CN109956561A - A kind of water quality cleansing agent and preparation method thereof - Google Patents
A kind of water quality cleansing agent and preparation method thereof Download PDFInfo
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- CN109956561A CN109956561A CN201910275076.8A CN201910275076A CN109956561A CN 109956561 A CN109956561 A CN 109956561A CN 201910275076 A CN201910275076 A CN 201910275076A CN 109956561 A CN109956561 A CN 109956561A
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/34—Biological treatment of water, waste water, or sewage characterised by the microorganisms used
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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Abstract
The present invention discloses a kind of water quality cleansing agent and preparation method thereof, is related to technical field of aquaculture.The water quality cleansing agent includes the raw material of following parts by weight: 8~11 parts and 50~65 parts 9~12 parts of the Chinese bulbul, 6~9 parts of the bark of ash, 8~11 parts of the coptis, 15~30 parts of radix rehmanniae recen, 10~19 parts of Asian puccoon, 15~18 parts of Cortex Phellodendri, 6~12 parts of kuh-seng, 16~18 parts of garden burnet, 9~12 parts of Java brucea, 10~15 parts of cordate houttuynia, 15~18 parts of the tuber of stemona, 12~15 parts of folium artemisiae argyi, 12~18 parts of garlic, 20~25 parts of tourmaline particles, 25~28 parts of medical stone powder, mix bacterium agent ethyl alcohol.The present invention is intended to provide a kind of impurity for not only adsorbing, settling in water body, but also the water quality cleansing agent of Nitrite, ammonia-nitrogen content can be effectively reduced.
Description
Technical field
The present invention relates to technical field of aquaculture, in particular to a kind of water quality cleansing agent and preparation method thereof.
Background technique
China's aquaculture production accounts for about 60% or more of whole world aquaculture production, accounts for about national total aquatic product production
78% or more, be qualified aquaculture big country, the world.With the high speed development of China's culture fishery, high density collection
The aquaculture model of reduction, which causes a large amount of residual bait, excrement, animals and plants corpse etc. to be deposited on pond bottom, causes black smelly bed mud siltation,
A large amount of disinfectants, antibiotic, the agrochemical put into during cultivation enters water body so that water eutrophication, noxious material are rich
Collection, so as to cause severe water pollution, aquatic animal disease takes place frequently.Meanwhile untreated breeding wastewater contains and largely has
The nutrients such as machine polluter, suspended matter, anti-microbial agents, medicament residue and nitrogen, phosphorus, direct emission can make Its Adjacent Waters
It is heavily contaminated, or even influence human health.Therefore, it is necessary to carry out purified treatment to aquaculture wastewater.
Traditional Water body cleansing agent main component is adsorbent, is placed directly in water body and recycles impurity absorption therein,
Defect is that catharsis is limited, and cleaning is not thorough, weaker to the clean-up effect of nitrite, ammonia nitrogen in water body.
Summary of the invention
The main object of the present invention is to propose a kind of water quality cleansing agent and preparation method thereof, it is desirable to provide one kind both adsorbed,
The impurity in water body is settled, and the water quality cleansing agent of the content of Nitrite, ammonia nitrogen can be effectively reduced.
To achieve the above object, the present invention proposes a kind of water quality cleansing agent, is used for aquaculture, the water quality cleansing agent packet
Include the raw material of following parts by weight: 9~12 parts of the Chinese bulbul, 6~9 parts of the bark of ash, 8~11 parts of the coptis, 15~30 parts of radix rehmanniae recen, Asian puccoon
10~19 parts, 15~18 parts of Cortex Phellodendri, 6~12 parts of kuh-seng, 16~18 parts of garden burnet, 9~12 parts of Java brucea, 10~15 parts of cordate houttuynia,
15~18 parts of the tuber of stemona, 12~18 parts of garlic, 20~25 parts of tourmaline particles, 25~28 parts of medical stone powder, mixes 12~15 parts of folium artemisiae argyi
8~11 parts and 50~65 parts ethyl alcohol of combined bacteria agent.
Optionally, the mix bacterium agent includes photosynthetic bacteria agent, denitrifying bacteria agent and bacillus agent, wherein described
The concentration of photosynthetic bacteria agent is 2.0 × 108~3.5 × 108CFU/g, the concentration of the denitrifying bacteria agent are 1.0 × 108~
2.5×108CFU/g, the concentration of the bacillus agent are 1.5 × 108~3.0 × 108CFU/g。
Optionally, the partial size of the tourmaline particles is 100~120 mesh.
