CN108821921A - A kind of capsicum specially imitates slow-release compound fertilizer and preparation method thereof - Google Patents
A kind of capsicum specially imitates slow-release compound fertilizer and preparation method thereof Download PDFInfo
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- CN108821921A CN108821921A CN201810982454.1A CN201810982454A CN108821921A CN 108821921 A CN108821921 A CN 108821921A CN 201810982454 A CN201810982454 A CN 201810982454A CN 108821921 A CN108821921 A CN 108821921A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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Abstract
The invention discloses a kind of capsicums specially to imitate slow-release compound fertilizer and preparation method thereof, and the capsicum specially imitates slow-release compound fertilizer, including following raw material:Urea, ammonium hydrogen carbonate, kainite, fermentation pig manure, fermentation leached tea oil slag, biogas residue, bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, vinegar grain, gangue, sustained release agent, soil conditioner, 1,3- butanediol, it is manufactured after everfermentation, filtering and concentrating dehydration, being granulated that the capsicum, which specially imitates slow-release compound fertilizer,.The utilization rate that capsicum of the invention specially imitates the fertilizer of slow-release compound fertilizer is high, and fertilizer injected volume is low, reduces costs.
Description
【Technical field】
The invention belongs to the preparation technical fields of fertilizer, and in particular to a kind of capsicum specially imitates slow-release compound fertilizer and its preparation side
Method.
【Background technique】
Chinese agriculture problems faced is severeer, and the status having a large population in a small area cannot take on a new look for a long time, to meet the people's
Chemical fertilizer is often largely applied in life requirement, China's agricultural production, and China produces and consumed the chemical fertilizer in the world 1/3, fertilizer efficiency at present
Utilization rate is low, be easy to cause pollution of area source, and wherein vegetables production is even more to need to consume a large amount of fertilizer, and capsicum is currently China first
Big cultivated area vegetables, play an important role, the important industry that even more many areas are shaken off poverty and set out on the road to prosperity in national life.Although city
There are many three element compound fertilizers to sell on, but specific aim is not strong, is unable to satisfy chili growth, or causes the mistake of certain element
Amount is lost and wastes, while increasing with the Chinese aged, and labour is reduced, especially Hunan mountain farming, Out-migrant for work
Personnel are more, and development is suitble to light simplified cultivation single fertilization technology to seem especially urgent.Therefore, only according to different geographical soil
The region that the optimization that earth, weather and crop feature carry out fertilizer formula could enhance fertilizer is applicable in effect, effectively solves local agriculture
Problems in industry fertilising.Development is suitble to the slow special release fertilizer of light simplified cultivation, improves contribution of the fertilizer to agricultural volume increase
Rate, it is particularly significant.
Capsicum dedicated biomass charcoal slow-release fertilizer is on the basis of capsicum nutritive peculiarity research, in conjunction with great number tested data
A kind of special complex fertilizer made of exploitation is augmented further according to local fertilizer provision from soil situation and required target output in use process
Straight fertilizer, can meet the needs of crop is to nutrient to the maximum extent, and balance nutrient supply improves utilization rate of fertilizer, effectively drops
The low nutrient loss because of caused by unreasonable fertilising reduces production cost, when can also solve peasant household and voluntarily preparing, part simple substance fertilizer
Material is not easy to buy, is formulated the problems such as inaccurate, arbitrariness is also big.And capsicum profession compound fertilizer currently on the market is when in use,
Nutriment is unable to satisfy the demand actually planted by the efficiency of Absorption By Hot Pepper Plant.
A kind of Chinese patent application document " composite slow-release fertilizer (application publication number for improving yield of hot pepper:
CN107778111A a kind of composite slow-release fertilizer for improving yield of hot pepper) " is disclosed, raw material includes by weight：A great number of elements
It 80-90 parts of fertilizer, 26-34 parts of fermentation pig manure, ferments leached tea oil slag 15-24 parts, 10-20 parts of biogas residue, 2-4 parts of bamboo charcoal powder, cinder 1-2
Part, 1-2 parts of vermiculite power, 0.2-0.8 parts of sepiolite powder, 0.2-1.2 parts of zinc borate, 0.5-1.5 parts of diatomite, 1-2 parts of quartz sand,
5-10 parts of sustained release agent.Sustained release agent includes by weight：2-4 parts of lotus root starch, 1-2 parts of locust bean gum, 2-4 parts of antibacterial coating agent.Antibacterial
Coating agent is prepared using following technique：By chitosan, fibroin, formic acid solution stirring, silver nitrate is added and continues to stir, is added
Glutaraldehyde is crosslinked to obtain antibacterial coating agent.The capsicum pungent for obtaining plantation is moderate, in good taste, it is ensured that the survival rate of capsicum
And growth efficiency, but during pepper planting, capsicum is low to the utilization rate of fertilizer, causes fertilizer injected volume big, at high cost.
【Summary of the invention】
The present invention provides a kind of capsicum and specially imitates slow-release compound fertilizer and preparation method thereof, to solve in Chinese patent application document
A kind of " composite slow-release fertilizer (application publication number for improving yield of hot pepper:CN107778111A utilization of the capsicum disclosed in) " to fertilizer
Rate is low, and fertilizer injected volume is big, problem at high cost.
In order to solve the above technical problems, the present invention uses following technical scheme:
A kind of capsicum specially imitates slow-release compound fertilizer, including following raw material：Urea, ammonium hydrogen carbonate, kainite, fermentation pig manure, hair
Ferment leached tea oil slag, bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, vinegar grain, gangue, delays biogas residue
Release agent, soil conditioner, 1,3 butylene glycol；
Sustained release agent, as unit of parts by weight, including following raw material：4-8 parts of diammonium hydrogen phosphate, 3-6 parts of lignin, bentonite
6-12 parts, 4-8 parts of polyethylene glycol, 2-5 parts of rice bran wax, 6-9 parts of ethyl acetate, 1-4 parts of chitosan, silane coupling agent KH-5602-
5 parts.
Soil conditioner, as unit of parts by weight, including following raw material：10-20 parts of cinder, mass fraction 15-25%
4-8 parts of ferric chloride solution, 3-9 parts of urea, 2-5 parts of sodium hydroxide, 1-4 parts of diatomite, 3-6 parts of salicylic acid, potassium peroxydisulfate 2-4
Part, 3-9 parts of polylactic acid, 2-5 parts of Silane coupling reagent KH-570；
The vinegar grain, gangue, sustained release agent, soil conditioner, 1,3 butylene glycol weight ratio be (10-20)：(8-12)：
(6-8)：(4-6)：(1-3).
