CN104671433A - Compound microbiological oxygenate for removing ammonia nitrogen in aquatic water and preparation method of compound microbiological oxygenate - Google Patents

Compound microbiological oxygenate for removing ammonia nitrogen in aquatic water and preparation method of compound microbiological oxygenate Download PDF

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Publication number
CN104671433A
CN104671433A CN201510066990.3A CN201510066990A CN104671433A CN 104671433 A CN104671433 A CN 104671433A CN 201510066990 A CN201510066990 A CN 201510066990A CN 104671433 A CN104671433 A CN 104671433A
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parts
ammonia nitrogen
complex microorganism
oxygenation agent
aquaculture water
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CN201510066990.3A
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CN104671433B (en
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牛晓君
王彩虹
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华南理工大学
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/34Biological treatment of water, waste water, or sewage characterised by the microorganisms used
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • C02F2101/16Nitrogen compounds, e.g. ammonia

Abstract

The invention belongs to the technical field of aquiculture and discloses a compound microbiological oxygenate for removing ammonia nitrogen in aquatic water and a preparation method of the compound microbiological oxygenate. The oxygenate is prepared from the following raw material components in parts by weight: 15-25 parts of zeolite powder, 10-15 parts of chlorite, 10-15 parts of citric acid, 15-20 parts of a powdery bacillus subtilis, photosynthetic bacterium and EM bacterium mixture, 5-15 parts of a proteolytic enzyme, 5-15 parts of silicate, 20-25 parts of sodium percarbonate, 5-10 parts of quicklime, 1-4 parts of ferrous sulfate, 3-5 parts of dextrin, 3-5 parts of starch slurry and 15-20 parts of a protective agent. The oxygenate disclosed by the invention is suitable for sterilizing, oxygenating and preventing and treating diseases in aquiculture and can be used for improving the water quality, reducing the ammonia nitrogen content in a water area, improving the water level transparency, improving the substrate and purifying water.

Description

A kind of complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen and preparation method thereof
Technical field
The invention belongs to technical field of aquaculture, be specifically related to a kind of complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen and preparation method thereof.
Background technology
The movement of aquatic animal and the residual bait of food are aquaculture nursery pond and the topmost source of pollution of growing pond, accumulate on all the year round at the bottom of pond, the objectionable impuritiess such as ammonia nitrogen, nitrite, hydrogen sulfide are resolved under the effect of harmful bacteria, cause pond stench, germ grows thickly, aquatic animal disease takes place frequently.
In aquaculture process, traditional oxygenation way can not meet the demand of culture fishery, the aerator of strong power easily makes fish, shrimp is injured, and dissolved oxygen skewness, general oxygenation way falls flat again, aquaculture water is caused to be in low dissolved oxygen state for a long time, cultivation object is ingested instability, bait utilization is less, immunizing power reduces, sickness rate is high and repeatability is large, have to strengthen dosage and dosing frequency, cause water quality deterioration thus, frequently change water, increase the weight of carrying capacity of environment, increase the mortality ratio etc. in cultivation and storage and transport process, finally cause huge financial loss.
Dissolved oxygen is the condition of medium in which fish live, and when oxygen is sufficient, fish is vigorous, digestibility is high, and growth is fast, efficiency of feed utilization improves; When oxygen is not enough, fish, due to being not suitable with in physiological response, making to ingest and digestibility reduction, and consume more energy.
In prior art, normally used oxygenation agent is all some Chemicals with disintegrating agent, tackiness agent, lubricant, although be conducive to the manufacturing processed of water oxygenation agent, but can not ammonia nitrogen, hydrogen sulfide and algae toxin well in planar water, and these Chemicals are dissolved in aquaculture water, the inner quality of fish, shrimp can be had influence on.In addition, the relevant record of complex microorganism oxygenation agent is not had in prior art.
Therefore, seek a kind of complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen is this area problem to be solved always.