Optionally, the partial size of the medical stone powder is 170~200 mesh.
In addition, being used to prepare above-mentioned water quality cleansing agent, institute the invention also provides a kind of preparation method of water quality cleansing agent
State the preparation method of water quality cleansing agent the following steps are included:
By the Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia, the tuber of stemona, folium artemisiae argyi
It is crushed with garlic note, mixing, obtains mixed component A；
It after the mixed component A, second alcohol and water are mixed, is boiled, retain medical fluid and the medical fluid is concentrated, be made
Extracting solution；
Mix bacterium agent, tourmaline particles, medical stone powder and the extracting solution are stirred and evenly mixed, mixed component B is obtained；
After the mixed component B modifier treatment, water quality cleansing agent of pelletizing to obtain.
Optionally, by the Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia, hundred
In the step of portion, folium artemisiae argyi and garlic crush and mix, and obtain mixed component A, the partial size of the mixed component A is 100~120 mesh.
Optionally, it after the mixed component A, second alcohol and water being mixed, is boiled, reservation medical fluid is simultaneously dense by the medical fluid
Contracting, be made extracting solution the step of include:
By the mixed component A, second alcohol and water mix after, under conditions of 5~8Mpa, 90~120 DEG C boil 120~
150min stands to tanning liquid temperature and is down to room temperature, filters, and retains medical fluid, and revolving obtains extracting solution after removing ethyl alcohol, wherein
The mass ratio of the water and ethyl alcohol is (2~3): 1.
Optionally, mix bacterium agent, tourmaline particles, medical stone powder and the extracting solution are stirred and evenly mixed, obtains mixed component B
The step of in, when the stirring, mixing speed is 80~110r/min, and mixing time is 45~60min.
Optionally, after the mixed component B modifier treatment, will pelletize water quality cleansing agent the step of in, the quenched place
When reason, refining temperature is 45~60 DEG C, and conditioning period is 50~60s.
Optionally, after the mixed component B modifier treatment, will pelletize water quality cleansing agent the step of in, when the granulation,
The mixed component B is sent into granulator and is pelletized, the ring moulds aperture of the granulator is set as 2.0~4.0mm, ring moulds
Compression ratio is set as 1:(4~6).
In technical solution provided by the invention, the Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Cortex Phellodendri, kuh-seng, garden burnet and Java brucea
Has effects that clearing heat and detoxicating, purging fire for removing toxin, Asian puccoon has bactericidal effect, and cordate houttuynia has the function of antibacterial, antiviral, Ke Yiti
The immunity of high fish body, the tuber of stemona are easy parasitic helminth with aquatic livestock and have expeling effect, wormwood to some in water body
Have the function of hemostasis, anti-inflammatory, these drug matchings are used not only can be with purifying water body, additionally it is possible to effectively improve aquatic livestock
Disease resistance, reduce the death rate of aquatic livestock；Nitrite is effectively reduced using mix bacterium agent, ammonia nitrogen contains
Amount, improves the concentration of oxygen in water；Tourmaline not only can effectively kill the bacterium in water, can also adjust the pH of water body
Value to neutrality, activated water molecule increases water oxygen level, to promote growth of aerobic microorganisms in mix bacterium agent, and then improves
The degradation rate of nitrite, ammonia nitrogen；Medical stone can not only adsorb the toxicant in water, and purifying water body can be with mineralising
Water body improves water quality, keeps aquatic livestock more healthy.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
Other relevant attached drawings are obtained according to these attached drawings.
Fig. 1 is the flow diagram of an embodiment of the preparation method of the water quality cleansing agent proposed.
The embodiments will be further described with reference to the accompanying drawings for the realization, the function and the advantages of the object of the present invention.
Specific embodiment
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, according to normal conditions or manufacturer builds
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
It should be noted that the meaning of the "and/or" occurred in full text, including three schemes arranged side by side, with " A and/or B "
For, the scheme including A scheme or B scheme or A and B while satisfaction.In addition, technical solution between each embodiment can be with
It is combined with each other, but must be based on can be realized by those of ordinary skill in the art, when phase occurs in the combination of technical solution
Mutual contradiction or cannot achieve when, will be understood that the combination of this technical solution is not present, also not the present invention claims protection scope
Within.