Further, the vinegar grain, gangue, sustained release agent, soil conditioner, 1,3-BDO weight ratio be 15.2：
10.3：7.1：5.3：2.1.
Further, as unit of parts by weight, including following raw material：20-40 parts of urea, 12-16 parts of ammonium hydrogen carbonate, potassium rush down
4-8 parts of salt, 3-9 parts of fermentation pig manure, fermentation leached tea oil slag 2-8 parts, 3-6 parts of biogas residue, 4-8 parts of bamboo charcoal powder, 3-6 parts of cinder, vermiculite power
2-5 parts, 1-5 parts of sepiolite powder, 4-8 parts of zinc borate, 3-9 parts of diatomite, 2-6 parts of quartz sand, 10-20 parts of vinegar grain, gangue 8-
12 parts, 6-8 parts of sustained release agent, 4-6 parts of soil conditioner, 1-3 parts of 1,3 butylene glycol.
Further, sustained release agent is prepared by following technique：Diammonium hydrogen phosphate, lignin and bentonite are mixed equal
It is even, it is warming up to 60-80 DEG C, keeps the temperature 10-20min, polyethylene glycol is subsequently added into and rice bran wax is uniformly mixed, in 350-650r/min
Revolving speed stirs 20-30min, and then the dry 20-40min in -30~-50 DEG C of freeze driers, it is mixed to be subsequently added into ethyl acetate
It closes uniformly, stirs 10-20min in 4500-5500r/min revolving speed, chitosan and silane coupling agent KH-560 mixing is then added
Uniformly, 3-5h then is stirred in 250-350r/min revolving speed, is then collected by centrifugation in 8500-12000r/min revolving speed, after washing
Freeze-drying obtains sustained release agent.
Further, soil conditioner is prepared by following technique：It is dried after cinder is washed, quality point is then added
Number be 15-25% ferric chloride solutions be uniformly mixed, in 80-100 DEG C of heating water bath 8-12h, be cooled to room temperature, then spend from
Sub- water washing is then warming up to 250-350 DEG C of calcining 4-6h, and grinding obtains material A after being cooled to room temperature；By material A, urea,
Sodium hydroxide, diatomite, salicylic acid, potassium peroxydisulfate, polylactic acid and Silane coupling reagent KH-570 are uniformly mixed, in 65-75 DEG C of perseverance
4-6h is stirred with 280-320r/min revolving speed in tepidarium, is then cooled to room temperature, suction filtration obtains sediment, then by sediment
In 45-55 DEG C of dry 44-52h, it is cooled to room temperature to obtain soil conditioner.
A kind of capsicum proposed by the present invention specially imitates the preparation method of slow-release compound fertilizer, includes the following steps：
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding,
Then material a is obtained after crossing 100-200 mesh sieve, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure mixing are added into material a
Uniformly, it in 30-40 DEG C of fermentation 10-20d, is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 50-60 DEG C, then by material c in
90-105 DEG C of drying obtains material d to water content≤6%；
S3, into material d, addition urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol are mixed
It closes uniformly, is warming up to 60-70 DEG C, keep the temperature 2-3h, stir 1-2h in 650-850r/min revolving speed, 20-40 mesh is made through pelletizer
Granular capsicum specially imitates slow-release compound fertilizer.
The invention has the advantages that:
(1) by the data of embodiment 1-3 and comparative example 7 as it can be seen that application embodiment 1-3 capsicum specially imitates slow-release compound fertilizer plantation
Capsicum, growth rate and survival rate significantly improve；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimal implementation
Example.
(2) by embodiment 1 and the data of comparative example 1-6 as it can be seen that vinegar grain, gangue, sustained release agent, soil conditioner, 1,3-
Butanediol specially imitates in slow-release compound fertilizer in preparation capsicum and plays synergistic effect, and collaboration improves capsicum and specially imitates slow-release compound fertilizer
Utilization of nutrients, this may be：
1) gangue is the solid waste discharged during coal mining process and coal washing, be one kind in coalification course with coal seam
A kind of lower, harder than the coal black and gray rock of phosphorus content of association not only has excellent absorbent properties, and as base fertilizer
Major ingredient its with excellent environmental-protecting performance, it is degradable, and the unsaturated bond on its surface can provide for hydrophily water-absorbent material
Binding site realizes the unsaturated side chain on gangue surface and sustained release auxiliary agent, soil conditioner and degradable release-controlled fills out
Material combines, and reinforcement the efficiency slow release performance of gangue, the nutriment and Fungicidal substance realized in base fertilizer obtain efficiently
It is abundant to realize the soil nutrient before capsicum seeding and seedling raising for release, and harmful bacteria is few, improves the survival rate and growth effect of seed
Rate.
2) diammonium hydrogen phosphate, lignin and bentonite are uniformly mixed, are kept the temperature after heating, be subsequently added into polyethylene glycol and rice
Chaff wax is uniformly mixed, stirring, then dry in freeze drier, is subsequently added into ethyl acetate mixing, and it is poly- that shell is then added
Sugar and silane coupling agent KH-560 are uniformly mixed, and are followed by stirring for, are then centrifuged for collecting, and freeze-drying obtains sustained release agent after washing.
It buffers filler using lignin and bentonite as porosity, and since lignin and bentonite surface area are big, hole is more, and surface
Hydroxy radical content it is high；Using chitosan as initiator, using silane coupling agent KH-560 as grafting agent, with ethyl acetate, poly- second
Two pure and mild rice bran waxs are realized as organic moulding material by the unsaturated bond on organic moulding material surface and lignin and swollen
Moisten the hydroxy combining on native surface, and under the action of swelling agent diammonium hydrogen phosphate, lignin and bentonite is furthermore achieved
The expansion of volume further increases the gap of sustained release agent after molding, improves cushion performance, wherein in chitosan macromolecular
There are active hydroxyl and amino, they have stronger chemical reaction ability, contain amino in dissolved solution, can pass through
In conjunction with negative electron the respiratory system of bacterium is destroyed, to realize the effect for inhibiting bacterial growth；Polylactic acid surface contains
There are the strongly hydrophilics groups such as carboxyl and hydroxyl abundant, good biocompatibility is degradable, and has porosity, in 1,3- fourth two
Under the grafting effect of alcohol, in conjunction with the unsaturated bond on gangue surface, act on bacterium surface makes carefully the hydroxyl on polylactic acid surface
The respiratory enzyme of bacterium inactivates, and kills bacterium to realize, it is excellent to impart the reinforcement system using the antibiotic and sterilizing of polylactic acid
Antibacterial reinforcing property；Lignin is as binder, it can be achieved that gangue, sustained release auxiliary agent, soil conditioner, polylactic acid, shell are poly-
Sugar combines stronger between each other, and collective effect is realized in base fertilizer to the height of nutriment in base fertilizer and antibacterial material
Imitate slow releasing function.Simultaneously by the unsaturated bond on a large amount of hydroxyl in sustained release agent surface and gangue surface 1,3 butylene glycol grafting
Combination is realized under effect, so that the cushion performance of modified sustained release agent be applied in the base fertilizer, realize in base fertilizer nutrient and
The efficient release of antibacterial material improves the survival rate and growth rate of capsicum.
