CN108096473A - Nurse one's health the medicine perfume and its processing technology of gynaecological disease - Google Patents
Nurse one's health the medicine perfume and its processing technology of gynaecological disease Download PDFInfo
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- CN108096473A CN108096473A CN201711382846.6A CN201711382846A CN108096473A CN 108096473 A CN108096473 A CN 108096473A CN 201711382846 A CN201711382846 A CN 201711382846A CN 108096473 A CN108096473 A CN 108096473A
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- perfume
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
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Abstract
The invention discloses a kind of medicine perfume for nursing one's health gynaecological disease, are prepared including following raw material：Motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal, Poplar Powder, water, binding material.The medicine of the conditioning gynaecological disease of the present invention is fragrant, can be directly entered lesion according to theoretical make of modern drug matching, play an important role of nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, good to difficult and complicated gynopathy conditioning effect, has no toxic side effect, environmentally protective, easy to use.
Description
Technical field
The present invention relates to a kind of medicine that can nurse one's health gynaecological disease is fragrant.
Background technology
The raw material of traditional medicine perfume is generally made of incense drug, wood powder, binding material and additivity material.Wherein, incense drug includes day
Right fragrance and some Chinese medicines.Perfume (or spice) on the market is broadly divided into reading partner perfume now, drives epidemic disease incense for eliminating plague, and purification air is fragrant with adjusting blood
Health care perfume (or spice) of pressure etc..At present, there is no the medicine that can nurse one's health gynecological disease is fragrant.
Culture of TCM is the rarity in China, with a long history with Chinese medicine treatment gynecological disease.Difficult and complicated cases of gynaecology and chronic
Disease, it can influence the normal life of people, but cannot effect a radical cure quickly.Traditional Chinese medical herbal treatment gynaecological disease is started with from Overall View,
Dispersing stagnated hepatoqi is strengthened the body resistance to consolidate the constitution, promoting blood circulation and removing blood stasis, and softening and resolving hard mass is clearing heat and detoxicating, and adjusting endocrine comprehensively makes gas lead to blood work, enlivens dirty
Internal organs, channels and collaterals are this, and qi and blood is uses, and qi and blood is the material base of human body, and internal organs are source of generating QI and blood, play the life for being in charge of blood
Into, have under one's command and run, it is the motive power of blood to adjust blood and balanced action, gas.Blood is the material base of menstruation, if internal organs work(
It can lack of proper care, qi and blood circulation will be affected, involve sea of blood function, then can cause the generation of various gynaecological diseases, such as ovarian cyst
Deng.Chinese traditional treatment can exempt the psychological pressure and mental burden that operation is brought to patient, adjust endocrine, strengthen immunity etc.,
Medication is convenient, does not operate on, does not hinder vigour, painful risk is small, and expense is low, markedly fast.Medicine perfume is made in Chinese medicine, is reduced
The toxic side effect that oral traditional Chinese medicine is brought is also convenient for being commonly used in daily life, not only plays therapeutic effect, moreover it is possible to play net
Change air, the effect of health care.
Incense drug and wood powder in usual medicine perfume (or spice) is generally powdered, relatively dissipates, it is not easy to strike up partnership, so also needing to add
The material that some is added to play adhesive effect.Existing medicine perfume (or spice) product also has the chemical classes binding material used, not only reduces medicine perfume
Quality, and the substance unfavorable to human body can be also generated in medicine perfume (or spice) combustion process.The medicine incense prescription of the present invention is scientific and reasonable, adjusts
Women qi-blood circulating is managed, there is good conditioning effect to difficult and complicated cases gynaecological disease.The present invention has no toxic side effect to medicine perfume (or spice), does not add
Add chemical adhesive, it is environmentally protective.
The content of the invention
The present invention provides a kind of medicine perfume for nursing one's health gynaecological disease and its processing technologys.The present invention adopts the following technical scheme that：
A kind of medicine for nursing one's health gynaecological disease is fragrant, and the raw material including following parts by weight is prepared：
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of non-irrigated lotuses
Grass, 1-3 portions of rhizoma cyperis, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos,
0.5-1.5 portions of santals, 3-9 parts of Poplar Powders, 10-30 parts of water, 2-6 parts of binding materials.
