CN108503044A - A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent and preparation method thereof - Google Patents
A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
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- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
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- C02F3/34—Biological treatment of water, waste water, or sewage characterised by the microorganisms used
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Abstract
The invention discloses a kind of water body flocculation oxygenation of cultivation factory to sterilize water purification agent and preparation method thereof, includes the raw material of following parts by weight：Modified absorption banket 40 50 parts, 10 16 parts of oxygenation agent, 12 parts of water purification biological agent, 8 10 parts of activated carbon, 79 parts of oyster shell whiting, 57 parts of nanometer additive, 10 14 parts of compound botanical extracting solution, 10 12 parts of shellac, 35 parts of humate.The present invention has the function of flocculation and purifying aquatic product cultivating water environment, heavy metal ion can be adsorbed, the pathogenic thalline of water body is killed simultaneously, improve beneficial microorganism content in water body, increase oxygen content of water, safety and environmental protection nontoxic to aquatic biological, material is easy to get, production cost is relatively low, technique is concise, has higher practical value and good application prospect.
Description
Technical field
The present invention relates to water purification technology fields, and in particular to a kind of cultivation factory water body flocculation oxygenation sterilization water purification agent and
Preparation method.
Background technology
With the fast development of culture fishery, today of scale high-density breeding is especially greatly developed, aquatic products is supported
The proportion grown in aquaculture continues to increase, and due to the continuous expansion of the market demand, the cultivation density at aquaculture family is not yet
Disconnected to increase, along with the lasting increasing of aquaculture density, the water quality deterioration situation brought can not be ignored, main to show
：Water pollution caused by fish faeces and human lives' sewage, the influence of rural sewage cause water quality deterioration.Some are supported
Family water quality severe exacerbation is grown, it is continuous worsening that ammonia nitrogen, nitrite, dissolved oxygen amount in water body etc. cultivate parameter；Beneficial algae
The case where active level is greatly reduced, aging and stagnant water getting worse, photosynthesis are reduced, and show there is no PH values in one day
Variation, or variation are atomic, are not suitable for the life growth of fish.Just because of the continuous worsening of aquatic environment, fish disease takes place frequently, and supports
Growing family largely uses the abuse degree of medical treatment, especially antibiotic to increase, to accelerate the deterioration of water quality situation, and to fish
Class meat has a negative impact, and germ develops immunity to drugs, and the difficulty of bigger is brought to the prevention of fish disease.Water purification agent is supported in aquatic products
Grow the most frequently used improver of water quality in industry, main function is by by feed clast, planktonic organism corpse, bottom sludge in water body
The suspended particulates of equal formation, which gather, to become larger, or forms floc sedimentation, is allowed to coagulation, achievees the purpose that purifying aquatic water.Water purification agent
Quality mainly according to turbidity removal rate, COD removal rates, solid suspension (SS) removal rate, weigh except indexs such as color effects.It is excellent
Water purification product can improve rapidly deteriorate water quality, prevent disease occur, improve culture efficiency.But existing market is applied in aquatic products
It cultivates in water purification agent, the eutrophication of water body can be caused, so as to cause the normal growth of aquatic products, and do not account for oxygen
Supply.
Water purification agent is the most frequently used improver of water quality in culture fishery, and main function is by the way that feed in water body is broken
The suspended particulates of the formation such as bits, planktonic organism corpse, bottom sludge, which gather, becomes larger or is formed floc sedimentation, is allowed to coagulation, reaches purification
The purpose of breeding water body.Aquaculture water purification agent various types, usual water purification agent is toxic, penetrating odor, while to environment
There is pollution, for environmental protection to greatest extent and avoid generating health, is badly in need of environmental science worker and researches and develops water purification effect
Fruit is good, cheap, environmental-friendly, non-secondary pollution water purification agent, and has wide Research Prospects and use value.