3) then soil conditioner is added ferric chloride solution and is uniformly mixed to dry after washing cinder, in heating water bath,
It is cooled to room temperature, is then washed with deionized, then heating calcining, grinding obtains material A after being cooled to room temperature；By material A,
Urea, sodium hydroxide, diatomite, salicylic acid, potassium peroxydisulfate, polylactic acid and Silane coupling reagent KH-570 are uniformly mixed, thermostatted water
It stirs, then cools to room temperature in bath, suction filtration obtains sediment, then by drying precipitate, is cooled to room temperature to obtain, with coal
Slag supplements minerals and micro member in soil using cinder minerals rich in and microelement as basic substance
Element, and due to cinder and diatomite surface hydroxyl rich in, under the initiation of potassium peroxydisulfate, realize salicylic acid and
The unsaturated bond on ethyl acetate surface Silane coupling reagent KH-570 graft modification effect under with cinder and diatomite surface hydroxyl
The combination of base, and by addition ferric chloride solution, urea and sodium hydroxide, further supplemented with ferro element, nitrogen and sodium member
Element has advanced optimized soil regulating effect；Due to obtaining its surface of soil conditioner as porous structure, and hydroxyl rich in
Base is realized in conjunction with gangue surface hydroxyl, the further reinforcement soil of gangue under the grafting effect of 1,3-BDO
Adjustment effect applies in the base fertilizer, can guarantee that base fertilizer in extra-nutrition elemental basis, is realized to soil trace element
Supplement is adjusted, and the balance of the elements such as optimization soil N P, K improves the growth efficiency and survival rate of capsicum.
(3) by the data of comparative example 8-10 as it can be seen that during pepper cultivation, in S1 in base fertilizer raw material, vinegar grain, gangue,
Sustained release agent, soil conditioner, 1,3 butylene glycol weight ratio not at (10-20)：(8-12)：(6-8)：(4-6)：(1-3) range
When interior, after carrying out pepper cultivation using pepper cultivation method, the number of the growth rate of capsicum and the numerical value of survival rate and embodiment 1-3
Value is very different, suitable with the numerical value of the prior art (comparative example 7) much larger than the numerical value of embodiment 1-3.It is controlled in embodiment 1-3
Vinegar grain in slow-release compound fertilizer, gangue, sustained release agent, soil is specially imitated using capsicum of the invention during pepper cultivation processed to adjust
Agent, 1,3-BDO reinforcement system, weight ratio adjust be respectively (10-20)：(8-12)：(6-8)：(4-6)：(1-3), can benefit
With the degradability of gangue, slow release and its unsaturated bond abundant, with superior sustained-release sustained release auxiliary agent and
Soil conditioner and aceticanhydride cooperation with excellent soil regulating power are realized under the graft modification effect of 1,3-BDO
The combination of hydroxyl and gangue surface unsaturated bond, imparts the excellent sustained release of gangue in modified sustained release agent and soil conditioner
Property and anti-microbial property, and polylactic acid and chitosan be as containing active hydroxyl and amino in chitosan macromolecular, in molecule, tool
There is stronger chemical reaction ability, it can be by combining negative electron to destroy the respiratory system of bacterium, to realize inhibition
The effect of bacterium；The strongly hydrophilics group such as a large amount of carboxyl and hydroxyl, and good biocompatibility are contained in polylactic acid surface, can drop
Solution, and there is porosity, under the grafting effect of 1,3-BDO, the hydroxyl on polylactic acid surface and the unsaturation on gangue surface
Bond is closed, and acting on bacterium surface by polylactic acid inactivates the respiratory enzyme of bacterium, is killed bacterium to realize, is utilized poly- cream
The antibiotic and sterilizing of acid imparts the excellent antibacterial reinforcing property of the reinforcement system, realizes vinegar grain, gangue, sustained release agent, soil
The mutual stronger combination of regulator, collective effect are specially imitated in slow-release compound fertilizer in capsicum, are realized to slow-release compound fertilizer
The high-efficiency sustained-release of middle nutriment acts on.
【Specific embodiment】
To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples belong to protection of the invention
Range, but do not limit the scope of the invention.
In embodiment, capsicum specially imitates slow-release compound fertilizer, as unit of parts by weight, including following raw material:Urea 20-40
Part, 12-16 parts of ammonium hydrogen carbonate, 4-8 parts of kainite, 3-9 parts of fermentation pig manure, fermentation leached tea oil slag 2-8 parts, 3-6 parts of biogas residue, bamboo charcoal powder
4-8 parts, 3-6 parts of cinder, 2-5 parts of vermiculite power, 1-5 parts of sepiolite powder, 4-8 parts of zinc borate, 3-9 parts of diatomite, quartz sand 2-6
Part, 10-20 parts of vinegar grain, 8-12 parts of gangue, 6-8 parts of sustained release agent, 4-6 parts of soil conditioner, 1-3 parts of 1,3 butylene glycol.
Sustained release agent is prepared by following technique：By weight by 4-8 parts of diammonium hydrogen phosphates, 3-6 parts of lignin and 6-12
Part bentonite is uniformly mixed, and is warming up to 60-80 DEG C, is kept the temperature 10-20min, is subsequently added into 4-8 parts of polyethylene glycol and 2-5 parts of rice brans
Wax is uniformly mixed, and stirs 20-30min in 350-650r/min revolving speed, then the dry 20- in -30~-50 DEG C of freeze driers
40min, is subsequently added into 6-9 parts of ethyl acetate and is uniformly mixed, and stirs 10-20min in 4500-5500r/min revolving speed, is then added
1-4 parts of chitosans and 2-5 parts of silane coupling agent KH-560 are uniformly mixed, and then stir 3-5h in 250-350r/min revolving speed, so
It is collected by centrifugation afterwards in 8500-12000r/min revolving speed, freeze-drying obtains sustained release agent after washing.