Traditional Water body cleansing agent main component is adsorbent, is placed directly in water body and recycles impurity absorption therein,
Defect is that catharsis is limited, and cleaning is not thorough, weaker to the clean-up effect of nitrite, ammonia nitrogen in water body.
In consideration of it, the present invention proposes a kind of water quality cleansing agent, it to be used for aquaculture, it is desirable to provide one kind was both adsorbed, settled
Impurity in water body, and the water quality cleansing agent of the content of Nitrite, ammonia nitrogen can be effectively reduced.The water quality cleansing agent
Raw material including following parts by weight: 9~12 parts of the Chinese bulbul, 6~9 parts of the bark of ash, 8~11 parts of the coptis, 15~30 parts of radix rehmanniae recen, purple
Careless 10~19 parts, 15~18 parts of Cortex Phellodendri, 6~12 parts of kuh-seng, 16~18 parts of garden burnet, 9~12 parts of Java brucea, cordate houttuynia 10~15
Part, 15~18 parts of the tuber of stemona, 12~15 parts of folium artemisiae argyi, 12~18 parts of garlic, 20~25 parts of tourmaline particles, medical stone powder 25~28
8~11 parts and 50~65 parts part, mix bacterium agent ethyl alcohol.
Wherein, the mix bacterium agent includes photosynthetic bacteria agent, denitrifying bacteria agent and bacillus agent, wherein the light
The concentration for closing bacteriocin is 2.0 × 108~3.5 × 108CFU/g, the concentration of the denitrifying bacteria agent are 1.0 × 108~2.5
×108CFU/g, the concentration of the bacillus agent are 1.5 × 108~3.0 × 108CFU/g.The partial size of the tourmaline particles
For 100~120 mesh.The partial size of the medical stone powder is 170~200 mesh.
The Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Cortex Phellodendri, kuh-seng, garden burnet and Java brucea have clearing heat and detoxicating, purging fire for removing toxin
Effect, Asian puccoon have a bactericidal effect, and cordate houttuynia has the function of antibacterial, antiviral, the immunity of fish body can be improved, the tuber of stemona is to water
Some in body to be easy parasitic helminth with aquatic livestock and have an expeling effect, wormwood has the function of hemostasis, anti-inflammatory, by this
A little drug matchings use not only can be with purifying water body, additionally it is possible to effectively improve the disease resistance of aquatic livestock, reduce aquatic livestock
The death rate.
Photosynthetic bacteria is some photosynthetic bacteriums that non-oxygen-production can be carried out using luminous energy, during self-reproduction
Carbon source, hydrogen donor can be done using small organic molecule, do nitrogen using water environment dissolved nitrogen (such as ammonium, nitrate, nitrite)
Source synthesizes organic nitrogen compound, therefore can digest small organic molecule, ammonium, nitrate, nitrite in water, and can improve in water
The concentration of dissolved oxygen plays the role of purifying water.Bacillus belongs to gram-positive bacteria, aerobic, can generate spore, is one
Class has the heterotroph of the Digest enzyme of high activity, high temperature resistant, resisting stress.Nitrate in water body, Asia can be effectively reduced in it
The content of nitrate, thus play the role of improving water quality, meanwhile, can also generate one kind in the metabolic process has inhibition or kills
The subtilin of other dead microorganisms, thus to improve water quality.Since photosynthetic bacteria cannot be using some big in water environment
Therefore photosynthetic bacteria and bacillus are combined by molecular organic, first by bacillus by the larger molecular organics in water body
(such as protein, fat, sugar) resolves into small organic molecule (such as amino acid, lower fatty acid, small molecular sugar), then again by
Photosynthetic bacteria, which is decomposed, to be utilized, so that the large and small molecular organic in water body be made to be fully utilized, clean-up effect reaches best.This
Outside, nitrobacteria is a kind of chemosynthetic autotroph bacterium, is the main existence energy using ammonia or nitrite, using carbon dioxide as
A kind of bacterium of primary carbon source is made of nitrite bacteria and two class physiology subgroup of nitrobacteria.Nitrite bacteria completes NH4 +It arrives
NO2 ?Conversion；And nitrobacteria completes NO2 ?To NO3 ?Conversion, to make the ammoniacal nitrogen and nitrous acid toxic to aquatic animal
Salt is converted into the nitrate nontoxic to aquatic animal, and nitrobacteria is doped in composite bacteria agent, compensates for photosynthetic bacteria well
Defect lower to Nitrite transformation efficiency and low to ammonia nitrogen conversion efficiency bacillus.Three's combination, effectively reduces
The content of Nitrite, ammonia nitrogen and active phosphorus.