Summary of the invention
In order to overcome the shortcoming of prior art with not enough, the object of the present invention is to provide a kind of complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.This oxygenation agent is suitable for sterilization used for aquiculture, oxygenation, the use of disease resistance, and can improve ammonia-nitrogen content in water quality, reduction waters.
Another object of the present invention is to the preparation method of the complex microorganism oxygenation agent that above-mentioned removal aquaculture water ammonia nitrogen is provided.
Object of the present invention is achieved through the following technical solutions:
Remove a complex microorganism oxygenation agent for aquaculture water ammonia nitrogen, be made up of following feed composition by weight: zeolite powder, 15-25 part; Chlorite, 10-15 part; Citric acid, 10-15 part; Powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, 15-20 part; Protease, 5-15 part; Silicate, 5-15 part; SPC-D, 20-25 part; Unslaked lime, 5-10 part; Ferrous sulfate, 1-4 part; Dextrin, 3-5 part; Starch slurry, 3-5 part; Protective material, 15-20 part;
The weight ratio of powdery genus bacillus in described powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, photosynthetic bacterium and EM bacterium is 2:1:1.
Described powdery genus bacillus comprises bacillus megaterium and gel-shaped spore bacillus, and the weight ratio of bacillus megaterium and gel-shaped spore bacillus is 1:1.
Described chlorite is Textone, potassium chlorite, calcium chlorite, magnesium chlorite or chlorous acid ammonium;
Described protective material is inorganic protective agent, and described inorganic protective agent is more than one in Calcium Chloride Powder Anhydrous, anhydrous sodium sulphate, anhydrous chlorides of rase sodium, Magnesium Chloride Anhydrous, anhydrous magnesium sulfate, sodium carbonate or sodium bicarbonate.
The preparation method of the complex microorganism oxygenation agent of described removal aquaculture water ammonia nitrogen, specifically comprises the following steps:
(1) dilute sulphuric acid is slowly added in zeolite carry out acidification; Zeolite after acidifying to be input in extrusion machine extruding for flap, the thickness≤3mm of flap, being transported to stoving oven carries out roasting, is pulverized after cooling, finally screens the zeolite powder of above-mentioned weight part with 100-120 mesh sieve for subsequent use;
(2) the powdery genus bacillus of above-mentioned weight part, photosynthetic bacterium and EM bacterium mixture is screened with 100-120 mesh sieve for subsequent use;
(3) in agitator, add the protective material of above-mentioned weight part, then add citric acid, stir 10-20 minute with the rotating speed of 200-300r/min, mix;
(4) again by the zeolite powder in step (1), (2) the powdery genus bacillus in, photosynthetic bacterium and EM bacterium mixture and remaining feed composition join in the agitator of step (3) successively, stir 10-20 minute with the rotating speed of 350-500r/min, mix and flood;
(5) by the mixing in step (4) and dipping after product all pour into fermentation hole in, heap fermentation 18-20 days, then pulls out and dries; Be ground into finely powdered afterwards, particle fineness is 0.05-0.1mm; (6) by the finely powdered product in step (5) through compactor compacting, and be divided in packing material according to different standard weights, obtain the complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.Described complex microorganism oxygenation agent particle diameter is 5mm-10mm.
The shape of described complex microorganism oxygenation agent is the spherical or little bulk of particle or sheet.
In step (1), the mass concentration of dilute sulphuric acid is 50%-60%; Acidificatoin time is 30-40 hour.
Described in step (1), the condition of roasting is for carry out roasting in 300-310 DEG C, makes flap water ratio be less than or equal to 2%.
Protectant effect keeps reaction to carry out in over dry environment; Chlorite and solid proton acid-respons have dioxide peroxide, and dioxide peroxide can be used as the sterilizing agent in aquaculture.Dioxide peroxide not only as sterilizing agent, also can do oxygenation agent simultaneously, is suitable for sterilization used for aquiculture, oxygenation, the use of disease resistance, and water quality can be improved, promote nitrification, reduce content, the improving pond substrate of ammonia nitrogen in waters, removal of hydrogen sulfide.
