CN108689852A - 一种从平卧菊三七中提取绿原酸和异绿原酸的方法 - Google Patents
一种从平卧菊三七中提取绿原酸和异绿原酸的方法 Download PDFInfo
- Publication number
- CN108689852A CN108689852A CN201810669757.8A CN201810669757A CN108689852A CN 108689852 A CN108689852 A CN 108689852A CN 201810669757 A CN201810669757 A CN 201810669757A CN 108689852 A CN108689852 A CN 108689852A
- Authority
- CN
- China
- Prior art keywords
- lour
- merr
- solution
- acid
- gynura procumbens
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/28016—Particle form
- B01J20/28021—Hollow particles, e.g. hollow spheres, microspheres or cenospheres
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/31—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of functional groups containing oxygen only in singly bound form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/11—Compounds covalently bound to a solid support
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810669757.8A CN108689852B (zh) | 2018-06-26 | 2018-06-26 | 一种从平卧菊三七中提取绿原酸和异绿原酸的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810669757.8A CN108689852B (zh) | 2018-06-26 | 2018-06-26 | 一种从平卧菊三七中提取绿原酸和异绿原酸的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN108689852A true CN108689852A (zh) | 2018-10-23 |
CN108689852B CN108689852B (zh) | 2021-01-26 |
Family
ID=63849371
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810669757.8A Active CN108689852B (zh) | 2018-06-26 | 2018-06-26 | 一种从平卧菊三七中提取绿原酸和异绿原酸的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108689852B (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109503728A (zh) * | 2018-11-26 | 2019-03-22 | 江西省科学院应用化学研究所 | 一种平卧菊三七叶粗多糖提取方法 |
CN111700927A (zh) * | 2020-08-11 | 2020-09-25 | 江西省科学院应用化学研究所 | 一种具有降血糖作用的药食同源组合物及其制备方法和应用 |
CN112645817A (zh) * | 2020-12-24 | 2021-04-13 | 江西省科学院应用化学研究所 | 高速逆流色谱分离纯化蔓三七花中咖啡酰奎宁酸类化合物的方法 |
CN113214085A (zh) * | 2021-04-14 | 2021-08-06 | 张洪胜 | 一种抗氧化活性的绿原酸衍生物及其制备方法 |
CN113893241A (zh) * | 2021-10-26 | 2022-01-07 | 广东省第二中医院(广东省中医药工程技术研究院) | 异绿原酸c在制备抗高脂血症药物中的应用 |
CN113995800A (zh) * | 2021-12-01 | 2022-02-01 | 完美(广东)日用品有限公司 | 一种含平卧菊三七提取物的组合物及其制备方法与应用 |
CN114315579A (zh) * | 2021-09-30 | 2022-04-12 | 湖南绿蔓生物科技股份有限公司 | 一种从加拿大一枝黄花中提取绿原酸和芦丁的方法 |
CN115590800A (zh) * | 2022-11-11 | 2023-01-13 | 温州古木生物科技有限公司(Cn) | 平卧菊三七提取物及其发酵提取物的制备和应用 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101602668A (zh) * | 2009-07-13 | 2009-12-16 | 江西省科学院应用化学研究所 | 一种绿原酸提取的方法 |
CN103497106B (zh) * | 2013-09-04 | 2015-01-07 | 四川圣湖生物科技有限公司 | 从绿咖啡豆提取绿原酸的方法 |
CN104418740A (zh) * | 2013-08-30 | 2015-03-18 | 中国科学院烟台海岸带研究所 | 从菊芋叶片中制备高纯度绿原酸的方法 |
