CN108785160A - A kind of transparent blue lotion of the pure natural crystal grain containing pearly-lustre or gel and the preparation method and application thereof - Google Patents
A kind of transparent blue lotion of the pure natural crystal grain containing pearly-lustre or gel and the preparation method and application thereof Download PDFInfo
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- CN108785160A CN108785160A CN201810662129.7A CN201810662129A CN108785160A CN 108785160 A CN108785160 A CN 108785160A CN 201810662129 A CN201810662129 A CN 201810662129A CN 108785160 A CN108785160 A CN 108785160A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses the transparent blue lotions or gel of a kind of pure natural crystal grain containing pearly-lustre, including Purslane extract magnolia obovata extract, and the weight ratio of Purslane extract magnolia obovata extract is 30-90：0.01-0.3.The present invention according to specified weight ratio by compounding Purslane extract with Magnolia cortex P.E, and it is aided with the lower alcohol of specified weight part, thickener, acid-base modifier and nonionic surfactant, pass through the coordinated of each component, the transparent blue lotion or gel for the pure natural crystal grain containing pearly-lustre being prepared are keeping skin wet, anti- scytitis, mitigate skin irritatin, nutritional ingredient is provided for skin, on the basis of the effect of building healthy skin, with pure natural, appearance transparent, crystal grain containing pearly-lustre, in nattier blue effect, it can be widely applied to cosmetics, in hair shampoo article.
Description
Technical field
The present invention relates to traditional Chinese medicine or daily use chemicals technical field, more particularly to a kind of transparent blue of the pure natural crystal grain containing pearly-lustre
Lotion or gel and the preparation method and application thereof.
Background technology
As environmental pollution increasingly aggravates and the prosperity of electronic product, environment prolong the injury of skin and electronic product
The working time idea of long people's skin makes people protect skin care, and skin consciousness is more and more stronger, and skin care item are more next in daily life
It is more important, become daily life required article from luxury goods before, while with the development of science and technology, fashionable element prevalence,
People require also to be gradually increased to the mode of appearance of cosmetics and skin care item, no longer meet common white emulsion system and list
The transparent system adjusted, it is colorful, dazzle cruel, pearly-lustre crystal grain increasingly and become the fashion that people pursue, additionally, due to environmental pollution and life
The flat raising of running water, people require also increasingly to improve to the quality requirement of skin care item and cosmetics and source, chemicals day
Gradually repelled, pure natural pure plant substance and pure natural form gain great popularity.
According to current Scientific Cognition, chemicals due to chemosynthesis reaction is incomplete, by-product is more, purification difficult,
The shortcomings of organic solvent residual, is increasingly repelled by numerous people, and has some vital plants, can not only treat disease
Disease, and can increasingly be liked by people with health, so-called food and medicine consangunity, scientific investigations showed that, chemical synthesis substance life
Object activity is well below pure plant substance, this is because acting synergistically between being present in endophytic pure natural substance.
To meet requirement of the people to fashionable element, skin care item and cosmetics form are dazzling.It is existing on the market to contain
The transparent system of pearly-lustre crystal grain, usually to add based on chemical substance pearling agent or colour particles, and pure natural pearly-lustre crystal grain is still
It does not find.Skin care item and cosmetic color are also that addition chemical synthesis pigment realizes that pure natural pigment is actually rare mostly simultaneously,
And it is also a major reason that pure natural pigment color is not complete.
Invention content
In consideration of it, the present invention is directed to provide the lotion or gel of a kind of pure natural, crystal grain containing pearly-lustre, transparent blue.
Technical scheme is as follows：
The transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre of the present invention, including Purslane extract magnolia obovata
Extract, and the weight ratio of Purslane extract magnolia obovata extract is 30-90：0.01-0.3.
