CN109319893A - A kind of efficient nano water purification agent and preparation method thereof - Google Patents

A kind of efficient nano water purification agent and preparation method thereof Download PDF

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Publication number
CN109319893A
CN109319893A CN201811196232.3A CN201811196232A CN109319893A CN 109319893 A CN109319893 A CN 109319893A CN 201811196232 A CN201811196232 A CN 201811196232A CN 109319893 A CN109319893 A CN 109319893A
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parts
nano
water purification
purification agent
efficient
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CN201811196232.3A
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Chinese (zh)
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滕丽阳
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Priority to CN201811196232.3A priority Critical patent/CN109319893A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/50Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/72Treatment of water, waste water, or sewage by oxidation
    • C02F1/722Oxidation by peroxides
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/04Disinfection

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

The invention discloses a kind of efficient nano water purification agent and preparation method thereof, each component including following mass fraction: 50-70 parts of nano silver, 40-60 parts of nano-titanium dioxide, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, 5-10 parts of nano-dispersing agent and 2-10 parts of oxygenate;The present invention can effectively remove impurities in water, sterilize antibacterial, and safe and non-toxic, without secondary pollution.

Description

A kind of efficient nano water purification agent and preparation method thereof
Technical field
The present invention relates to a kind of water purification agents, and in particular to a kind of efficient nano water purification agent and preparation method thereof.
Background technique
Water purification agent is exactly to throw that water purification, mesh can be played the role of with the aitiogenic medicaments of impurity other in water into the water Before, common water purification agent, which chemically constitutes, is divided into inorganic, organic and inorganic-organic hybrid water purification agent three categories, wherein inorganic The water purification agent of class is mainly active silicic acid, rare earth metal salt such as poly-aluminium lithium etc., aluminium and molysite and its hydrating polymer, this kind of net Aqua single use limitation is larger, and when use generally requires to add other auxiliary substances, and using the net of compounds Aqua is easy to produce secondary pollution, so, to solve the above problems, developing a kind of efficient nano water purification agent and preparation method thereof very It is necessary to.
Summary of the invention
The purpose of the invention is to overcome the deficiencies in the prior art, and provide a kind of efficient nano water purification agent and its preparation Method can effectively remove impurities in water, sterilize antibacterial, and safe and non-toxic, without secondary pollution.
The object of the present invention is achieved like this: a kind of efficient nano water purification agent, each component including following mass fraction: 50-70 parts of nano silver, 40-60 parts of nano-titanium dioxide, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, carboxymethyl cellulose 8-12 parts plain, 5-10 parts of nano-dispersing agent and 2-10 parts of oxygenate.
The oxygenate mainly uses sodium peroxide as oxygenate.
A kind of preparation method of efficient nano water purification agent, the preparation method comprises the following steps:
(1) proper amount of nano silver powder, nano-zinc oxide powder, nano oxidized titanium powder are taken, is mixed uniformly, is mixed Object.
(2) 210-230 parts of deionized waters and 10-20 parts of nanometer point are added in obtained mixture in step (1) Powder obtains solution A after being mixed evenly under the conditions of 25-35 DEG C of water temperature.
(3) a certain amount of clean water is added into the pill tank with agitating device, the case where opening agitating device Under, carboxymethyl cellulose is slowly equably spread in pill tank, is kept stirring, merges carboxymethyl cellulose and water completely, Until carboxymethyl cellulose it is evenly dispersed in water, without significantly big lumps object in the presence of, can stop stirring, Stop being added under agitation in obtained solution A described in step (2) after standing 30-45min after stirring, adjusts blender and turn Speed is 350-450r/min, and mixing time 10-15min obtains solution B.
(4) proper amount of active carbon and oxygenate are taken, is added in solution B obtained by step (3) under agitation, is adjusted Blender revolving speed is 435-550r/min, and mixing time 20-30min obtains the semi-finished product of efficient nano water purification agent.