The present invention provides the processing technology of the medicine perfume of above-mentioned conditioning gynaecological disease：Including weighing each raw material by weight, by benefit
Brittle Falsepimpernel Herb, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal are respectively in 45-65
When DEG C dry 6-12 is small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input Poplar Powder,
It is stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after water, binding material, mixture is obtained, by mixture
Finished medicines perfume is obtained after compression moulding, drying.
Preferably, the present invention provides the processing technology of the medicine perfume of above-mentioned conditioning gynaecological disease：Including weighing each original by weight
Material distinguishes motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal
When 45-65 DEG C of dry 6-12 is small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input
It is stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after Poplar Powder, water, binding material, obtains mixture, it will
Mixture is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm, then disk is fragrant into a diameter of 12-15cm, plate-like that weight is 25-30g,
Finished medicines perfume is obtained after 45-55 DEG C of drying, the moisture content of finished medicines perfume is 10-12%.
A kind of medicine for nursing one's health gynaecological disease is fragrant, and the raw material including following parts by weight is prepared：
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of non-irrigated lotuses
Grass, 1-3 portions of rhizoma cyperis, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos,
0.5-1.5 portions of santals, Poplar Powder, 10-30 parts of water, the 2-6 parts of binding materials of 3-9 parts of modifications.
The present invention also provides the processing technologys of the medicine perfume of above-mentioned conditioning gynaecological disease：It, will including weighing each raw material by weight
Motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal are respectively in 45-
When 65 DEG C of dry 6-12 are small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input is modified
Poplar Powder, water, stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after binding material, obtain mixture,
Finished medicines perfume will be obtained after mixture compression moulding, drying.
Preferably, the present invention also provides above-mentioned conditioning gynaecological disease medicine perfume processing technology：It is each including weighing by weight
Raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal point
Not when 45-65 DEG C of dry 6-12 is small, 50-80 mesh sieves are crushed, puts into mixer, throws after each raw material after crushing is mixed
It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after entering modified Poplar Powder, water, binding material
Mixture, is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm by mixture, then disk is into a diameter of 12-15cm, the disk that weight is 25-30g
Shape is fragrant, finished medicines perfume is obtained after dry at 45-55 DEG C, the moisture content of finished medicines perfume is 10-12%.
Preferably, the preparation method of the Poplar Powder of the modification includes mixing 25-75g Poplar Powders, 10-40mL ionic liquids
It is put into after conjunction in mixer, is 40-45 DEG C, is stirred 30-50 minutes with 200-400 revs/min of rotating speed in temperature, discharge, is close
Envelope, is placed in the drying box that temperature is 70-85 DEG C 30-60 minutes, obtains mixture A, and mixture A is added in 120-250g water
In, it is stirred 30-60 minutes at 30-45 DEG C, with 100-300 revs/min of rotating speed, filtering, by filtering gained precipitation 30-60g
After acetone, the washing of 45-90g ethyl alcohol, when 40-55 DEG C of dry 12-24 is small, modified Poplar Powder is obtained；The ionic liquid is
- 3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine are (1-4) in mass ratio：The mixture of (1-4).
It is further preferred that the preparation method of the Poplar Powder of the modification is included 25-75g Poplar Powders, 10-40mL ions
It is put into after liquid mixing in mixer, is 40-45 DEG C, is stirred 30-50 minutes with 200-400 revs/min of rotating speed in temperature, go out
Material, sealing, are placed in the drying box that temperature is 70-85 DEG C 30-60 minutes, obtain mixture A, and mixture A is added in 120-
It in 250g water, is stirred 30-60 minutes at 30-45 DEG C, with 100-300 revs/min of rotating speed, filtering, filtering gained precipitation is used
After 30-60g acetone, the washing of 45-90g ethyl alcohol, when 40-55 DEG C of dry 12-24 is small, mixture B is obtained, with glacial acetic acid by 15-
45g mass fractions are that the pH of the ethanol water of 85-95% is adjusted to 3-4, add in 0.85-1.7g modifying agent I, are uniformly mixed,
Mixed liquor C is obtained, is put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, is 60-75 in temperature
DEG C, stirred 50-100 minute with 300-500 revs/min of rotating speed, discharge, when 40-60 DEG C of dry 24-48 is small, be modified
Poplar Powder；The ionic liquid is that -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine are (1-4) in mass ratio：(1-4's) is mixed
Close object；The modifying agent I is oleamide, vinyltrimethoxysilane, isopropyl three (dioctylphyrophosphoric acid acyloxy) titanium
One or more mixture in acid esters.
It is further preferred that the ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4
Mixture.