SPC-D is a kind of oxygenation agent, can decompose rapidly, discharge the free oxygen in a large amount of water solubles after SPC-D contacts with water.
Unslaked lime and water react and generate calcium hydroxide, there are sterilization and alga-inhibiting action, and the pH value of water surrounding can be regulated, reduce the concentration of the objectionable impuritiess such as ammonia nitrogen, carbonic acid gas, hydrogen sulfide in water, improve waterplant to the utilization ratio of calcium, phosphorus, promote that anaerobic bacteria flora at the bottom of pond decomposes the mineralising of organic matter and soil ulmin, make the colloidal solid precipitation suspended in water, transparency increases, and water quality is grown fat, be conducive to planktonic organism breeding, for animals and plants provide corresponding nutritive substance.
Ferrous sulfate has purification improvement result to water quality, can improve the adsorption effect of natural mineral sorbent material to harmful toxins such as ammonia nitrogen, hydrogen sulfide and algae, and can play the effect regulating cultivation water pH value.
Under the effect of dextrin and starch, water oxygenation agent (particle/sheet/spherical/little bulk etc.) is under the prerequisite keeping same oxygen content, adds the function of slowly-releasing, three-dimensional oxygenation; Compared with common oxygenation agent, stability and the persistence of its oxygenation effect are better.The effect of dextrin and starch is the release rate of slowly-releasing oxygen, only has its addition suitable, and oxygenation agent just can be made to play best effect.Testing surface, the addition in the present invention is optimum proportioning.
Compared with the prior art, the present invention has the following advantages:
1, this product can deeply penetrate at the bottom of pond, mud at the bottom of fast decoupled pond, residual bait, ight soil, animals and plants corpse and organic debris at the bottom of degraded pond, composite microbial bacteria used can the objectionable impurities such as ammonia nitrogen, nitrite, Algae toxins at the bottom of active adsorption pond, improve redox potential and dissolved oxygen at the bottom of pond, reduce water body acidity, stablize water pH value, trace element supplement, to flood transparency, the object reach improvement substrate, purifying water.
2, the ammonia nitrogen of oxygenation agent removal aquaculture water of the present invention is effective.
3, manufacturing process of the present invention is simple, easy to make, invests little.
Embodiment
Below in conjunction with embodiment, the present invention is further detailed explanation, but embodiments of the present invention are not limited thereto.
Embodiment 1
Remove a complex microorganism oxygenation agent for aquaculture water ammonia nitrogen, be made up of the raw material of following weight part: the zeolite powder of 100-120 mesh sieve choosing, 15 parts; Chlorite, 15 parts; Citric acid, 10 parts; The powdery genus bacillus that 100-120 mesh sieve selects, photosynthetic bacterium and EM bacterium mixture, 20 parts; Protease, 5 parts; Silicate, 15 parts; SPC-D, 20 parts; Unslaked lime, 10 parts; Ferrous sulfate, 1 part; Dextrin, 5 parts; Starch slurry, 3 parts; Protective material, 20 parts;
The weight ratio of powdery genus bacillus in described powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, photosynthetic bacterium and EM bacterium is 2:1:1; Described powdery genus bacillus comprises bacillus megaterium and gel-shaped spore bacillus, and the weight ratio of bacillus megaterium and gel-shaped spore bacillus is 1:1.
Described chlorite is Textone; Described protective material is inorganic protective agent, and described inorganic protective agent is Calcium Chloride Powder Anhydrous.