Invention content
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of water body flocculation oxygenation of cultivation factory to sterilize water purification
Agent, the water purification agent have the function of flocculation and purifying aquatic product cultivating water environment, can adsorb heavy metal ion, while killing water
Body causes a disease thalline, improves beneficial microorganism content in water body, increases oxygen content of water, safety nontoxic to aquatic biological
Environmental protection, material is easy to get, production cost is relatively low, technique is concise, has higher practical value and good application prospect.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention provides a kind of water body flocculation oxygenation of cultivation factory to sterilize water purification agent, includes the raw material of following parts by weight：
Modified absorption banket 40-50 parts, 10-16 parts of oxygenation agent, 1-2 parts of water purification biological agent, 8-10 parts of activated carbon, oyster shell whiting 7-9
Part, 5-7 parts of nanometer additive, 10-14 parts of compound botanical extracting solution, 10-12 parts of shellac, 3-5 parts of humate.
Preferably, the cultivation factory water body flocculation oxygenation sterilization water purification agent includes the raw material of following parts by weight：
Modified absorption banket 45 parts, 13 parts of oxygenation agent, 1.5 parts of water purification biological agent, 9 parts of activated carbon, the addition of oyster shell whiting 8 part, nanometer
6 parts of object, 12 parts of compound botanical extracting solution, 11 parts of shellac, 4 parts of humate.
Preferably, the modified preparation method of banketing of adsorbing is：By attapulgite, diatomite temperature be 480-520 DEG C
Lower calcining 1-2h, after cooling, ball milling crosses 100-200 mesh sieve, after then impregnating 2-4h in the acetic acid solution of 8-10%, takes out, goes
Ion water washing is added and is equivalent to attapulgite, the Silane coupling agent KH550 of diatomite total weight 2-4%, phase to neutrality
When in attapulgite, diatomite total weight 1-3% sldium lauryl sulfate and be equivalent to attapulgite, diatomite total weight 3-5%
Niobium carbide stir 15-25min under 400-600r/min speed conditions after, addition be equivalent to attapulgite, diatomite gross weight
The chitosan solution that the mass fraction of amount 8% is 10% is stirred and heated to 30-45 DEG C, reacts 3-5h, centrifuges, fully washes
It washs, is dried in vacuo, is ground up, sieved to obtain the final product.
Preferably, the water purification biological agent is streptococcus fecalis, photosynthetic bacteria, nitrobacteria, bacillus subtilis according to weight
Measure ratio 2:1:2:The mixture of 3 compositions.
Preferably, the oxygenation agent is SODIUM PERCARBONATE, calper calcium peroxide and percarbamide according to weight ratio 2:3:1 composition mixes
Close object.
Preferably, the preparation method of the compound botanical extracting solution is：By violet, China pink, the lily of the valley, crape myrtle according to weight
Than 3:2:4:The water that 10-12 times of cauline leaf quality is added in opposite mixture gross mass is added after 1 crushing and decocts 1-2h, filtering is collected
Decoction liquor and filter residue；The water that filter residue is added to 8-10 times of filter residue quality decocts 2-3h again, filters to obtain decoction liquor, and merging is decocted twice
Boil liquid and the 1/4-1/3 for being concentrated into original volume, obtain concentrate.
Preferably, the nanometer additive is nano zine oxide, nano-titanium dioxide, nano cupric oxide according to weight ratio 3:
2:The mixture of 1 composition.
Preferably, the humate is sodium humate, potassium humate and citric acid according to weight ratio 2:2:1 composition mixes
Close object.
The present invention also provides the preparation methods that water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation, include the following steps：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 10-15 minutes, and stirring turns
Fast 150-250r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues to stir 25-35 points
Clock adds water purification biological agent, oxygenation agent, continues stirring 5-10 minutes, obtains mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24-48 hours, 2-6 DEG C refrigerates the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
Preferably, the preparation process of the cultivation factory water body flocculation oxygenation sterilization water purification agent is：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 13 minutes, speed of agitator
200r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues stirring 30 minutes, adds
Water purification biological agent, oxygenation agent continue stirring 7 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, 4 DEG C refrigerate the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
Compared with prior art, the present invention has following advantageous effect：
（1）The modified absorption added in a kind of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present invention is banketed, mainly to recessed
Convex stick soil, diatomite carry out a series of modifications, can greatly improve gap between the hole banketed, enhance its absorption property,
Removal organic polluter can effectively be absorbed can settle heavy metal ion, the remote super similar adsorbent of adsorption capacity again.