The weight ratio of only adjustment Purslane extract magnolia obovata extract is 30-90：0.01-0.3, what is be prepared is pure
Naturally the transparent blue lotion of the crystal grain containing pearly-lustre or gel are keeping skin wet, anti-scytitis, are mitigating skin irritatin, are
On the basis of the effect of skin offer nutritional ingredient, structure healthy skin, there is pure natural, appearance transparent, crystal grain containing pearly-lustre, in light
The effect of blue.And when the weight ratio of Purslane extract magnolia obovata extract is excessive（More than 90：0.01）, the breast that is prepared
Liquid or gel, pearly-lustre crystal grain is less, and mode of appearance is not glittering, and cost is higher；And when Purslane extract magnolia obovata extracts
The weight ratio of object is too small（Less than 30：0.3）, the lotion or gel being prepared, pearly-lustre crystal grain distribution is uneven, and moisturizing,
Anti-inflammatory efficacy can reduce.
Preferably, the weight ratio of the Purslane extract magnolia obovata extract is 70-85：0.02-0.2, more preferably
80：0.06.
The transparent blue lotion or gel of the above-mentioned pure natural crystal grain containing pearly-lustre further include 5-30 parts and go by weight
Ionized water, 1-10 part lower alcohol, 0.01-5 parts of thickeners, 0.1-2 parts of acid-base modifiers and 0.1-5 parts of non-ionic surface actives
Agent.
Preferably, the lower alcohol is selected from one or more of glycerine, 1,3- butanediols, sorbierite；The thickener
Selected from one or more of Carbomer981, xanthans, carrageenan；The acid-base modifier is selected from arginine, citric acid
One or more of sodium, sodium hydroxide；The nonionic surfactant is selected from Cremophor RH40, PEG-60 is hydrogenated
One or more of castor oil, CO-40.
The invention also discloses the transparent blue lotion of the above-mentioned pure natural crystal grain containing pearly-lustre or the preparation method of gel, packets
Include following steps：
1）Acid-base modifier is dispersed in deionized water and is completely dissolved；
2）Magnolia cortex P.E is dispersed in nonionic surfactant；
3）Thickener Carbomer981 powder is dispersed in deionized water and is completely dissolved；
4）Purslane extract is added into lower alcohol, thickener according to proportioning, is stirred evenly, is then added and is already dispersed in
Magnolia cortex P.E in nonionic surfactant is eventually adding the acid-base modifier decomposed completely in deionized water,
PH value is adjusted to skin optimum range to get the transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre.
In addition, the invention also discloses the transparent blue lotion of the above-mentioned pure natural crystal grain containing pearly-lustre being prepared or coagulating
Application of the glue in cosmetics, hair shampoo article.
Compared with prior art, the present invention has following excellent effect：
The present invention is aided with specified weight by compounding Purslane extract according to specified weight ratio with Magnolia cortex P.E
The lower alcohol, thickener, acid-base modifier and nonionic surfactant of part are prepared by the coordinated of each component
The pure natural crystal grain containing pearly-lustre transparent blue lotion or gel keep skin wet, anti-scytitis, mitigate skin thorn
On the basis of the effect of swashing, nutritional ingredient is provided, healthy skin is built for skin, there is pure natural, appearance transparent, it is brilliant containing pearly-lustre
Grain is in nattier blue effect, can be widely applied in cosmetics, hair shampoo article.
Description of the drawings
Fig. 1 is the micro- sem observation pearly-lustre crystal grain figure of embodiment 1；
Fig. 2 is the micro- sem observation pearly-lustre crystal grain figure of embodiment 4；
Fig. 3 is the micro- sem observation pearly-lustre crystal grain figure of comparative example 1.
Specific implementation mode
It is further illustrated the present invention below by specific implementation mode, following embodiment is the preferable embodiment party of the present invention
Formula, but embodiments of the present invention are not limited by following embodiments.
The raw material such as table 1 that the embodiment of the present invention and comparative example use, but it is not limited only to these raw materials：
Table 1
Micro- sem observation pearly-lustre crystal grain：Tabletting is made in lotion or gel, is seen using microscope in the case where amplifying 400 times
It examines, the results are shown in Figure 1 for observation.
Pearly-lustre feature：It is not natural that chemical pearling agent, which is added,.
Mode of appearance：It is placed in suitable environment, uses naked eyes paired observation.
