CN108383383A - A kind of preparation process of no ground-coat enamel low temperature transmutation zirconium white glaze - Google Patents
A kind of preparation process of no ground-coat enamel low temperature transmutation zirconium white glaze Download PDFInfo
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- CN108383383A CN108383383A CN201810317510.XA CN201810317510A CN108383383A CN 108383383 A CN108383383 A CN 108383383A CN 201810317510 A CN201810317510 A CN 201810317510A CN 108383383 A CN108383383 A CN 108383383A
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Abstract
The invention belongs to ceramic manufacturing fields, and in particular to a kind of preparation process of no ground-coat enamel low temperature transmutation zirconium white glaze.This kind includes feldspar powder, boric acid, barium borate, lime stone, zinc oxide, lead oxide, lead silicate, bentonite without ground-coat enamel low temperature transmutation zirconium white glaze.Above-mentioned glaze formula glaze is at low cost, it is easy to use, firing temperature is low, with unique artistic feeling, this kind has the background color of zirconium white color half-light without the glazing effect that ground-coat enamel low temperature transmutation zirconium white glaze is burnt out, and irregular black splotch is uniformly distributed on background color, the size of black splotch and respectively density change according to ceramic type and glazing thickness, glaze carries stone shape, and slightly trickling tends to effect, and artistic effect is unique.The porcelain made using this kind of glaze improves product specification and selling price, has higher economic value；In addition this kind of glaze can be produced with bulk industrial, can Rapid Popularization, using simple, there is stronger competitiveness on the market.
Description
The application is the divisional application of " no ground-coat enamel low temperature transmutation zirconium white glaze formula, method of preparation and use ", original application
The applying date be August in 2015 27, application No. is：CN201510534544.0.
Technical field
The invention belongs to ceramic manufacturing fields, and in particular to a kind of preparation process of no ground-coat enamel low temperature transmutation zirconium white glaze.
Background technology
When furnace transmutation glaze, that is, implements are burnt into kiln, since, containing there are many pigmentation element, oxidized or reduction goes out in kiln
Unexpected glaze colours effect is presented after kiln.Traditional furnace transmutation glaze is burnt into for high temperature, and firing temperature is at 1200 DEG C or more, firing
Time, firing temperature was high, the time is long, and energy loss is big mostly at 12 more than hour, caused of high cost and not environmentally；And show
There is the glazing effect of lightweight white clouds pottery furnace transmutation glaze single, kind is dull, can not cater to the consumer demand of different individual characteies.
To solve the above problems, the patent of invention of Patent No. 201110133469.9 discloses a kind of Transmutation glaze white cloud ceramics
And its manufacture craft, this kind of Transmutation glaze white cloud ceramics, including white clouds greenwave body and impose on white clouds pottery billet surface on glaze layer, should
Glaze layer include directly apply white clouds make pottery billet surface ground-coat enamel and impose on the overglaze on ground-coat enamel face；The each component of ground-coat enamel includes low temperature
Lead free soldering, coloring oxide, calcium carbonate, alkaline earth metal compound, part kaolin；The each component of the overglaze is by weight ratio
For low-temperature lead-free frit, part zinc oxide, part titanium oxide, coloring oxide, part kaolin.The firing temperature of this kind of furnace transmutation glaze, which is appointed, to be needed
Between 1080-1100 DEG C, the glazed surface burnt out forms naturally crystallization flower.With constantly carrying for people's living standard
Height also constantly changes aesthetic diversified demand, if it is low to develop a kind of firing temperature, has and is different from traditional transmutation effect
The glaze of fruit, can meet aesthetic diversified demand has positive meaning again.
Invention content
In order to solve deficiency in the prior art, the present invention provides a kind of preparations of no ground-coat enamel low temperature transmutation zirconium white glaze
Technique.
It is as follows in parts by weight without ground-coat enamel low temperature transmutation zirconium white glaze：30-45 parts of feldspar powder, 10-15 parts of boric acid, boron
Sour barium 1-5 parts, 5-10 parts of lime stone, 5-10 parts of zinc oxide, 20-30 parts of lead oxide, 5-10 parts of lead silicate, bentonite 0-5.
Optimization, glaze formula is as follows in parts by weight：35 parts of feldspar powder, 12 parts of boric acid, 3 parts of barium borate, lime stone 8
Part, 6 parts of zinc oxide, 26 parts of lead oxide, 10 parts of lead silicate.
Optimization, glaze formula is as follows in parts by weight：39 parts of feldspar powder, 14 parts of boric acid, 5 parts of barium borate, lime stone 6
Part, 8 parts of zinc oxide, 22 parts of lead oxide, 6 parts of lead silicate.