(5) moisture in the semi-finished product of efficient nano water purification agent obtained in step (4) is removed, obtains solid, as The efficient nano water purification agent.
By adopting the above-described technical solution, the beneficial effects of the present invention are:
(1) by nanometer materials such as nano silver, nano-titanium dioxides, has the effect of sterilization antibiotic and sterilizing, purifying water effect is more It is good and safe and non-toxic, it is without secondary pollution;
(2) active carbon, carboxymethyl cellulose are used, suspended matter in water can be effectively adsorbed, wherein the active carbon just big adsorption capacity of area By force, there is the effect of flocculation, drainage deodorization.
Specific embodiment
Below by embodiment, technical solution of the present invention is described in further detail.
A kind of efficient nano water purification agent, each component including following mass fraction: 50-70 parts of nano silver, nanometer titanium dioxide 40-60 parts of titanium, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, 5-10 parts of nano-dispersing agent With 2-10 parts of oxygenate.
The oxygenate mainly uses sodium peroxide as oxygenate.
A kind of preparation method of efficient nano water purification agent, the preparation method comprises the following steps:
(1) proper amount of nano silver powder, nano-zinc oxide powder, nano oxidized titanium powder are taken, is mixed uniformly, is mixed Object.
(2) 210-230 parts of deionized waters and 10-20 parts of nanometer point are added in obtained mixture in step (1) Powder obtains solution A after being mixed evenly under the conditions of 25-35 DEG C of water temperature.
(3) a certain amount of clean water is added into the pill tank with agitating device, the case where opening agitating device Under, carboxymethyl cellulose is slowly equably spread in pill tank, is kept stirring, merges carboxymethyl cellulose and water completely, Until carboxymethyl cellulose it is evenly dispersed in water, without significantly big lumps object in the presence of, can stop stirring, Stop being added under agitation in obtained solution A described in step (2) after standing 30-45min after stirring, adjusts blender and turn Speed is 350-450r/min, and mixing time 10-15min obtains solution B.
(4) proper amount of active carbon and oxygenate are taken, is added in solution B obtained by step (3) under agitation, is adjusted Blender revolving speed is 435-550r/min, and mixing time 20-30min obtains the semi-finished product of efficient nano water purification agent.
(5) moisture in the semi-finished product of efficient nano water purification agent obtained in step (4) is removed, obtains solid, as The efficient nano water purification agent.
Wherein, nano silver has the effect of broad-spectrum antiseptic, strong bactericidal, and antibacterial is lasting, safe and non-toxic;Nano zine oxide It can be used as antibacterial agent;Nano-titanium oxide can greatly reduce the bacterial population in water, without mutagenesis after drinking, reach safety and drink The standard of water can effectively kill the harmful bacterias such as Escherichia coli, yellow glucose fungus, prevent from infecting, have the function of deodourizing; Nano zine oxide can be used as antibacterial agent;Active carbon has the characteristics that flocculating effect and drainage effect;Carboxymethyl cellulose can be used as Dirt adsorbent.
Embodiment one:
A kind of efficient nano water purification agent, each component including following mass fraction: 50-70 parts of nano silver, nano-titanium dioxide 40- 60 parts, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, 5-10 parts of nano-dispersing agent and confession 2-10 parts of oxygen agent;Its preparation method is as described above.
Embodiment two:
A kind of efficient nano water purification agent, each component including following mass fraction: 50-70 parts of nano silver, nano-titanium dioxide 40- 60 parts, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, 5-10 parts of nano-dispersing agent and confession 2-10 parts of oxygen agent;Its preparation method is as described above.
Embodiment three:
A kind of efficient nano water purification agent, each component including following mass fraction: 50-70 parts of nano silver, nano-titanium dioxide 40- 60 parts, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, 5-10 parts of nano-dispersing agent and confession 2-10 parts of oxygen agent;Its preparation method is as described above.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations, although Referring to above-described embodiment, invention is explained in detail, it should be understood by a person of ordinary skill in the art that still may be used With modifications or equivalent substitutions are made to specific embodiments of the invention, and repaired without departing from any of spirit and scope of the invention Change or equivalent replacement, is intended to be within the scope of the claims of the invention.