Tourmaline is a kind of natural minerals of multielement, and tourmaline particles are with environmental functional property: having far infrared hair
Function is penetrated, so as to kill the bacterium in water；Can produce anion under the conditions of passive, so as to adjust the pH value of water to
It is neutral；Activated water molecule increases molecular oxygen-containing amount, to promote aerobic microbiological in mix bacterium agent (such as in composite bacteria agent
Bacillus, nitrobacteria) growth, and then improve the degradation rate of nitrite, ammonia nitrogen.Meanwhile tourmaline particles partial size compared with
Hour, water can be made to release more anions, and the far infrared wave band of little particulate release more can effectively kill water bacteria, because
This, in the present embodiment, the partial size of the tourmaline particles is 100~120 mesh.
Medical stone is a kind of natural medicinal stone, rich in multiple beneficial in the nutrient of human health, and is had stronger molten
Property and adsorptivity out.Water body is handled with medical stone, on the one hand, can be adsorbed in water by suction-operated because of the agriculture caused by polluting
Medicine residue and various bacteria, purifying water body；On the other hand, beneficial element can also be dissolved out into water, mineralising water body improves water
Matter keeps aquatic livestock more healthy.When too small due to medical stone powder partial size, too small particle can suspend in water, it is difficult to it separates,
Water quality is influenced instead, and when partial size is excessive, absorption and dissolution efficiency in water can be relatively low, therefore, in the present embodiment, excellent
Selecting partial size is the medical stone powder of 170~200 mesh.
In addition, being used to prepare above-mentioned water quality cleansing agent, institute the invention also provides a kind of preparation method of water quality cleansing agent
State the preparation method of water quality cleansing agent the following steps are included:
Step S10, by the Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia,
The tuber of stemona, folium artemisiae argyi and garlic note are crushed, are mixed, and obtain mixed component A.
The partial size of the mixed component A is 100~120 mesh.
The Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia, the tuber of stemona, folium artemisiae argyi and
Garlic is solid, to make its effective component be fully extracted out, before extraction, and preferably by its pulverization process, after crushing,
The partial size of mixed component A is preferably 100~120 mesh.
Step S20, it after mixing the mixed component A, second alcohol and water, is boiled, retains medical fluid and by the medical fluid
Extracting solution is made in concentration.
The effective component of Chinese medicine is extracted, there are many method, ethyl alcohol can be added, water directly decocts, it can also be with
It is dipped into ethanol.Sufficiently and rapidly to extract the effective component in medicinal material, the utilization rate of medicinal material is improved, in this hair
In a bright embodiment, extracted using the method that high pressure boils, concrete operations are as follows:
By the mixed component A, second alcohol and water mix after, under conditions of 5~8Mpa, 90~120 DEG C boil 120~
150min stands to tanning liquid temperature and is down to room temperature, filters, and retains medical fluid, and revolving obtains extracting solution after removing ethyl alcohol, wherein
The mass ratio of the water and ethyl alcohol is (2~3): 1.
Step S30, mix bacterium agent, tourmaline particles, medical stone powder and the extracting solution are stirred and evenly mixed, obtains mixed component
B。
When the stirring, mixing speed is 80~110r/min, and mixing time is 45~60min.
Step S40, by after the mixed component B modifier treatment, water quality cleansing agent of pelletizing to obtain.
Before granulation, first by mixed component B modifier treatment, the water content of mixed component B not only can be effectively controlled, benefit
In pelletizing forming, the stability of water quality cleansing agent in water can also be improved, it is made to give full play to the effect of purifying water.At this
In embodiment, when carrying out modifier treatment, refining temperature is set as 45~60 DEG C, and conditioning period is set as 50~60s, preferably
60s.By strict control conditioning period and temperature, water quality cleansing agent can be avoided while ensuring preferable quenched effect
Effective component be destroyed.