Optimization, glaze formula is as follows in parts by weight：42 parts of feldspar powder, 11 parts of boric acid, 5 parts of barium borate, lime stone 5
Part, 6 parts of zinc oxide, 24 parts of lead oxide, 7 parts of lead silicate.
Optimization, glaze formula is as follows in parts by weight：32 parts of feldspar powder, 15 parts of boric acid, 5 parts of barium borate, lime stone 7
Part, 5 parts of zinc oxide, 28 parts of lead oxide, 8 parts of lead silicate.
Preparation method without ground-coat enamel low temperature transmutation zirconium white glaze, which is characterized in that include the following steps：
Step 1, according to glaze formula weighing and proportioning, by feldspar powder, boric acid, barium borate, lime stone, zinc oxide, oxidation
Lead, lead silicate, and the water of 40-50% is added；
Bentonite is added after 12-18 hours, if there is glaze slip precipitates in step 2, ball milling；
Step 3, the glaze that step 2 is obtained are sieved for use, are made without ground-coat enamel low temperature transmutation zirconium white glaze.
Further, the glaze in step 3 crosses 200 mesh sieve.
Application method without ground-coat enamel low temperature transmutation zirconium white glaze, which is characterized in that include the following steps：
Step 1, light ceramics green body is prepared；
Step 2, it will impose on light ceramics green body, place 5-10 hours without ground-coat enamel low temperature transmutation zirconium white glaze；
Step 3, whether there is or not the ceramic bodies of ground-coat enamel low temperature transmutation zirconium white glaze to be put into oxidizing flame firing in kiln, firing by
Temperature is between 980 DEG C -1060 DEG C.
Further, the enameling method in step 2 is leaching glaze or glaze spraying.
Further, in step 3, after ceramic body enters kiln, kiln is brought rapidly up to firing temperature, naturally cold after firing
But.
Seen from the above description, the preparation process of no ground-coat enamel low temperature transmutation zirconium white glaze provided by the invention has as follows
Advantageous effect：First, glaze is at low cost, used raw material is all easy to get, and manufacture craft is simple；Second is that user
It just, only need to be in billet surface last layer glaze without ground-coat enamel without ground-coat enamel low temperature transmutation zirconium white glaze using this kind；Third, burning
Low at temperature, kiln can be realized between only needing 980 DEG C -1060 DEG C in firing temperature of this kind without ground-coat enamel low temperature transmutation zirconium white glaze
Become effect, it is energy saving；Fourth, there is unique artistic feeling, the glaze that this kind is burnt out without ground-coat enamel low temperature transmutation zirconium white glaze
Effect has the background color of zirconium white color half-light, and irregular black splotch, the size of black splotch are uniformly distributed on background color
Density changes according to ceramic type and glazing thickness respectively, and glaze carries stone shape, and slightly trickling tends to effect, artistic effect
It is unique；The porcelain made using this kind of glaze improves product specification and selling price, has higher economic value；In addition should
Kind of glaze can produce with bulk industrial, can Rapid Popularization, using simple, there is stronger competitiveness on the market.
Specific implementation mode
For a better understanding of the technical solution of the present invention, embodiment provided by the invention is described below in detail.
It is as follows in parts by weight without ground-coat enamel low temperature transmutation zirconium white glaze：30-45 parts of feldspar powder, 10-15 parts of boric acid, boron
Sour barium 1-5 parts, 5-10 parts of lime stone, 5-10 parts of zinc oxide, 20-30 parts of lead oxide, 5-10 parts of lead silicate, bentonite 0-5.
Specific embodiment one：
Glaze formula is as follows in parts by weight：35 parts of feldspar powder, 12 parts of boric acid, 3 parts of barium borate, 8 parts of lime stone, oxidation
6 parts of zinc, 26 parts of lead oxide, 10 parts of lead silicate.
The preparation method of above-mentioned no ground-coat enamel low temperature transmutation zirconium white glaze, includes the following steps：
Step 1, according to glaze formula weighing and proportioning, by feldspar powder, boric acid, barium borate, lime stone, zinc oxide, oxidation
Lead, lead silicate, and 50% water is added；
Bentonite is added after 16 hours, if there is glaze slip precipitates in step 2, ball milling；
The glaze that step 2 obtains is crossed 200 mesh sieve for use, is made without ground-coat enamel low temperature transmutation zirconium white glaze by step 3.
The application method of above-mentioned no ground-coat enamel low temperature transmutation zirconium white glaze, includes the following steps：
Step 1, light ceramics green body is prepared；
Step 2, it will impose on light ceramics green body, place 8 hours without ground-coat enamel low temperature transmutation zirconium white glaze, enameling method is
Soak glaze；
Step 3, whether there is or not the ceramic bodies of ground-coat enamel low temperature transmutation zirconium white glaze to be put into oxidizing flame firing in kiln, firing by
Temperature is between 980 DEG C -1060 DEG C, and after ceramic body enters kiln, kiln is brought rapidly up to firing temperature, natural cooling after firing.
