JP2023101510A - Production method of natural hot spring concentrate - Google Patents
Production method of natural hot spring concentrate Download PDFInfo
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- JP2023101510A JP2023101510A JP2023074849A JP2023074849A JP2023101510A JP 2023101510 A JP2023101510 A JP 2023101510A JP 2023074849 A JP2023074849 A JP 2023074849A JP 2023074849 A JP2023074849 A JP 2023074849A JP 2023101510 A JP2023101510 A JP 2023101510A
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- Prior art keywords
- hot spring
- natural hot
- minerals
- concentrate
- natural
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- 230000017423 tissue regeneration Effects 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
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- UDKYUQZDRMRDOR-UHFFFAOYSA-N tungsten Chemical compound [W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W][W] UDKYUQZDRMRDOR-UHFFFAOYSA-N 0.000 description 1
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- Fertilizers (AREA)
- Cultivation Of Plants (AREA)
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- Non-Alcoholic Beverages (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
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Abstract
Description
本発明は、ミネラル含有鉱石を天然温泉に添加し、無機酸処理することにより、天然温泉に含まれる温泉成分の増強による温浴効果や体内組織中のミネラル栄養素の補給、天然温泉中の細菌の除菌、殺菌、脱臭、消臭、湯温が低い状態での温浴効果による睡眠導入、調味料として様々な食品へ添加することによる味の改善や栄養補給を行う。 In the present invention, mineral-containing ore is added to a natural hot spring and treated with an inorganic acid to enhance the hot spring components contained in the natural hot spring, providing a warm bath effect, replenishing mineral nutrients in the body tissue, eliminating bacteria in the natural hot spring, sterilizing, deodorizing, and deodorizing, inducing sleep due to the hot bath effect in a low temperature state, and improving the taste and nutritional supplementation by adding it to various foods as a seasoning.
天然鉱物中には、カルシウム、シリコン、アルミニウム、鉄等の主要金属を始め微量金属に至るまでの種々の金属元素がミネラルとして多く含まれており、これらのミネラルは、一般に、動物や植物等の生体にとって必須の微量元素となっている。 Natural minerals contain a large amount of various metal elements as minerals, ranging from major metals such as calcium, silicon, aluminum and iron to trace metals, and these minerals are generally essential trace elements for living organisms such as animals and plants.
従来、これらの金属元素は、一般に天然温泉や金属や塩の形で提供されているが、実際に、生体にとって必要な量をこれらから摂取することは難しく、また、現実に摂取したとしても、これが生体にとって吸収されやすい状態になるとは限らず、その可能吸収率は低いものでしかなかった。 Conventionally, these metal elements are generally provided in the form of natural hot springs, metals, or salts, but it is actually difficult to ingest the amounts required by the body from these sources, and even if they are actually ingested, they are not necessarily in a state that is easily absorbed by the body, and the possible absorption rate is only low.
本発明者は、天然温泉に含有する有効成分であるミネラルを増強すべく鋭意研究を重ねた結果、ミネラル含有鉱石に鉱酸を作用させると多くのミネラル分が生体に吸収しやすい形で溶出すること、及びこのミネラル分は温泉成分を増強するばかりでなく、温浴効果を高め、体内のミネラル成分バランスを整え、風呂内の細菌の抗菌、脱臭、消臭、湯温が低い、つまり身体への負担が低い状態での温浴効果による睡眠導入、調味料として様々な食品へ添加することによるに利用し得る有用性を有するものであることを見出し、本発明を完成するに至った。特に、このミネラルは口腔内または舌下噴霧により吸収することが、非特許文献1に示されている。図1によれば、静脈注射が一番高く99%であるのに対して、口腔内または舌下噴霧による吸収率は、95%である。これは、10%である錠剤、20%であるカプセル、45%である経皮パッチ、50%である舌下液、80%である筋肉注射よりも高い結果となっている。
As a result of extensive research to enhance minerals, which are active ingredients contained in natural hot springs, the present inventors found that when mineral acids are applied to mineral-containing ores, many minerals are eluted in a form that is easily absorbed by the body, and that these minerals not only enhance the hot spring ingredients, but also enhance the hot bath effect, balance the mineral ingredients in the body, antibacterial, deodorize, and deodorize bacteria in the bath. The inventors have found that it has usefulness that can be utilized by adding it to foods, and have completed the present invention. In particular, Non-Patent
そこで、本発明の目的は、動物や植物等の生体にとって必須の微量元素である金属元素からなるミネラルを生体にとって必要な量を摂取することができ、可能吸収率の高いミネラルを液体として提供することにある。 Accordingly, an object of the present invention is to provide minerals composed of metal elements, which are essential trace elements for living organisms such as animals and plants, in the form of liquids that allow the living organisms to ingest the required amount and have a high possible absorbability.
また、本発明は、温浴施設や飲食店における清掃溶液等に有用であって、人体に有害な化学物質を用いず安全な清掃用品を作ることを目的とするものである。 Another object of the present invention is to produce a safe cleaning product that is useful as a cleaning solution in hot bath facilities and restaurants, and that does not use chemical substances that are harmful to the human body.
更に、本発明は、ミネラルを用いたヘアケア製品を生成し、有機物並びに無機物を酸化する特性を有する天然温泉濃縮液を提供することを目的とするものである。 A further object of the present invention is to provide a natural hot spring concentrate that produces hair care products using minerals and has the property of oxidizing organic as well as inorganic substances.
更に、本発明は、ミネラルを用いた口腔ケア製品を生成し、有機物並びに無機物を酸化する特性を有する天然温泉濃縮液を提供することを目的とするものである。 It is a further object of the present invention to provide a natural spa concentrate with properties of oxidizing organic as well as inorganic substances to form oral care products with minerals.
更に、本発明は、ミネラルを用いたボディケア製品を生成し、有機物並びに無機物を酸化する特性を有する天然温泉濃縮液を提供することを目的とするものである。 A further object of the present invention is to provide a natural hot spring concentrate with properties of oxidizing organic as well as inorganic substances to form mineral body care products.
本発明の目的を解決する為に、本発明に係る水中有機物並びに無機物酸化処理用天然温泉濃縮液は、天然温泉成分とミネラルを含有する鉱物の無機酸処理物とを含む含金属酸性溶液であって、温泉液中の有機物並びに無機物とを含みこれらを酸化する特性を有することを特徴とする。 In order to achieve the object of the present invention, the natural hot spring concentrate for oxidizing organic and inorganic substances in water according to the present invention is a metal-containing acidic solution containing natural hot spring components and inorganic acid-treated minerals containing minerals.
天然温泉濃縮液は、主要成分として1~20g/リットルのアルミニウム、1~20g/リットルの鉄、1~10g/リットルのマグネシウム及び1~10g/リットルのカリウムを含有し、その比重は1.1~1.5、pHが0.1~2.0である。 The natural hot spring concentrate contains 1-20 g/liter aluminum, 1-20 g/liter iron, 1-10 g/liter magnesium and 1-10 g/liter potassium as main components, and its specific gravity is 1.1-1.5 and pH is 0.1-2.0.
天然温泉濃縮液は、金属成分として、アルミニウム、鉄、マグネシウム及びカリウムを多量に含み、そして、リン、チタン、カルシウム、マンガン、ナトリウム、シリコン、コバルト、リチウム、銅、ニッケル、亜鉛及びバリウムからなる金属の大部分を含み、且つヒ素、鉛、水銀、クロムを含まない。 Natural hot spring concentrate contains a large amount of aluminum, iron, magnesium and potassium as metal components, and contains most of the metals consisting of phosphorus, titanium, calcium, manganese, sodium, silicon, cobalt, lithium, copper, nickel, zinc and barium, and does not contain arsenic, lead, mercury and chromium.
また、本発明に係るウイルス不活化剤は、天然温泉成分とミネラルを含有する鉱物の無機酸処理物とを含む含金属酸性溶液であって、温泉液中の有機物並びに無機物とを含みこれらを酸化する特性を有することを特徴とする水中有機物並びに無機物酸化処理用天然温泉濃縮液からなる。 Further, the virus inactivating agent according to the present invention is a metal-containing acidic solution containing natural hot spring components and inorganic acid-treated minerals containing minerals.
さらに、ウイルス不活化剤は、主要成分として1~20g/リットルのアルミニウム、1~20g/リットルの鉄、1~10g/リットルのマグネシウム及び1~10g/リットルのカリウムを含有し、その比重は1.1~1.5、pHが0.1~2.0である。 Furthermore, the virus inactivating agent contains 1-20 g/liter aluminum, 1-20 g/liter iron, 1-10 g/liter magnesium and 1-10 g/liter potassium as main components, and has a specific gravity of 1.1-1.5 and a pH of 0.1-2.0.