The preparation method of the complex microorganism oxygenation agent of described removal aquaculture water ammonia nitrogen, specifically comprises the following steps:
(1) by concentration be 50% dilute sulphuric acid slowly add in zeolite and carry out acidification, acidificatoin time controls at 40 hours; Zeolite after acidifying to be input in extrusion machine extruding for flap, the thickness≤3mm of flap, being transported to stoving oven carries out roasting, and maturing temperature controls at 310 DEG C, is pulverized after cooling, finally screens the zeolite powder of above-mentioned weight part with 120 mesh sieves for subsequent use;
(2) the powdery genus bacillus of above-mentioned weight part, photosynthetic bacterium and EM bacterium mixture is screened with 120 mesh sieves for subsequent use;
(3) in agitator, add the protective material of above-mentioned weight part, then add citric acid, stir 15 minutes with the rotating speed of 300r/min, mix;
(4) again the powdery genus bacillus in step (1) mesolite powder, step (2), photosynthetic bacterium and EM bacterium mixture and remaining feed composition are joined in the agitator of step (3) successively, stir 150 minutes with the rotating speed of 400r/m, mix and flood;
(5) by the mixing in step (4) and dipping after product all pour into fermentation hole in, heap fermentation 20 days, then pulls out and dries; Be ground into finely powdered afterwards, particle fineness is 0.05-0.1mm;
(6) by the finely powdered product of above-mentioned drying through compactor compacting, and be divided in packing material according to different standard weights, obtain the complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.
Embodiment 2
Remove a complex microorganism oxygenation agent for aquaculture water ammonia nitrogen, be made up of the raw material of following weight part: the zeolite powder of 100-120 mesh sieve choosing, 25 parts; Chlorite, 10 parts; Citric acid, 15 parts; The powdery genus bacillus that 100-120 mesh sieve selects, photosynthetic bacterium and EM bacterium mixture, 15 parts; Protease, 15 parts; Silicate, 5 parts; SPC-D, 25 parts; Unslaked lime, 5 parts; Ferrous sulfate, 4 parts; Dextrin, 3 parts; Starch slurry, 5 parts; Protective material, 15 parts; The weight ratio of powdery genus bacillus in described powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, photosynthetic bacterium and EM bacterium is 2:1:1.
Described powdery genus bacillus comprises bacillus megaterium and gel-shaped spore bacillus, and weight ratio is 1:1.
Described chlorite is Textone; Described protective material is the mixture of Calcium Chloride Powder Anhydrous and anhydrous sodium sulphate.
The preparation method of the complex microorganism oxygenation agent of described removal aquaculture water ammonia nitrogen, specifically comprises the following steps:
(1) by mass concentration be 60% dilute sulphuric acid slowly add in zeolite and carry out acidification, acidificatoin time controls at 35 hours; Zeolite after acidifying being input to extruding in extrusion machine is flap, thickness≤the 3mm of flap, be transported to stoving oven and carry out roasting, maturing temperature controls at 310 DEG C, for to be pulverized after making water ratio≤2% of flap cool, finally screen the zeolite powder of above-mentioned weight part with 120 mesh sieves for subsequent use;
(2) the powdery genus bacillus of above-mentioned weight part, photosynthetic bacterium and EM bacterium mixture is screened with 100 mesh sieves for subsequent use;
(3) in agitator, add the protective material of above-mentioned weight part, then add citric acid, stir 18 minutes with the rotating speed of 300r/min, mix;
(4) again the powdery genus bacillus in step (1) mesolite powder, step (2), photosynthetic bacterium and EM bacterium mixture and remaining feed composition are joined in the agitator of step (3) successively, stir 15 minutes with the rotating speed of 500r/m, mix and flood;
(5) by the mixing in step (4) and dipping after product all pour into fermentation hole in, heap fermentation 20 days, then pulls out and dries; Be ground into finely powdered afterwards, particle fineness is 0.05-0.1mm;
(6) by the finely powdered product of above-mentioned drying through compactor compacting, and be divided in packing material according to different standard weights, obtain the complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.