Soil conditioner is prepared by following technique：It dries after 10-20 parts of cinders are washed by weight, is then added
The ferric chloride solution that 4-8 parts of mass fractions are 15-25% is uniformly mixed, and in 80-100 DEG C of heating water bath 8-12h, is cooled to room
Then temperature is washed with deionized, be then warming up to 250-350 DEG C of calcining 4-6h, and grinding obtains material A after being cooled to room temperature；
Material A, 3-9 parts of urea, 2-5 parts of sodium hydroxides, 1-4 parts of diatomite, 3-6 parts of salicylic acids, 2-4 parts of potassium peroxydisulfates, 3-9 parts are gathered
Lactic acid and 2-5 parts of Silane coupling reagent KH-570s are uniformly mixed, with the stirring of 280-320r/min revolving speed in 65-75 DEG C of water bath with thermostatic control
4-6h is then cooled to room temperature, and suction filtration obtains sediment, is then cooled to room temperature sediment in 45-55 DEG C of dry 44-52h
Obtain soil conditioner.
The capsicum specially imitates the preparation method of slow-release compound fertilizer, includes the following steps:
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding,
Then material a is obtained after crossing 100-200 mesh sieve, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure mixing are added into material a
Uniformly, it in 30-40 DEG C of fermentation 10-20d, is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 50-60 DEG C, then by material c in
90-105 DEG C of drying obtains material d to water content≤6%；
S3, into material d, addition urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol are mixed
It closes uniformly, is warming up to 60-70 DEG C, keep the temperature 2-3h, stir 1-2h in 650-850r/min revolving speed, 20-40 mesh is made through pelletizer
Granular capsicum specially imitates slow-release compound fertilizer.
Below by more specifically examples illustrate the present invention.
Embodiment 1
A kind of capsicum specially imitates slow-release compound fertilizer, as unit of parts by weight, including following raw material:31 parts of urea, ammonium hydrogen carbonate
13.8 parts, 5.7 parts of kainite, 5.8 parts of fermentation pig manure, fermentation 4.7 parts of leached tea oil slag, 4.6 parts of biogas residue, 5.8 parts of bamboo charcoal powder, cinder
4.4 parts, 3.5 parts of vermiculite power, 3.6 parts of sepiolite powder, 5.8 parts of zinc borate, 5.7 parts of diatomite, 4.7 parts of quartz sand, 16 parts of vinegar grain,
9 parts of gangue, 7.2 parts of sustained release agent, 5.1 parts of soil conditioner, 2.7 parts of 1,3 butylene glycol.
Sustained release agent is prepared by following technique：By weight by 6.1 parts of diammonium hydrogen phosphates, 4.3 parts of lignin and 9.2 parts
Bentonite is uniformly mixed, and is warming up to 73 DEG C, keeps the temperature 14min, is subsequently added into 5 parts of polyethylene glycol and 3.4 parts of rice bran waxs are uniformly mixed,
26min is stirred in 488r/min revolving speed, then the dry 30min in -40 DEG C of freeze driers, is subsequently added into 7.5 parts of acetic acid second
Ester is uniformly mixed, and stirs 15min in 5000r/min revolving speed, 2.5 part of 7.5 chitosan and 3.4 parts of silane coupling agents are then added
KH-560 is uniformly mixed, and is then stirred 4h in 280r/min revolving speed, is then collected by centrifugation in 10500r/min revolving speed, cold after washing
Jelly is dried to obtain sustained release agent.
Soil conditioner is prepared by following technique：It is dried after 15 parts of cinders are washed by weight, is then added 6 parts
The ferric chloride solution that mass fraction is 20% is uniformly mixed, and in 90 DEG C of heating water bath 10h, is cooled to room temperature, is then used deionization
Water washing is then warming up to 300 DEG C of calcining 5h, and grinding obtains material A after being cooled to room temperature；By material A, 6 parts of urea, 3 parts of hydrogen
Sodium oxide molybdena, 2.5 parts of diatomite, 4.5 parts of salicylic acids, 3 parts of potassium peroxydisulfates, 6 parts of polylactic acid and 3.5 parts of Silane coupling reagent KH-570s are mixed
It closes uniformly, 5h is stirred with 300r/min revolving speed in 70 DEG C of waters bath with thermostatic control, is then cooled to room temperature, suction filtration obtains sediment, connects
By sediment in 50 DEG C of dry 48h, be cooled to room temperature to obtain soil conditioner.
The capsicum specially imitates the preparation method of slow-release compound fertilizer, includes the following steps:
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding,
Then material a is obtained after crossing 150 mesh sieve, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure are added into material a and is uniformly mixed,
In 35 DEG C of fermentation 15d, it is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 55 DEG C, then by material c in 100 DEG C
Drying obtains material d to water content≤6%；
S3, into material d, addition urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol are mixed
It closes uniformly, is warming up to 65 DEG C, keep the temperature 2.5h, stir 1.5h in 750r/min revolving speed, it is granular peppery that 30 mesh are made through pelletizer
Green pepper specially imitates slow-release compound fertilizer.
Embodiment 2
A kind of capsicum specially imitates slow-release compound fertilizer, as unit of parts by weight, including following raw material:20 parts of urea, ammonium hydrogen carbonate
16 parts, 4 parts of kainite, 9 parts of fermentation pig manure, fermentation 2 parts of leached tea oil slag, 6 parts of biogas residue, 4 parts of bamboo charcoal powder, 6 parts of cinder, 2 parts of vermiculite power,
5 parts of sepiolite powder, 4 parts of zinc borate, 9 parts of diatomite, 2 parts of quartz sand, 20 parts of vinegar grain, 8 parts of gangue, 8 parts of sustained release agent, soil tune
Save 4 parts of agent, 3 parts of 1,3 butylene glycol.
Sustained release agent is prepared by following technique：By weight by 4 parts of diammonium hydrogen phosphates, 6 parts of lignin and 6 parts of bentonites
It is uniformly mixed, is warming up to 80 DEG C, keep the temperature 10min, be subsequently added into 8 parts of polyethylene glycol and 2 parts of rice bran waxs are uniformly mixed, in 650r/
Min revolving speed stirs 20min, then the dry 20min in -50 DEG C of freeze driers, and it is equal to be subsequently added into 9 parts of ethyl acetate mixing
It is even, 20min is stirred in 4500r/min revolving speed, 1 part of chitosan is then added and 5 parts of silane coupling agent KH-560 are uniformly mixed, connects
In 250r/min revolving speed stir 5h, be then collected by centrifugation in 8500r/min revolving speed, after washing freeze-drying obtain sustained release agent.
