CN108619430A - Smilax is fresh to carry vacuum drying powder decoction pieces - Google Patents
Smilax is fresh to carry vacuum drying powder decoction pieces Download PDFInfo
- Publication number
- CN108619430A CN108619430A CN201810733376.1A CN201810733376A CN108619430A CN 108619430 A CN108619430 A CN 108619430A CN 201810733376 A CN201810733376 A CN 201810733376A CN 108619430 A CN108619430 A CN 108619430A
- Authority
- CN
- China
- Prior art keywords
- smilax
- decoction
- fresh
- water
- vacuum drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/90—Smilacaceae (Catbrier family), e.g. greenbrier or sarsaparilla
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Abstract
The invention discloses a kind of " smilax is fresh to carry vacuum drying powder decoction pieces ", are primarily characterized in that:Smilax harvesting after, take advantage of it is fresh wash, be sliced, squeezing the juice, extracting, after extracting solution is condensed into clear cream, then be dried under vacuum to water content be less than 10%, crush, be sieved after be vacuum-packed.This prepared slice quality is stablized, and can both enter decoction decocting, can also directly enter pill, powder, tablet, capsule, is conducive to carry, Clinical practice is convenient.
Description
Technical field
The invention belongs to prepared slices of Chinese crude drugs technical fields, especially belong to the manufacture field of smilax medicine materical crude slice.
Background technology
Chinese medicine smilax is liliaceous plant smilacis glabraSmilax glabraRoxb. dry rhizome has removing toxic substances,
Dehumidifying, easing joint movement effect.The limbs contraction being mainly used for caused by syphilis and mercury poisoning, arthralgia and myalgia;Damp and hot stranguria with turbid discharge, band
Under, carbuncle swells, scrofula, the treatment of mange etc. is a herb common on tcm clinical practice.The processing method of traditional smilax is:
After medicinal material is excavated, fibrous root, cleaning, drying are removed;Or fresh-cut flakiness is taken advantage of, and it is dry, it is packaged, storage and transportation.To after medicine materical crude slice factory, then wash
It washs, soften, be sliced, dry, pack.Such medicine materical crude slice volume is big, and Hygienic Standard is poor, is easy to make moist, mildew, is unfavorable for taking care of,
Storage and transportation cost are high.In addition, such smilax prepared slice quality stability is poor, clinical efficacy is difficult to ensure, patient takes
Inconvenience works slow.Therefore, develop a kind of stable quality is reliable, storage/transportation is at low cost, be conducive to keeping, carry and user
Just, rapid-action novel smilax medicine materical crude slice, it is imperative.Smilax medicine materical crude slice currently on the market, other than traditional medicine materical crude slice, also
There are two kinds of forms of Ultramicro-powder medicine materical crude slice and concentrated granular medicine materical crude slice, but both using traditional medicine materical crude slice as raw material, quality is decided by pass
The quality of system medicine materical crude slice, and ultramicro decoction piece cannot solve the problems, such as that medicinal material pollutes;Concentrated granular can only extract water-soluble components.
Invention content
The invention discloses a kind of " smilax is fresh to carry vacuum drying powder decoction pieces ", are primarily characterized in that:In smilax
After harvesting, clean in time, removal impurity and the dis-medicinal part such as silt, in taken advantage of in 24 hours using fresh herb tap water clean and be cut into 2 ~
The piece of 5mm thickness.The piece that this cuts is added in the water of 1 ~ 5 times of 50 ~ 70 DEG C of weight, impregnate and is constantly stirred 5 ~ 30 minutes, filtering,
Dregs pressing takes juice.The water that 5 ~ 10 times of weight is added in the gained dregs of a decoction is boiled 10 ~ 30 minutes, is filtered while hot, the dregs of a decoction squeeze again
Juice collects concoction.Merge above-mentioned concoction, crosses 60 ~ 100 mesh sieve, be concentrated under reduced pressure, temperature is 50 ~ 75 DEG C, and being concentrated into relative density is
1.15 ~ 1.25 clear cream.The clear cream of gained is dried under vacuum to water content at 60 ~ 80 DEG C and is less than 10%, is crushed, 60 mesh sieve is crossed,
Vacuum packaging is to get finished product.Finished product medicine materical crude slice contains astilbin(C21H22O11)No less than 0.50%.
The clinical general usage amount of this smilax medicine materical crude slice is 1 ~ 5g, can both enter decoction decoction, take after mixing it with water, also can directly enter pill,
In powder, capsule and tablet, to substantially increase the convenience and compliance of Clinical practice, be conducive to controlling for clinical acute disease
It treats.