It is further preferred that the modifying agent I is vinyltrimethoxysilane.
Preferably, the binding material is mixing one or more in sunflower seed dregs adhesive, guar gum, carragheen
Object.
It is further preferred that the binding material is sunflower seed dregs adhesive, the preparation method of the sunflower seed dregs adhesive
Including 120-240 parts of sunflower seed dregs powder, 200-400 parts of water, 12-18 parts of modifying agent II, 8-12 parts of potassium hydroxide are uniformly mixed,
Be warming up to 55-75 DEG C, temperature be 55-75 DEG C, that 3.5-7 is stirred with 200-300 revs/min of rotating speed is small when, naturally cool to
30-45 DEG C, 11.5-23 parts of glutaraldehydes are added in, divides kind at 30-45 DEG C, with 250-400 revs/min of rotating speed stirring 25-45, obtains
To sunflower seed dregs adhesive；The modifying agent II is one or more in polyvinyl alcohol, neopelex, urea
Mixture.
It is further preferred that it is (3-5) in mass ratio that the modifying agent II, which is polyvinyl alcohol, neopelex,:
The mixture of (1-2).
It is further preferred that it is 3 in mass ratio that the modifying agent II, which is polyvinyl alcohol, neopelex,:2 it is mixed
Close object.
The medicine of the conditioning gynaecological disease of the present invention is fragrant, can be directly entered lesion according to theoretical make of modern drug matching, have
There are nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, it is good to difficult and complicated gynopathy conditioning effect, it has no toxic side effect, green ring
It protects, it is easy to use.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be each preferably to get the present invention in any combination
Embodiment.
Specific embodiment
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality
It applies among a scope.The experimental method of actual conditions is not specified in the following example, according to conventional methods and conditions or according to business
Product specification selects.
In following embodiments, primary raw material and instrument used are as follows：
Motherwort, Classification system：Leonurus artemisia (Laur.) S.Y.Hu F have inducing diuresis to remove edema, shrink uterus
The effect of effect, is the key medicine that ancient Chinese medicine doctor is used for treating gynaecological disease, and the present invention dries herb using the ground of motherwort.
Radix Salviae Miltiorrhizae, the dry root of labiate Radix Salviae Miltiorrhizae Salvia miltiorrhiza Bge. have promoting blood circulation, promoting menstruation
The effect of analgesic, relieving restlessness that clears away heart-fire, cool blood to disappear carbuncle.
Radix Angelicae Sinensis, be umbelliferae angelica Angelica sinensis (Oliv.) Diels dry root, have enrich blood and
Blood, menstruction regulating and pain relieving, the effect of moisturize laxation, anticancer.
Rhizome of chuanxiong is the dry rhizome of samphire Rhizoma Chuanxiong Ligusticum chuanxiong Hort., acrid in flavour and warm in nature.Return
Liver, courage, pericardium channel, blood-activating and qi-promoting, wind-expelling pain-stopping.
Radix Astragali, specifically used astragalus mongolicus (Classification system：Astragalus membranaceus(Fish)
Bungevar.Mongholicus (Bunge) Hsiao) dry root, control shortness of breath and palpitation, weak, collapse, spontaneous perspiration, night sweat, physically weak
Edema, chronic nephritis, chronic diarrhea, rectal prolapse, the prolapse of uterus, ulcer is difficult to burst, the long disunion of the open sore part.
Eclipta prostrata is catananche's Eclipta prostrata (Classification system：Eclipta prostrata) ground drying herb,
Have effects that tonify the liver and kidney, blood-stanching and blood-cooling.
Rhizoma cyperi, Classification system：Cyperus rotundus L. are the dry rhizome of sedge nutgrass flatsedge, for liver depression
The stagnation of the circulation of vital energy, distending pain in the chest and hypochondrium, hernia pain, swollen breasts, the taste stagnation of the circulation of vital energy, gastral cavity abdomen ruffian is bored, turgor pain, irregular menstruation, closed dysmenorrhea.
Rhizoma Atractylodis Macrocephalae, the dry rhizome of feverfew Rhizoma Atractylodis Macrocephalae Atractylodes macrocephala Koidz. have invigorating the spleen
The effect of QI invigorating, eliminate dampness and have diuretic effect, hidroschesis, tocolysis, for spleen eating less, abdominal distention diarrhea, phlegm retention anti-dazzle nervous, oedema, spontaneous perspiration, movement of the foetus is not
Peace.