Soil conditioner is prepared by following technique：It is dried after 10 parts of cinders are washed by weight, is then added 8 parts
The ferric chloride solution that mass fraction is 15% is uniformly mixed, and in 100 DEG C of heating water bath 8h, is cooled to room temperature, is then used deionization
Water washing is then warming up to 350 DEG C of calcining 4h, and grinding obtains material A after being cooled to room temperature；By material A, 9 parts of urea, 2 parts of hydrogen
Sodium oxide molybdena, 4 parts of diatomite, 3 parts of salicylic acids, 4 parts of potassium peroxydisulfates, 3 parts of polylactic acid and 5 parts of Silane coupling reagent KH-570 mixing are equal
It is even, 4h is stirred with 320r/min revolving speed in 65 DEG C of waters bath with thermostatic control, is then cooled to room temperature, suction filtration obtains sediment, then will
Sediment is cooled to room temperature to obtain soil conditioner in 55 DEG C of dry 44h.
The capsicum specially imitates the preparation method of slow-release compound fertilizer, includes the following steps:
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding,
Then material a is obtained after sieving with 100 mesh sieve son, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure are added into material a and is uniformly mixed,
In 40 DEG C of fermentation 10d, it is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 60 DEG C, then by material c in 90 DEG C
Drying obtains material d to water content≤6%；
S3, into material d, addition urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol are mixed
It closes uniformly, is warming up to 70 DEG C, keep the temperature 2h, stir 1h in 850r/min revolving speed, it is special that the granular capsicum of 40 mesh is made through pelletizer
Imitate slow-release compound fertilizer.
Embodiment 3
A kind of capsicum specially imitates slow-release compound fertilizer, as unit of parts by weight, including following raw material:40 parts of urea, ammonium hydrogen carbonate
12 parts, 8 parts of kainite, 3 parts of fermentation pig manure, fermentation 8 parts of leached tea oil slag, 3 parts of biogas residue, 8 parts of bamboo charcoal powder, 3 parts of cinder, 5 parts of vermiculite power,
1 part of sepiolite powder, 8 parts of zinc borate, 3 parts of diatomite, 6 parts of quartz sand, 10 parts of vinegar grain, 12 parts of gangue, 6 parts of sustained release agent, soil
6 parts of regulator, 1 part of 1,3 butylene glycol.
Sustained release agent is prepared by following technique：By weight by 8 parts of diammonium hydrogen phosphates, 3 parts of lignin and 12 parts of swellings
Soil is uniformly mixed, and is warming up to 60 DEG C, keeps the temperature 20min, is subsequently added into 4 parts of polyethylene glycol and 5 parts of rice bran waxs are uniformly mixed, in
350r/min revolving speed stirs 30min, and then the dry 40min in -30 DEG C of freeze driers, it is mixed to be subsequently added into 6 parts of ethyl acetate
It closes uniformly, stirs 10min in 5500r/min revolving speed, 4 parts of chitosans are then added and 2 parts of silane coupling agent KH-560 mixing are equal
It is even, 3h then is stirred in 350r/min revolving speed, is then collected by centrifugation in 12000r/min revolving speed, freeze-drying is delayed after washing
Release agent.
Soil conditioner is prepared by following technique：It is dried after 20 parts of cinders are washed by weight, is then added 4 parts
The ferric chloride solution that mass fraction is 25% is uniformly mixed, and in 80 DEG C of heating water bath 12h, is cooled to room temperature, is then used deionization
Water washing is then warming up to 250 DEG C of calcining 6h, and grinding obtains material A after being cooled to room temperature；By material A, 3 parts of urea, 5 parts of hydrogen
Sodium oxide molybdena, 1 part of diatomite, 6 parts of salicylic acids, 2 parts of potassium peroxydisulfates, 9 parts of polylactic acid and 2 parts of Silane coupling reagent KH-570 mixing are equal
It is even, 6h is stirred with 280r/min revolving speed in 75 DEG C of waters bath with thermostatic control, is then cooled to room temperature, suction filtration obtains sediment, then will
Sediment is cooled to room temperature to obtain soil conditioner in 45 DEG C of dry 52h.
The capsicum specially imitates the preparation method of slow-release compound fertilizer, includes the following steps:
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding,
Then material a is obtained after crossing 200 mesh sieve, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure are added into material a and is uniformly mixed,
In 30 DEG C of fermentation 20d, it is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 50 DEG C, then by material c in 105 DEG C
Drying obtains material d to water content≤6%；
S3, into material d, addition urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol are mixed
It closes uniformly, is warming up to 60 DEG C, keep the temperature 3h, stir 2h in 650r/min revolving speed, it is special that the granular capsicum of 20 mesh is made through pelletizer
Imitate slow-release compound fertilizer.
Comparative example 1
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack vinegar grain, gangue, sustained release agent, soil conditioner and 1,3 butylene glycol.
Comparative example 2
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack vinegar grain.
Comparative example 3
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack gangue.
Comparative example 4
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack sustained release agent.
Comparative example 5
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack soil conditioner.
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
In lack 1,3 butylene glycol.
Comparative example 7
Using Chinese patent application document, " a kind of capsicum specially imitates slow-release compound fertilizer (application publication number:CN107778111A)"
The technique preparation capsicum of embodiment 1-4 specially imitates slow-release compound fertilizer.
Comparative example 8
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
Middle vinegar grain is 9 parts, gangue is 13 parts, sustained release agent is 5 parts, soil conditioner is 7 parts, 1,3 butylene glycol is 0.8 part.
Comparative example 9
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
Middle vinegar grain is 22 parts, gangue is 7 parts, sustained release agent is 9 parts, soil conditioner is 3 parts, 1,3 butylene glycol is 5 parts.
Comparative example 10
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparation capsicum specially imitates the raw material of slow-release compound fertilizer
Middle vinegar grain is 7 parts, gangue is 15 parts, sustained release agent is 4 parts, soil conditioner is 7 parts, 1,3 butylene glycol is 0.8 part.
It tests and was carried out in herbage base in 2016-2017 years, 17.6 DEG C of average annual temperature, 40 DEG C of max. daily temperature, extremely
- 9.3 DEG C of low temperature, experimental field soil is sandy loam for this, and the soil fertility of 0~20cm soil layer is：Organic matter 18.4g/kg, alkali-hydrolyzable nitrogen
68.3mg/kg, available phosphorus 133mg/kg, available potassium 82.4mg/kg, soil pH 5.6.
