CN108383196A - Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof - Google Patents
Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof Download PDFInfo
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- CN108383196A CN108383196A CN201810281612.0A CN201810281612A CN108383196A CN 108383196 A CN108383196 A CN 108383196A CN 201810281612 A CN201810281612 A CN 201810281612A CN 108383196 A CN108383196 A CN 108383196A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/28—Treatment of water, waste water, or sewage by sorption
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
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- C02F1/00—Treatment of water, waste water, or sewage
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- C02F1/286—Treatment of water, waste water, or sewage by sorption using natural organic sorbents or derivatives thereof
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
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- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
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Abstract
The invention discloses a kind of antibacterial decontamination environment-friendly high-efficiency water purification agents and preparation method thereof, include the raw material of following parts by weight：57 parts of charcoal, 15 25 parts of ore filler, 35 parts of nanometer additive, 24 parts of plant sterilization extract, 10 20 parts of adsorption stuffing, 46 parts of water body improver, 68 parts of chitosan.The present invention can largely kill the microorganisms and pathogenic bacteria in water body, and energy quick adsorption goes removal organic polluter that can settle heavy metal ion again, additionally it is possible to decompose the chlorine residue in water, increase oxygen content in water, environmental protection safe to the human body is nontoxic；Simultaneously the present invention oxygenation water purification agent advantages of nontoxic raw materials, material is easy to get, production cost is relatively low, technique is concise, as oxygenation water purification agent used for aquiculture have higher practical value and good application prospect.
Description
Technical field
The present invention relates to water purification technology fields, and in particular to the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and its preparation
Method.
Background technology
Water purification agent is the most frequently used improver of water quality in culture fishery, and main function is by the way that feed in water body is broken
The suspended particulates of the formation such as bits, planktonic organism corpse, bottom sludge, which gather, to become larger, or forms floc sedimentation, is allowed to coagulation, reaches purification
The purpose of breeding water body.Water purification agent quality mainly according to turbidity removal rate, COD removal rates, solid suspension (SS) removal rate, remove
The indexs such as color effect are weighed.Excellent water purification product, which can be improved rapidly, to be deteriorated water quality, prevents disease generation, improves cultivation effect
Benefit.But existing market is applied in aquaculture water purification agent, can cause the eutrophication of water body, so as to cause the normal of aquatic products
Growth, and do not account for the supply of oxygen.
Water purification agent is the most frequently used improver of water quality in culture fishery, and main function is by the way that feed in water body is broken
The suspended particulates of the formation such as bits, planktonic organism corpse, bottom sludge, which gather, becomes larger or is formed floc sedimentation, is allowed to coagulation, reaches purification
The purpose of breeding water body.Aquaculture water purification agent various types, usual water purification agent is toxic, penetrating odor, while to environment
There is pollution, for environmental protection to greatest extent and avoid generating health, is badly in need of environmental science worker and researches and develops water purification effect
Fruit is good, cheap, environmental-friendly, non-secondary pollution water purification agent, and has wide Research Prospects and use value.
Invention content
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of antibacterial decontamination environment-friendly high-efficiency water purification agents, this is net
Aqua can largely kill the microorganisms and pathogenic bacteria in water body, and energy quick adsorption goes removal organic polluter that can sink again
Heavy metal ion drops, additionally it is possible to decompose the chlorine residue in water, increase oxygen content in water, environmental protection safe to the human body is nontoxic；Together
When the present invention oxygenation water purification agent advantages of nontoxic raw materials, material is easy to get, production cost is relatively low, technique is concise, as increasing used for aquiculture
Oxygen water purification agent has higher practical value and good application prospect.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention provides a kind of antibacterial decontamination environment-friendly high-efficiency water purification agents, include the raw material of following parts by weight：
5-7 parts of charcoal, 15-25 parts of ore filler, 3-5 parts of nanometer additive, 2-4 parts of plant sterilization extract, adsorption stuffing
10-20 parts, 4-6 parts of water body improver, 6-8 parts of chitosan.
Preferably, the antibacterial decontamination environment-friendly high-efficiency water purification agent includes the raw material of following parts by weight：
6 parts of charcoal, 20 parts of ore filler, 4 parts of nanometer additive, 3 parts of plant sterilization extract, 15 parts of adsorption stuffing, water body
5 parts of improver, 7 parts of chitosan.