Radix Paeoniae Alba, Classification system：Cynanchum otophyllum, Ranunculaceae Radix Paeoniae Alba platymiscium are cohosh Chinese herbaceous peonies
Dry root, smooth liver and relieve pain, nourishing blood for regulating menstruation, astringing YIN to stop sweating.For dizziness of having a headache, hypochondriac pain, abdominal pain, four limbs contraction pain, blood deficiency chlorosis,
Irregular menstruation.
Rhizoma Gastrodiae, orchid Rhizoma Gastrodiae (Classification system：Gastrodia elata Bl.) dry tuber, suppressing hyperactive liver for calming endogenous wind stops
Convulsion belongs to the Inflammation Zhijing medicine of medicine for calming liver and calming endopathic wind subordinate classification.
Chinese cassia tree, Classification system：Cinnamomum cassia Presl, for the dry bark of canella Chinese cassia tree, complement
Sun, warming spleen and stomach, removing internal cold, promoting blood circulation.
Poria cocos is the dry sclerotia of On Polyporaceae Poria cocos Poria cocos (Schw.) Wolf, for oedema oliguria,
Phlegm retention anti-dazzle nervous, spleen eating less, loose stool diarrhea, confused and worried, insomnia of palpitating with fear.
Santal is the heartwood of Santalaceae santal platymiscium santal Santalum album L. trunks.
Poplar Powder, specifically used white poplar (Classification system：Populus alba L) wood powder, 80 mesh of grain size.
Sunflower seed dregs powder, substance of the sunflower seeds after direct leaching squeezes grease, the sunflower seed dregs powder that the present invention uses
Meet the primary standard in GB/T 22463-2008,50 mesh of grain size.
- 3 butyl imidazole chlorine of 1- methyl, No. CAS：79917-90-1.
Butyl-pyridinium chlorine, No. CAS：1124-64-7.
Acetone, No. CAS：67-64-1.
Ethyl alcohol, No. CAS：64-17-5.
Glacial acetic acid, No. CAS：64-19-7.
Oleamide, No. CAS：301-02-0.
Vinyltrimethoxysilane, No. CAS：2768-02-7.
Isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, No. CAS：67691-13-8.
Potassium hydroxide, No. CAS：1310-58-3.
Glutaraldehyde, No. CAS：111-30-8.
Polyvinyl alcohol, average degree of polymerization 2400-2500, molecular weight 118000-124000.
Neopelex, No. CAS：25155-30-0.
Urea, No. CAS：57-13-6.
Guar gum, No. CAS：9000-30-0.
In following embodiments, used test method is as follows：
Burning time tests：Medicine prepared by Example is fragrant, lights, and the fragrant completely burned off spent time of record medicine repeats 5
It is secondary, it is averaged.
Flexural strength is tested：Regulation according to GB/T 18416-2009 is tested.
It is further illustrated the present invention below by the mode of embodiment, unless otherwise specified, used number is attached most importance to
Measure number.
Embodiment 1
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared：
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part
Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of Poplar Powders, 18 parts of water, 2 parts it is viscous
Ramming material.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows：Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis,
Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed
80 mesh sieves are put into after each raw material after crushing is mixed in mixer, at 45 DEG C, with 200 after input Poplar Powder, water, binding material
Rev/min rotating speed stir 30 minutes, obtain mixture, mixture be pressed into the perfume (or spice) of a diameter of 4.0mm, then disk is into a diameter of
12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 2
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared：
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part
Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts
Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows：Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed
In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C
30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed
Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is changed
The Poplar Powder of property；The ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 4 in mass ratio:1 mixture.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows：Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis,
Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed
80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C,
Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into
A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 3
It is substantially the same manner as Example 2, it differs only in, in the present embodiment 3, the preparation method of the Poplar Powder of the modification
It is as follows：It is put into after 25g Poplar Powders, 10mL ionic liquids are mixed in mixer, is 40 DEG C, with 300 revs/min of turn in temperature
Speed stirring 30 minutes, discharging, sealing are placed in the drying box that temperature is 70 DEG C 30 minutes, obtain mixture A, mixture A is added
Enter in 120g water, stirred 30 minutes at 30 DEG C, with 100 revs/min of rotating speed, cross 200 mesh sieves, by filtering gained precipitation 30g
After acetone, the washing of 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, modified Poplar Powder is obtained；The ionic liquid is -3 fourth of 1- methyl
Base imidazoles chlorine, butyl-pyridinium chlorine are 1 in mass ratio:1 mixture.