（2）A kind of water purification biological agent of cultivation factory water body flocculation oxygenation sterilization water purification agent addition of the present invention is excrement hammer
Bacterium, photosynthetic bacteria, nitrobacteria, bacillus subtilis are proliferated soon during decomposing organic matter, will be a large amount of organic in water body
Object has flocculation for synthesizing own cells tissue, reduces the concentration of the ammoniacal nitrogen in excreta, reduces row
The indigestion object for letting out object, has purified water body.
（3）A kind of oxygenation agent of cultivation factory water body flocculation oxygenation sterilization water purification agent addition of the present invention is mainly percarbonic acid
Sodium, calper calcium peroxide and percarbamide can effectively improve water body oxygen content, prevent aquatic biological anoxic, oxygenation effect bright
Aobvious, use of banketing is adsorbed in cooperation, significantly reduces the rate of release of oxygenation agent, reaches the work for improving the oxygenation effect duration
With.
（4）In a kind of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present invention nanometer additive be nano zine oxide,
Nano-titanium dioxide, nano cupric oxide, on the one hand its to bacterial cell membrane have destruction, to play sterilization, disinfection
Effect；On the other hand hydrogen and oxygen can be split water into, to be supplied to the oxygen of aquatic products abundance, is effectively increased water body
Dissolved oxygen amount does not generate any secondary pollution, safety and environmental protection.
（5）A kind of plant sterilization extract of cultivation factory water body flocculation oxygenation sterilization water purification agent addition of the present invention, pure day
Right plant antimicrobial, bactericidal effect is strong, to safety of human and livestock, alleviates environmental pollution, broad-spectrum, the quick-acting and good spy of lasting effect
Point, enhances bactericidal effect, when carrying out water body disinfection sterilization, additionally it is possible to by assimilating raising aquatic products to aquatic biological
The immunity of itself.
（6）A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present invention has flocculation and purifying aquatic product cultivating water
The effect of environment can adsorb heavy metal ion, while kill the pathogenic thalline of water body, improve beneficial microorganism in water body and contain
Amount increases oxygen content of water, and, safety and environmental protection nontoxic to aquatic biological, material is easy to get, production cost is relatively low, technique is concise,
With higher practical value and good application prospect.
Specific implementation mode
With reference to specific embodiment, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1.
Water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation of the present embodiment, includes the raw material of following parts by weight：
Modified absorption banket 40 parts, 10 parts of oxygenation agent, 1 part of water purification biological agent, 8 parts of activated carbon, 7 parts of oyster shell whiting, nanometer additive 5
Part, 10 parts of compound botanical extracting solution, 10 parts of shellac, 3 parts of humate.
Being modified in the present embodiment adsorbs preparation method of banketing：It is forged at being 480 DEG C in temperature by attapulgite, diatomite
1h is burnt, after cooling, ball milling crosses 100-200 mesh sieve, after then impregnating 2h in 8% acetic acid solution, takes out, deionized water washing
To neutrality, add be equivalent to by attapulgite, diatomite total weight 2% Silane coupling agent KH550, be equivalent to attapulgite,
The sldium lauryl sulfate of diatomite total weight 1% and be equivalent to attapulgite, diatomite total weight 3% niobium carbide in 400r/min
It after stirring 15min under speed conditions, is added and is equivalent to attapulgite, the shell that the mass fraction of diatomite total weight 8% is 10% gathers
Sugar juice is stirred and heated to 30 DEG C, reacts 3h, centrifuges, and fully washs, and vacuum drying is ground up, sieved to obtain the final product.
Water purification biological agent in the present embodiment is streptococcus fecalis, photosynthetic bacteria, nitrobacteria, bacillus subtilis according to weight
Measure ratio 2:1:2:The mixture of 3 compositions.
Oxygenation agent in the present embodiment is SODIUM PERCARBONATE, calper calcium peroxide and percarbamide according to weight ratio 2:3:1 composition
Mixture.
The preparation method of compound botanical extracting solution in the present embodiment is：By violet, China pink, the lily of the valley, crape myrtle according to weight
Measure ratio 3:2:4:The water that 10-12 times of cauline leaf quality is added in opposite mixture gross mass is added after 1 crushing and decocts 1-2h, filtering is received
Collect decoction liquor and filter residue；The water that filter residue is added to 8-10 times of filter residue quality decocts 2-3h again, filters to obtain decoction liquor, merges twice
Decoction liquor and the 1/4-1/3 for being concentrated into original volume, obtain concentrate.