Slow-release compound fertilizer is specially imitated to the capsicum of embodiment 1-3 and comparative example 1-9 and carries out indices detection, obtained detection
As a result such as following table：
Note：Growth rate is every the plant height of survey in 2 months, and it is H1 that adjacent test point measures plant height for the first time, is finally measured as
H2, growth rate=(∣ H2-H1 ∣/H1) × 100%.
As seen from the above table:
(1) by the data of embodiment 1-3 and comparative example 7 as it can be seen that application embodiment 1-3 capsicum specially imitates slow-release compound fertilizer plantation
Capsicum, growth rate and survival rate significantly improve；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimal implementation
Example.
(2) by embodiment 1 and the data of comparative example 1-6 as it can be seen that vinegar grain, gangue, sustained release agent, soil conditioner, 1,3-
Butanediol specially imitates in slow-release compound fertilizer in preparation capsicum and plays synergistic effect, and collaboration improves capsicum and specially imitates slow-release compound fertilizer
Utilization of nutrients, this may be：
1) gangue is the solid waste discharged during coal mining process and coal washing, be one kind in coalification course with coal seam
A kind of lower, harder than the coal black and gray rock of phosphorus content of association not only has excellent absorbent properties, and as base fertilizer
Major ingredient its with excellent environmental-protecting performance, it is degradable, and the unsaturated bond on its surface can provide for hydrophily water-absorbent material
Binding site realizes the unsaturated side chain on gangue surface and sustained release auxiliary agent, soil conditioner and degradable release-controlled fills out
Material combines, and reinforcement the efficiency slow release performance of gangue, the nutriment and Fungicidal substance realized in base fertilizer obtain efficiently
It is abundant to realize the soil nutrient before capsicum seeding and seedling raising for release, and harmful bacteria is few, improves the survival rate and growth effect of seed
Rate.
2) diammonium hydrogen phosphate, lignin and bentonite are uniformly mixed, are kept the temperature after heating, be subsequently added into polyethylene glycol and rice
Chaff wax is uniformly mixed, stirring, then dry in freeze drier, is subsequently added into ethyl acetate mixing, and it is poly- that shell is then added
Sugar and silane coupling agent KH-560 are uniformly mixed, and are followed by stirring for, are then centrifuged for collecting, and freeze-drying obtains sustained release agent after washing.
It buffers filler using lignin and bentonite as porosity, and since lignin and bentonite surface area are big, hole is more, and surface
Hydroxy radical content it is high；Using chitosan as initiator, using silane coupling agent KH-560 as grafting agent, with ethyl acetate, poly- second
Two pure and mild rice bran waxs are realized as organic moulding material by the unsaturated bond on organic moulding material surface and lignin and swollen
Moisten the hydroxy combining on native surface, and under the action of swelling agent diammonium hydrogen phosphate, lignin and bentonite is furthermore achieved
The expansion of volume further increases the gap of sustained release agent after molding, improves cushion performance, wherein in chitosan macromolecular
There are active hydroxyl and amino, they have stronger chemical reaction ability, contain amino in dissolved solution, can pass through
In conjunction with negative electron the respiratory system of bacterium is destroyed, to realize the effect for inhibiting bacterial growth；Polylactic acid surface contains
There are the strongly hydrophilics groups such as carboxyl and hydroxyl abundant, good biocompatibility is degradable, and has porosity, in 1,3- fourth two
Under the grafting effect of alcohol, in conjunction with the unsaturated bond on gangue surface, act on bacterium surface makes carefully the hydroxyl on polylactic acid surface
The respiratory enzyme of bacterium inactivates, and kills bacterium to realize, it is excellent to impart the reinforcement system using the antibiotic and sterilizing of polylactic acid
Antibacterial reinforcing property；Lignin is as binder, it can be achieved that gangue, sustained release auxiliary agent, soil conditioner, polylactic acid, shell are poly-
Sugar combines stronger between each other, and collective effect is realized in base fertilizer to the height of nutriment in base fertilizer and antibacterial material
Imitate slow releasing function.Simultaneously by the unsaturated bond on a large amount of hydroxyl in sustained release agent surface and gangue surface 1,3 butylene glycol grafting
Combination is realized under effect, so that the cushion performance of modified sustained release agent be applied in the base fertilizer, realize in base fertilizer nutrient and
The efficient release of antibacterial material improves the survival rate and growth rate of capsicum.
3) then soil conditioner is added ferric chloride solution and is uniformly mixed to dry after washing cinder, in heating water bath,
It is cooled to room temperature, is then washed with deionized, then heating calcining, grinding obtains material A after being cooled to room temperature；By material A,
Urea, sodium hydroxide, diatomite, salicylic acid, potassium peroxydisulfate, polylactic acid and Silane coupling reagent KH-570 are uniformly mixed, thermostatted water
It stirs, then cools to room temperature in bath, suction filtration obtains sediment, then by drying precipitate, is cooled to room temperature to obtain, with coal
Slag supplements minerals and micro member in soil using cinder minerals rich in and microelement as basic substance
Element, and due to cinder and diatomite surface hydroxyl rich in, under the initiation of potassium peroxydisulfate, realize salicylic acid and
The unsaturated bond on ethyl acetate surface Silane coupling reagent KH-570 graft modification effect under with cinder and diatomite surface hydroxyl
The combination of base, and by addition ferric chloride solution, urea and sodium hydroxide, further supplemented with ferro element, nitrogen and sodium member
Element has advanced optimized soil regulating effect；Due to obtaining its surface of soil conditioner as porous structure, and hydroxyl rich in
Base is realized in conjunction with gangue surface hydroxyl, the further reinforcement soil of gangue under the grafting effect of 1,3-BDO
Adjustment effect applies in the base fertilizer, can guarantee that base fertilizer in extra-nutrition elemental basis, is realized to soil trace element
Supplement is adjusted, and the balance of the elements such as optimization soil N P, K improves the growth efficiency and survival rate of capsicum.