Embodiment 3
Remove a complex microorganism oxygenation agent for aquaculture water ammonia nitrogen, be made up of the raw material of following weight part: the zeolite powder of 100-120 mesh sieve choosing, 20 parts; Chlorite, 13 parts; Citric acid, 12 parts; The powdery genus bacillus that 100-120 mesh sieve selects, photosynthetic bacterium and EM bacterium mixture, 18 parts; Protease, 10 parts; Silicate, 10 parts; SPC-D, 22 parts; Unslaked lime, 8 parts; Ferrous sulfate, 2 parts; Dextrin, 4 parts; Starch slurry, 4 parts; Protective material, 17 parts; In described powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, the weight ratio of three is 2:1:1.
Described powdery genus bacillus comprises bacillus megaterium and gel-shaped spore bacillus, and weight ratio is 1:1.
Described chlorite is calcium chlorite; Described protective material is anhydrous sodium sulphate.
The preparation method of the complex microorganism oxygenation agent of described removal aquaculture water ammonia nitrogen comprises the following steps:
(1) by concentration be 50% dilute sulphuric acid slowly add in zeolite and carry out acidification, acidificatoin time controls at 40 hours; Zeolite after acidifying to be input in extrusion machine extruding for flap, the thickness≤3mm of flap, being transported to stoving oven carries out roasting, and maturing temperature controls at 300 DEG C, is pulverized after cooling, finally screens the zeolite powder of above-mentioned weight part with 120 mesh sieves for subsequent use;
(2) the powdery genus bacillus of above-mentioned weight part, photosynthetic bacterium and EM bacterium mixture is screened with 120 mesh sieves for subsequent use;
(3) in agitator, add the protective material of above-mentioned weight part, then add citric acid, stir 20 minutes with the rotating speed of 260r/min, mix;
(4) the powdery genus bacillus more just in step (1) mesolite powder, step (2), photosynthetic bacterium and EM bacterium mixture and remaining feed composition join in the agitator of step (3) successively, stir 20 minutes with the rotating speed of 400r/min, mix and flood;
(5) by the mixing in step (4) and dipping after product all pour into fermentation hole in, heap fermentation 18 days, then pulls out and dries; Be ground into finely powdered afterwards, particle fineness is 0.05-0.1mm;
(6) by the finely powdered product of above-mentioned drying through compactor compacting, and be divided in packing material according to different standard weights, obtain the complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.
Described complex microorganism oxygenation agent particle diameter is 5mm-10mm.
The above is only preferred embodiment of the present invention, and be not restriction the present invention being made to other form, any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the Equivalent embodiments of equivalent variations.But everyly do not depart from technical solution of the present invention content, any simple modification, equivalent variations and the remodeling done above embodiment according to technical spirit of the present invention, still belong to the protection domain of technical solution of the present invention.

Claims (10)

1. remove a complex microorganism oxygenation agent for aquaculture water ammonia nitrogen, it is characterized in that: be made up of following feed composition by weight: zeolite powder, 15-25 part; Chlorite, 10-15 part; Citric acid, 10-15 part; Powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, 15-20 part; Protease, 5-15 part; Silicate, 5-15 part; SPC-D, 20-25 part; Unslaked lime, 5-10 part; Ferrous sulfate, 1-4 part; Dextrin, 3-5 part; Starch slurry, 3-5 part; Protective material, 15-20 part.
2. remove the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 1, it is characterized in that: the weight ratio of powdery genus bacillus in described powdery genus bacillus, photosynthetic bacterium and EM bacterium mixture, photosynthetic bacterium and EM bacterium is 2:1:1;
Described powdery genus bacillus comprises bacillus megaterium and gel-shaped spore bacillus, and the weight ratio of bacillus megaterium and gel-shaped spore bacillus is 1:1.
3. remove the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 1, it is characterized in that: described chlorite is Textone, potassium chlorite, calcium chlorite, magnesium chlorite or chlorous acid ammonium;
Described protective material is inorganics protective material.