In addition, ring moulds compression ratio is the ratio of the effective length in ring moulds hole and the minimum diameter in ring moulds hole, setting is suitable
Ring moulds compression ratio can control the hardness of the particle of extrusion.It in the present embodiment, can will be described when carrying out granulation step
Mixed component B is sent into granulator and pelletizes, and the ring moulds aperture of the granulator is set as 2.0~4.0mm, ring moulds compression ratio
It is set as 1:(4~6).
Technical solution of the present invention is described in further detail below in conjunction with specific embodiments and the drawings, it should be understood that
Following embodiment is only used to explain the present invention, is not intended to limit the present invention.
Embodiment 1
By 2.0 × 108The agent of CFU/g photosynthetic bacteria, 2.2 × 108The agent of CFU/g denitrifying bacteria, 1.5 × 108CFU/g gemma
Bacillus agent mixing, is made mix bacterium agent, spare.
With weighing the 12g Chinese bulbul, the 6g bark of ash, the 11g coptis, 20g radix rehmanniae recen, 10g Asian puccoon, 18g Cortex Phellodendri, 11g kuh-seng, 16g
Elm, 9g Java brucea, 15g cordate houttuynia, the 17g tuber of stemona, 14g folium artemisiae argyi and 15g garlic are sent into pulverizer and are crushed to 120 mesh, must mix
Component A.
50g ethyl alcohol and 100g water are added in mixed component A, stirred evenly.Mixture after being stirred is added together
Enter into high pressure tanning kettle, boiled under conditions of 7Mpa, 110 DEG C, after boiling 150min, stand cooling, when tanning liquid
Temperature be cooled to room temperature, will tanning liquid filtering, retain medical fluid.Medical fluid is sent into Rotary Evaporators, revolving removes ethyl alcohol, obtains
Extracting solution.
120 mesh tourmaline particles 25g, 180 mesh medical stone powder 25g, mix bacterium agent 8g are weighed, are added in extracting solution,
It is stirred under the speed of 80r/min, mixed component B is made after stirring 45min.
Mixed component B is sent into granulator, it is 60 DEG C that the technological parameter for adjusting granulator, which is refining temperature, conditioning period
For 60s, ring moulds aperture is set as 2.0mm, and ring moulds compression ratio is set as 1:5, obtains water quality cleansing agent.Measure the water quality cleansing agent
Hardness is 0.4kgf；Moisture content is 8wt%.
Embodiment 2
By 3.5 × 108The agent of CFU/g photosynthetic bacteria, 1.0 × 108The agent of CFU/g denitrifying bacteria, 3.0 × 108CFU/g gemma
Bacillus agent mixing, is made mix bacterium agent, spare.
With weighing the 9g Chinese bulbul, the 9g bark of ash, the 8g coptis, 15g radix rehmanniae recen, 19g Asian puccoon, 17g Cortex Phellodendri, 10g kuh-seng, 16.4g
Elm, 10g Java brucea, 10g cordate houttuynia, the 16g tuber of stemona, 13g folium artemisiae argyi and 16g garlic are sent into pulverizer and are crushed to 110 mesh, obtain mixed
It is combined a point A.
55g ethyl alcohol and 165g water are added in mixed component A, stirred evenly.Mixture after being stirred is added together
Enter into high pressure tanning kettle, boiled under conditions of 6Mpa, 120 DEG C, after boiling 130min, stand cooling, when tanning liquid
Temperature be cooled to room temperature, will tanning liquid filtering, retain medical fluid.Medical fluid is sent into Rotary Evaporators, revolving removes ethyl alcohol, obtains
Extracting solution.
110 mesh tourmaline particles 20g, 200 mesh medical stone powder 27g, mix bacterium agent 10g are weighed, are added in extracting solution,
It is stirred under the speed of 90r/min, mixed component B is made after stirring 50min.
Mixed component B is sent into granulator, it is 45 DEG C that the technological parameter for adjusting granulator, which is refining temperature, conditioning period
For 60s, ring moulds aperture is set as 3.0mm, and ring moulds compression ratio is set as 1:4, obtains water quality cleansing agent.Measure the water quality cleansing agent
Hardness is 0.6kgf；Moisture content is 10wt%.