Embodiment 4
It is substantially the same manner as Example 2, it differs only in, in the present embodiment 4, the preparation method of the Poplar Powder of the modification
It is as follows：It is put into after 25g Poplar Powders, 10mL ionic liquids are mixed in mixer, is 40 DEG C, with 300 revs/min of turn in temperature
Speed stirring 30 minutes, discharging, sealing are placed in the drying box that temperature is 70 DEG C 30 minutes, obtain mixture A, mixture A is added
Enter in 120g water, stirred 30 minutes at 30 DEG C, with 100 revs/min of rotating speed, cross 200 mesh sieves, by filtering gained precipitation 30g
After acetone, the washing of 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, modified Poplar Powder is obtained；The ionic liquid is -3 fourth of 1- methyl
Base imidazoles chlorine, butyl-pyridinium chlorine are 1 in mass ratio:4 mixture.
Embodiment 5
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared：
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part
Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts
Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows：Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed
In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C
30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed
Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is mixed
Object B is closed, the pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, mixes
It closes uniformly, obtains mixed liquor C, put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, in temperature
It is stirred 50 minutes for 60 DEG C, with 300 revs/min of rotating speed, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder；Institute
State that ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4 mixture；The modifying agent I is
Oleamide.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows：Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis,
Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed
80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C,
Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into
A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 6
It is substantially the same manner as Example 5, it differs only in, in the present embodiment 6, the modifying agent I is vinyl trimethoxy
Base silane.
Embodiment 7
It is substantially the same manner as Example 5, it differs only in, in the present embodiment 7, (two is pungent for isopropyl three for the modifying agent I
Base pyrophosphoric acid acyloxy) titanate esters.
Comparative example 1
It is substantially the same manner as Example 5, it differs only in, in this comparative example 1, the preparation method of the Poplar Powder of the modification
It is as follows：The pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, obtains
Mixed liquor is uniformly sprayed at 25g Poplar Powders surface by mixed liquor, then put into mixer in, temperature for 60 DEG C, with 300 turns/
The rotating speed of minute stirs 50 minutes, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder；The modifying agent I is ethylene
Base trimethoxy silane.
Embodiment 8
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared：
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part
Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts
Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows：Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed
In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C
30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed
Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is mixed
Object B is closed, the pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, mixes
It closes uniformly, obtains mixed liquor C, put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, in temperature
It is stirred 50 minutes for 60 DEG C, with 300 revs/min of rotating speed, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder；Institute
State that ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4 mixture；The modifying agent I is
Vinyltrimethoxysilane.
The binding material is sunflower seed dregs adhesive.
The preparation method of the sunflower seed dregs adhesive is as follows：By 120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent
IIth, 8 parts of potassium hydroxide are uniformly mixed, and 55 DEG C are warming up to 2 DEG C/min of speed, are 55 DEG C, with 200 revs/min in temperature
When rotating speed stirring 3.5 is small, 30 DEG C are naturally cooled to, adds in 11.5 parts of glutaraldehydes, is stirred at 30 DEG C, with 250 revs/min of rotating speed
25 points of kinds, obtain sunflower seed dregs adhesive；The modifying agent II is polyvinyl alcohol.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows：Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis,
Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed
80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C,
Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into
A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 9
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 9, the preparation side of the sunflower seed dregs adhesive
Method is as follows：120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/min
Speed be warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C, add
Enter 11.5 parts of glutaraldehydes, stir 25 points of kinds at 30 DEG C, with 250 revs/min of rotating speed, obtain sunflower seed dregs adhesive；It is described to change
Property agent II be neopelex.
Embodiment 10
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 10, the preparation of the sunflower seed dregs adhesive
Method is as follows：120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/minute
The speed of clock is warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C,
11.5 parts of glutaraldehydes are added in, 25 points of kinds is stirred at 30 DEG C, with 250 revs/min of rotating speed, obtains sunflower seed dregs adhesive；It is described
Modifying agent II is urea.
Embodiment 11
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 11, the preparation of the sunflower seed dregs adhesive
Method is as follows：120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/minute
The speed of clock is warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C,
11.5 parts of glutaraldehydes are added in, 25 points of kinds is stirred at 30 DEG C, with 250 revs/min of rotating speed, obtains sunflower seed dregs adhesive；It is described
Modifying agent II is that polyvinyl alcohol, neopelex are 3 in mass ratio:2 mixture.