CN104931620A (zh) * | 2015-07-03 | 2015-09-23 | 唐和斌 | 平卧菊三七中绿原酸类成分的分离和含量测定方法 |
CN104418741B (zh) * | 2013-08-30 | 2016-03-16 | 中国科学院烟台海岸带研究所 | 一种从菊芋叶片中提取纯化绿原酸的方法 |
CN107056615A (zh) * | 2017-03-10 | 2017-08-18 | 江西省科学院应用化学研究所 | 一种从植物中制备高纯度绿原酸的方法 |
-
2018
- 2018-06-26 CN CN201810669757.8A patent/CN108689852B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101602668A (zh) * | 2009-07-13 | 2009-12-16 | 江西省科学院应用化学研究所 | 一种绿原酸提取的方法 |
CN104418740A (zh) * | 2013-08-30 | 2015-03-18 | 中国科学院烟台海岸带研究所 | 从菊芋叶片中制备高纯度绿原酸的方法 |
CN104418741B (zh) * | 2013-08-30 | 2016-03-16 | 中国科学院烟台海岸带研究所 | 一种从菊芋叶片中提取纯化绿原酸的方法 |
CN103497106B (zh) * | 2013-09-04 | 2015-01-07 | 四川圣湖生物科技有限公司 | 从绿咖啡豆提取绿原酸的方法 |
CN104931620A (zh) * | 2015-07-03 | 2015-09-23 | 唐和斌 | 平卧菊三七中绿原酸类成分的分离和含量测定方法 |
CN107056615A (zh) * | 2017-03-10 | 2017-08-18 | 江西省科学院应用化学研究所 | 一种从植物中制备高纯度绿原酸的方法 |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109503728A (zh) * | 2018-11-26 | 2019-03-22 | 江西省科学院应用化学研究所 | 一种平卧菊三七叶粗多糖提取方法 |
CN111700927A (zh) * | 2020-08-11 | 2020-09-25 | 江西省科学院应用化学研究所 | 一种具有降血糖作用的药食同源组合物及其制备方法和应用 |
CN111700927B (zh) * | 2020-08-11 | 2021-07-30 | 江西省科学院应用化学研究所 | 一种具有降血糖作用的药食同源组合物及其制备方法和应用 |
CN112645817A (zh) * | 2020-12-24 | 2021-04-13 | 江西省科学院应用化学研究所 | 高速逆流色谱分离纯化蔓三七花中咖啡酰奎宁酸类化合物的方法 |
CN113214085A (zh) * | 2021-04-14 | 2021-08-06 | 张洪胜 | 一种抗氧化活性的绿原酸衍生物及其制备方法 |
CN114315579A (zh) * | 2021-09-30 | 2022-04-12 | 湖南绿蔓生物科技股份有限公司 | 一种从加拿大一枝黄花中提取绿原酸和芦丁的方法 |
CN114315579B (zh) * | 2021-09-30 | 2024-04-26 | 湖南绿蔓生物科技股份有限公司 | 一种从加拿大一枝黄花中提取绿原酸和芦丁的方法 |
CN113893241A (zh) * | 2021-10-26 | 2022-01-07 | 广东省第二中医院(广东省中医药工程技术研究院) | 异绿原酸c在制备抗高脂血症药物中的应用 |
CN113995800A (zh) * | 2021-12-01 | 2022-02-01 | 完美(广东)日用品有限公司 | 一种含平卧菊三七提取物的组合物及其制备方法与应用 |
CN113995800B (zh) * | 2021-12-01 | 2022-09-13 | 完美(广东)日用品有限公司 | 一种含平卧菊三七提取物的组合物及其制备方法与应用 |
CN115590800A (zh) * | 2022-11-11 | 2023-01-13 | 温州古木生物科技有限公司(Cn) | 平卧菊三七提取物及其发酵提取物的制备和应用 |
CN115590800B (zh) * | 2022-11-11 | 2023-08-04 | 温州古木生物科技有限公司 | 平卧菊三七提取物及其发酵提取物的制备和应用 |
Also Published As
Publication number | Publication date |
---|---|
CN108689852B (zh) | 2021-01-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN108689852A (zh) | 一种从平卧菊三七中提取绿原酸和异绿原酸的方法 | |
US10196417B2 (en) | Baicalin magnesium compound and its preparation method and application | |
CN102391385B (zh) | 一种霍山石斛中生物活性多糖的提取、纯化方法 | |
CN111087285B (zh) | 一种从铁皮石斛中提取联苄类化合物的方法及其应用 | |
CN105816518A (zh) | 一种核桃青皮酚类天然抗氧化剂及其制备方法和应用 | |
CN104306428B (zh) | 一种从绞股蓝中提取纯化绞股蓝皂苷的方法 | |
CN110105458A (zh) | 从罗汉果甜苷提取废液中提取多糖和d-甘露醇的方法 | |