Preferably, the charcoal is prepared by the following method：Rice straw, cotton stalk are dried to aqueous
Amount is 20% hereinafter, then cutting or smashing, is put into carbide furnace, under limited oxygen condition, be warming up to the speed of 15 DEG C/min
350-450 DEG C, constant temperature keeps 5-10min, is cooled to room temperature with water filtering when going out charcoal, then dries charcoal, crushes to get biology
Charcoal.
Preferably, the ore filler is medical stone, tourmaline, zeolite according to weight ratio 4:2:The mixture of 1 composition.
Preferably, the nanometer additive is nano zine oxide, nano cuprous oxide, nano-titanium dioxide according to weight ratio
1:2:The mixture of 1 composition.
Preferably, the preparation method of the plant sterilization extract is：By Eupatorium adenophorum cauline leaf, moringa seeds, folium artemisiae argyi, aloe
According to weight ratio 3:2:4:The ethyl alcohol that the determining alcohol of opposite 2-4 times of mixture gross mass is 95% is added after 1 crushing, is heated to reflux
1-2h filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to the determining alcohol of 2-4 times of filter residue quality again, is heated back
Flow 1-2h, filtering and impurity removing merges filtered fluid, removes ethyl alcohol, is concentrated into after the 1/3-1/2 of original volume to obtain the final product.
Preferably, the adsorption stuffing is attapulgite, shell powder, diatomite according to weight ratio 3:1:2 compositions mix
Close object.
Preferably, the water body improver is L-AA, five water citric acids, malic acid, lauric acid according to 2:1:2:3
The mixture of composition.
The present invention also provides a kind of preparation methods of antibacterial decontamination environment-friendly high-efficiency water purification agent, include the following steps：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 10-15 minutes, speed of agitator 150-250r/min, sequentially adds mixture A, charcoal made from step 2, after
Continuous stirring 25-35 minutes, obtains mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24-48 hours, it is finished product to be sent into drying in dryer, and drying temperature is 70-80 DEG C, and drying time obtains for 1-2 hours
The antibacterial decontamination environment-friendly high-efficiency water purification agent of invention.
Preferably, the preparation process of the antibacterial decontamination environment-friendly high-efficiency water purification agent is：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 13 minutes, speed of agitator 200r/min, sequentially adds mixture A, charcoal made from step 2, continue to stir
30 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, it is finished product to be sent into drying in dryer, and drying temperature is 75 DEG C, what drying time was invented for 1.5 hours
Antibacterial decontamination environment-friendly high-efficiency water purification agent.
Compared with prior art, the present invention has following advantageous effect：
（1）The charcoal added in a kind of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present invention, had both realized the sustainable of resource
It utilizes, can effectively absorb removal organic polluter not only but also heavy metal ion can be settled.
（2）A kind of nanometer additive of antibacterial decontamination environment-friendly high-efficiency water purification agent addition of the present invention is nano zine oxide, receives
Rice cuprous oxide, nano-titanium dioxide, on the one hand its to bacterial cell membrane have destruction, to play sterilization, disinfection
Effect；On the other hand hydrogen and oxygen can be split water into, to be supplied to the oxygen of aquatic products abundance, is effectively increased water body
Dissolved oxygen amount does not generate any secondary pollution, safety and environmental protection.
（3）The activated carbon added in a kind of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present invention has very strong adsorption capacity
Each pollutant that can effectively absorb in water body effectively purifies water.
（4）Attapulgite, shell powder, the diatomite that a kind of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present invention uses,
On the one hand aggregation sedimentation is carried out to the suspended matter in water, achievees the purpose that purifying sterilizing water, while such as hormone, agriculture can be absorbed
The substances such as medicine, virus, toxin and heavy metal ion, on the other hand it, which is used as, is sustained main body, enables to the oxygenation of the present invention
Water purification agent persistent, each substance slow release, effect is more preferable, and shell powder also has certain bactericidal property in addition.