The test method of color：It the weight transparency emulsion such as weighs, chromascope is used to carry out Lab value measurement.Color is different,
Lab Value Datas are inconsistent, Δ E<1 and Δ E values it is smaller, parallel laboratory test Δ E variations are little three times, are considered as the lotion of colour stable.
Stimulate the test method mitigated：HaCaT cells are added different after the stimulation of the lauryl sodium sulfate of various concentration
The lotion or gel of amount measure its cells survival rate with cell survival rate analysis counter, show that stimulation mitigates efficacy outcomes.
Moisturizing, anti-inflammatory efficacy：Bibliography[1]、[2]、[3], Purslane extract magnolia obovata extract have outstanding moisturizing,
Anti-inflammatory properties；Addition Purslane extract magnolia obovata extract appropriate, can play complementary moisturizing, antiphlogistic effects.
The test method of preservation challenge：Sample is taken to dispense each 100g, one bottle of addition mixed cell, one bottle is added mixing very
Bacterium is respectively placed in corresponding incubator, that is, the sample for adding bacterial suspension is placed in 30-35 DEG C of incubator, and addition fungi is outstanding
The sample of liquid is placed in 20-25 DEG C of incubator.Sample after inoculation is lived in challenge process by intervals sample detection
Bacterium number.Sample time is set to：After inoculation immediately（0 day）, 7 days, 14 days, 21 days, 28 days.Corresponding culture medium is selected when sample detection
It is detected.Detection method can refer to《Checked operation regulation（Yeast and mold）》With《Checked operation regulation (total plate count)》
It carries out.The results are shown in Table 3 for embodiment 1.
Stability：Sample is placed under 50 DEG C of high temperature, 4 DEG C of low temperature, room temperature and illumination condition, observe its color change,
Whether lotion is layered.Color is unchanged and lotion is not layered to be considered as and have good stability.
Embodiment 1-5 and comparative example 1-4：The transparent blue lotion of the pure natural crystal grain containing pearly-lustre or the preparation of gel
Acid-base modifier is dispersed in deionized water and is completely dissolved；Magnolia cortex P.E is dispersed in nonionic surfactant
In；Thickener Carbomer981 powder is dispersed in deionized water and is completely dissolved；According to the proportioning of table 2 by Purslane extract
It is added into lower alcohol, thickener, stirs evenly, the Cortex Magnoliae Officinalis extraction being already dispersed in nonionic surfactant is then added
Object is eventually adding the acid-base modifier decomposed completely in deionized water, adjusts pH value to skin optimum range to get pure
The naturally transparent blue lotion or gel of the crystal grain containing pearly-lustre.
The each group distribution ratio of table 2 embodiment 1-5 and comparative example 1-4（Parts by weight）
The preservation challenge of 3 embodiment 1 of table analyzes testing result
Bibliography：
【1】Kingdom is beautiful, Wang Lu, Wang Wei, waits the Hebei water extract of Portulaca oleracea L anti-inflammatory effects research [J] medicine, and 2014,20
(11):1866-1868.
【2】Qin Xiaozhi, wangdan, Zhang Hongying wait anti-inflammatory and antalgic resisting oxygen lack [J] Chinese Hospitals of purslane difference extracts
Pharmaceutical journal, 2010,30 (22):1909-1911.
Liu Ying, Zhou Rujun, Fu Junfan wait Cortex Magnoliae Officinalis bacteriostatic active ingredients Study on Extraction Method [J] Chinese medicines, 2009,32 (5):
791-794。
Claims (6)
1. the transparent blue lotion or gel of a kind of pure natural crystal grain containing pearly-lustre, which is characterized in that including Purslane extract
Magnolia obovata extract, and the weight ratio of Purslane extract magnolia obovata extract is 30-90：0.01-0.3.
2. the transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre according to claim 1, which is characterized in that institute
The weight ratio for stating Purslane extract magnolia obovata extract is 70-85：0.02-0.2, preferably 80：0.06.