CN110818585B (zh) | 一种从九香虫中同时制备五种多巴胺类化合物的分离方法 | |
CN103242398A (zh) | 二氢黄酮化合物及其制备方法与应用 | |
CN102154428B (zh) | 一种人参皂苷Rh2的制备方法 | |
CN107286264A (zh) | 大枣营养物质分离的深加工方法 | |
CN113264974B (zh) | 一种乙型强心苷的制备及其抗血管生成应用 | |
CN100453550C (zh) | 人参皂苷Rb2的制备工艺 | |
CN109010456A (zh) | 一种从覆盆子中提取α-葡萄糖苷酶抑制剂的方法 | |
WO2012061984A1 (zh) | 制备芍药内酯苷和芍药苷的方法 | |
CN102219782B (zh) | 一种从天然产物中提取分离牡荆素和异牡荆素的方法 | |
CN108359021B (zh) | 一种快速制备具有抗病毒和免疫调节活性的亚麻籽多糖的方法 | |
CN110467643A (zh) | 从平卧菊三七中提取脑苷脂的方法及脑苷脂的用途 | |
CN104857245A (zh) | 紫萼玉簪花总皂苷的制备方法和应用 | |
CN108484401A (zh) | 一种从新鲜金银花中提取绿原酸的工艺 | |
CN112794925B (zh) | 一种阳春砂多糖及其制备方法和应用 | |
CN101804122B (zh) | 番茄水溶性皂苷提取物、其制备方法及其应用 | |
CN111620917B (zh) | 一种异牡荆素-2″-O-β-D-吡喃葡萄糖苷、其制备方法及应用 | |
CN113444136B (zh) | 一种抗乳腺癌的乙型强心苷的制备及其抗肝癌应用 | |
CN110772549A (zh) | 一种鸦胆子汇总抗肿瘤新成分的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210914 Address after: 330200 Room 303, third floor, South Building, apartment in evergreen science and Technology Park, No. 399 Jingdong Avenue, Nanchang high tech Industrial Development Zone, Nanchang, Jiangxi Province Patentee after: Jiangxi mansanqi Health Technology Co.,Ltd. Patentee after: INSTITUTE OF APPLIED CHEMISTRY, JIANGXI ACADEMY OF SCIENCES Patentee after: JIANGXI HUAZIREN AGRICULTURAL DEVELOPMENT Co.,Ltd. Address before: Jiangxi Academy of Sciences, 7777 Changdong Avenue, Nanchang, Jiangxi 330200 Patentee before: INSTITUTE OF APPLIED CHEMISTRY, JIANGXI ACADEMY OF SCIENCES Patentee before: JIANGXI HUAZIREN AGRICULTURAL DEVELOPMENT Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
CP01 | Change in the name or title of a patent holder |
Address after: 330200 Room 303, third floor, South Building, apartment in evergreen science and Technology Park, No. 399 Jingdong Avenue, Nanchang high tech Industrial Development Zone, Nanchang, Jiangxi Province Patentee after: Jiangxi Mansanqi Health Technology Co.,Ltd. Patentee after: INSTITUTE OF APPLIED CHEMISTRY, JIANGXI ACADEMY OF SCIENCES Patentee after: JIANGXI HUAZIREN AGRICULTURAL DEVELOPMENT Co.,Ltd. Address before: 330200 Room 303, third floor, South Building, apartment in evergreen science and Technology Park, No. 399 Jingdong Avenue, Nanchang high tech Industrial Development Zone, Nanchang, Jiangxi Province Patentee before: Jiangxi mansanqi Health Technology Co.,Ltd. Patentee before: INSTITUTE OF APPLIED CHEMISTRY, JIANGXI ACADEMY OF SCIENCES Patentee before: JIANGXI HUAZIREN AGRICULTURAL DEVELOPMENT Co.,Ltd. |
|
CP01 | Change in the name or title of a patent holder |