（5）A kind of plant sterilization extract of antibacterial decontamination environment-friendly high-efficiency water purification agent addition of the present invention, pure plant
Antiseptic, bactericidal effect is strong, to safety of human and livestock, alleviates environmental pollution, broad-spectrum, the quick-acting and good feature of lasting effect increases
Strong bactericidal effect, when carrying out water body disinfection sterilization, the largely microorganisms and pathogenic bacteria in kill water body.
（6）The present invention it is a kind of it is antibacterial decontamination environment-friendly high-efficiency water purification agent addition ore additive be mainly zeolite, vermiculite,
Serpentine can greatly improve the efficiency of water purification agent with activated carbon, attapulgite synergistic effect；The L-AA of addition, five
Water citric acid, malic acid, lauric acid, on the one hand can effectively improve water PH value, can greatly improve the anti-virus ability of aquatic products,
Increase its internal resistance.
（7）A kind of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present invention can largely kill the microorganism in water body
And pathogenic bacteria, energy quick adsorption go removal organic polluter that can settle heavy metal ion again, additionally it is possible to decompose the chlorine residue in water, increase
Add oxygen content in water, environmental protection safe to the human body nontoxic；The oxygenation water purification agent advantages of nontoxic raw materials of the present invention, material are easy simultaneously
, production cost is relatively low, technique is concise, there is higher practical value as oxygenation water purification agent used for aquiculture and good answer
Use foreground.
Specific implementation mode
With reference to specific embodiment, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1.
The antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind of the present embodiment, includes the raw material of following parts by weight：
5 parts of charcoal, 15 parts of ore filler, 3 parts of nanometer additive, 2 parts of plant sterilization extract, 10 parts of adsorption stuffing, water body
4 parts of improver, 6 parts of chitosan.
What the charcoal in the present embodiment was prepared by the following method：Rice straw, cotton stalk are dried to and contained
Water is 20% hereinafter, then cutting or smashing, is put into carbide furnace, under limited oxygen condition, be warming up to the speed of 15 DEG C/min
350 DEG C, constant temperature keeps 5min, is cooled to room temperature with water filtering when going out charcoal, then dries charcoal, crushes to get charcoal.
Ore filler in the present embodiment is medical stone, tourmaline, zeolite according to weight ratio 4:2:The mixture of 1 composition.
Nanometer additive in the present embodiment is nano zine oxide, nano cuprous oxide, nano-titanium dioxide according to weight
Than 1:2:The mixture of 1 composition.
The preparation method of plant sterilization extract in the present embodiment is：By Eupatorium adenophorum cauline leaf, moringa seeds, folium artemisiae argyi, reed
Luxuriant growth is according to weight ratio 3:2:4:The ethyl alcohol that the determining alcohol of opposite 2 times of mixture gross mass is 95% is added after 1 crushing, is heated to reflux
1h filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to the determining alcohol of 2 times of filter residue quality again, is heated to reflux 1h,
Filtering and impurity removing merges filtered fluid, removes ethyl alcohol, is concentrated into behind the 1/3 of original volume to obtain the final product.
Adsorption stuffing in the present embodiment is attapulgite, shell powder, diatomite according to weight ratio 3:1:2 compositions mix
Close object.
Water body improver in the present embodiment is L-AA, five water citric acids, malic acid, lauric acid according to 2:1:2:
The mixture of 3 compositions.
A kind of preparation method of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 10 minutes, speed of agitator 150r/min, sequentially adds mixture A, charcoal made from step 2, continue to stir
25 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24 hours, it is finished product to be sent into drying in dryer, and drying temperature is 70 DEG C, the drying time suppression invented in 1 hour
Bacterium decontaminates environment-friendly high-efficiency water purification agent.
Embodiment 2.
The antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind of the present embodiment, includes the raw material of following parts by weight：
7 parts of charcoal, 25 parts of ore filler, 5 parts of nanometer additive, 4 parts of plant sterilization extract, 20 parts of adsorption stuffing, water body
6 parts of improver, 8 parts of chitosan.
What the charcoal in the present embodiment was prepared by the following method：Rice straw, cotton stalk are dried to and contained
Water is 20% hereinafter, then cutting or smashing, is put into carbide furnace, under limited oxygen condition, be warming up to the speed of 15 DEG C/min
450 DEG C, constant temperature keeps 10min, is cooled to room temperature with water filtering when going out charcoal, then dries charcoal, crushes to get charcoal.