(3) by the data of comparative example 8-10 as it can be seen that during pepper cultivation, in S1 in base fertilizer raw material, vinegar grain, gangue,
Sustained release agent, soil conditioner, 1,3 butylene glycol weight ratio not at (10-20)：(8-12)：(6-8)：(4-6)：(1-3) range
When interior, after carrying out pepper cultivation using pepper cultivation method, the number of the growth rate of capsicum and the numerical value of survival rate and embodiment 1-3
Value is very different, suitable with the numerical value of the prior art (comparative example 7) much larger than the numerical value of embodiment 1-3.It is controlled in embodiment 1-3
Vinegar grain in slow-release compound fertilizer, gangue, sustained release agent, soil is specially imitated using capsicum of the invention during pepper cultivation processed to adjust
Agent, 1,3-BDO reinforcement system, weight ratio adjust be respectively (10-20)：(8-12)：(6-8)：(4-6)：(1-3), can benefit
With the degradability of gangue, slow release and its unsaturated bond abundant, with superior sustained-release sustained release auxiliary agent and
Soil conditioner and aceticanhydride cooperation with excellent soil regulating power are realized under the graft modification effect of 1,3-BDO
The combination of hydroxyl and gangue surface unsaturated bond, imparts the excellent sustained release of gangue in modified sustained release agent and soil conditioner
Property and anti-microbial property, and polylactic acid and chitosan be as containing active hydroxyl and amino in chitosan macromolecular, in molecule, tool
There is stronger chemical reaction ability, it can be by combining negative electron to destroy the respiratory system of bacterium, to realize inhibition
The effect of bacterium；The strongly hydrophilics group such as a large amount of carboxyl and hydroxyl, and good biocompatibility are contained in polylactic acid surface, can drop
Solution, and there is porosity, under the grafting effect of 1,3-BDO, the hydroxyl on polylactic acid surface and the unsaturation on gangue surface
Bond is closed, and acting on bacterium surface by polylactic acid inactivates the respiratory enzyme of bacterium, is killed bacterium to realize, is utilized poly- cream
The antibiotic and sterilizing of acid imparts the excellent antibacterial reinforcing property of the reinforcement system, realizes vinegar grain, gangue, sustained release agent, soil
The mutual stronger combination of regulator, collective effect are specially imitated in slow-release compound fertilizer in capsicum, are realized to slow-release compound fertilizer
The high-efficiency sustained-release of middle nutriment acts on.
The above content is it cannot be assumed that present invention specific implementation is only limited to these instructions, for the technical field of the invention
Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (6)
1. a kind of capsicum specially imitates slow-release compound fertilizer, which is characterized in that including following raw material：Urea, ammonium hydrogen carbonate, kainite, hair
Ferment pig manure, fermentation leached tea oil slag, biogas residue, bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, vinegar grain,
Gangue, sustained release agent, soil conditioner, 1,3 butylene glycol；
Sustained release agent, as unit of parts by weight, including following raw material：4-8 parts of diammonium hydrogen phosphate, 3-6 parts of lignin, bentonite 6-12
Part, 4-8 parts of polyethylene glycol, 2-5 parts of rice bran wax, 6-9 parts of ethyl acetate, 1-4 parts of chitosan, KH-5602-5 parts of silane coupling agent；
Soil conditioner, as unit of parts by weight, including following raw material：10-20 parts of cinder, the chlorine that mass fraction is 15-25%
Change ferrous solution 4-8 parts, 3-9 parts of urea, 2-5 parts of sodium hydroxide, 1-4 parts of diatomite, 3-6 parts of salicylic acid, 2-4 parts of potassium peroxydisulfate,
3-9 parts of polylactic acid, 2-5 parts of Silane coupling reagent KH-570；
The vinegar grain, gangue, sustained release agent, soil conditioner, 1,3 butylene glycol weight ratio be (10-20)：(8-12)：(6-
8)：(4-6)：(1-3).
2. capsicum according to claim 1 specially imitates slow-release compound fertilizer, which is characterized in that the vinegar grain, gangue, sustained release
Agent, soil conditioner, 1,3 butylene glycol weight ratio be 15.2：10.3：7.1：5.3：2.1.
3. capsicum according to claim 1 specially imitates slow-release compound fertilizer, which is characterized in that as unit of parts by weight, including with
Lower raw material：20-40 parts of urea, 12-16 parts of ammonium hydrogen carbonate, 4-8 parts of kainite, 3-9 parts of fermentation pig manure, fermentation leached tea oil slag 2-8 parts,
3-6 parts of biogas residue, 4-8 parts of bamboo charcoal powder, 3-6 parts of cinder, 2-5 parts of vermiculite power, 1-5 parts of sepiolite powder, 4-8 parts of zinc borate, diatomite
3-9 parts, 2-6 parts of quartz sand, 10-20 parts of vinegar grain, 8-12 parts of gangue, 6-8 parts of sustained release agent, 4-6 parts of soil conditioner, 1,3- fourth
1-3 parts of glycol.
4. capsicum according to claim 1 specially imitates slow-release compound fertilizer, which is characterized in that sustained release agent is by following technique system
It is standby：Diammonium hydrogen phosphate, lignin and bentonite are uniformly mixed, are warming up to 60-80 DEG C, 10-20min is kept the temperature, is subsequently added into poly-
Ethylene glycol and rice bran wax are uniformly mixed, and stir 20-30min in 350-650r/min revolving speed, then dry in -30~-50 DEG C of freezings
Dry 20-40min in dry machine, is subsequently added into ethyl acetate and is uniformly mixed, and stirs 10-20min in 4500-5500r/min revolving speed,
Then chitosan is added and silane coupling agent KH-560 is uniformly mixed, then stirs 3-5h in 250-350r/min revolving speed, then
It is collected by centrifugation in 8500-12000r/min revolving speed, freeze-drying obtains sustained release agent after washing.
5. capsicum according to claim 1 specially imitates slow-release compound fertilizer, which is characterized in that soil conditioner by following technique into
Row preparation：It is dried after cinder is washed, the ferric chloride solution that mass fraction is 15-25% is then added and is uniformly mixed, in 80-
100 DEG C of heating water bath 8-12h, are cooled to room temperature, are then washed with deionized, and are then warming up to 250-350 DEG C of calcining 4-6h,
Grinding obtains material A after being cooled to room temperature；By material A, urea, sodium hydroxide, diatomite, salicylic acid, potassium peroxydisulfate, polylactic acid
It is uniformly mixed with Silane coupling reagent KH-570,4-6h is stirred with 280-320r/min revolving speed in 65-75 DEG C of water bath with thermostatic control, then
It is cooled to room temperature, suction filtration obtains sediment, then is cooled to room temperature to obtain soil in 45-55 DEG C of dry 44-52h by sediment
Regulator.