Nanometer additive in the present embodiment is nano zine oxide, nano-titanium dioxide, nano cupric oxide according to weight ratio
3:2:The mixture of 1 composition.
Humate in the present embodiment is sodium humate, potassium humate and citric acid according to weight ratio 2:2:1 composition
Mixture.
A kind of preparation method of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 10 minutes, speed of agitator
150r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues stirring 25 minutes, adds
Water purification biological agent, oxygenation agent continue stirring 5 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24 hours, 2 DEG C refrigerate the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
Embodiment 2.
Water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation of the present embodiment, includes the raw material of following parts by weight：
Modified absorption banket 50 parts, 16 parts of oxygenation agent, 2 parts of water purification biological agent, 10 parts of activated carbon, 9 parts of oyster shell whiting, nanometer additive
7 parts, 14 parts of compound botanical extracting solution, 12 parts of shellac, 5 parts of humate.
Being modified in the present embodiment adsorbs preparation method of banketing：It is forged at being 520 DEG C in temperature by attapulgite, diatomite
2h is burnt, after cooling, ball milling crosses 100-200 mesh sieve, after then impregnating 4h in 10% acetic acid solution, takes out, deionized water washing
To neutrality, add be equivalent to by attapulgite, diatomite total weight 4% Silane coupling agent KH550, be equivalent to attapulgite,
The sldium lauryl sulfate of diatomite total weight 3% and be equivalent to attapulgite, diatomite total weight 5% niobium carbide in 600r/min
It after stirring 25min under speed conditions, is added and is equivalent to attapulgite, the shell that the mass fraction of diatomite total weight 8% is 10% gathers
Sugar juice is stirred and heated to 45 DEG C, reacts 5h, centrifuges, and fully washs, and vacuum drying is ground up, sieved to obtain the final product.
Water purification biological agent in the present embodiment is streptococcus fecalis, photosynthetic bacteria, nitrobacteria, bacillus subtilis according to weight
Measure ratio 2:1:2:The mixture of 3 compositions.
Oxygenation agent in the present embodiment is SODIUM PERCARBONATE, calper calcium peroxide and percarbamide according to weight ratio 2:3:1 composition
Mixture.
The preparation method of compound botanical extracting solution in the present embodiment is：By violet, China pink, the lily of the valley, crape myrtle according to weight
Measure ratio 3:2:4:The water that 12 times of cauline leaf quality is added in opposite mixture gross mass is added after 1 crushing and decocts 1-2h, filters, collects and decoct
Boil liquid and filter residue；The water that filter residue is added to 10 times of filter residue quality decocts 3h again, filters to obtain decoction liquor, merges twice that decoction liquor is simultaneously
It is concentrated into the 1/3 of original volume, obtains concentrate.
Nanometer additive in the present embodiment is nano zine oxide, nano-titanium dioxide, nano cupric oxide according to weight ratio
3:2:The mixture of 1 composition.
Humate in the present embodiment is sodium humate, potassium humate and citric acid according to weight ratio 2:2:1 composition
Mixture.
A kind of preparation method of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 15 minutes, speed of agitator
250r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues stirring 35 minutes, adds
Water purification biological agent, oxygenation agent continue stirring 10 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 48 hours, 6 DEG C refrigerate the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
Embodiment 3.
Water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation of the present embodiment, includes the raw material of following parts by weight：
Modified absorption banket 45 parts, 13 parts of oxygenation agent, 1.5 parts of water purification biological agent, 9 parts of activated carbon, the addition of oyster shell whiting 8 part, nanometer
6 parts of object, 12 parts of compound botanical extracting solution, 11 parts of shellac, 4 parts of humate.
