test result：
The measurement of physical and chemical index, concrete outcome are as shown in table 1.
1 embodiment 5~8 of table, the physical and chemical index testing result of comparative example 2,3
It is above-mentioned the experimental results showed that, embodiment 5~8 and comparative example 2,3 preparation-obtained sample stable in physicochemical property.
Embodiment 11
The test inhibited tyrosinase activity：
1, prepared by test solution
Using sample obtained by the embodiment of the present invention 1~5, comparative example 1~3 as test specimen.
Examples 1 to 4,1 test specimen 0.2g of comparative example or so are measured respectively, use the PBS buffer solution of pH 6.8 respectively
It is settled in 20mL volumetric flask, mixes, obtain each test sample mother liquor；Each test sample mother liquor 1mL or so is taken, respectively with pH's 6.8
PBS buffer solution is settled in 20mL volumetric flask, is mixed to get embodiment 1-3, each test solution of comparative example 1.
Embodiment 5, comparative example 2,3 test specimen 1g or so are weighed respectively, use the PBS buffer solution constant volume of pH 6.8 respectively
It into 20mL volumetric flask, mixes, ultrasonic extraction 5~10 minutes, is filtered with 0.22 μm of sterilised membrane filter, filtrate is embodiment 5, right
Each test solution of ratio 2,3.
2, test method
Test sample solution is drawn, is added in reaction tube by 2 method of table, obtains 4 groups of reaction solutions of C1, C2, T1, T2,
3 groups of parallel tests of every group of setting, shaking are uniformly mixed, and set 37 DEG C of water-bath insulation reactions 10 minutes, then in each test tube respectively
Tyrosinase solution is added, is reacted 5 minutes in 37 DEG C, is measured at 475nm with spectrophotometer immediately after clock reaction
The absorbance value of each sample reaction solution, is denoted as AC1、AC2、AT1、AT2。
2 reaction solution of table composition
3, test result
The inhibiting rate to tyrosinase is calculated as follows：
Tyrosinase inhibition rate %=[1- (AT1-AT2)/(AC1-AC2)] × 100%
AT1-AT2：Sample solution absorbance value changes；
AC1-AC2：Blank control absorbance value changes.
The test inhibited tyrosinase activity, concrete outcome are as shown in table 3.
The tyrosinase inhibition rate measurement result of 3 the embodiment of the present invention 1~5 of table, comparative example 1~3
Test result shows：Examples 1 to 5 group has stronger tyrosinase activity rejection ability, and inhibiting rate is high
In comparative example group；Tyrosinase is the major rate-limiting enzyme in melanin forming process, and the sample of Examples 1 to 5 group can pass through suppression
Tyrosinase activity processed, the effect of reducing the formation of melanin and reach skin whitening.And use active Chinese drug component of the present invention
The tyrosinase activity inhibitory effect of active ingredient of Chinese herbs made from the preparation method of ingredient is more preferably.
Embodiment 12
The test of scavenging ability of DPPH free radical measurement：
1, prepared by test solution
Using sample obtained by the embodiment of the present invention 1~5, comparative example 1~3 as test specimen.
Examples 1 to 4,1 test specimen 0.2g of comparative example or so are measured respectively, are settled to 20mL volumetric flask with DMSO respectively
In, it mixes, obtains each test sample mother liquor；Each test sample mother liquor 0.5mL or so is taken, is settled in 20mL volumetric flask with DMSO respectively,
It mixes to get Examples 1 to 4, each test solution of comparative example 1.
Embodiment 5, comparative example 2,3 test specimen 0.5g or so are weighed respectively, are settled in 20mL volumetric flask with DMSO, are mixed
Even each test solution to get embodiment 5, comparative example 2,3.
2, test method
10 each test solutions of μ L are taken to be put into 96 hole elisa Plates respectively, 150 μM of DPPH- ethyl alcohol for adding 90 μ L is molten
Liquid mixes, and places at room temperature after ten minutes, and sample absorbance is measured under 512nm wavelength and is denoted as A；10 μ L each sample are respectively taken respectively
The ethanol solution that 90 μ L are added in solution mixes, and is measured in the same method sample absorbance and is denoted as B；It is added 90 μ L's in DMSO with 10 μ L of method
150 μM of DPPH- ethanol solution mixes, and is measured in the same method sample absorbance and is denoted as A1。
3, test result：
Sample is calculated as follows to the removing percentage of DPPH：
To removing percentage=[A of DPPH1-(A-B)]/A1× 100%
Clearance rate is calculated according to formula above.Radical scavenging activities testing result is shown in Table 4.
The clearance rate measurement result to DPPH of 4 the embodiment of the present invention 1~5 of table, comparative example 1~3
Test result shows：Examples 1 to 5 group has stronger DPPH free radical scavenging ability, and clearance rate is above comparison
Example group.Aging and interior free yl are excessive and (or) Scavenging activity decline is closely related, and Examples 1 to 5 group sample has very
Strong DPPH free radical scavenging ability, can remove free radical excessive in skin, inhibit skin aging from source, inhibit wrinkle
It is formed.
Embodiment 13
Using effect test：
1, sample
Using sample obtained by the embodiment of the present invention 5 as test specimen.
2, test method
Choose subject 5, women, the age between 30-50 year old, skin there are different degrees of skin of face drying,
Dull pitch-dark, face/eye part skin relaxation or face/eye have a wrinkle phenomenon, after daily face cleaning, coat this on facial skin
Face cream prepared by inventive embodiments 5 is appropriate, once in the morning and once at night；Continuous use 30 days.Its use feeling, dermatoglyph are evaluated after 30 days
Situation.