Embodiment 3
By 3.0 × 108The agent of CFU/g photosynthetic bacteria, 2.5 × 108The agent of CFU/g denitrifying bacteria, 2.0 × 108CFU/g gemma
Bacillus agent mixing, is made mix bacterium agent, spare.
With weighing the 10g Chinese bulbul, the 8g bark of ash, the 10g coptis, 30g radix rehmanniae recen, 12g Asian puccoon, 16g Cortex Phellodendri, 6g kuh-seng, 18g
Elm, 11g Java brucea, 11g cordate houttuynia, the 15g tuber of stemona, 12g folium artemisiae argyi and 18g garlic are sent into pulverizer and are crushed to 100 mesh, obtain mixed
It is combined a point A.
60g ethyl alcohol and 150g water are added in mixed component A, stirred evenly.Mixture after being stirred is added together
Enter into high pressure tanning kettle, boiled under conditions of 5Mpa, 100 DEG C, after boiling 120min, stand cooling, when tanning liquid
Temperature be cooled to room temperature, will tanning liquid filtering, retain medical fluid.Medical fluid is sent into Rotary Evaporators, revolving removes ethyl alcohol, obtains
Extracting solution.
100 mesh tourmaline particles 21g, 170 mesh medical stone powder 26g, mix bacterium agent 9g are weighed, are added in extracting solution,
It is stirred under the speed of 100r/min, mixed component B is made after stirring 60min.
Mixed component B is sent into granulator, it is 50 DEG C that the technological parameter for adjusting granulator, which is refining temperature, conditioning period
For 50s, ring moulds aperture is set as 4.0mm, and ring moulds compression ratio is set as 1:6, obtains water quality cleansing agent.Measure the water quality cleansing agent
Hardness is 0.5kgf；Moisture content is 9wt%.
Embodiment 4
By 2.5 × 108The agent of CFU/g photosynthetic bacteria, 1.5 × 108The agent of CFU/g denitrifying bacteria, 2.5 × 108CFU/g gemma
Bacillus agent mixing, is made mix bacterium agent, spare.
With weighing the 11g Chinese bulbul, the 7g bark of ash, the 9g coptis, 25g radix rehmanniae recen, 15g Asian puccoon, 15g Cortex Phellodendri, 12g kuh-seng, 17g
Elm, 12g Java brucea, 12g cordate houttuynia, the 18g tuber of stemona, 12g folium artemisiae argyi and 14g garlic are sent into pulverizer and are crushed to 100 mesh, obtain mixed
It is combined a point A.
65g ethyl alcohol and 130g water are added in mixed component A, stirred evenly.Mixture after being stirred is added together
Enter into high pressure tanning kettle, boiled under conditions of 8Mpa, 100 DEG C, after boiling 140min, stand cooling, when tanning liquid
Temperature be cooled to room temperature, will tanning liquid filtering, retain medical fluid.Medical fluid is sent into Rotary Evaporators, revolving removes ethyl alcohol, obtains
Extracting solution.
100 mesh tourmaline particles 22g, 180 mesh medical stone powder 28g, mix bacterium agent 11g are weighed, are added in extracting solution,
It is stirred under the speed of 100r/min, mixed component B is made after stirring 55min.
Mixed component B is sent into granulator, it is 60 DEG C that the technological parameter for adjusting granulator, which is refining temperature, conditioning period
For 55s, ring moulds aperture is set as 3.0mm, and ring moulds compression ratio is set as 1:5, obtains water quality cleansing agent.Measure the water quality cleansing agent
Hardness is 0.4kgf；Moisture content is 8wt%.
Embodiment 5
By 2.8 × 108The agent of CFU/g photosynthetic bacteria, 2.0 × 108The agent of CFU/g denitrifying bacteria, 1.8 × 108CFU/g gemma
Bacillus agent mixing, is made mix bacterium agent, spare.
With weighing the 10g Chinese bulbul, the 6g bark of ash, the 7g coptis, 18g radix rehmanniae recen, 17g Asian puccoon, 17g Cortex Phellodendri, 8g kuh-seng, 17.5g
16~18 parts of elm, 9~12 parts of 9g Java brucea, 14g cordate houttuynia, the 15g tuber of stemona, 15g folium artemisiae argyi and 12g garlic are sent into powder in pulverizer
120 mesh are broken to, mixed component A is obtained.