Claims (3)

1. a kind of efficient nano water purification agent, it is characterised in that: each component including following mass fraction: 50-70 parts of nano silver is received Rice 40-60 parts of titanium dioxide, 20-30 parts of nano zine oxide, 10-15 parts of active carbon, 8-12 parts of carboxymethyl cellulose, nano-dispersed 5-10 parts and oxygenate 2-10 parts of agent.
2. a kind of efficient nano water purification agent according to claim 1, it is characterised in that: the oxygenate mainly uses peroxide Change sodium as oxygenate.
3. a kind of preparation method of efficient nano water purification agent, it is characterised in that: the preparation method comprises the following steps:
(1) proper amount of nano silver powder, nano-zinc oxide powder, nano oxidized titanium powder are taken, is mixed uniformly, is mixed Object;
(2) 210-230 parts of deionized waters and 10-20 parts of nano-dispersing agent is added in obtained mixture in step (1), Under the conditions of 25-35 DEG C of water temperature, solution A is obtained after being mixed evenly;
(3) a certain amount of clean water is added into the pill tank with agitating device, it, will in the case where opening agitating device Carboxymethyl cellulose is slowly equably spread in pill tank, is kept stirring, and merges carboxymethyl cellulose and water completely, until carboxylic Methylcellulose is evenly dispersed in water, without apparent big lumps object in the presence of, can stop stirring, stop stirring It is added in obtained solution A described in step (2) under agitation after standing 30-45min after mixing, adjusting blender revolving speed is 350-450r/min, mixing time 10-15min, obtains solution B;
(4) proper amount of active carbon and oxygenate are taken, is added in solution B obtained by step (3) under agitation, stirring is adjusted Machine revolving speed is 435-550r/min, and mixing time 20-30min obtains the semi-finished product of efficient nano water purification agent;
(5) moisture in the semi-finished product of efficient nano water purification agent obtained in step (4) is removed, solid is obtained, it is as described Efficient nano water purification agent.
CN201811196232.3A 2018-10-15 2018-10-15 A kind of efficient nano water purification agent and preparation method thereof Pending CN109319893A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110127786A (en) * 2019-06-17 2019-08-16 广州先护特农业科技有限公司 A kind of composition, preparation method and its application in drink water purifying field

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2451698A1 (en) * 1973-11-08 1975-05-22 Ciba Geigy Ag METHODS FOR CLEANING UP INDUSTRIAL WASTE
CN104445459A (en) * 2014-11-13 2015-03-25 苏州市相城区盛胡特种养殖专业合作社 High-efficiency nano water clarifying agent and preparation method thereof
CN108383196A (en) * 2018-04-02 2018-08-10 合肥卓畅农业科技有限公司 Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof
CN108503044A (en) * 2018-04-11 2018-09-07 合肥卓畅农业科技有限公司 A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2451698A1 (en) * 1973-11-08 1975-05-22 Ciba Geigy Ag METHODS FOR CLEANING UP INDUSTRIAL WASTE
CN104445459A (en) * 2014-11-13 2015-03-25 苏州市相城区盛胡特种养殖专业合作社 High-efficiency nano water clarifying agent and preparation method thereof
CN108383196A (en) * 2018-04-02 2018-08-10 合肥卓畅农业科技有限公司 Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof
CN108503044A (en) * 2018-04-11 2018-09-07 合肥卓畅农业科技有限公司 A kind of cultivation factory water body flocculation oxygenation sterilization water purification agent and preparation method thereof

Non-Patent Citations (4)

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Title
中国大百科全书出版社编辑部: "《中国大百科全书 化学 1》", 28 February 1989 *
商平,申俊峰,赵瑞华等编著: "《环境矿物材料》", 31 January 2008 *
范长华 主编: "《化工建设项目咨询手册》", 30 June 1992 *
阮国洪 主编: "《水与人类健康》", 31 July 2017 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110127786A (en) * 2019-06-17 2019-08-16 广州先护特农业科技有限公司 A kind of composition, preparation method and its application in drink water purifying field

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Application publication date: 20190212