3. the transparent blue lotion or gel, feature of the pure natural crystal grain containing pearly-lustre according to claim 1 or 2 exist
In further including 5-30 parts of deionized waters, 1-10 parts of lower alcohols, 0.01-5 parts of thickeners, 0.1-2 parts of soda acid tune by weight
Save agent and 0.1-5 portions of nonionic surfactants.
4. the transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre according to claim 3, which is characterized in that institute
It states lower alcohol and is selected from one or more of glycerine, 1,3- butanediols, sorbierite；The thickener is selected from Carbomer981, xanthan
One or more of glue, carrageenan；The one kind of the acid-base modifier in arginine, sodium citrate, sodium hydroxide
Or it is several；The nonionic surfactant in Cremophor RH40, PEG-60 rilanit specials, CO-40 one
Kind is several.
5. a kind of transparent blue lotion of pure natural crystal grain containing pearly-lustre according to any one of claims 1-4 or the system of gel
Preparation Method, which is characterized in that include the following steps：
1）Acid-base modifier is dispersed in deionized water and is completely dissolved；
2）Magnolia cortex P.E is dispersed in nonionic surfactant；
3）Thickener Carbomer981 powder is dispersed in deionized water and is completely dissolved；
4）Purslane extract is added into lower alcohol, thickener according to proportioning, is stirred evenly, is then added and is already dispersed in
Magnolia cortex P.E in nonionic surfactant is eventually adding the acid-base modifier decomposed completely in deionized water,
PH value is adjusted to skin optimum range to get the transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre.
6. the transparent blue lotion or gel of the pure natural crystal grain containing pearly-lustre being prepared such as claim 5 in cosmetics, wash
Application in hair care product.
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| CN201810662129.7A CN108785160A (en) | 2018-06-25 | 2018-06-25 | A kind of transparent blue lotion of the pure natural crystal grain containing pearly-lustre or gel and the preparation method and application thereof |
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| CN109481364A (en) * | 2018-12-07 | 2019-03-19 | 广州市禾基生物科技有限公司 | A kind of pure natural light blue lotion and the preparation method and application thereof containing liquid crystalline phase |
| CN109620776A (en) * | 2019-02-02 | 2019-04-16 | 广州市禾基生物科技有限公司 | Composition, gel and its preparation method and application |
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|---|---|---|---|---|
| CN109481364A (en) * | 2018-12-07 | 2019-03-19 | 广州市禾基生物科技有限公司 | A kind of pure natural light blue lotion and the preparation method and application thereof containing liquid crystalline phase |
| CN109620776A (en) * | 2019-02-02 | 2019-04-16 | 广州市禾基生物科技有限公司 | Composition, gel and its preparation method and application |
| CN109620776B (en) * | 2019-02-02 | 2022-02-01 | 广东省禾基生物科技有限公司 | Composition, gel and preparation method and application thereof |
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Address after: 510000 No. 9 Liuwei Street, Hualong Town, Panyu District, Guangzhou, Guangdong Province 101, 201 and 301 Applicant after: Guangdong Heji Biotechnology Co., Ltd. Address before: 510000 No. 9 Liuwei Street, Hualong Town, Panyu District, Guangzhou, Guangdong Province 101, 201 and 301 Applicant before: GUANGZHOU HEJI BIOTECHNOLOGY CO., LTD. |
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Address after: Room 406, floor 4, building B, enterprise service center, Guangzhou (Qingyuan) industrial transfer park, Qingcheng District, Qingyuan City, Guangzhou City, Guangdong Province Applicant after: Guangdong Heji Biotechnology Co., Ltd. Address before: 510000 101, 201, 301, No. 1, Liu Wei street, Hualong Town, Panyu District, Guangzhou, Guangdong, China (1) Applicant before: Guangdong Heji Biotechnology Co., Ltd. |
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Inventor after: He Tinggang Inventor after: Zhang Wenhuan Inventor after: Zhang Bing Inventor after: Ai Yong Inventor before: He Tinggang Inventor before: Ding Boxin Inventor before: Zhang Wenhuan Inventor before: Zhang Bing Inventor before: Ai Yong |
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Application publication date: 20181113 |