CN108118531A - 一种羊毛定型剂及其制备方法 - Google Patents

一种羊毛定型剂及其制备方法 Download PDF

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CN108118531A
CN108118531A CN201711305633.3A CN201711305633A CN108118531A CN 108118531 A CN108118531 A CN 108118531A CN 201711305633 A CN201711305633 A CN 201711305633A CN 108118531 A CN108118531 A CN 108118531A
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setting agent
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储平
徐有琦
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Jiangsu New Lucky Polytron Technologies Inc
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Abstract

本发明公开了一种羊毛定型剂及其制备方法,所述羊毛定型剂由如下重量份数的原料组成:硫代乙醇酸铵1‑3份、聚乙二醇辛基苯基醚3‑5份、酒石酸2‑4份、硬脂酸铝1‑3份、乙酰化羊毛脂3‑5份、羟甲基纤维素1‑3份、柠檬酸钠5‑7份、仲烷基磺酸钠10‑15份、氯化镁5‑7份、尿素1‑3份、去离子水20‑30份。本发明的羊毛定型剂能使羊毛及其混纺织物在汽蒸和拉幅中保持织物尺寸的稳定性,通过处理织物表面更柔滑、细腻,对羊毛有轻微的剥磷效果。本发明的羊毛定型剂制造工艺简单易操作,原料价格低廉易获得,且无毒无害,对人体不刺激,挥发性低。