加えて、ウイルス不活化剤は、金属成分として、アルミニウム、鉄、マグネシウム及びカリウムを多量に含み、そして、リン、チタン、カルシウム、マンガン、ナトリウム、シリコン、コバルト、リチウム、銅、ニッケル、亜鉛及びバリウムからなる金属の大部分を含み、且つヒ素、鉛、水銀、クロムを含まない。 In addition, the virus inactivating agent contains large amounts of aluminum, iron, magnesium and potassium as metal components, and contains most of the metals consisting of phosphorus, titanium, calcium, manganese, sodium, silicon, cobalt, lithium, copper, nickel, zinc and barium, and does not contain arsenic, lead, mercury, chromium.
続いて、本発明に係る水中有機物並びに無機物酸化処理用天然温泉濃縮液からなる液肥は、天然温泉成分とミネラルを含有する鉱物の無機酸処理物とを含む含金属酸性溶液であって、温泉液中の有機物並びに無機物とを含みこれらを酸化する特性を有することを特徴とする。 Next, the liquid fertilizer comprising a natural hot spring concentrate for oxidizing organic substances in water and inorganic substances according to the present invention is a metal-containing acidic solution containing natural hot spring components and inorganic acid-treated minerals containing minerals.
さらに、液肥は、主要成分として1~20g/リットルのアルミニウム、1~20g/リットルの鉄、1~10g/リットルのマグネシウム及び1~10g/リットルのカリウムを含有し、その比重は1.1~1.5、pHが0.1~2.0である。 Furthermore, the liquid fertilizer contains 1-20 g/liter aluminum, 1-20 g/liter iron, 1-10 g/liter magnesium and 1-10 g/liter potassium as main components, and has a specific gravity of 1.1-1.5 and a pH of 0.1-2.0.
この液肥は、金属成分として、アルミニウム、鉄、マグネシウム及びカリウムを多量に含み、そして、リン、チタン、カルシウム、マンガン、ナトリウム、シリコン、コバルト、リチウム、銅、ニッケル、亜鉛及びバリウムからなる金属の大部分を含み、且つヒ素、鉛、水銀、クロムを含まない。 This liquid fertilizer contains a large amount of aluminum, iron, magnesium and potassium as metal components, and contains most of the metals consisting of phosphorus, titanium, calcium, manganese, sodium, silicon, cobalt, lithium, copper, nickel, zinc and barium, and does not contain arsenic, lead, mercury and chromium.
以上詳述したように、本発明の水中有機物並びに無機物酸化処理用天然温泉濃縮液は、動植物及び魚貝類の成長を促進する作用があり、また、OHラジカルを生成し有機物を酸化する特性を有しているので、汚水や用水中の有機物や細菌類を減少せしめる作用を有し、特に、種々の汚水もしくは用水の清浄化、細菌の抗菌、脱臭、消臭、アオコの除去、ヘドロ処理、植物種子の発芽促進、動植物体の成長促進等を中心として、農園芸分野、水産分野、廃水処理分野、水道事業等において、種々の添加剤の有効成分として広く利用することができるものである。 As described in detail above, the natural hot spring concentrate for oxidizing organic matter and inorganic matter of the present invention has the action of promoting the growth of animals, plants, and fish and shellfish, and has the property of generating OH radicals and oxidizing organic matter, so it has the action of reducing organic matter and bacteria in sewage and service water. It can be widely used as an active ingredient of various additives in the agricultural and horticultural field, the fishery field, the wastewater treatment field, the water supply business, etc.
このような目的を達成する本発明は、以下の(1)~(3)の技術的手段から構成されるものである。 The present invention, which achieves such objects, consists of the following technical means (1) to (3).
(1)腐食系鉱物の無機酸処理物からなる含金属酸性溶液であって、これを天然温泉に添加することにより、その水溶液中の有機物並びに無機物を酸化する特性を有することを特徴とする水中有機物並びに無機物酸化処理用天然温泉無機ブレンドしたものである。
ここで、本発明に係る天然温泉濃縮液は、好適にはナトリウム:100ml/L~200ml/L、 マグネシウム:2000ml/L~4000ml/L、シリカ:10ml/L~40ml/L、リン: 100ml/L~400ml/L、カリウム;1000ml/L~4000ml/L、カルシウム:100ml/L~500ml/L、チタン:500ml/L~1000ml/L、クロム;3ml/L~20ml/L、マンガン:50ml/L~200ml/L、鉄分;5000ml/L~30000ml/L、コバルト:2ml/L~10ml/L、銅;2ml/L~20ml/L、亜鉛;10ml/L~30ml/L、ゲルマニウム;10ml/L以下、セレン:1ml/L~10ml/L、モリブデン:5ml/L以下とから構成される。
本発明に係る天然温泉濃縮液は、より好適には、ナトリウム:170ml/L、 マグネシウム:3000ml/L、シリカ:28ml/L、リン: 300ml/L、カリウム;2500ml/L、カルシウム:400ml/L、チタン:860ml/L、クロム;8ml/L、マンガン:140ml/L、鉄分;10000ml/L、コバルト:4ml/L、銅;8ml/L、亜鉛;17ml/L、ゲルマニウム;1ml/L以下、セレン:5ml/L、モリブデン:0.5ml/L以下とするのが望ましい。
(1) A metal-containing acidic solution made of corrosive minerals treated with an inorganic acid, which, when added to a natural hot spring, has the property of oxidizing organic and inorganic substances in the aqueous solution. Natural hot spring inorganic blend for oxidation treatment of organic substances and inorganic substances in water.
Here, the natural hot spring concentrate according to the present invention preferably contains sodium: 100 ml/L to 200 ml/L, magnesium: 2000 ml/L to 4000 ml/L, silica: 10 ml/L to 40 ml/L, phosphorus: 100 ml/L to 400 ml/L, potassium: 1000 ml/L to 4000 ml/L, calcium: 100 ml/L to 500 ml/L, titanium: 500 ml/L. L~1000ml/L Chromium: 3ml/L~20ml/L Manganese: 50ml/L~200ml/L Iron: 5000ml/L~30000ml/L Cobalt: 2ml/L~10ml/L Copper: 2ml/L~20ml/L Zinc: 10ml/L~30ml/L Germanium: 10ml/L or less Selenium: 1ml/L~10ml/L , molybdenum: 5 ml/L or less.
The natural hot spring concentrate according to the present invention is more preferably sodium: 170ml/L, magnesium: 3000ml/L, silica: 28ml/L, phosphorus: 300ml/L, potassium: 2500ml/L, calcium: 400ml/L, titanium: 860ml/L, chromium: 8ml/L, manganese: 140ml/L, iron: 10000ml/L, cobalt: 4ml/L, copper: 8ml/L. , zinc: 17 ml/L, germanium: 1 ml/L or less, selenium: 5 ml/L, molybdenum: 0.5 ml/L or less.
(2)主要成分として1~20g/リットルのアルミニウム、1~20g/リットルの鉄、1~10g/リットルのマグネシウム及び1~10g/リットルのカリウムを含有し、その比重は1.1~1.5、pHが0.1~2.0である前記無機物酸化処理用天然温泉無機ブレンドしたものである。 (2) It contains 1 to 20 g/liter of aluminum, 1 to 20 g/liter of iron, 1 to 10 g/liter of magnesium and 1 to 10 g/liter of potassium as main components, and has a specific gravity of 1.1 to 1.5 and a pH of 0.1 to 2.0.
(3)金属成分として、アルミニウム、鉄、マグネシウム及びカリウムを多量に含み、そして、リン、チタン、カルシウム、マンガン、ナトリウム、シリコン、コバルト、リチウム、銅、ニッケル、亜鉛及びバリウムからなる金属の大部分を含み、且つヒ素、鉛、水銀、クロムを含まない前記(1)記載の天然温泉濃縮液である。 (3) The natural hot spring concentrate according to (1) above, which contains a large amount of aluminum, iron, magnesium and potassium as metal components, and contains most of the metals consisting of phosphorus, titanium, calcium, manganese, sodium, silicon, cobalt, lithium, copper, nickel, zinc and barium, and does not contain arsenic, lead, mercury or chromium.
本発明の天然温泉濃縮液は、腐食系鉱物、例えば黒雲母を使用し、必要により前処理した後、これに鉱酸を作用させ、更にこれを分離することにより得られるものである。また、黒雲母の前処理は、鉱酸を効率よく作用させるために、必要により採用されるものであり、当該前処理は、例えば、黒雲母の風化土壌を適宜のサイズに、粉砕すること等により行われる。 The natural hot spring concentrate of the present invention is obtained by using corrosive minerals such as biotite, pretreating it if necessary, reacting it with a mineral acid, and separating it. In addition, pretreatment of biotite is adopted as necessary in order to allow mineral acid to act efficiently, and the pretreatment is performed, for example, by pulverizing the weathered soil of biotite into an appropriate size.