The present invention solve traditional smilax medicine materical crude slice is bulky, carrying cost is high, be unfavorable for keeping, easily mildew it is infested,
The shortcomings such as the poor, unstable quality of hygiene condition, due to being to take advantage of fresh extraction, quality is than ultramicro grinding medicine materical crude slice and concentrated granular
Medicine materical crude slice is more preferable.
Specific embodiment
It after rhizoma smilacis glabrae medicinal material is harvested, cleans, removes impurity and the dis-medicinal parts such as silt, using fresh herb is taken advantage of in 6 hours certainly
Water is cleaned, and is cut into the piece of 3mm thickness.This piece is added to 70 DEG C of pure water of 5 times of weight, is stirred 30 minutes, filtering, the dregs of a decoction
Press extracting juice.The pure water for adding 8 times of weight into the above-mentioned dregs of a decoction again is boiled 20 minutes and is extracted, filters while hot, the dregs of a decoction are again
It is secondary to squeeze the juice, collect concoction.Merge above-mentioned concoction, be concentrated under reduced pressure, temperature is to be set as 70 DEG C, and it is 1.20 to be concentrated into relative density
Clear cream.It is 8% that the clear cream of gained is dried under vacuum at 80 DEG C to water content, is crushed, and crosses 60 mesh sieve, vacuum packaging to get at
Product.Finished product medicine materical crude slice astilbin(C21H22O11)Content is 0.55%.
Claims (2)
1. a kind of smilax is fresh to carry vacuum drying powder decoction pieces, it is primarily characterized in that:After smilax harvesting, clean in time,
Impurity and the dis-medicinal part such as silt are removed, in the piece for taking advantage of using fresh herb tap water in 24 hours and cleaning and being cut into 2 ~ 5mm thickness, addition 1 ~
The water of 5 times of 50 ~ 70 DEG C of weight is impregnated and is constantly stirred 5 ~ 30 minutes, and filtering, dregs pressing takes juice;5 are added in the gained dregs of a decoction
The water of ~ 10 times of weight is boiled 10 ~ 30 minutes, is filtered while hot, and the dregs of a decoction are squeezed the juice again, collects concoction;Merge above-mentioned concoction, cross 60 ~
100 mesh sieve, and are concentrated under reduced pressure, and temperature is 50 ~ 75 DEG C, are concentrated into the clear cream that relative density is 1.15 ~ 1.25;The clear cream of gained is existed
It is dried under vacuum to water content at 60 ~ 80 DEG C and is less than 10%, crushes, crosses 60 mesh sieve, is vacuum-packed to get finished product;Finished product medicine materical crude slice, which contains, to be fallen
Bride's glycosides(C21H22O11)No less than 0.50%.
2. smilax according to claim 1 is fresh to carry vacuum drying powder decoction pieces, it is primarily characterized in that:Clinic generally makes
Dosage is 1 ~ 5g, can both enter decoction decoction, take after mixing it with water, and also can directly enter in pill, powder, capsule and tablet.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201810733376.1A CN108619430A (en) | 2018-07-06 | 2018-07-06 | Smilax is fresh to carry vacuum drying powder decoction pieces |
Applications Claiming Priority (1)
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CN201810733376.1A CN108619430A (en) | 2018-07-06 | 2018-07-06 | Smilax is fresh to carry vacuum drying powder decoction pieces |
Publications (1)
Publication Number | Publication Date |
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CN108619430A true CN108619430A (en) | 2018-10-09 |
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CN201810733376.1A Pending CN108619430A (en) | 2018-07-06 | 2018-07-06 | Smilax is fresh to carry vacuum drying powder decoction pieces |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107362182A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern |
CN107412303A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of eupatorium |
CN107432883A (en) * | 2017-08-25 | 2017-12-05 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lopseed |
CN107582624A (en) * | 2017-08-25 | 2018-01-16 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin |
CN108186690A (en) * | 2018-03-21 | 2018-06-22 | 山西省医药与生命科学研究院 | A kind of Chinese medicine processing method |
-
2018
- 2018-07-06 CN CN201810733376.1A patent/CN108619430A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107362182A (en) * | 2017-08-25 | 2017-11-21 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of phoenix-tail fern |
CN107412303A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of eupatorium |
CN107432883A (en) * | 2017-08-25 | 2017-12-05 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lopseed |
CN107582624A (en) * | 2017-08-25 | 2018-01-16 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of Pogostemon cablin |
CN108186690A (en) * | 2018-03-21 | 2018-06-22 | 山西省医药与生命科学研究院 | A kind of Chinese medicine processing method |
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WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20181009 |
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