Description

一种羊毛定型剂及其制备方法
技术领域
本发明属于纺织品技术领域,更具体是涉及一种羊毛定型剂及其制备方法。
背景技术
羊毛织物性能优异,如:吸汗透气、柔软、防敏感、容易清洗、不易起毛球等,但是羊毛织物易皱、缩水、易变形,从而影响了羊毛织物的应用,因此需要羊毛定型剂对其的形貌进行定型,从而拓宽羊毛织物的应用范围。
发明内容
本发明的目的在于提供一种羊毛定型剂及其制备方法,以解决上述背景技术中提出的问题。
为实现上述目的,本发明提供如下技术方案:
一种羊毛定型剂,所述羊毛定型剂包括如下重量份数的原料:硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份、酒石酸2-4份、硬脂酸铝1-3份、乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份、仲烷基磺酸钠10-15份、氯化镁5-7份、尿素1-3份、去离子水20-30份。
优选地,按照重量份数,包括以下组分:硫代乙醇酸铵1份、聚乙二醇辛基苯基醚3份、酒石酸2份、硬脂酸铝1份、乙酰化羊毛脂3份、羟甲基纤维素1份、柠檬酸钠5份、仲烷基磺酸钠10份、氯化镁5份、尿素1份、去离子水20份。
优选地,按照重量份数,包括以下组分:硫代乙醇酸铵2份、聚乙二醇辛基苯基醚4份、酒石酸3份、硬脂酸铝2份、乙酰化羊毛脂4份、羟甲基纤维素2份、柠檬酸钠6份、仲烷基磺酸钠13份、氯化镁6份、尿素2份、去离子水25份。
优选地,按照重量份数,包括以下组分:硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份、酒石酸4份、硬脂酸铝3份、乙酰化羊毛脂5份、羟甲基纤维素3份、柠檬酸钠7份、仲烷基磺酸钠15份、氯化镁7份、尿素3份、去离子水30份。
本发明还公开了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水20-30份,油浴加热,氮气环境,冷凝回流,升高温度至70-80℃;
步骤2,加入硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份,500-1000转/分钟,搅拌5-10分钟;
步骤3,加入pH调节剂,调节pH为5-7;
步骤4,加入乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份,500-1000转/分钟,搅拌20-30分钟;
步骤5,降低温度至40-60℃,加入pH调节剂,调节pH值为8-9;
步骤6,加入酒石酸2-4份、硬脂酸铝1-3份、仲烷基磺酸钠10-15份,500-1000转/分钟,搅拌30-40分钟;
步骤7,加入尿素1-3份、氯化镁5-7份,500-1000转/分钟,搅拌10-20分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
优选地,所述pH调节剂为盐酸、醋酸、柠檬酸、碳酸钠、氢氧化钠中的一种或者一种以上。
与现有技术相比,本发明的有益效果是:
1、本发明的羊毛定型剂制造工艺简单易操作,原料价格低廉易获得,且无毒无害,对人体不刺激,挥发性低。
2、本发明的羊毛定型剂所用各种原料之间相互配伍、协同作用,共同组成性能优异的产品。
3、本发明的羊毛定型剂在应用过程中不产生有毒的气体或固体物质。
4、本发明的羊毛定型剂能使羊毛及其混纺织物在汽蒸和拉幅中保持织物尺寸的稳定性,通过处理织物表面更柔滑、细腻,对羊毛有轻微的剥磷效果。
5、本发明的羊毛定型剂水洗牢度性能优异。
6、本发明的羊毛定型剂应用织物之后不影响织物本身的柔软性、透气性及其本身的机械性能。
7、本发明的羊毛定型剂使用方便,可以通过浸渍、辊涂、喷涂等方式施加到织物。
8、本发明的羊毛定型剂处理的织物可防缩防皱,定型效果好,免熨烫,具有挺括、丰满、不污等特点。
9、简化工艺,操作安全简单,易于工业化生产。
10、本发明的使用可收到良好的经济效益。
具体实施实例
本发明公开了一种羊毛定型剂,按照重要份数,包括以下组分:硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份、酒石酸2-4份、硬脂酸铝1-3份、乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份、仲烷基磺酸钠10-15份、氯化镁5-7份、尿素1-3份、去离子水20-30份。
本发明还提供了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水20-30份,油浴加热,氮气环境,冷凝回流,升高温度至70-80℃;
步骤2,加入硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份,500-1000转/分钟,搅拌5-10分钟;
步骤3,加入适量pH调节剂,调节pH为5-7;
步骤4,加入乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份,500-1000转/分钟,搅拌20-30分钟;
步骤5,降低温度至40-60℃,加入适量pH调节剂,调节pH值为8-9;
步骤6,加入酒石酸2-4份、硬脂酸铝1-3份、仲烷基磺酸钠10-15份,500-1000转/分钟,搅拌30-40分钟;
步骤7,加入尿素1-3份、氯化镁5-7份,500-1000转/分钟,搅拌10-20分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
实施例1
本发明公开了一种羊毛定型剂,按照重要份数,包括以下组分:硫代乙醇酸铵1份、聚乙二醇辛基苯基醚3份、酒石酸2份、硬脂酸铝1份、乙酰化羊毛脂3份、羟甲基纤维素1份、柠檬酸钠5份、仲烷基磺酸钠10份、氯化镁5份、尿素1份、去离子水20份。
本发明还提供了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水20份,油浴加热,氮气环境,冷凝回流,升高温度至70℃;
步骤2,加入硫代乙醇酸铵1份、聚乙二醇辛基苯基醚3份,500转/分钟,搅拌5分钟;
步骤3,加入适量pH调节剂,调节pH为5;
步骤4,加入乙酰化羊毛脂3份、羟甲基纤维素1份、柠檬酸钠5份,500转/分钟,搅拌20分钟;
步骤5,降低温度至40℃,加入适量pH调节剂,调节pH值为8;
步骤6,加入酒石酸2份、硬脂酸铝1份、仲烷基磺酸钠10份,500转/分钟,搅拌30分钟;
步骤7,加入尿素1份、氯化镁5份,500转/分钟,搅拌10分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
实施例2
本发明公开了一种羊毛定型剂,按照重要份数,包括以下组分:硫代乙醇酸铵2份、聚乙二醇辛基苯基醚4份、酒石酸3份、硬脂酸铝2份、乙酰化羊毛脂4份、羟甲基纤维素2份、柠檬酸钠6份、仲烷基磺酸钠13份、氯化镁6份、尿素2份、去离子水25份。
本发明还提供了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水25份,油浴加热,氮气环境,冷凝回流,升高温度至75℃;
步骤2,加入硫代乙醇酸铵2份、聚乙二醇辛基苯基醚4份,800转/分钟,搅拌8分钟;
步骤3,加入适量pH调节剂,调节pH为6;
步骤4,加入乙酰化羊毛脂4份、羟甲基纤维素2份、柠檬酸钠6份,800转/分钟,搅拌20分钟;
步骤5,降低温度至50℃,加入适量pH调节剂,调节pH值为8.5;
步骤6,加入酒石酸3份、硬脂酸铝2份、仲烷基磺酸钠13份,800转/分钟,搅拌35分钟;
步骤7,加入尿素2份、氯化镁6份,800转/分钟,搅拌10分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
实施例3
本发明公开了一种羊毛定型剂,按照重要份数,包括以下组分:硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份、酒石酸4份、硬脂酸铝3份、乙酰化羊毛脂5份、羟甲基纤维素3份、柠檬酸钠7份、仲烷基磺酸钠15份、氯化镁7份、尿素3份、去离子水30份。
本发明还提供了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水30份,油浴加热,氮气环境,冷凝回流,升高温度至80℃;
步骤2,加入硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份,1000转/分钟,搅拌10分钟;
步骤3,加入适量pH调节剂,调节pH为7;
步骤4,加入乙酰化羊毛脂5份、羟甲基纤维素3份、柠檬酸钠7份,900转/分钟,搅拌25分钟;
步骤5,降低温度至60℃,加入适量pH调节剂,调节pH值为9;
步骤6,加入酒石酸4份、硬脂酸铝3份、仲烷基磺酸钠15份,1000转/分钟,搅拌30分钟;
步骤7,加入尿素3份、氯化镁7份,1000转/分钟,搅拌20分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
实施例4
本发明公开了一种羊毛定型剂,按照重要份数,包括以下组分:硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份、酒石酸3份、硬脂酸铝1份、乙酰化羊毛脂3份、羟甲基纤维素3份、柠檬酸钠5份、仲烷基磺酸钠10份、氯化镁7份、尿素1份、去离子水20份。
本发明还提供了一种羊毛定型剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入去离子水20份,油浴加热,氮气环境,冷凝回流,升高温度至75℃;
步骤2,加入硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份,900转/分钟,搅拌5分钟;
步骤3,加入适量pH调节剂,调节pH为7;
步骤4,加入乙酰化羊毛脂3份、羟甲基纤维素3份、柠檬酸钠5份,800转/分钟,搅拌25分钟;
步骤5,降低温度至40℃,加入适量pH调节剂,调节pH值为8;
步骤6,加入酒石酸3份、硬脂酸铝1份、仲烷基磺酸钠10份,900转/分钟,搅拌30分钟;
步骤7,加入尿素1份、氯化镁7份,500-1000转/分钟,搅拌10-20分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
上述列举的各种实施例,在不矛盾的前提下,可以相互组合实施,本领域技术人员可结合上文对实施例的解释,作为对不同实施例中的技术特征进行组合的依据。
测试例
采用实施例1、2、3、4的羊毛定型剂处理羊毛织物,将得到的羊毛织物进行性能测试,测试结果如下:
实施例 毡缩率(%)
1 5.34
2 4.79
3 4.24
4 4.08
尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。