3, test result
Evaluation criterion：Use feeling is experienced by volunteer's readme；Skin colour, texture situation pass through the intuitive observation of naked eyes.
Wherein, effectively it is：It visually observes facial skin obviously to bleach, texture obviously attenuates greasy, and microgroove significantly reduces and deep line shoals；One
As be：It visually observes skin slightly to bleach, texture is slightly shoaled, reduced than wrinkle before testing, but is reduced unobvious；In vain：
It is not any change before skin colour, texture and experiment.
Test result is shown in Table 5.
Compact whitening and moistening skin face cream of the table 5 containing active ingredient of Chinese herbs tries out table
As can be known from the results of Table 5, after using compact whitening and moistening skin face cream 30 days containing active ingredient of Chinese herbs, most people
Use feeling is good；And fine and smooth, the water profit that can obviously make that skin and muscles are fair, skin pattern can be improved；There is no an example allergy, skin occur not
Phenomena such as suitable.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of compact whitening and moistening skin composition containing active ingredient of Chinese herbs, which is characterized in that include active ingredient of Chinese herbs, institute
State the extract that active ingredient of Chinese herbs is the raw material comprising following parts by weight：5~20 parts of safflower, 10~30 parts of almond, Rhizoma Chuanxiong
10~20 parts, 10~30 parts of Radix Angelicae Sinensis, 15~50 parts of the rhizoma bolbostemmae and 15~40 parts of polygonum cuspidate.
2. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as described in claim 1, which is characterized in that described compact
Whitening and moistening skin composition also includes active peptides, and the active peptides include at least one in oligopeptides -1, collagen and silk peptide
Kind；Preferably, the active peptides include the component of following parts by weight：0.00001~0.001 part of oligopeptides -1, collagen
0.1~2 part and 0.1~2 part of silk peptide.
3. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 2, which is characterized in that described compact
Whitening and moistening skin composition includes the component of following weight percentage：Active ingredient of Chinese herbs 0.2~5%, active peptides ingredient 0.2
~4.1%, antioxidant 0.05~1%, emollients 1~25%, moisturizer 5~20% and emulsifier 0.5~4%.
4. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as described in claim 1, which is characterized in that the Chinese medicine is living
The preparation method of property ingredient is：The raw material of active ingredient of Chinese herbs is extracted using Extraction solvent to get the active Chinese drug component
Ingredient；The weight ratio of the raw material and Extraction solvent is：Raw material：Extraction solvent=1:3~10.
5. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 4, which is characterized in that the Chinese medicine
The preparation method of active constituent is：
(a), the raw material of active ingredient of Chinese herbs is added in Extraction solvent, is impregnated 36~72 hours in 25~50 DEG C, filtering to get
The active ingredient of Chinese herbs；The weight ratio of the raw material and Extraction solvent is：Raw material：Extraction solvent=1:3~8；
Or (b), by the raw material of active ingredient of Chinese herbs be added in Extraction solvent, 90~105 DEG C are heated to, keeps the temperature 1.5~3 hours,
20~50 DEG C are cooled to, is filtered to get the active ingredient of Chinese herbs；The weight ratio of the raw material and Extraction solvent is：Raw material：
Extraction solvent=1:5~10；
(a) or (b) in, Extraction solvent be water, glycerol, polyethylene glycol 400, Macrogol 600, n-butanol, ethyl acetate,
At least two in camellia oil and sesame oil.
6. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 5, which is characterized in that the extraction
Solvent is grouped as by least two groups of following weight percentage：Water 10~50%, glycerol 30~50%, polyethylene glycol 400
10~50%, Macrogol 600 10~50%, ethyl acetate 1~15%, n-butanol 1~15%, 10~40% and of camellia oil
Sesame oil 10~40%.
7. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 3, which is characterized in that described soft and moist
Agent include carbonic acid dioctyl ester, saualane, white oil, cetanol, myristyl myristate, shea butter, beeswax, jojoba oil,
Sweet Almond Oil, olive oil, Glycerin, mixed triester with caprylic acid capric acid, cetostearyl alcohol, stearyl alcohol, at least one in cyclic dimethyl polysiloxane
Kind.
8. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 3, which is characterized in that the antioxygen
Agent includes vitamin E；The moisturizer include glycerol, butanediol, 1,2- propylene glycol, Sodium Hyaluronate, Sensiva SC50,
One of 1,2- hexylene glycol and trehalose；The emulsifier includes emulsification glycerin monostearate, polyoxyethylene (2) stearyl alcohol
At least one of ether/polyoxyethylene (21) tristearin alcohol ether, match Bick 305.
9. the compact whitening and moistening skin composition containing active ingredient of Chinese herbs as claimed in claim 3, which is characterized in that described compact
Whitening and moistening skin composition also includes thickener and preservative；Weight hundred of the thickener in the compact whitening and moistening skin composition
Dividing content is 0.05~2%；The preservative the compact whitening and moistening skin composition weight percentage be 0.05~
0.5%；The thickener includes at least one of xanthan gum, ammonium acryloyl taurate/VP copolymer.
10. a kind of compact whitening and moistening skin composition comprising described in any one of claim 1~9 containing active ingredient of Chinese herbs
Skin care item, the skin care item are cream, lotion, face cream, Essence or facial mask.
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