当該前処理をした後の鉱酸による処理は、鉱酸水溶液を黒雲母の風化土壌に作用させ、溶出処理すればよい。鉱酸としては、硫酸を用いる。鉱酸処理は、必要により加熱温度下で行うことが好ましく、必要なミネラル分が黒雲母から溶出するまで継続する。 The treatment with a mineral acid after the pretreatment may be carried out by applying a mineral acid aqueous solution to the weathered biotite soil to perform an elution treatment. Sulfuric acid is used as the mineral acid. Mineral acid treatment is preferably performed at a heating temperature if necessary, and is continued until necessary mineral components are eluted from the biotite.
更に、上記鉱酸処理物は、固液分離することにより、液状物と固形分に分離される。固液分離手段としては、例えば、フィルタープレス等が用いられ、必要により更に分離、精製して有機物並びに無機物を酸化する作用を有する水中有機物並びに無機物酸化処理用天然温泉濃縮液が分取される。具体的には、その製造工程を、図2に示す。 Further, the mineral acid-treated product is separated into a liquid and a solid by solid-liquid separation. As a solid-liquid separation means, for example, a filter press or the like is used, and if necessary, organic substances in water having the action of further separating and purifying them to oxidize organic substances and inorganic substances and natural hot spring concentrates for oxidizing inorganic substances are fractionated. Specifically, the manufacturing process is shown in FIG.
本発明の製造工程の第一の工程は、黒雲母の風化土壌を原土として掘削する工程である(S2)。 The first step of the manufacturing process of the present invention is the step of excavating weathered soil of biotite as original soil (S2).
第二の工程は、この原土を溶出するための鉱酸を保管するタンクに蓄積する(S4)。鉱酸としては、塩酸、硝酸、硫酸、酢酸、炭酸などが用いられる。 In the second step, the mineral acid for eluting this raw soil is stored in a tank (S4). Mineral acids include hydrochloric acid, nitric acid, sulfuric acid, acetic acid, and carbonic acid.
続いて、第三の工程は、鉱酸は希釈層で希釈される(S6)。純水で希釈するが、ここで、温泉潜水で希釈しても良い。 Subsequently, in the third step, the mineral acid is diluted with a dilution layer (S6). Although it is diluted with pure water, it may also be diluted with hot spring diving here.
第四の工程は、希釈された酸で、原土が原土ホッパーの中で攪拌される(S8)。 The fourth step is to agitate the raw soil in a raw soil hopper with diluted acid (S8).
第五の工程では、酸と攪拌された原土は、原土峻別設備でより粒度の細かい原土に峻別されて原料となる(S10)。 In the fifth step, the acid and agitated original soil are sorted into finer-grained raw soil by the raw soil sorting equipment to be used as raw materials (S10).
第六の工程では、峻別された原料がさらに原料ホッパーに貯蔵され、底開式のじょうご型の口から落下させて取り出される(S12)。 In the sixth step, the sorted raw materials are further stored in a raw material hopper, and dropped from a funnel-shaped opening with an open bottom to be taken out (S12).
第七の工程で、原料ホッパーから取りされた原料は抽出槽に移される(S14)。 In the seventh step, the raw material taken from the raw material hopper is transferred to an extraction tank (S14).
第八の工程で、分級機が粒形の大きな4mm以上の礫や岩を分別する(S16)。分級された規格より大きな粒形の4mm以上の礫や岩は、残留岩として廃棄される(S18)。規格より小さな砂、シルト、ミネラル、水分は中継槽に格納される(S20)。 In the eighth step, a classifier separates gravel and rocks having a large particle size of 4 mm or more (S16). The classified pebbles and rocks having a grain size larger than the standard size of 4 mm or more are discarded as residual rocks (S18). Sand, silt, minerals and moisture smaller than the standard are stored in the relay tank (S20).
第九の工程で、中継槽の小さな砂、シルト、ミネラル、水分は、フィルタープレスによって濾され、小さな砂、シルトは残留土として廃棄される(S24)。 In the ninth step, small sand, silt, minerals and moisture in the relay tank are filtered by a filter press, and the small sand and silt are discarded as residual soil (S24).
第十の工程で、ミネラル、水分、残留物は、濾液槽で、残留物が沈殿すし、上澄みとしてミネラルと水分のミネラル混合液が貯液される(S26)。 In the tenth step, minerals, water and residues are deposited in a filtrate tank, and a mineral mixture of minerals and water is stored as a supernatant (S26).
第十一の工程で、特定の温泉地の源泉から取水した温泉地固有の成分が含まれた温泉水を予め温泉水タンクに格納する(S30)。温泉としては、例えば、草津温泉であれば、草津温泉水の源泉水を格納する。 In the eleventh step, hot spring water containing components unique to the hot spring, taken from the source of a specific hot spring, is stored in advance in a hot spring water tank (S30). For example, if the hot spring is Kusatsu hot spring, the source water of Kusatsu hot spring water is stored.
第十二の工程で、濾液槽に格納されたミネラルと水分のミネラル混合液と、温泉水とが混合槽で攪拌されて混合して混合槽において天然温泉濃縮液が生成される(S28)。 In the twelfth step, the mineral mixture of minerals and water stored in the filtrate tank and the hot spring water are agitated and mixed in the mixing tank to produce a natural hot spring concentrate in the mixing tank (S28).
第十三の工程で、混合槽にある天然温泉濃縮液は、用途に応じて、瓶、ペットボトル、缶、ビニール袋などの容器に格納されて製品化される(S32)。 In the thirteenth step, the natural hot spring concentrate in the mixing tank is put into a container such as a bottle, a PET bottle, a can, a plastic bag, etc., and commercialized (S32).
この様にして得られた本発明の天然温泉濃縮液の性質は以下の通りである。
1.温泉成分分量:ミネラル分を塩類換算重量で20%以上含む。
2.温泉成分内訳:(1)アルミニウム、鉄、マグネシウム及びカリウムを多量に含む。
(2)リン、チタン、カルシウム、マンガン、ナトリウム、シリコン、コバルト、リチウム、銅、ニッケル、亜鉛、バリウムの大部分を含む。
(3)ヒ素、鉛、水銀、クロムを含まない。
The properties of the natural hot spring concentrate of the present invention thus obtained are as follows.
1. Hot spring component content: Contains 20% or more of mineral content in terms of salt content.
2. Hot spring component breakdown: (1) Contains a large amount of aluminum, iron, magnesium and potassium.
(2) Contains most of phosphorus, titanium, calcium, manganese, sodium, silicon, cobalt, lithium, copper, nickel, zinc and barium.
(3) Does not contain arsenic, lead, mercury or chromium.
3.比重:1.1~1.54.pH:0.1~2.05.作用:■天然温泉に温泉成分のミネラルを添加することで泉質が大きく向上し、保温、保湿、腰痛や肌荒れなどに改善効果が見られる。
(実施例1)
3. Specific gravity: 1.1-1.54. pH: 0.1-2.05. Function: ■ By adding hot spring minerals to natural hot springs, the quality of the hot springs is greatly improved, and effects such as heat retention, moisturizing, lower back pain, and rough skin can be seen.
(Example 1)
以上の方法によって形成された天然温泉濃縮液を、発明者が別途発明した特許第6523960号で示される温泉ミスト吸引施設において温泉ミストとして用いたところ未使用時と使用経過後について比較した図を図3~8に示す。いずれもオリゴスキャン社有害重金属及び必須・参考ミネラル非侵襲・短時間測定でラマン分光法を用いたオリゴスキャン装置を用いて測定した。測定対象は、各被験者の手掌4か所である。測定光は、UV・タングステンランプであり、その波長は380nm~730nmである。必須ミネラルの摂取について、天然温泉濃縮液未使用時(図3)、天然温泉濃縮液6か月使用時(図4)、有害ミネラルの排出について、天然温泉濃縮液未使用時(図5)、天然温泉濃縮液6か月使用時(図6)、免疫力について、天然温泉濃縮液未使用時(図7)、天然温泉濃縮液6か月使用時(図8)に各被験者の手掌4か所からオリゴスキャン装置を用いて測定した結果の各成分について示す。測定結果には測定値(単位:μg/mg Tissues)とグラフが表示される。必須・参考ミネラルのグラフではデータベースを元に標準範囲±1SD範囲内をグリーンゾーン、±1SD<±2SDをイエローゾーン、±2SD<レッドゾーンと表記する。 The natural hot spring concentrate formed by the above method was used as a hot spring mist in a hot spring mist suction facility shown in Patent No. 6523960, which was invented separately by the inventor. All of them were measured using the Oligoscan equipment using Raman spectroscopy in a non-invasive and short-time measurement of harmful heavy metals and essential/reference minerals manufactured by Oligoscan. Measurement targets were four palms of each subject. The measurement light is a UV/tungsten lamp with a wavelength of 380 nm to 730 nm. Intake of essential minerals when not using concentrated natural hot spring (Fig. 3) and after six months of use (Fig. 4), discharge of harmful minerals when not using concentrated natural hot spring (Fig. 5) and after six months of using concentrated natural hot spring (Fig. 6). Measurement results are displayed as measured values (unit: μg/mg Tissues) and graphs. In the graph of essential/reference minerals, based on the database, the standard range ±1SD is indicated as the green zone, ±1SD<±2SD as the yellow zone, and ±2SD<red zone.