Claims (6)

1.一种羊毛定型剂,其特征在于:所述羊毛定型剂包括如下重量份数的原料:硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份、酒石酸2-4份、硬脂酸铝1-3份、乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份、仲烷基磺酸钠10-15份、氯化镁5-7份、尿素1-3份、去离子水20-30份。
2.根据权利要求1所述的羊毛定型剂,其特征在于:按照重量份数,包括以下组分:硫代乙醇酸铵1份、聚乙二醇辛基苯基醚3份、酒石酸2份、硬脂酸铝1份、乙酰化羊毛脂3份、羟甲基纤维素1份、柠檬酸钠5份、仲烷基磺酸钠10份、氯化镁5份、尿素1份、去离子水20份。
3.根据权利要求1所述的羊毛定型剂,其特征在于:按照重量份数,包括以下组分:硫代乙醇酸铵2份、聚乙二醇辛基苯基醚4份、酒石酸3份、硬脂酸铝2份、乙酰化羊毛脂4份、羟甲基纤维素2份、柠檬酸钠6份、仲烷基磺酸钠13份、氯化镁6份、尿素2份、去离子水25份。
4.根据权利要求1所述的羊毛定型剂,其特征在于:按照重量份数,包括以下组分:硫代乙醇酸铵3份、聚乙二醇辛基苯基醚5份、酒石酸4份、硬脂酸铝3份、乙酰化羊毛脂5份、羟甲基纤维素3份、柠檬酸钠7份、仲烷基磺酸钠15份、氯化镁7份、尿素3份、去离子水30份。
5.一种采用上述权利要求1-4中任一所述羊毛定型剂的制备方法,其特征在于:具体步骤包括:
步骤1,在反应釜中加入去离子水20-30份,油浴加热,氮气环境,冷凝回流,升高温度至70-80℃;
步骤2,加入硫代乙醇酸铵1-3份、聚乙二醇辛基苯基醚3-5份,500-1000转/分钟,搅拌5-10分钟;
步骤3,加入pH调节剂,调节pH为5-7;
步骤4,加入乙酰化羊毛脂3-5份、羟甲基纤维素1-3份、柠檬酸钠5-7份,500-1000转/分钟,搅拌20-30分钟;
步骤5,降低温度至40-60℃,加入pH调节剂,调节pH值为8-9;
步骤6,加入酒石酸2-4份、硬脂酸铝1-3份、仲烷基磺酸钠10-15份,500-1000转/分钟,搅拌30-40分钟;
步骤7,加入尿素1-3份、氯化镁5-7份,500-1000转/分钟,搅拌10-20分钟;
步骤8,关停搅拌,得到配制好的液体羊毛定型剂;
步骤9,静置冷却至反应釜中液体羊毛定型剂低于20℃,放料封装,制得成品。
6.根据权利要求5所述的制备方法,其特征在于:所述pH调节剂为盐酸、醋酸、柠檬酸、碳酸钠、氢氧化钠中的一种或者一种以上。
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