4. remove the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 3, it is characterized in that: described inorganic protective agent is more than one in Calcium Chloride Powder Anhydrous, anhydrous sodium sulphate, anhydrous chlorides of rase sodium, Magnesium Chloride Anhydrous, anhydrous magnesium sulfate, sodium carbonate or sodium bicarbonate.
5. according to any one of Claims 1 to 4, remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen, it is characterized in that: specifically comprise the following steps:
(1) dilute sulphuric acid is slowly added in zeolite carry out acidification; Zeolite after acidifying to be input in extrusion machine extruding for flap, the thickness≤3mm of flap, being transported to stoving oven carries out roasting, is pulverized after cooling, finally screens the zeolite powder of above-mentioned weight part with 100-120 mesh sieve for subsequent use;
(2) the powdery genus bacillus of above-mentioned weight part, photosynthetic bacterium and EM bacterium mixture is screened with 100-120 mesh sieve for subsequent use;
(3) in agitator, add the protective material of above-mentioned weight part, then add citric acid, be uniformly mixed;
(4) again by the zeolite powder in step (1), (2) the powdery genus bacillus in, photosynthetic bacterium and EM bacterium mixture and remaining feed composition join in the agitator of step (3) successively, are uniformly mixed and flood;
(5) by the mixing in step (4) and dipping after product all pour into fermentation hole in, heap fermentation, then pulls out and dries; Be ground into finely powdered afterwards;
(6) by the finely powdered product in step (5) through compactor compacting, and be divided in packing material according to different standard weights, obtain the complex microorganism oxygenation agent removing aquaculture water ammonia nitrogen.
6. remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 5, it is characterized in that: in step (1), the mass concentration of dilute sulphuric acid is 50%-60%; Acidificatoin time is 30-40 hour.
7. remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 5, it is characterized in that: described in step (1), the condition of roasting is for carry out roasting in 300-310 DEG C, make flap water ratio be less than or equal to 2%.
8. remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 5, it is characterized in that: the time of heap fermentation described in step (5) is 18-20 days.
9. remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 5, it is characterized in that: described in step (5), the particle fineness of finely powdered product is 0.05-0.1mm.
10. remove the preparation method of the complex microorganism oxygenation agent of aquaculture water ammonia nitrogen according to claim 5, it is characterized in that: described in step (3), stirring velocity is 200-300r/min, churning time is 10-20 minute; Described in step (3), stirring velocity is 350-500r/min, and churning time is 10-20 minute.
CN201510066990.3A 2015-02-09 2015-02-09 A kind of complex microorganism oxygenation agent removing breeding water body ammonia nitrogen and preparation method thereof CN104671433B (en)

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CN107555607B (en) * 2017-08-21 2020-10-27 吴杨 Biological composite oxygen increasing agent and preparation method thereof
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CN107473400A (en) * 2017-08-31 2017-12-15 安徽秀安生态农业有限公司 A kind of giant salamander water conditioner
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CN108094448A (en) * 2017-12-26 2018-06-01 庞庆华 A kind of stable breeding place dry disinfection powder and its preparation process
CN108585133A (en) * 2018-04-25 2018-09-28 江苏新亿源环保科技有限公司 A kind of preparation method of water body for aquaculture clean-up oxygenation agent
CN108640456A (en) * 2018-06-11 2018-10-12 日照澳可生生物科技有限公司 A kind of black smelly modifying agent of aquaculture substrate
CN109052655A (en) * 2018-07-04 2018-12-21 合肥帧讯低温科技有限公司 A kind of disinfection oxygenation agent used for aquiculture
CN108975484A (en) * 2018-08-28 2018-12-11 天津农学院 A kind of enzymatic oxygenation water adjusting agent and its preparation and application
CN109133367A (en) * 2018-09-13 2019-01-04 捷艾悉环保科技(上海)有限公司 Suitable for aquaculture and the cleanser of river deodorization and the preparation method and application thereof

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