The fracture resistence force test result of the present embodiment 11 is 4.7N, when burning time is 10.4 small.
Test case 1
Medicine incense prescription science of the present invention, plays an important role of nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, with conditioning gynaecological disease,
It is with obvious effects, have no toxic side effect, it is easy to use.
Li Hong, 37 years old, hypogastralgia had leukorrhea, once repeatedly did flushing medicine-feeding, and had little effect, with external itch, waist
Tail pain later on the basis of normal developing medicine-feeding treatment, carries out auxiliary treatment using the medicine of the present invention is fragrant, descends tiffin daily
The fragrant disk of medicine of the present invention is fired, until the medicine perfume (or spice) after-flame treatment end of one day, after being used continuously 7 days, hypogastralgia mitigates, and leukorrhea is extensive
Multiple normal, external itch disappears, and waist tail feeling of pain disappears.
Test case 2
The medicine for the conditioning gynaecological disease that the present invention is processed is fragrant to carry out fracture resistence force test, and test result is shown in Table 1.
Table 1：Fracture resistence force test result table
| Fracture resistence force/N | |
| Embodiment 1 | 2.6 |
| Embodiment 2 | 2.8 |
| Embodiment 3 | 2.9 |
| Embodiment 4 | 3.2 |
| Embodiment 5 | 3.3 |
| Embodiment 6 | 3.6 |
| Embodiment 7 | 3.4 |
| Embodiment 8 | 4.1 |
| Embodiment 9 | 4.3 |
| Embodiment 10 | 3.9 |
| Comparative example 1 | 2.7 |
The medicine of the conditioning gynaecological disease of the present invention is fragrant to have good fracture resistance, is hardly damaged, and transports, stores conveniently.With
Embodiment 1 is compared, and embodiment 2-4 carries out the aggregate Poplar Powder of medicine perfume ion liquid modified processing, ion liquid modified rear poplar
Fibre length, toughness, the surface roughness of wood powder change, and the medicine perfume (or spice) flexural strength for preparing improves.Embodiment 5-7
Surface modification further is carried out to ion liquid modified Poplar Powder, respectively using oleamide, vinyltrimethoxysilane,
(dioctylphyrophosphoric acid acyloxy) titanate esters of isopropyl three are as modifying agent, Poplar Powder functionalisation of surfaces after modification, with gluing
The combination power of ramming material is improved.Using new sunflower seed dregs adhesive, sunflower seeds gluing when embodiment 8-10 prepares medicine perfume (or spice)
Containing substantial amounts of protein in agent, the strand of protein is fully extended by carrying out surface modification to protein, is reused
Crosslinking agent is crosslinked, and obtains high viscosity adhesive, the fragrant anti-folding of the medicine processed using sunflower seeds adhesive as binding material
Ability further improves.
Test case 3
The fragrant progress burning time test of medicine to the conditioning gynaecological disease that the present invention processes.Test result is shown in Table 2.
Table 2：Burning time test result table
| Burning time/h | |
| Embodiment 1 | 7.6 |
| Embodiment 4 | 8.3 |
| Embodiment 6 | 9.0 |
| Embodiment 8 | 9.4 |
| Embodiment 9 | 9.5 |
| Embodiment 10 | 9.2 |
| Comparative example 1 | 7.9 |
The medicine of the present invention fragrant burning time is long, and duration of efficacy is long.It was found that compared with embodiment 1-6, embodiment 8-10
Using sunflower seeds adhesive as binding material, medicine perfume (or spice) structure is improved, and burning time extends.
The preferred embodiment of the present invention described in detail above.It should be appreciated that those of ordinary skill in the art without
Creative work is needed according to the present invention can to conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.
Claims (10)
1. a kind of medicine for nursing one's health gynaecological disease is fragrant, which is characterized in that the raw material including following parts by weight is prepared：
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of Eclipta prostratas, 1-3
Part rhizoma cyperi, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5
Part santal, 3-9 parts of Poplar Powders, 10-30 parts of water, 2-6 parts of binding materials.
2. a kind of medicine for nursing one's health gynaecological disease is fragrant, which is characterized in that the raw material including following parts by weight is prepared：
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of Eclipta prostratas, 1-3
Part rhizoma cyperi, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5
Part santal, Poplar Powder, 10-30 parts of water, the 2-6 parts of binding materials of 3-9 parts of modifications.