必須ミネラルの摂取について図3と図4を比較すると、天然温泉濃縮液を用いることで主要ミネラルについての吸収量は、カリウムが265%増加し、カルシウムが25%増加し、ナトリウム6%増加し、硫黄も0.6%増加することがわかる。 Comparing Figures 3 and 4 for the intake of essential minerals, it can be seen that the absorption of major minerals by using the natural hot spring concentrate increased by 265% for potassium, increased by 25% for calcium, increased by 6% for sodium, and increased by 0.6% for sulfur.
また、微量ミネラルについても、銅が198%、モリブデンが139%、バナジウムが158%、亜鉛が50%、クロムが31%、コバルトが25%、ヨウ素が11%、鉄が10%、ホウ素が9.8%それぞれ増大した。 Trace minerals also increased by 198% for copper, 139% for molybdenum, 158% for vanadium, 50% for zinc, 31% for chromium, 25% for cobalt, 11% for iodine, 10% for iron, and 9.8% for boron.
有害ミネラルの排出について図5と図6について比較すると、バリウムが72%減少し、タリウムが66%減少し、トリウムが65%減少し、ヒ素が62%、ビスマスが49%減少し、アンチモンが28%減少し、カドミウムが26%減少し、水銀が22%減少し、ベリリウムが2.5%減少することが明らかになった。有害ミネラルが9種類減少することが明らかになった。 A comparison of Figures 5 and 6 for harmful mineral emissions reveals a 72% decrease in barium, a 66% decrease in thallium, a 65% decrease in thorium, a 62% decrease in arsenic, a 49% decrease in bismuth, a 28% decrease in antimony, a 26% decrease in cadmium, a 22% decrease in mercury, and a 2.5% decrease in beryllium. It became clear that 9 types of harmful minerals were reduced.
免疫力について、図7,8より、潜在的な課題としてトータル重金属無毒性は要注意75%から許容範囲65%に改善し、アシドーシス/酸性症は要注意79%から良好33%に改善、糖尿素因は許容範囲50%から良好27%に改善、アレルギーリスクは許容範囲53%から良好33%に改善した。 7 and 8, as potential issues, total heavy metal non-toxicity improved from 75% requiring caution to 65% acceptable, acidosis/acidosis improved from 79% requiring caution to 33% good, diabetic diathesis improved from 50% acceptable to 27% good, and allergy risk improved from 53% acceptable to 33% good.
また、生理機能として、酵素の状態は、要注意21%から良好97%に改善、緑の消化器は、要注意25%から良好89%に改善、代謝は要注意27%から許容範囲50%に改善、免疫システムは要注意21%から良好88%に改善、認知機能は、要注意33%から良好79%に改善、ホルモン状態等は、要注意33%から良好79%に改善、組織修復は、許容範囲50%から良好74%に改善、感情の状態は、要注意27%から良好75%に改善、心血管系は、要注意28%から良好72%に改善、神経系は要注意32%から良好87%に改善した。以上から潜在的な課題や生理機能についても本発明に係る天然温泉濃縮液によってトータルに改善している。
(実施例2)
In terms of physiological functions, the enzyme status improved from 21% requiring caution to 97% good, the green digestive system improved from 25% requiring caution to 89% good, the metabolism improved from 27% requiring caution to 50% acceptable, the immune system improved from 21% needing attention to 88% good, the cognitive function improved from 33% needing attention to 79% good, the hormone status improved from 33% needing attention to 79% good, and tissue repair improved from 50% to good 79%. Emotional state improved from caution 27% to good 75%, cardiovascular system improved from caution 28% to good 72%, nervous system improved from caution 32% to good 87%. From the above, potential problems and physiological functions are totally improved by the natural hot spring concentrate according to the present invention.
(Example 2)
前記方法で形成された天然温泉濃縮液を用いた第2の実施例について説明する。天然温泉濃縮液によるウイルス不活性化試験を行った。天然温泉濃縮液の2000倍希釈液と試験対照としてリン酸緩衝液(PBS(-))を用いて、インフルエンザウイルスへの不活性効果について評価した。ウイルス株は、Influenza virus H1N1 A/PR/8/34 (ATCC VR-1469)を用いた。また、宿主細胞はMDCK細胞(イヌ腎細胞)(ATCC CCL-34)を用いた。 A second embodiment using the natural hot spring concentrate formed by the above method will now be described. A virus inactivation test was conducted using a natural hot spring concentrate. Using a 2000-fold dilution of the natural hot spring concentrate and a phosphate buffer (PBS(-)) as a test control, the inactivation effect on the influenza virus was evaluated. The virus strain used was Influenza virus H1N1 A/PR/8/34 (ATCC VR-1469). MDCK cells (canine kidney cells) (ATCC CCL-34) were used as host cells.
試験方法は、第一に天然温泉濃縮液0.01mLを精製水0.99mLに添加し、100倍希釈溶液を作成した。さらに、この天然温泉濃縮液100倍希釈溶液0.15mLを精製水2.85mLに添加し、2000倍希釈溶液を作成した。 First, 0.01 mL of the natural hot spring concentrate was added to 0.99 mL of purified water to prepare a 100-fold diluted solution. Furthermore, 0.15 mL of this 100-fold diluted natural hot spring concentrate was added to 2.85 mL of purified water to prepare a 2000-fold diluted solution.
天然温泉濃縮液2000倍希釈溶液1.08mLをチューブに分注後、リン酸緩衝液(PBS)を用いて5~10x105pfu/ml調整したインフルエンザ溶液0.12mL混合し、攪拌したものを試験液とした。 After dispensing 1.08 mL of a 2000-fold diluted natural hot spring concentrate into a tube, 0.12 mL of an influenza solution adjusted to 5 to 10 x 105 pfu/mL using phosphate buffer (PBS) was mixed and stirred to obtain a test solution.
試験液は室温下で静置し、反応を行った。所定時間(直後、1分、5分)経過ごとに試験液から0.12mlの溶液を回収し、0.2%ウシ血清含有ダルベッコ改変イーグル培地(FBS-DMEM培地)1.08mlと混合した。0.2%FBS-DMEM培地による希釈を複数回繰り返し、10倍段階希釈系を作成した。10倍段階希釈系を事前に準備した宿主細胞に各1ml・WELL滴下し、37℃ 5% CO2下で1時間感染処理を行った。 The test solution was allowed to stand at room temperature for reaction. 0.12 ml of the solution was collected from the test solution at predetermined time intervals (immediately, 1 minute, 5 minutes) and mixed with 1.08 ml of Dulbecco's modified Eagle's medium containing 0.2% bovine serum (FBS-DMEM medium). Dilution with 0.2% FBS-DMEM medium was repeated multiple times to prepare a 10-fold serial dilution series. Each 1 ml/WELL of the 10-fold serial dilution series was dropped onto the host cells prepared in advance, and infected at 37° C., 5% CO 2 for 1 hour.
ウイルス感染後、細胞上清を0.8%オキソイド寒天溶液に置換し、37℃ 5% CO2下で2日間培養した。プラークの形成を目視で確認した後、5%グルタルアルデヒド溶液で固定し、メチレンブルー染色を行い、形成されたプラーク数の測定データを元にウイルス感染力を測定した。 After virus infection, the cell supernatant was replaced with a 0.8% oxoid agar solution and cultured for 2 days at 37°C and 5% CO2 . After visually confirming the formation of plaques, the cells were fixed with a 5% glutaraldehyde solution, stained with methylene blue, and the virus infectivity was measured based on the number of plaques formed.
本試験は2回実施し、2回の平均値を元に、天然温泉濃縮液2000倍希釈溶液による不活性化率を評価した。
表1、図9に示すようにリン酸緩衝液(PBS(-))は、インフルエンザ感染力価に継時変化は一切ないのに対して、天然温泉濃縮液2000倍希釈溶液では、30秒程度でインフルエンザ感染力価が激減し10pfu/ml以下に落ちている。これは表からも明確である。 As shown in Table 1 and Figure 9, the phosphate buffer solution (PBS(-)) did not change the influenza infection titer over time, whereas the 2000-fold dilution of the natural hot spring concentrate drastically reduced the influenza infection titer to 10 pfu/ml or less in about 30 seconds. This is also clear from the table.