60g ethyl alcohol and 180g water are added in mixed component A, stirred evenly.Mixture after being stirred is added together
Enter into high pressure tanning kettle, boiled under conditions of 6Mpa, 90 DEG C, after boiling 135min, stand cooling, when tanning liquid
Temperature is cooled to room temperature, and by tanning liquid filtering, retains medical fluid.Medical fluid is sent into Rotary Evaporators, revolving removes ethyl alcohol, must mention
Take liquid.
120 mesh tourmaline particles 24g, 190 mesh medical stone powder 25g, mix bacterium agent 10g are weighed, are added in extracting solution,
It is stirred under the speed of 110r/min, mixed component B is made after stirring 45min.
Mixed component B is sent into granulator, it is 55 DEG C that the technological parameter for adjusting granulator, which is refining temperature, conditioning period
For 60s, ring moulds aperture is set as 2.0mm, and ring moulds compression ratio is set as 1:4, obtains water quality cleansing agent.Measure the water quality cleansing agent
Hardness is 0.6kgf；Moisture content is 11wt%.
Application effect detects (one)
The ratio of 45g water quality cleansing agent is added in every cube of aquaculture pond sewage, respectively prepares above-described embodiment 1~5
Water quality cleansing agent is uniformly shed into hybridized prussian carp aquaculture pond, is shed within every 13 days primary.Blank control is set simultaneously.Water treatment
Effect is as shown in table 1.
1 hybridized prussian carp culturing pool treatment effect of table
By upper table 1 it is found that compared with blank control group, the test group of the water quality water purification agent of Examples 1 to 5 preparation has been shed
Ammonia nitrogen, nitrate nitrogen, nitrite nitrogen, COD value significantly reduce, dissolved oxygen concentration dramatically increases, and hybridized prussian carp survival rate is significantly
Rise, illustrates that water quality cleansing agent clean-up effect proposed by the present invention is significant, ammonia nitrogen in water body, nitrate nitrogen, Asia can be effectively reduced
Nitrate nitrogen, COD content improve the concentration of dissolved oxygen in aquaculture pond, are conducive to the cultivation of hybridized prussian carp.
Application effect detects (two)
The ratio of 45g water quality cleansing agent is added in every cube of aquaculture pond sewage, respectively prepares above-described embodiment 1~5
Water quality cleansing agent is uniformly shed into river prawn aquaculture pond, is shed within every 12 days primary.Blank control is set simultaneously.Water treatment effect
As shown in table 2.
2 river prawn culturing pool treatment effect of table
By upper table 2 it is found that compared with blank control group, the test group of the water quality water purification agent of Examples 1 to 5 preparation has been shed
Ammonia nitrogen, nitrate nitrogen, nitrite nitrogen, COD value significantly reduce, dissolved oxygen concentration dramatically increases, river prawn survival rate substantial increase,
Illustrate that water quality cleansing agent clean-up effect proposed by the present invention is significant, ammonia nitrogen in water body, nitrate nitrogen, nitrous state can be effectively reduced
Nitrogen, COD content improve the concentration of aquaculture pond oxygen in water, are conducive to the cultivation of river prawn.
Application effect detects (three)
The ratio of 45g water quality cleansing agent is added in every cube of aquaculture pond sewage, respectively prepares above-described embodiment 1~5
Water quality cleansing agent is uniformly shed into turtle culture pond, is shed within every 15 days primary.Blank control is set simultaneously.Water treatment effect
As shown in table 3.
3 turtle culture pond water treatment efficiency of table
By upper table 3 it is found that compared with blank control group, the test group of the water quality water purification agent of Examples 1 to 5 preparation has been shed
Ammonia nitrogen, nitrate nitrogen, nitrite nitrogen, COD value significantly reduce, dissolved oxygen concentration dramatically increases, soft-shelled turtle survival rate substantial increase,
Illustrate that water quality cleansing agent clean-up effect proposed by the present invention is significant, ammonia nitrogen in water body, nitrate nitrogen, nitrous state can be effectively reduced
Nitrogen, COD content improve the concentration of dissolved oxygen in aquaculture pond, are conducive to the cultivation of soft-shelled turtle.
The above is only a preferred embodiment of the present invention, is not intended to limit the scope of the invention, for this field
For technical staff, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any
Modification, equivalent replacement, improvement etc. should all be included within the scope of the present invention.