Ore filler in the present embodiment is medical stone, tourmaline, zeolite according to weight ratio 4:2:The mixture of 1 composition.
Nanometer additive in the present embodiment is nano zine oxide, nano cuprous oxide, nano-titanium dioxide according to weight
Than 1:2:The mixture of 1 composition.
The preparation method of plant sterilization extract in the present embodiment is：By Eupatorium adenophorum cauline leaf, moringa seeds, folium artemisiae argyi, reed
Luxuriant growth is according to weight ratio 3:2:4:The ethyl alcohol that the determining alcohol of opposite 4 times of mixture gross mass is 95% is added after 1 crushing, is heated to reflux
2h filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to the determining alcohol of 4 times of filter residue quality again, is heated to reflux 2h,
Filtering and impurity removing merges filtered fluid, removes ethyl alcohol, is concentrated into behind the 1/2 of original volume to obtain the final product.
Adsorption stuffing in the present embodiment is attapulgite, shell powder, diatomite according to weight ratio 3:1:2 compositions mix
Close object.
Water body improver in the present embodiment is L-AA, five water citric acids, malic acid, lauric acid according to 2:1:2:
The mixture of 3 compositions.
A kind of preparation method of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 15 minutes, speed of agitator 250r/min, sequentially adds mixture A, charcoal made from step 2, continue to stir
35 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 48 hours, it is finished product to be sent into drying in dryer, and drying temperature is 80 DEG C, what drying time was invented for 1-2 hours
Antibacterial decontamination environment-friendly high-efficiency water purification agent.
Embodiment 3.
The antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind of the present embodiment, includes the raw material of following parts by weight：
6 parts of charcoal, 20 parts of ore filler, 4 parts of nanometer additive, 3 parts of plant sterilization extract, 15 parts of adsorption stuffing, water body
5 parts of improver, 7 parts of chitosan.
What the charcoal in the present embodiment was prepared by the following method：Rice straw, cotton stalk are dried to and contained
Water is 20% hereinafter, then cutting or smashing, is put into carbide furnace, under limited oxygen condition, be warming up to the speed of 15 DEG C/min
400 DEG C, constant temperature keeps 7min, is cooled to room temperature with water filtering when going out charcoal, then dries charcoal, crushes to get charcoal.
Ore filler in the present embodiment is medical stone, tourmaline, zeolite according to weight ratio 4:2:The mixture of 1 composition.
Nanometer additive in the present embodiment is nano zine oxide, nano cuprous oxide, nano-titanium dioxide according to weight
Than 1:2:The mixture of 1 composition.
The preparation method of plant sterilization extract in the present embodiment is：By Eupatorium adenophorum cauline leaf, moringa seeds, folium artemisiae argyi, reed
Luxuriant growth is according to weight ratio 3:2:4:The ethyl alcohol that the determining alcohol of opposite 3 times of mixture gross mass is 95% is added after 1 crushing, is heated to reflux
1.5h filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to the determining alcohol of 3 times of filter residue quality again, is heated to reflux
1.5h, filtering and impurity removing merge filtered fluid, remove ethyl alcohol, are concentrated into after the 1/3-1/2 of original volume to obtain the final product.
Adsorption stuffing in the present embodiment is attapulgite, shell powder, diatomite according to weight ratio 3:1:2 compositions mix
Close object.
Water body improver in the present embodiment is L-AA, five water citric acids, malic acid, lauric acid according to 2:1:2:
The mixture of 3 compositions.
A kind of preparation method of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 13 minutes, speed of agitator 200r/min, sequentially adds mixture A, charcoal made from step 2, continue to stir
30 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, it is finished product to be sent into drying in dryer, and drying temperature is 75 DEG C, what drying time was invented for 1.5 hours
Antibacterial decontamination environment-friendly high-efficiency water purification agent.