従って、天然温泉濃縮液2000倍希釈溶液のインフルエンザウイルスに対する不活化効果を評価した。インフルエンザウイルスにはH1N1血清型のA/PR/8/34株を用いた。天然温泉濃縮液2000倍希釈溶液は作用直後から99.988%以上のウイルス不活化効果が確認された。
(実施例3)
Therefore, the effect of inactivating the influenza virus of a 2000-fold diluted natural hot spring concentrate was evaluated. The influenza virus used was the H1N1 serotype A/PR/8/34 strain. A 2000-fold diluted natural hot spring concentrate was confirmed to have a virus inactivation effect of 99.988% or more immediately after the action.
(Example 3)
天然温泉濃縮液肥について About Natural Hot Spring Concentrated Liquid Fertilizer
天然温泉濃縮液肥は、肥料というよりは光合成増強資材としての機能を有する。主に葉面散布により作物の光合成を20-30%高める。水稲の種籾消毒。育苗での使用した例について説明する。品種はコシヒカリであり、籾消毒に500倍に希釈した天然温泉濃縮液肥を用い、播種前3日間芽出し、浸漬され、発芽後3回2000倍水素面散布される。 Natural hot spring concentrated liquid fertilizer has a function as a photosynthesis enhancement material rather than a fertilizer. Increases crop photosynthesis by 20-30%, mainly through foliar application. Rice seed disinfection. An example of use in raising seedlings will be described. The cultivar is Koshihikari, and 500-fold diluted natural hot spring concentrated liquid fertilizer is used for paddy disinfection, germinated for 3 days before sowing, immersed, and sprayed with 2000-fold hydrogen surface three times after germination.
天然温泉濃縮液肥を前記の条件で育成することで、発芽率が極めて良好である。また、いわゆるバカ苗と呼ばれる不良育成苗の発生が存在しない。また、慣行として使用される種子消毒剤を一切使用することなく育成が可能であった。さらに田植え直後の活着生育の開始も従来の開始日より4~5日早まった。さらに、天然温泉濃縮液肥は他の液肥の希釈水として利用可能である。図10に出荷前の苗半作を示す。右側の従来手法の苗半作に対して、左側の天然温泉濃縮液肥を用いた苗半作は節間が詰まり、その茎が太く根の張りが良くなった。
(実施例4)
By cultivating the natural hot spring concentrated liquid fertilizer under the above conditions, the germination rate is extremely good. In addition, there is no generation of poorly grown seedlings called so-called stupid seedlings. In addition, it was possible to grow without using any conventional seed disinfectant. Furthermore, the start of epiphytic growth immediately after rice planting was earlier than the conventional start date by 4 to 5 days. Furthermore, natural hot spring concentrated liquid fertilizer can be used as dilution water for other liquid fertilizers. Fig. 10 shows half-cropping of seedlings before shipment. The half-cropping of seedlings using the conventional method on the right side, and the half-cropping of seedlings using the natural hot spring concentrated liquid fertilizer on the left side clogged the internodes, resulting in thicker stems and better root tension.
(Example 4)
次に、本発明の天然温泉濃縮液の有用性について説明する。
1.天然温泉の成分増量分野における利用本発明の天然温泉濃縮液を家庭用風呂に例えば、50-5,000ppm水溶液を0.1ml/L程度希釈することによりさら湯をミネラル成分豊富な温泉に変換し保温、保湿効果を高め、水溶化したミネラルが経皮から浸透しミネラルの補給を行うことが可能である。これにより温泉を採掘したり、運搬を行うことなく場所を問わず温泉湯治を行うことが可能になる。
(実施例5)
Next, the usefulness of the natural hot spring concentrate of the present invention will be described.
1. Use in the field of increasing the amount of ingredients in natural hot springs The natural hot spring concentrate of the present invention can be used in home baths. For example, by diluting a 50-5,000 ppm aqueous solution to about 0.1 ml/L, the Sarayu can be converted into a hot spring rich in mineral components, enhancing heat retention and moisturizing effects. This makes it possible to treat hot springs anywhere without mining or transporting hot springs.
(Example 5)
天然温泉の飲料分野における利用 本発明の天然温泉濃縮液を飲料水等に添加することで良質のマルチミネラルを含有する温泉水を生成し、現代人のミネラル不足を解消することが可能である。5年以上にわたる利用実績の中で、その日の体調によって酸味を感じたり、苦味や血のようなしょっぱい味になったりすることがわかってきた。推察するにこれは舌下の粘膜が不足、つまり身体が欲しているミネラルを先に吸収しようとしてそれが味の変化になって現れたと考えられる。実際二日酔いや便秘等には即効性のある効果が認められた。
天然温泉の調味料分野における利用 本発明の天然温泉濃縮液を調味料として様々な料理に添加することで(1)肉質を柔らかくしたり、(2)ドレッシング等に使用することで食品中に含まれるミネラルを補ったり、(3)酸味を加えることで味を引き締めたり、(4)魚等の生臭さを解消したりすることが可能である。
(実施例7)
Use of natural hot springs in the field of seasoning By adding the natural hot spring concentrate of the present invention as a seasoning to various dishes, it is possible to (1) soften the meat quality, (2) supplement minerals contained in foods by using it in dressings, etc., (3) tighten the taste by adding sourness, and (4) eliminate the fishy smell of fish and the like.
(Example 7)
天然温泉の清掃分野における利用 本発明の天然温泉濃縮液を50-5,000ppm水溶液を用いて0.1-100ml/m2程度散布することにより殺菌と洗浄を行うことができる。従来用いてきた塩素系の清掃・消臭材からの転換をすることで環境にも人体にも安全な製品の開発が可能である。
(実施例8)
Use in the field of cleaning natural hot springs Sterilization and cleaning can be performed by spraying about 0.1-100 ml/m2 of the natural hot spring concentrate of the present invention using a 50-5,000 ppm aqueous solution. It is possible to develop products that are safe for both the environment and the human body by switching from the chlorine-based cleaning and deodorizing materials that have been used in the past.
(Example 8)
天然温泉の化粧品分野における利用 本発明の天然温泉濃縮液を50-5,000ppm水溶液に希釈して髪の毛や顔や体にスプレーすることによりミネラルが浸透し、髪の毛のダメージを緩和し、ボリュームを出し、肌をなめらかに保つことが可能になる。
(実施例9)
Use of natural hot springs in the field of cosmetics By diluting the natural hot spring concentrate of the present invention into a 50-5,000 ppm aqueous solution and spraying it on the hair, face and body, the minerals permeate the hair, making it possible to create volume and keep the skin smooth.
(Example 9)
脱臭、消臭分野における利用本発明の天然温泉濃縮液を悪臭源に対して、例えば、50~5,000ppm水溶液を0.1~100ml/m2 程度散布することにより、悪臭を除去することができる。本発明の天然温泉濃縮液を有効成分とする脱臭剤、消臭剤組成物は、溶液、固体、エアゾール等の形態で、し尿そのもの及びトイレ、ゴミ処理場、養鶏・養豚場等の悪臭防止に、また、冷蔵庫、靴箱、ペット飼育舎等の消臭に、更に、口臭、ワキガ等の体臭防止等に、広く利用することが可能である。
(実施例10)
Use in the field of deodorization and deodorization Bad odors can be removed by spraying the natural hot spring concentrate of the present invention against the odor source, for example, by spraying 0.1 to 100 ml/m 2 of a 50 to 5,000 ppm aqueous solution. The deodorant and deodorant composition containing the natural hot spring concentrate of the present invention as an active ingredient can be widely used in the form of a solution, solid, aerosol, etc., to prevent bad odors such as human waste itself, toilets, garbage disposal sites, poultry and pig farms, refrigerators, shoe boxes, pet breeding houses, etc., and also to prevent body odors such as bad breath and armpits.
(Example 10)
微生物や植物の培養、成長加速分野における利用 本発明の天然温泉濃縮液を50-5,000ppm水溶液に希釈し微生物や植物の培養に適用し、浸漬、散布することにより、成長が加速することができる。特に水耕栽培において優れた作用を有する。また組織内のミネラル量を増加することが可能になる。
本発明の天然温泉濃縮液を有利に使用できる微生物としては、ミドリムシやクロレラ、糀酵素、水耕栽培、路地栽培、温室栽培、土壌栽培を問わず、キュウリ、トマト、ナス、ピーマン、ネギ、ブロッコリー、エンドウ、インゲン、ゴボウ、カイワレ大根、ミツバ、ホーレン草、葉ネギ、イチゴ、スイカ、メロン等の野菜類;ミカン、ネーブル、ポンカン、ハッサク、桃、梨、柿、イチジク、ネクタリン、ブドウ、リンゴ等の果樹類;菊、バラ、デンファレ、オンシジウム、コチョウラン、ブーゲンビリア、黒木、モンステラ、ハイビスカス、アレカシア、黄金ガジュマル、幸福の木、カーネーション、ガーベラ、シクラメン、サイネリア、ジュリアン、ベゴニア、ストック、菜の花等の花卉類;芝、葉たばこ、茶、椎茸等が挙げられる。更には、野菜、果物の鮮度保持、及び花卉類の保命効果にも有用である。
(実施例11)
Use in the field of culturing and accelerating the growth of microorganisms and plants The natural hot spring concentrate of the present invention can be diluted to a 50-5,000 ppm aqueous solution, applied to the culture of microorganisms and plants, soaked, and sprayed to accelerate growth. In particular, it has an excellent effect in hydroponics. Also, it becomes possible to increase the amount of minerals in the tissue.