3. the medicine of conditioning gynaecological disease according to claim 2 is fragrant, which is characterized in that the preparation side of the Poplar Powder of the modification
Method includes：Will 25-75g Poplar Powders, 10-40mL ionic liquids mix after put into mixer in, temperature for 40-45 DEG C, with
200-400 revs/min of rotating speed stirs 30-50 minutes, and discharging, sealing are placed in 30-60 in the drying box that temperature is 70-85 DEG C
Minute, mixture A is obtained, mixture A is added in 120-250g water, is stirred at 30-45 DEG C, with 100-300 revs/min of rotating speed
It mixes 30-60 minutes, filters, after filtering gained precipitation is washed with 30-60g acetone, 45-90g ethyl alcohol, in 40-55 DEG C of dry 12-
24 it is small when, obtain modified Poplar Powder；The ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is in mass ratio
(1-4)：The mixture of (1-4).
4. the medicine of the conditioning gynaecological disease according to Claims 2 or 3 is fragrant, which is characterized in that the system of the Poplar Powder of the modification
Preparation Method includes：Will 25-75g Poplar Powders, 10-40mL ionic liquids mix after put into mixer in, temperature for 40-45 DEG C,
It is stirred 30-50 minutes with 200-400 revs/min of rotating speed, discharging, sealing are placed in 30- in the drying box that temperature is 70-85 DEG C
60 minutes, mixture A is obtained, mixture A is added in 120-250g water, at 30-45 DEG C, with 100-300 revs/min of rotating speed
Stirring 30-60 minutes, filtering, after filtering gained precipitation is washed with 30-60g acetone, 45-90g ethyl alcohol, in 40-55 DEG C of drying
When 12-24 is small, obtain mixture B, with glacial acetic acid by the pH for the ethanol water that 15-45g mass fractions are 85-95% adjust to
3-4 adds in 0.85-1.7g modifying agent I, is uniformly mixed, obtains mixed liquor C, uniformly sprays whole mix to mixture B surface
It is put into after closing liquid C in mixer, is 60-75 DEG C, is stirred 50-100 minutes with 300-500 revs/min of rotating speed in temperature, go out
Material when 40-60 DEG C of dry 24-48 is small, obtains modified Poplar Powder；The ionic liquid for -3 butyl imidazole chlorine of 1- methyl,
Butyl-pyridinium chlorine is (1-4) in mass ratio：The mixture of (1-4)；The modifying agent I is oleamide, vinyl trimethoxy
One or more mixture in silane, isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters.
5. the medicine of conditioning gynaecological disease according to claim 1 or 2 is fragrant, which is characterized in that the binding material is sunflower seed dregs
One or more mixtures in adhesive, guar gum, carragheen.
6. the medicine of conditioning gynaecological disease according to claim 5 is fragrant, which is characterized in that the preparation of the sunflower seed dregs adhesive
Method includes：120-240 parts of sunflower seed dregs powder, 200-400 parts of water, 12-18 parts of modifying agent II, 8-12 parts of potassium hydroxide are mixed
Uniformly, be warming up to 55-75 DEG C, temperature be 55-75 DEG C, that 3.5-7 is stirred with 200-300 revs/min of rotating speed is small when, it is naturally cold
But to 30-45 DEG C, 11.5-23 parts of glutaraldehydes are added in, at 30-45 DEG C, with 250-400 revs/min of 25-45 points of rotating speed stirring
Kind, obtain sunflower seed dregs adhesive；The modifying agent II for polyvinyl alcohol, neopelex, one kind in urea or
A variety of mixtures.
7. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 1, which is characterized in that including weighing by weight
Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal
Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer,
It stirs 30-90 minutes, is mixed at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into Poplar Powder, water, binding material
Material obtains finished medicines perfume after mixture compression moulding, drying.
8. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 2, which is characterized in that including weighing by weight
Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal
Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer,
It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into modified Poplar Powder, water, binding material
To mixture, finished medicines perfume is obtained after mixture compression moulding, drying.
9. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 8, which is characterized in that including weighing by weight
Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal
Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer,
It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into modified Poplar Powder, water, binding material
To mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm, then disk into a diameter of 12-15cm, weight be 25-30g's
Plate-like is fragrant, and finished medicines perfume is obtained after dry at 45-55 DEG C.
10. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to any one of claim 7-9, which is characterized in that finished product
The moisture content of medicine perfume is 10-12%.
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