Being modified in the present embodiment adsorbs preparation method of banketing：It is forged at being 520 DEG C in temperature by attapulgite, diatomite
2h is burnt, after cooling, ball milling crosses 100-200 mesh sieve, after then impregnating 3h in 9% acetic acid solution, takes out, deionized water washing
To neutrality, add be equivalent to by attapulgite, diatomite total weight 3% Silane coupling agent KH550, be equivalent to attapulgite,
The sldium lauryl sulfate of diatomite total weight 2% and be equivalent to attapulgite, diatomite total weight 4% niobium carbide in 500r/min
It after stirring 20min under speed conditions, is added and is equivalent to attapulgite, the shell that the mass fraction of diatomite total weight 8% is 10% gathers
Sugar juice is stirred and heated to 35 DEG C, reacts 4h, centrifuges, and fully washs, and vacuum drying is ground up, sieved to obtain the final product.
Water purification biological agent in the present embodiment is streptococcus fecalis, photosynthetic bacteria, nitrobacteria, bacillus subtilis according to weight
Measure ratio 2:1:2:The mixture of 3 compositions.
Oxygenation agent in the present embodiment is SODIUM PERCARBONATE, calper calcium peroxide and percarbamide according to weight ratio 2:3:1 composition
Mixture.
The preparation method of compound botanical extracting solution in the present embodiment is：By violet, China pink, the lily of the valley, crape myrtle according to weight
Measure ratio 3:2:4:The water that 11 times of cauline leaf quality is added in opposite mixture gross mass is added after 1 crushing and decocts 1.5h, filters, collects and decoct
Boil liquid and filter residue；The water that filter residue is added to 9 times of filter residue quality decocts 2.5h again, filters to obtain decoction liquor, merges decoction liquor twice
And it is concentrated into the 1/4-1/3 of original volume, obtain concentrate.
Nanometer additive in the present embodiment is nano zine oxide, nano-titanium dioxide, nano cupric oxide according to weight ratio
3:2:The mixture of 1 composition.
Humate in the present embodiment is sodium humate, potassium humate and citric acid according to weight ratio 2:2:1 composition
Mixture.
A kind of preparation method of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 13 minutes, speed of agitator
200r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues stirring 30 minutes, adds
Water purification biological agent, oxygenation agent continue stirring 7 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, 4 DEG C refrigerate the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent of the present invention has flocculation and purifying aquatic product cultivating water ring
The effect in border can adsorb heavy metal ion, while kill the pathogenic thalline of water body, improve beneficial microorganism content in water body,
Increase oxygen content of water, safety and environmental protection nontoxic to aquatic biological, material is easy to get, production cost is relatively low, technique is concise, tool
There are higher practical value and good application prospect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. water purification agent is sterilized in a kind of water body flocculation oxygenation of cultivation factory, which is characterized in that include the raw material of following parts by weight：
Modified absorption banket 40-50 parts, 10-16 parts of oxygenation agent, 1-2 parts of water purification biological agent, 8-10 parts of activated carbon, oyster shell whiting 7-9
Part, 5-7 parts of nanometer additive, 10-14 parts of compound botanical extracting solution, 10-12 parts of shellac, 3-5 parts of humate.
2. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1, which is characterized in that the cultivation
Factory's water body flocculation oxygenation sterilization water purification agent includes the raw material of following parts by weight：
Modified absorption banket 45 parts, 13 parts of oxygenation agent, 1.5 parts of water purification biological agent, 9 parts of activated carbon, the addition of oyster shell whiting 8 part, nanometer
6 parts of object, 12 parts of compound botanical extracting solution, 11 parts of shellac, 4 parts of humate.
3. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
Preparation method of banketing is adsorbed in modification：1-2h is calcined at being 480-520 DEG C in temperature by attapulgite, diatomite, after cooling, ball
Honed 100-200 mesh sieve, after then impregnating 2-4h in the acetic acid solution of 8-10%, takes out, and deionized water is washed to neutrality, then
Be added be equivalent to by attapulgite, diatomite total weight 2-4% Silane coupling agent KH550, be equivalent to attapulgite, diatomite
The sldium lauryl sulfate of total weight 1-3% and the niobium carbide of attapulgite, diatomite total weight 3-5% are equivalent in 400-600r/
It after stirring 15-25min under min speed conditions, is added and is equivalent to attapulgite, the mass fraction of diatomite total weight 8% is 10%
Chitosan solution, be stirred and heated to 30-45 DEG C, react 3-5h, centrifuge, fully wash, vacuum drying is ground up, sieved
To obtain the final product.
4. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
Water purification biological agent is streptococcus fecalis, photosynthetic bacteria, nitrobacteria, bacillus subtilis according to weight ratio 2:1:2:3 compositions mix
Close object.
5. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
Oxygenation agent is SODIUM PERCARBONATE, calper calcium peroxide and percarbamide according to weight ratio 2:3:The mixture of 1 composition.
6. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
The preparation method of compound botanical extracting solution is：By violet, China pink, the lily of the valley, crape myrtle according to weight ratio 3:2:4:It is added after 1 crushing
The water that 10-12 times of cauline leaf quality is added in opposite mixture gross mass decocts 1-2h, and decoction liquor and filter residue are collected in filtering；By filter residue
The water that 8-10 times of filter residue quality is added decocts 2-3h again, filters to obtain decoction liquor, merges decoction liquor twice and is concentrated into original volume
1/4-1/3, obtain concentrate.
7. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
Nanometer additive is nano zine oxide, nano-titanium dioxide, nano cupric oxide according to weight ratio 3:2:The mixture of 1 composition.
8. water purification agent is sterilized in a kind of cultivation factory water body flocculation oxygenation according to claim 1 or 2, which is characterized in that described
Humate is sodium humate, potassium humate and citric acid according to weight ratio 2:2:The mixture of 1 composition.
9. a kind of method preparing cultivation factory water body flocculation oxygenation sterilization water purification agent as claimed in claim 1 or 2, feature exist
In including the following steps：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 10-15 minutes, and stirring turns
Fast 150-250r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues to stir 25-35 points
Clock adds water purification biological agent, oxygenation agent, continues stirring 5-10 minutes, obtains mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24-48 hours, 2-6 DEG C refrigerates the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
10. a kind of preparation method of cultivation factory water body flocculation oxygenation sterilization water purification agent according to claim 9, feature exist
In the step is：
Step 1 weighs prepare each component raw material as required；
Modified absorption is banketed, in oyster shell whiting, nanometer additive addition homogenizer, stirs to get mixture A by step 2；
Suitable water, shellac, compound botanical extracting solution are added in blender by step 3, are stirred 13 minutes, speed of agitator
200r/min sequentially adds mixture A, activated carbon made from humate, step 2, continues stirring 30 minutes, adds
Water purification biological agent, oxygenation agent continue stirring 7 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, 4 DEG C refrigerate the cultivation factory water body flocculation oxygenation sterilization water purification agent invented.
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| CN109053260A (en) * | 2018-09-13 | 2018-12-21 | 安徽乐农环保科技有限公司 | Balanced nutritious organic carbon source and preparation method thereof |
| CN109179555A (en) * | 2018-10-15 | 2019-01-11 | 滕丽阳 | A kind of compound purifying agent for sewage and preparation method thereof |
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| CN109179555A (en) * | 2018-10-15 | 2019-01-11 | 滕丽阳 | A kind of compound purifying agent for sewage and preparation method thereof |
| CN109319893A (en) * | 2018-10-15 | 2019-02-12 | 滕丽阳 | A kind of efficient nano water purification agent and preparation method thereof |
| CN109502765A (en) * | 2018-12-31 | 2019-03-22 | 盐城工学院 | A kind of probiotics and preparation method thereof for hybridized prussian carp water improvement |
| CN110255837A (en) * | 2019-06-20 | 2019-09-20 | 天津市金水族水产养殖有限公司 | A kind of modifying agent for bottom material of pond for breeding and its preparation, application method |
| CN110316836A (en) * | 2019-07-08 | 2019-10-11 | 天津市晨辉饲料有限公司 | A kind of Mobyneb modifying agent for bottom material of pond for breeding and its preparation and application |
| CN110304738A (en) * | 2019-07-09 | 2019-10-08 | 李洪 | A kind of cleanser and preparation method thereof for aquaculture |
| CN110506871A (en) * | 2019-09-27 | 2019-11-29 | 珠海海龙生物科技有限公司 | A kind of mixed feed and preparation method thereof of Pelteobagrus fulvidraco megathermal period stabilizing water quality |
| CN111087085A (en) * | 2019-12-24 | 2020-05-01 | 中国市政工程西北设计研究院有限公司 | In-situ remediation method for black and odorous water body sediment |
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Application publication date: 20180907 |