6. the preparation method that a kind of capsicum according to claim 1-5 specially imitates slow-release compound fertilizer, which is characterized in that
Include the following steps：
S1, by bamboo charcoal powder, cinder, vermiculite power, sepiolite powder, zinc borate, diatomite, quartz sand, gangue co-grinding, then
Material a is obtained after crossing 100-200 mesh sieve, vinegar grain, biogas residue, fermentation leached tea oil slag and fermentation pig manure are added into material a and is uniformly mixed,
In 30-40 DEG C of fermentation 10-20d, it is cooled to room temperature to obtain material b；
S2, material b is filtered to take into filtrate, filtrate is then concentrated to get material c in 50-60 DEG C, then by material c in 90-105
It is DEG C dry to water content≤6%, obtain material d；
S3, urea, ammonium hydrogen carbonate, kainite, sustained release agent, soil conditioner and 1,3 butylene glycol mixing are added into material d
It is even, it is warming up to 60-70 DEG C, keeps the temperature 2-3h, 1-2h is stirred in 650-850r/min revolving speed, 20-40 mesh particle is made through pelletizer
The capsicum of shape specially imitates slow-release compound fertilizer.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110100519A (en) * | 2019-03-06 | 2019-08-09 | 湖南省蔬菜研究所 | A kind of fertilizing method for improving soil property, improving capsicum vitamin C and protein content |
| CN110862195A (en) * | 2019-11-28 | 2020-03-06 | 衡阳思迈科科技有限公司 | Utilize processing apparatus of aquatic plant secondary purification electrically conductive silver thick liquid production sewage |
| CN111150642A (en) * | 2019-12-27 | 2020-05-15 | 刘敏 | Cervical vertebra moxa-moxibustion physiotherapy equipment based on draw cartridge bag |
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| CN113713777A (en) * | 2021-09-13 | 2021-11-30 | 湖南农业大学 | Preparation method of eggshell powder vomitoxin adsorbent |
| CN115417728A (en) * | 2022-08-09 | 2022-12-02 | 河南省烟草公司南阳市公司 | Low-nitrogen high-carbon disease-resistant bio-organic fertilizer and preparation method thereof |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103483095A (en) * | 2013-10-11 | 2014-01-01 | 西南大学 | Special slow/controlled release compound fertilizer for capsicum, and preparation method thereof |
| CN103708949A (en) * | 2013-12-16 | 2014-04-09 | 天津丰润园精细化工科技有限公司 | Special sustained-release organic fertilizer for colored pepper and hot pepper, and preparation method thereof |
| CN104774074A (en) * | 2015-02-02 | 2015-07-15 | 陈凯 | Preparation method of special compound fertilizer for preventing and treating capsicum seedling blight |
| CN106146094A (en) * | 2016-07-13 | 2016-11-23 | 江传国 | A kind of Non-polluted Hot Pepper fertilizer and preparation method thereof |
| CN106396982A (en) * | 2016-11-29 | 2017-02-15 | 袁家和 | Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer |
| CN106588308A (en) * | 2016-12-03 | 2017-04-26 | 安徽爱能洁生物科技有限公司 | Compound organic fertilizer used for rice planting and having high slow release property as well as preparation method of compound organic fertilizer |
| CN107098746A (en) * | 2017-04-27 | 2017-08-29 | 中国农业科学院麻类研究所 | A kind of capsicum Special compound microbial fertilizer and preparation method thereof |
| CN107311767A (en) * | 2017-07-26 | 2017-11-03 | 望江县乡缘农业有限责任公司 | A kind of organic slow-release composite fertilizer purified for paddy soil |
| CN107759331A (en) * | 2017-11-14 | 2018-03-06 | 安徽百卉园林有限公司 | A kind of gardens high Slow release organic fertilizer of anti-soil hardening |
| CN107778111A (en) * | 2017-11-17 | 2018-03-09 | 定远县诚信种植专业合作社 | A kind of composite slow-release fertilizer for improving yield of hot pepper |
| CN107814623A (en) * | 2017-11-14 | 2018-03-20 | 安徽百卉园林有限公司 | A kind of gardens antimicrobial sustained-release organic fertilizer |
-
2018
- 2018-08-27 CN CN201810982454.1A patent/CN108821921A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103483095A (en) * | 2013-10-11 | 2014-01-01 | 西南大学 | Special slow/controlled release compound fertilizer for capsicum, and preparation method thereof |
| CN103708949A (en) * | 2013-12-16 | 2014-04-09 | 天津丰润园精细化工科技有限公司 | Special sustained-release organic fertilizer for colored pepper and hot pepper, and preparation method thereof |
| CN104774074A (en) * | 2015-02-02 | 2015-07-15 | 陈凯 | Preparation method of special compound fertilizer for preventing and treating capsicum seedling blight |
| CN106146094A (en) * | 2016-07-13 | 2016-11-23 | 江传国 | A kind of Non-polluted Hot Pepper fertilizer and preparation method thereof |
| CN106396982A (en) * | 2016-11-29 | 2017-02-15 | 袁家和 | Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer |
| CN106588308A (en) * | 2016-12-03 | 2017-04-26 | 安徽爱能洁生物科技有限公司 | Compound organic fertilizer used for rice planting and having high slow release property as well as preparation method of compound organic fertilizer |
| CN107098746A (en) * | 2017-04-27 | 2017-08-29 | 中国农业科学院麻类研究所 | A kind of capsicum Special compound microbial fertilizer and preparation method thereof |
| CN107311767A (en) * | 2017-07-26 | 2017-11-03 | 望江县乡缘农业有限责任公司 | A kind of organic slow-release composite fertilizer purified for paddy soil |
| CN107759331A (en) * | 2017-11-14 | 2018-03-06 | 安徽百卉园林有限公司 | A kind of gardens high Slow release organic fertilizer of anti-soil hardening |
| CN107814623A (en) * | 2017-11-14 | 2018-03-20 | 安徽百卉园林有限公司 | A kind of gardens antimicrobial sustained-release organic fertilizer |
| CN107778111A (en) * | 2017-11-17 | 2018-03-09 | 定远县诚信种植专业合作社 | A kind of composite slow-release fertilizer for improving yield of hot pepper |
Non-Patent Citations (2)
| Title |
|---|
| 张忠武等: "缓释肥及平衡施肥对干制辣椒氮磷钾吸收的影响 ", 《西北农业学报》 * |
| 韩桂琪等: "专用缓释肥对辣椒生物性状、品质及产量的影响 ", 《贵州农业科学》 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110100519A (en) * | 2019-03-06 | 2019-08-09 | 湖南省蔬菜研究所 | A kind of fertilizing method for improving soil property, improving capsicum vitamin C and protein content |
| CN110100519B (en) * | 2019-03-06 | 2022-05-17 | 湖南省蔬菜研究所 | Fertilizing method for improving soil property and increasing vitamin C and protein content of capsicum |
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Application publication date: 20181116 |