Claims (10)
1. a kind of water quality cleansing agent is used for aquaculture, which is characterized in that the water quality cleansing agent includes following parts by weight
Raw material: 9~12 parts of the Chinese bulbul, 6~9 parts of the bark of ash, 8~11 parts of the coptis, 15~30 parts of radix rehmanniae recen, 10~19 parts of Asian puccoon, Cortex Phellodendri 15
~18 parts, 6~12 parts of kuh-seng, 16~18 parts of garden burnet, 9~12 parts of Java brucea, 10~15 parts of cordate houttuynia, 15~18 parts of the tuber of stemona, Chinese mugwort
12~15 parts of leaf, 12~18 parts of garlic, 20~25 parts of tourmaline particles, 25~28 parts of medical stone powder, 8~11 parts of mix bacterium agent and
50~65 parts of ethyl alcohol.
2. water quality cleansing agent as described in claim 1, which is characterized in that the mix bacterium agent includes photosynthetic bacteria agent, anti-nitre
Change bacteriocin and bacillus agent, wherein the concentration of the photosynthetic bacteria agent is 2.0 × 108~3.5 × 108CFU/g is described anti-
The concentration of nitrobacteria agent is 1.0 × 108~2.5 × 108CFU/g, the concentration of the bacillus agent are 1.5 × 108~3.0
×108CFU/g。
3. water quality cleansing agent as described in claim 1, which is characterized in that the partial size of the tourmaline particles is 100~120
Mesh.
4. water quality cleansing agent as described in claim 1, which is characterized in that the partial size of the medical stone powder is 170~200 mesh.
5. a kind of preparation method of such as described in any item water quality cleansing agents of Claims 1-4, which is characterized in that including following
Step:
By the Chinese bulbul, the bark of ash, the coptis, radix rehmanniae recen, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia, the tuber of stemona, folium artemisiae argyi and big
Garlic powder is broken and mixes, and obtains mixed component A；
It after the mixed component A, second alcohol and water are mixed, is boiled, retain medical fluid and the medical fluid is concentrated, be made and extract
Liquid；
Mix bacterium agent, tourmaline particles, medical stone powder and the extracting solution are stirred and evenly mixed, mixed component B is obtained；
After the mixed component B modifier treatment, water quality cleansing agent of pelletizing to obtain.
6. the preparation method of water quality cleansing agent as claimed in claim 5, which is characterized in that by the Chinese bulbul, the bark of ash, the coptis, life
Glutinous rehmannia, Asian puccoon, Cortex Phellodendri, kuh-seng, garden burnet, Java brucea, cordate houttuynia, the tuber of stemona, folium artemisiae argyi and garlic crush and mix, and obtain mixed component A
The step of in, the partial size of the mixed component A is 100~120 mesh.
7. the preparation method of water quality cleansing agent as claimed in claim 5, which is characterized in that by the mixed component A, ethyl alcohol and
It after water mixing, is boiled, retain medical fluid and includes: the step of being concentrated the medical fluid, extracting solution is made
By the mixed component A, second alcohol and water mix after, under conditions of 5~8Mpa, 90~120 DEG C boil 120~
150min stands to tanning liquid temperature and is down to room temperature, filters, and retains medical fluid, and revolving obtains extracting solution after removing ethyl alcohol, wherein
The mass ratio of the water and ethyl alcohol is (2~3): 1.
8. the preparation method of water quality cleansing agent as claimed in claim 5, which is characterized in that by mix bacterium agent, tourmaline particles,
In the step of medical stone powder and the extracting solution stir and evenly mix, obtain mixed component B, when the stirring, mixing speed is 80~
110r/min, mixing time are 45~60min.
9. the preparation method of water quality cleansing agent as claimed in claim 5, which is characterized in that by the quenched place mixed component B
After reason, pelletize water quality cleansing agent the step of in, when the modifier treatment, refining temperature is 45~60 DEG C, conditioning period 50
~60s.
10. the preparation method of water quality cleansing agent as claimed in claim 5, which is characterized in that by the quenched place mixed component B
After reason, pelletize water quality cleansing agent the step of in, when the granulation, the mixed component B is sent into granulator and is pelletized,
The ring moulds aperture of the granulator is set as 2.0~4.0mm, and ring moulds compression ratio is set as 1:(4~6).
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Application publication date: 20190702 |