A kind of antibacterial decontamination environment-friendly high-efficiency water purification agent of the present invention can largely kill microorganism in water body and
Pathogenic bacteria, energy quick adsorption go removal organic polluter that can settle heavy metal ion again, additionally it is possible to decompose the chlorine residue in water, increase
Oxygen content in water, environmental protection safe to the human body are nontoxic；Simultaneously the present invention oxygenation water purification agent advantages of nontoxic raw materials, material be easy to get,
Production cost is relatively low, technique is concise, has higher practical value and good application as oxygenation water purification agent used for aquiculture
Foreground.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. a kind of antibacterial decontamination environment-friendly high-efficiency water purification agent, which is characterized in that include the raw material of following parts by weight：
5-7 parts of charcoal, 15-25 parts of ore filler, 3-5 parts of nanometer additive, 2-4 parts of plant sterilization extract, adsorption stuffing
10-20 parts, 4-6 parts of water body improver, 6-8 parts of chitosan.
2. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1, which is characterized in that the antibacterial decontamination ring
Protect the raw material that efficient water-purifying agent includes following parts by weight：
6 parts of charcoal, 20 parts of ore filler, 4 parts of nanometer additive, 3 parts of plant sterilization extract, 15 parts of adsorption stuffing, water body
5 parts of improver, 7 parts of chitosan.
3. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the charcoal
It is prepared by the following method：Rice straw, cotton stalk are dried to water content 20% hereinafter, then cutting or powder
Essence is put into carbide furnace, and under limited oxygen condition, 350-450 DEG C is warming up to the speed of 15 DEG C/min, and constant temperature keeps 5-10min,
It is cooled to room temperature with water filtering when going out charcoal, then dries charcoal, is crushed to get charcoal.
4. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the ore is filled out
Material is medical stone, tourmaline, zeolite according to weight ratio 4:2:The mixture of 1 composition.
5. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the nanometer adds
Add that object is nano zine oxide, nano cuprous oxide, nano-titanium dioxide is according to weight ratio 1:2:The mixture of 1 composition.
6. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the plant kills
The preparation method of fungus extract is：By Eupatorium adenophorum cauline leaf, moringa seeds, folium artemisiae argyi, aloe according to weight ratio 3:2:4:Add after 1 crushing
Enter the ethyl alcohol that the determining alcohol of opposite 2-4 times of mixture gross mass is 95%, is heated to reflux 1-2h, filters to obtain filter residue, again by filter residue
It is secondary that the ethyl alcohol for being 95% relative to the determining alcohol of 2-4 times of filter residue quality is added, it is heated to reflux 1-2h, filtering and impurity removing merges and filters
Liquid removes ethyl alcohol, is concentrated into after the 1/3-1/2 of original volume to obtain the final product.
7. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the absorption is filled out
Material is attapulgite, shell powder, diatomite according to weight ratio 3:1:The mixture of 2 compositions.
8. the antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind according to claim 1 or 2, which is characterized in that the water body changes
Kind agent is L-AA, five water citric acids, malic acid, lauric acid according to 2:1:2:The mixture of 3 compositions.
9. a kind of method preparing antibacterial decontamination environment-friendly high-efficiency water purification agent as claimed in claim 1 or 2, which is characterized in that packet
Include following steps：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 10-15 minutes, speed of agitator 150-250r/min, sequentially adds mixture A, charcoal made from step 2, after
Continuous stirring 25-35 minutes, obtains mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 24-48 hours, it is finished product to be sent into drying in dryer, and drying temperature is 70-80 DEG C, and drying time obtains for 1-2 hours
The antibacterial decontamination environment-friendly high-efficiency water purification agent of invention.
10. a kind of preparation method of antibacterial decontamination environment-friendly high-efficiency water purification agent according to claim 9, which is characterized in that institute
Stating step is：
Step 1 weighs prepare each component raw material as required；
Ore filler, adsorption stuffing are added in high speed disintegrator and are crushed, added in grinder and be fully ground by step 2, mistake
100 mesh sieve, and obtain mixture A；
Chitosan, nanometer additive, water body improver, plant sterilization extract, suitable water are added to blender by step 3
In, it stirs 13 minutes, speed of agitator 200r/min, sequentially adds mixture A, charcoal made from step 2, continue to stir
30 minutes, obtain mixture B；
Mixture B made from step 3 is mixed and molding granulation in pellet press is added by step 4, then shaped granule is natural
It dries, after 36 hours, it is finished product to be sent into drying in dryer, and drying temperature is 75 DEG C, what drying time was invented for 1.5 hours
Antibacterial decontamination environment-friendly high-efficiency water purification agent.
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