Microorganisms for which the natural hot spring concentrate of the present invention can be advantageously used include euglena, chlorella, koji enzyme, hydroponics, alley cultivation, greenhouse cultivation, and soil cultivation. Fruit trees such as figs, nectarines, grapes, apples; Furthermore, it is useful for preserving the freshness of vegetables and fruits and preserving the life of flowering plants.
(Example 11)
水産養殖における利用本発明の天然温泉濃縮液を水槽に20~500ppm程度添加することにより、養殖魚類及び貝類の摂餌が良好となり、生育が促進される等の効果が奏される。また、生餌となるワムシ、ミジンコ等の微小動物の繁殖がさかんとなり、また、水棲植物が迅速に繁茂する。 Use in aquaculture By adding about 20 to 500 ppm of the natural hot spring concentrate of the present invention to a water tank, the feeding of cultured fish and shellfish is improved, and effects such as promotion of growth are exhibited. In addition, microscopic animals such as rotifers and daphnids that serve as live food proliferate, and aquatic plants grow rapidly.
本発明の天然温泉濃縮液を利用することによって、生育が促進される養殖魚類の例としては、銀鮭、キングサーモン、ヤマメ、ニジマス、ウグイ、ハヤ、タナゴ、鯉、鮒、うなぎ、なまず、どじょう類等の淡水養殖魚;メジナ、メバル、ソイ、ヒラメ、鯛、カワハギ等の海水養殖魚;グッピー、オスカー、エンゼルフィッシュ、ネオンテトラ等の熱帯魚;オニテナガエビ、藻エビ、蟹類等の甲殻類;アワビ、真珠貝、カキ、帆立貝等の貝類が挙げられる。
(実施例12)
Examples of farmed fish whose growth is promoted by using the natural hot spring concentrate of the present invention include freshwater farmed fish such as coho salmon, king salmon, yamame trout, rainbow trout, dace, haya, tanago, carp, crucian carp, eel, catfish, and loaches; seawater farmed fish such as porgies, rockfish, soy, flounder, sea bream, filefish; crustaceans such as freshwater shrimp, seaweed shrimp, and crabs; shellfish such as abalone, pearl oysters, oysters, and scallops;
(Example 12)
汚水処理分野における利用本発明の天然温泉濃縮液を100~50,000ppm程度汚水中に添加することにより、汚水中に含まれる有機物を分解、析出、凝集、沈降せしめ、汚水をきれいな水に変えることが可能となる。本発明の天然温泉濃縮液により処理可能な汚水の例としては、水産加工廃水、家畜屎尿、養鶏廃水、人間屎尿、化学産業廃水等が挙げられる。
(実施例13)
Application in the field of sewage treatment By adding 100 to 50,000 ppm of the natural hot spring concentrate of the present invention to sewage, it is possible to decompose, precipitate, aggregate, and settle organic matter contained in sewage, thereby turning sewage into clean water. Examples of sewage that can be treated with the natural hot spring concentrate of the present invention include marine processing wastewater, livestock manure, poultry farming wastewater, human manure, and chemical industry wastewater.
(Example 13)
用水浄化分野における利用本発明の天然温泉濃縮液を水道水に20~500ppm程度加えることにより、溶解性有機物の析出除去と、次亜塩素酸ソーダそのもの及び塩素殺菌の際に副生成物として生じるトリハロメタンを分解、析出させて無毒化、無臭化することができ、更にミネラル分が補給されるので、水道水を無菌状でミネラルウォーターに変えることができる。また、湖沼水や、河川水に本発明の天然温泉濃縮液を添加し、これらの水中に含まれている有機物や微生物を分解、析出、凝集、濾過することにより安全な飲料水とすることができる。
(実施例14)
Application in the field of water purification By adding about 20 to 500 ppm of the natural hot spring concentrate of the present invention to tap water, it is possible to precipitate and remove soluble organic matter, decompose and precipitate sodium hypochlorite itself and trihalomethane produced as a by-product during chlorine sterilization, and detoxify and deodorize the water. In addition, by adding the natural hot spring concentrate of the present invention to lake water and river water, organic substances and microorganisms contained in these waters are decomposed, precipitated, aggregated, and filtered to make safe drinking water.
(Example 14)
殺菌消毒分野に於ける利用本発明の天然温泉濃縮液を水に100~1,000ppm加えることにより、抗菌作用のある水溶液とすることができるために、例えば、風呂、温泉、プール等の湯水の処理に有用であり、更に、現在、殺菌のために次亜塩素酸ソーダを使用している全利用分野への応用が可能である。
(実施例15)
Use in the field of sterilization and disinfection By adding 100 to 1,000 ppm of the natural hot spring concentrate of the present invention to water, it is possible to make an aqueous solution with antibacterial action.
(Example 15)
黒雲母を粉砕、篩別して4メッシュ以下の粉体とした。この粉体1m3 に25~50%硫酸1m3 を加え、80℃で4時間100rpm(1分間当りの回転数)によって攪拌し、次いで50rpmで1時間攪拌した。次いで、この混合物をフィルタープレスにかけ固液分離し、精製して、OHラジカルを生成し有機物を酸化する作用を有する液状物1.5m3 を得た。得られた天然温泉濃縮液のpHは0.2であり、これについて組成成分を分析した結果を表3に示す。
表3の結果から明らかなように、本発明の天然温泉濃縮液は、多種のミネラル分を多量に含むものであった。
(実施例16)
As is clear from the results in Table 3, the natural hot spring concentrate of the present invention contained a large amount of various minerals.
(Example 16)
花崗岩の風化体である蛭石を粉砕、篩別して4メッシュ以下の粉体とした。この粉体1m3 に25~50%硫酸1m3 を加え、80℃で4時間100rpm(1分間当りの回転数)によって攪拌し、次いで50rpmで1時間攪拌した。次いで、この混合物をフィルタープレスにかけ固液分離し、精製して、OHラジカルを生成し有機物を酸化する作用を有する液状物1.5m3 を得た。 Vermiculite, which is a weathered granite, was pulverized and sieved to powder of 4 mesh or less. 1 m 3 of 25-50% sulfuric acid was added to 1 m 3 of this powder and stirred at 80° C. for 4 hours at 100 rpm (rotations per minute) and then at 50 rpm for 1 hour. Then, this mixture was subjected to a filter press for solid-liquid separation and purification to obtain 1.5 m 3 of a liquid having the action of generating OH radicals and oxidizing organic matter.
この結果から明らかなように、水道水では半値幅が132Hzであったのに対し、水道水に天然温泉濃縮液を加えた後の半値幅は74Hzとなり、水の会合体であるクラスターが小さくなっていることが示された。なお、現在、クラスターの小さい水ほど良質の水、あるいは美味い水、活性水等と言われ生体にとって有益な水とされている。
(実施例17)
As is clear from this result, the half-value width was 132 Hz in tap water, whereas the half-value width after adding the natural hot spring concentrate to tap water was 74 Hz, indicating that the clusters, which are aggregates of water, became smaller. At present, water with smaller clusters is said to be of better quality, more delicious, more active, and more beneficial to living organisms.
(Example 17)
養殖魚に対する使用:養鰻に使用する水(井水自然)に、100ppmの濃度で本発明の天然温泉濃縮液を加え、その効果を調べた。養鰻に使用する養殖槽は250トンであり、この中で鰻の稚魚を32,000匹飼育した。飼育方法は、従来と全く同様に給餌して行った。 Use for cultured fish: The natural hot spring concentrate of the present invention was added at a concentration of 100 ppm to water used for cultivating eels (Imizu Shizen), and its effect was investigated. A culture tank used for cultivating eels is 250 tons, and 32,000 juvenile eels were bred in this tank. The breeding method was feeding in exactly the same way as before.