Specific embodiment two,
Glaze formula is as follows in parts by weight：39 parts of feldspar powder, 14 parts of boric acid, 5 parts of barium borate, 6 parts of lime stone, oxidation
8 parts of zinc, 22 parts of lead oxide, 6 parts of lead silicate.
Specific embodiment three,
Glaze formula is as follows in parts by weight：42 parts of feldspar powder, 11 parts of boric acid, 5 parts of barium borate, 5 parts of lime stone, oxidation
6 parts of zinc, 24 parts of lead oxide, 7 parts of lead silicate.
Specific embodiment four,
Glaze formula is as follows in parts by weight：32 parts of feldspar powder, 15 parts of boric acid, 5 parts of barium borate, 7 parts of lime stone, oxidation
5 parts of zinc, 28 parts of lead oxide, 8 parts of lead silicate.
Specific embodiment two to four, the preparation method of no ground-coat enamel low temperature transmutation zirconium white glaze, includes the following steps：
Step 1, according to glaze formula weighing and proportioning, by feldspar powder, boric acid, barium borate, lime stone, zinc oxide, oxidation
Lead, lead silicate, and the water of 40-50% is added；
Bentonite is added after 12-18 hours, if there is glaze slip precipitates in step 2, ball milling；
Step 3, the glaze that step 2 is obtained are sieved for use, are made without ground-coat enamel low temperature transmutation zirconium white glaze.
Application method without ground-coat enamel low temperature transmutation zirconium white glaze, which is characterized in that include the following steps：
Step 1, light ceramics green body is prepared；
Step 2, it will impose on light ceramics green body, place 5-10 hours, glazing side without ground-coat enamel low temperature transmutation zirconium white glaze
Method is leaching glaze or glaze spraying；
Step 3, whether there is or not the ceramic bodies of ground-coat enamel low temperature transmutation zirconium white glaze to be put into oxidizing flame firing in kiln, firing by
Temperature is between 980 DEG C -1060 DEG C, and after ceramic body enters kiln, kiln is brought rapidly up to firing temperature, natural cooling after firing.
Above-mentioned no ground-coat enamel low temperature transmutation zirconium white glaze glaze is at low cost, used raw material is all easy to get, and makes
Make simple for process；It is easy to use, it only need to be one in billet surface without ground-coat enamel without ground-coat enamel low temperature transmutation zirconium white glaze using this kind
Layer glaze；Firing temperature is low, and firing temperature of this kind without ground-coat enamel low temperature transmutation zirconium white glaze only needs 980 DEG C -1060 DEG C
Between transmutation effect can be realized, it is energy saving；With unique artistic feeling, this kind is burnt without ground-coat enamel low temperature transmutation zirconium white glaze
The glazing effect made has the background color of zirconium white color half-light, and irregular black splotch, black are uniformly distributed on background color
The size of spot and respectively density change according to ceramic type and glazing thickness, and glaze carries stone shape, and slightly trickling tends to effect
Fruit, artistic effect are unique.
The porcelain made using this kind of glaze improves product specification and selling price, has higher economic value；Separately
Outer this kind of glaze can produce with bulk industrial, can Rapid Popularization, using simple, there is stronger competitiveness on the market.
The above, only present pre-ferred embodiments, therefore cannot be limited the scope of implementation of the present invention with this, i.e., according to
Equivalent changes and modifications made by scope of the present invention patent and description all should still belong to the model that patent of the present invention covers
In enclosing.
Claims (2)
1. a kind of preparation method of no ground-coat enamel low temperature transmutation zirconium white glaze, which is characterized in that the glaze formula is according to parts by weight
Meter is as follows：30-45 parts of feldspar powder, 10-15 parts of boric acid, 1-5 parts of barium borate, 5-10 parts of lime stone, 5-10 parts of zinc oxide, lead oxide
20-30 parts, 5-10 parts of lead silicate, bentonite 0-5,
Preparation includes the following steps：
Step 1, according to glaze formula weighing and proportioning, by 30-45 parts of feldspar powder, 10-15 parts of boric acid, 1-5 parts of barium borate, lime
5-10 parts of stone, 5-10 parts of zinc oxide, 20-30 parts of lead oxide, 5-10 parts of lead silicate, bentonite 0-5, and the water of 40-50% is added；
Bentonite is added after 12-18 hours, if there is glaze slip precipitates in step 2, ball milling；
Step 3, the glaze that step 2 is obtained are sieved for use, are made without ground-coat enamel low temperature transmutation zirconium white glaze.
2. the preparation method of no ground-coat enamel low temperature transmutation zirconium white glaze according to claim 1, it is characterised in that：In step 3
Glaze cross 200 mesh sieve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810317510.XA CN108383383B (en) | 2015-08-27 | 2015-08-27 | Preparation process of bottom glaze-free low-temperature transmutation zirconium white glaze |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810317510.XA CN108383383B (en) | 2015-08-27 | 2015-08-27 | Preparation process of bottom glaze-free low-temperature transmutation zirconium white glaze |
| CN201510534544.0A CN105236742B (en) | 2015-08-27 | 2015-08-27 | Without ground-coat enamel low temperature transmutation zirconium white glaze, method of preparation and use |
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| CN201510534544.0A Division CN105236742B (en) | 2015-08-27 | 2015-08-27 | Without ground-coat enamel low temperature transmutation zirconium white glaze, method of preparation and use |
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| Publication Number | Publication Date |
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| CN108383383A true CN108383383A (en) | 2018-08-10 |
| CN108383383B CN108383383B (en) | 2021-02-09 |
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| CN201810317510.XA Active CN108383383B (en) | 2015-08-27 | 2015-08-27 | Preparation process of bottom glaze-free low-temperature transmutation zirconium white glaze |
| CN201510534544.0A Active CN105236742B (en) | 2015-08-27 | 2015-08-27 | Without ground-coat enamel low temperature transmutation zirconium white glaze, method of preparation and use |
| CN201810317063.8A Active CN108358448B (en) | 2015-08-27 | 2015-08-27 | Use method of bottomless glaze low-temperature transmutation glaze |
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| CN201510534544.0A Active CN105236742B (en) | 2015-08-27 | 2015-08-27 | Without ground-coat enamel low temperature transmutation zirconium white glaze, method of preparation and use |
| CN201810317063.8A Active CN108358448B (en) | 2015-08-27 | 2015-08-27 | Use method of bottomless glaze low-temperature transmutation glaze |
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| CN108383383B (en) * | 2015-08-27 | 2021-02-09 | 福建省德化县冠鸿陶瓷有限公司 | Preparation process of bottom glaze-free low-temperature transmutation zirconium white glaze |
| CN106830881A (en) * | 2017-04-06 | 2017-06-13 | 潮州市潮安区皓强瓷业有限公司 | The production method of domestic ceramics transmutation color glaze product |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102718562A (en) * | 2012-06-11 | 2012-10-10 | 卡罗比亚釉料（昆山）有限公司 | Leaded milky-white frit for ceramic preparation |
| CN102924126A (en) * | 2012-11-30 | 2013-02-13 | 山东炳坤腾泰陶瓷科技有限公司 | Milky-white frit for zirconium-free glaze and method for producing milky-white frit for zirconium-free glaze |
| CN103342542A (en) * | 2013-06-28 | 2013-10-09 | 李学武 | Method for manufacturing porcelain artware by combining processes of jun porcelain, Ru porcelain and peony porcelain |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2318759C1 (en) * | 2006-11-02 | 2008-03-10 | Юлия Алексеевна Щепочкина | White enamel |
| CN103964900B (en) * | 2014-05-12 | 2015-10-21 | 成都朋和科技有限公司 | A kind of sky blue furnace transmutation glaze formula and preparation method thereof |
| CN104058790B (en) * | 2014-06-26 | 2015-08-05 | 德化恒忆陶瓷艺术股份有限公司 | A kind of furnace transmutation glaze and using method thereof |
| CN108383383B (en) * | 2015-08-27 | 2021-02-09 | 福建省德化县冠鸿陶瓷有限公司 | Preparation process of bottom glaze-free low-temperature transmutation zirconium white glaze |
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2015
- 2015-08-27 CN CN201810317510.XA patent/CN108383383B/en active Active
- 2015-08-27 CN CN201510534544.0A patent/CN105236742B/en active Active
- 2015-08-27 CN CN201810317063.8A patent/CN108358448B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102718562A (en) * | 2012-06-11 | 2012-10-10 | 卡罗比亚釉料（昆山）有限公司 | Leaded milky-white frit for ceramic preparation |
| CN102924126A (en) * | 2012-11-30 | 2013-02-13 | 山东炳坤腾泰陶瓷科技有限公司 | Milky-white frit for zirconium-free glaze and method for producing milky-white frit for zirconium-free glaze |
| CN103342542A (en) * | 2013-06-28 | 2013-10-09 | 李学武 | Method for manufacturing porcelain artware by combining processes of jun porcelain, Ru porcelain and peony porcelain |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105236742B (en) | 2018-05-22 |
| CN108358448A (en) | 2018-08-03 |
| CN105236742A (en) | 2016-01-13 |
| CN108383383B (en) | 2021-02-09 |
| CN108358448B (en) | 2021-07-13 |
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