この結果、飼育開始後160~180日で稚魚から成魚となり、従来に比べ生育期間が大幅に短縮された。また、飼育期間中、pHは6~6.7で安定しており、溶存酸素量(DO)も多く、微生物量も平均1.5×103 程度となった。更に、飼育水の色度が1.4~1.8程度となり、従来は透視度が10cm位であったものが底まで見えるようになった。更にまた、飼育水中のカルシウムイオン量が従来は2,600ppm程度であったものが550~580ppmに低下した。なお、飼育期間中に病害の発生は認められず、生存率はほぼ100%であった。
(実施例18)
As a result, juvenile fish changed to adult fish in 160 to 180 days after the start of breeding, and the growth period was greatly shortened compared to the conventional method. Moreover, during the breeding period, the pH was stable at 6 to 6.7, the amount of dissolved oxygen (DO) was large, and the amount of microorganisms was about 1.5×10 3 on average. Furthermore, the chromaticity of the breeding water was about 1.4 to 1.8, and the bottom was now visible, whereas the transparency was about 10 cm in the past. Furthermore, the amount of calcium ions in breeding water was reduced from about 2,600 ppm to 550-580 ppm. No disease was observed during the breeding period, and the survival rate was almost 100%.
(Example 18)
実施例14で得られた天然温泉濃縮液を500ppmになるように水に溶解し、これを噴射ガス(LPG)とともにエアゾール容器に充填し、消臭スプレーを調製した。この消臭スプレーを、通常の家庭の冷蔵庫に噴霧したところ、冷蔵庫中の腐敗臭(悪臭)が直ちになくなった。その効果は翌日まで持続した。また、この消臭スプレーを悪臭のあるトイレに噴霧したところ悪臭がなくなり、その効果は3時間持続した。また、この消臭スプレーを歯槽膿漏の口臭で悩む人の口にスプレーしたところ、口臭が消えその効果は30分間持続したままであった。更に、この消臭スプレーを獣臭のある犬小屋に噴霧したところ獣臭が消え、その効果は6時間持続した。 The natural hot spring concentrate obtained in Example 14 was dissolved in water to a concentration of 500 ppm, and this was filled in an aerosol container together with a propellant gas (LPG) to prepare a deodorant spray. When this deodorizing spray was sprayed on an ordinary household refrigerator, the putrid smell (bad smell) in the refrigerator disappeared immediately. The effect lasted until the next day. Also, when this deodorizing spray was sprayed on a toilet with a bad smell, the bad smell disappeared and the effect lasted for 3 hours. In addition, when this deodorant spray was sprayed on the mouth of a person suffering from bad breath caused by alveolar pyorrhea, the bad breath disappeared and the effect continued for 30 minutes. Furthermore, when this deodorizing spray was sprayed on a dog house with animal odor, the animal odor disappeared and the effect lasted for 6 hours.
更に、悪臭源として、糞臭のある鳥かご、幼児用おむつ、列車に付属する循環式トイレ、ゴミ処理廃棄場、熱帯魚の水槽等を選定し、同様に処理したところ、同様の結果が得られた。
(実施例19)
In addition, bird cages with fecal odors, baby diapers, circulating toilets attached to trains, waste disposal sites, tropical fish tanks, etc. were selected as foul odor sources, and similar results were obtained when they were treated in the same manner.
(Example 19)
アオコの発生が認められる昆陽池(兵庫県伊丹市)の水について、実施例14で得たのと同じ天然温泉濃縮液をアオコ除去剤として使用することにより、生活用水や飲料水に利用できる程度に浄化できるかどうかを検討した。 The water of Koyo Pond (Itami City, Hyogo Prefecture), where the occurrence of blue-green algae is observed, was examined whether it could be purified to the extent that it could be used for domestic use and drinking water by using the same natural hot spring concentrate obtained in Example 14 as a blue-green algae remover.
試験は、鉄板製の、側面に直径約30cmの透明アクリル製の窓を取り付けて、作業中に水槽内部の状況を観察できるようにした角型10トン水槽に池の水10トンをポンプで送り込み、これに薬剤自動添加装置、浮上汚泥回収装置を設置して、実施例1で得たのと同じ天然温泉濃縮液によって池の水を処理し、COD、SS、全りん、全窒素及びアオコを含む各種藻類の量の変化を検討した。Q323
(実施例20)
In the test, 10 tons of pond water was pumped into a rectangular 10-ton water tank, which was made of an iron plate and had a transparent acrylic window with a diameter of about 30 cm on the side so that the state inside the tank could be observed during operation. Q323
(Example 20)
某神社の池で数十年に亘って堆積したヘドロをスラリーポンプにより吸い上げて200リットル容器のポリエチレン製タンクに採取した。これに、蛭石(バーミキュライト)由来の無機酸処理物(商品名:ルフロックス、シマニシ科研社製)を200ml添加し、攪拌し、30分間放置した。30分後にスラリーは上澄液100リットルと濃縮スラリー100リットルに分離した。上澄水をサイフォンにより排出して、濃縮ヘドロのスラリー(水分30%)を得た。上澄のpHは、pH6.5であったので、そのまま池に還流させた。濃縮ヘドロのスラリーは、肥料と混合、乾燥させ、土壌改良剤として使用することができた。
(実施例21)
Sludge accumulated over several decades in a pond of a certain shrine was sucked up by a slurry pump and collected in a 200-liter polyethylene tank. To this, 200 ml of an inorganic acid-treated product derived from vermiculite (trade name: Ruflox, manufactured by Shimanishi Kaken Co., Ltd.) was added, stirred, and allowed to stand for 30 minutes. After 30 minutes, the slurry separated into 100 liters of supernatant liquid and 100 liters of concentrated slurry. The supernatant water was siphoned off to obtain a concentrated sludge slurry (
(Example 21)
次に、実施例20で得られた濃縮ヘドロのスラリーに高分子凝集剤(中性アニオン系、アコフロックA-110、三井サイアナミット社製)を100ppm(乾量換算10g)添加し、攪拌して、濃縮ヘドロのスラリーをゼラチン状に凝集させた。 Next, 100 ppm (10 g of dry weight) of a polymer flocculant (neutral anionic, ACOFLOC A-110, manufactured by Mitsui Cyanamit Co., Ltd.) was added to the concentrated sludge slurry obtained in Example 20, and the mixture was stirred to coagulate the concentrated sludge slurry into a gelatinous state.
次いで、別の200リットル容量のポリタンク(底から20cm高い処に格子を設け、その上に合成繊維の濾過布を敷いた)を用意し、上記ゼラチン状に凝集させたスラリーを入れた。これを、16時間放置した後、濾過脱水を行った結果、スラリー中の水分は20%に脱水されるとともに、濾過液として、濁りのない澄明な、且つ悪臭の除去された無臭の水が得られた。濾過液は、そのまま池に還流させた。 Next, another 200-liter plastic tank (with a grid placed 20 cm above the bottom and a filter cloth made of synthetic fibers laid thereon) was prepared, and the above-described gelatinous and agglomerated slurry was put therein. After leaving it for 16 hours, it was dehydrated by filtration. As a result, the water content in the slurry was dehydrated to 20%, and clear, odorless water without turbidity was obtained as a filtrate. The filtrate was directly returned to the pond.
更に、このスラリーを7日間天日乾燥した結果、水分は12%迄脱水され固形状のヘドロ乾燥物が得られた。
(実施例22)
Further, this slurry was dried in the sun for 7 days, and as a result, the water content was dehydrated to 12% and a solid dried sludge was obtained.
(Example 22)
本発明の天然温泉濃縮液を50~100ppmの濃度で水に溶解し、この水溶液を農作物の種子浸漬及び葉面散布などにより適用することにより、発芽、発根の促進、葉、茎、枝の伸長、果実の熟成と糖度増加、樹勢強化等において優れた結果を示した。特に、水耕栽培において、従来法と比べ優れた結果を示した。また、本発明の天然温泉濃縮液は、各種ミネラルをバランス良く、しかも吸収の良い状態で含んでいるので、ミネラルの欠乏が原因となって発生する各種の農病害から農作物を守る作用を有することが分った。 By dissolving the natural hot spring concentrate of the present invention in water at a concentration of 50 to 100 ppm and applying this aqueous solution by soaking the seeds of agricultural crops and spraying them on the foliage, etc., excellent results were shown in terms of germination, acceleration of rooting, elongation of leaves, stems and branches, ripening of fruits, increase in sugar content, and strengthening of tree vigor. In particular, in hydroponics, it showed excellent results compared to the conventional method. In addition, since the natural hot spring concentrate of the present invention contains various minerals in a well-balanced and well-absorbed state, it has been found to have the effect of protecting crops from various agricultural diseases caused by mineral deficiency.
その他に、(1)温泉の有効成分ミネラルを大量に含有させることで温泉濃縮原液を生産、(2)天然温泉に天然ミネラルを添加することで良質な飲用ミネラル水を生産、(3)食卓用のミネラル調味料の生産、(4)殺菌作用を利用した清掃用の溶液、(5)天然ミネラルを含んだ化粧品、(6)OHラジカルを生成し有機物並びに無機物を酸化する作用を有する。(7)水のクラスターを小さくする作用を有する。(8)脱臭、消臭作用を有する。(9)微生物や植物の培養、成長加速作用を有する。(10)懸濁物質を凝集する作用を有する。 In addition, (1) production of hot spring concentrated undiluted solution by adding a large amount of active minerals of hot springs, (2) production of high-quality drinking mineral water by adding natural minerals to natural hot springs, (3) production of mineral seasoning for table use, (4) cleaning solution using bactericidal action, (5) cosmetics containing natural minerals, (6) OH radicals are generated and has the action of oxidizing organic and inorganic substances. (7) It has the effect of reducing clusters of water. (8) It has deodorizing and deodorizing action. (9) It has the effect of culturing and accelerating the growth of microorganisms and plants. (10) It has an action of flocculating suspended solids.
本発明の天然温泉濃縮液の作用機序は、未だ明らかでない部分も有るが、次のように推察される。すなわち、本発明の天然温泉濃縮液原料である温泉シェール層から鉱酸抽出したミネラル液(商品名:ルフロックス)を廃水に添加すると、ガスが発生し、二相分離が起こるとともにCODが低下する。分析の結果、発生したガスはCO2 であることが判明している。このことは、廃水中の有機物がルフロックスにより酸化されたからであると考えられる。ESRによる測定結果から、ルフロックスの添加により酸化力の強いOHラジカルが生成することが計測された。 The mechanism of action of the natural hot spring concentrate of the present invention is still partially unclear, but is presumed as follows. That is, when the mineral liquid (trade name: Ruflox) extracted with mineral acid from the hot spring shale layer, which is the raw material of the natural hot spring concentrate of the present invention, is added to wastewater, gas is generated, two-phase separation occurs, and COD decreases. Analysis revealed that the gas generated was CO2. It is considered that this is because the organic matter in the wastewater was oxidized by Ruflox. From the ESR measurement results, it was determined that the addition of Ruflox generated OH radicals with strong oxidizing power.
また、天然温泉濃縮液の好適な出発原料の1つである黒雲母は、フィロ珪酸塩に属する化合物であり、層状構造をなしている。そして、必要により行われる前処理、次いで鉱酸処理することによりこれらのイオンを始めとする各種のイオンが、単純イオンの他、複イオン、錯イオン又は水溶性酸化物の形で溶出するものと考えられる。フィロ珪酸塩のうち特に黒雲母が良い理由は、黒雲母自身が他の鉱物と比べ多種類のミネラル分を含んでおり、また、黒雲母の場合、構造的にこれらミネラル分を抽出しやすいためである。また、花崗岩の風化体である蛭石も同じことが言える。 Biotite, which is one of the preferred starting materials for natural hot spring concentrates, is a compound belonging to phyllosilicates and has a layered structure. It is believed that various ions including these ions are eluted in the form of multiple ions, complex ions or water-soluble oxides in addition to simple ions by pretreatment, if necessary, followed by mineral acid treatment. The reason why biotite is particularly good among phyllosilicates is that biotite itself contains a wide variety of minerals compared to other minerals, and in the case of biotite, these minerals are structurally easy to extract. The same can be said for vermiculite, which is a weathered body of granite.
得られた天然温泉濃縮液に含まれるこれらのミネラル分は、天然に徐々に溶出されるものと同じであるため、動植物等の生体に必須的要素であり、その成長を促進するものと推察される。 Since these minerals contained in the obtained natural hot spring concentrate are the same as those that are gradually eluted naturally, they are essential elements for living organisms such as animals and plants, and are presumed to promote their growth.
Claims (3)
前記天然温泉濃縮液は、ナトリウム:100ml/L~200ml/L、 マグネシウム:2000ml/L~4000ml/L、シリカ:10ml/L~40ml/L、リン: 100ml/L~400ml/L、カリウム;1000ml/L~4000ml/L、カルシウム:100ml/L~500ml/L、チタン:500ml/L~1000ml/L、クロム;3ml/L~20ml/L、マンガン:50ml/L~200ml/L、鉄分;5000ml/L~30000ml/L、コバルト:2ml/L~10ml/L、銅;2ml/L~20ml/L、亜鉛;10ml/L~30ml/L、ゲルマニウム;10ml/L以下、セレン:1ml/L~10ml/L、モリブデン:5ml/L以下とから構成する水中有機物並びに無機物酸化処理用天然温泉濃縮液の製造方法。 A metal-containing acidic solution containing natural hot spring ingredients and inorganic acid-treated minerals containing minerals, characterized by containing organic and inorganic substances in the hot spring liquid and having the property of oxidizing organic substances and inorganic substances in water. A method for producing a natural hot spring concentrate for oxidation treatment,
The natural hot spring concentrate contains sodium: 100ml/L to 200ml/L, magnesium: 2000ml/L to 4000ml/L, silica: 10ml/L to 40ml/L, phosphorus: 100ml/L to 400ml/L, potassium: 1000ml/L to 4000ml/L, calcium: 100ml/L to 500ml/L, titanium: 500ml/L to 1000ml/L. L, Chromium: 3ml/L - 20ml/L, Manganese: 50ml/L - 200ml/L, Iron: 5000ml/L - 30000ml/L, Cobalt: 2ml/L - 10ml/L, Copper: 2ml/L - 20ml/L, Zinc: 10ml/L - 30ml/L, Germanium: 10ml/L or less, Selenium: 1ml/L - 10ml/L, Molybdenum: 5ml/L A method for producing a natural hot spring concentrate for oxidizing organic matter in water and inorganic matter, comprising L or less.
前記天然温泉濃縮液は、ナトリウム:100ml/L~200ml/L、 マグネシウム:2000ml/L~4000ml/L、シリカ:10ml/L~40ml/L、リン: 100ml/L~400ml/L、カリウム;1000ml/L~4000ml/L、カルシウム:100ml/L~500ml/L、チタン:500ml/L~1000ml/L、クロム;3ml/L~20ml/L、マンガン:50ml/L~200ml/L、鉄分;5000ml/L~30000ml/L、コバルト:2ml/L~10ml/L、銅;2ml/L~20ml/L、亜鉛;10ml/L~30ml/L、ゲルマニウム;10ml/L以下、セレン:1ml/L~10ml/L、モリブデン:5ml/L以下とから構成されるウイルス不活化剤の製造方法。 A metal-containing acidic solution containing natural hot spring ingredients and inorganic acid-treated minerals containing minerals, characterized in that it contains organic substances and inorganic substances in hot spring liquid and has the property of oxidizing organic substances and inorganic substances in water.
The natural hot spring concentrate contains sodium: 100ml/L to 200ml/L, magnesium: 2000ml/L to 4000ml/L, silica: 10ml/L to 40ml/L, phosphorus: 100ml/L to 400ml/L, potassium: 1000ml/L to 4000ml/L, calcium: 100ml/L to 500ml/L, titanium: 500ml/L to 1000ml/L. L, Chromium: 3ml/L - 20ml/L, Manganese: 50ml/L - 200ml/L, Iron: 5000ml/L - 30000ml/L, Cobalt: 2ml/L - 10ml/L, Copper: 2ml/L - 20ml/L, Zinc: 10ml/L - 30ml/L, Germanium: 10ml/L or less, Selenium: 1ml/L - 10ml/L, Molybdenum: 5ml/L A method for producing a virus inactivating agent comprising L or less.
前記天然温泉濃縮液は、ナトリウム:100ml/L~200ml/L、 マグネシウム:2000ml/L~4000ml/L、シリカ:10ml/L~40ml/L、リン: 100ml/L~400ml/L、カリウム;1000ml/L~4000ml/L、カルシウム:100ml/L~500ml/L、チタン:500ml/L~1000ml/L、クロム;3ml/L~20ml/L、マンガン:50ml/L~200ml/L、鉄分;5000ml/L~30000ml/L、コバルト:2ml/L~10ml/L、銅;2ml/L~20ml/L、亜鉛;10ml/L~30ml/L、ゲルマニウム;10ml/L以下、セレン:1ml/L~10ml/L、モリブデン:5ml/L以下とから構成される液肥の製造方法。 A metal-containing acidic solution containing natural hot spring ingredients and inorganic acid-treated minerals containing minerals, characterized by containing organic substances and inorganic substances in the hot spring liquid and having the property of oxidizing them.
The natural hot spring concentrate contains sodium: 100ml/L to 200ml/L, magnesium: 2000ml/L to 4000ml/L, silica: 10ml/L to 40ml/L, phosphorus: 100ml/L to 400ml/L, potassium: 1000ml/L to 4000ml/L, calcium: 100ml/L to 500ml/L, titanium: 500ml/L to 1000ml/L. L, Chromium: 3ml/L - 20ml/L, Manganese: 50ml/L - 200ml/L, Iron: 5000ml/L - 30000ml/L, Cobalt: 2ml/L - 10ml/L, Copper: 2ml/L - 20ml/L, Zinc: 10ml/L - 30ml/L, Germanium: 10ml/L or less, Selenium: 1ml/L - 10ml/L, Molybdenum: 5ml/L A method for producing a liquid fertilizer comprising L or less.
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