CN108096473A - Nurse one's health the medicine perfume and its processing technology of gynaecological disease - Google Patents

Nurse one's health the medicine perfume and its processing technology of gynaecological disease Download PDF

Info

Publication number
CN108096473A
CN108096473A CN201711382846.6A CN201711382846A CN108096473A CN 108096473 A CN108096473 A CN 108096473A CN 201711382846 A CN201711382846 A CN 201711382846A CN 108096473 A CN108096473 A CN 108096473A
Authority
CN
China
Prior art keywords
parts
mixture
medicine
radix
perfume
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201711382846.6A
Other languages
Chinese (zh)
Other versions
CN108096473B (en
Inventor
阮小军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIAXING SOFTTER BIOTECHNOLOGY Co.,Ltd.
Original Assignee
阮小军
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 阮小军 filed Critical 阮小军
Priority to CN201711382846.6A priority Critical patent/CN108096473B/en
Publication of CN108096473A publication Critical patent/CN108096473A/en
Application granted granted Critical
Publication of CN108096473B publication Critical patent/CN108096473B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/533Leonurus (motherwort)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/06Fungi, e.g. yeasts
    • A61K36/07Basidiomycota, e.g. Cryptococcus
    • A61K36/076Poria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/23Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/232Angelica
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/23Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/236Ligusticum (licorice-root)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/284Atractylodes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/481Astragalus (milkvetch)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/537Salvia (sage)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/54Lauraceae (Laurel family), e.g. cinnamon or sassafras
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/65Paeoniaceae (Peony family), e.g. Chinese peony
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/71Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/76Salicaceae (Willow family), e.g. poplar
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/89Cyperaceae (Sedge family)
    • A61K36/8905Cyperus (flatsedge)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/898Orchidaceae (Orchid family)
    • A61K36/8988Gastrodia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/46Ingredients of undetermined constitution or reaction products thereof, e.g. skin, bone, milk, cotton fibre, eggshell, oxgall or plant extracts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0087Galenical forms not covered by A61K9/02 - A61K9/7023

Landscapes

  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Gastroenterology & Hepatology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of medicine perfume for nursing one's health gynaecological disease, are prepared including following raw material:Motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal, Poplar Powder, water, binding material.The medicine of the conditioning gynaecological disease of the present invention is fragrant, can be directly entered lesion according to theoretical make of modern drug matching, play an important role of nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, good to difficult and complicated gynopathy conditioning effect, has no toxic side effect, environmentally protective, easy to use.

Description

Nurse one's health the medicine perfume and its processing technology of gynaecological disease
Technical field
The present invention relates to a kind of medicine that can nurse one's health gynaecological disease is fragrant.
Background technology
The raw material of traditional medicine perfume is generally made of incense drug, wood powder, binding material and additivity material.Wherein, incense drug includes day Right fragrance and some Chinese medicines.Perfume (or spice) on the market is broadly divided into reading partner perfume now, drives epidemic disease incense for eliminating plague, and purification air is fragrant with adjusting blood Health care perfume (or spice) of pressure etc..At present, there is no the medicine that can nurse one's health gynecological disease is fragrant.
Culture of TCM is the rarity in China, with a long history with Chinese medicine treatment gynecological disease.Difficult and complicated cases of gynaecology and chronic Disease, it can influence the normal life of people, but cannot effect a radical cure quickly.Traditional Chinese medical herbal treatment gynaecological disease is started with from Overall View, Dispersing stagnated hepatoqi is strengthened the body resistance to consolidate the constitution, promoting blood circulation and removing blood stasis, and softening and resolving hard mass is clearing heat and detoxicating, and adjusting endocrine comprehensively makes gas lead to blood work, enlivens dirty Internal organs, channels and collaterals are this, and qi and blood is uses, and qi and blood is the material base of human body, and internal organs are source of generating QI and blood, play the life for being in charge of blood Into, have under one's command and run, it is the motive power of blood to adjust blood and balanced action, gas.Blood is the material base of menstruation, if internal organs work( It can lack of proper care, qi and blood circulation will be affected, involve sea of blood function, then can cause the generation of various gynaecological diseases, such as ovarian cyst Deng.Chinese traditional treatment can exempt the psychological pressure and mental burden that operation is brought to patient, adjust endocrine, strengthen immunity etc., Medication is convenient, does not operate on, does not hinder vigour, painful risk is small, and expense is low, markedly fast.Medicine perfume is made in Chinese medicine, is reduced The toxic side effect that oral traditional Chinese medicine is brought is also convenient for being commonly used in daily life, not only plays therapeutic effect, moreover it is possible to play net Change air, the effect of health care.
Incense drug and wood powder in usual medicine perfume (or spice) is generally powdered, relatively dissipates, it is not easy to strike up partnership, so also needing to add The material that some is added to play adhesive effect.Existing medicine perfume (or spice) product also has the chemical classes binding material used, not only reduces medicine perfume Quality, and the substance unfavorable to human body can be also generated in medicine perfume (or spice) combustion process.The medicine incense prescription of the present invention is scientific and reasonable, adjusts Women qi-blood circulating is managed, there is good conditioning effect to difficult and complicated cases gynaecological disease.The present invention has no toxic side effect to medicine perfume (or spice), does not add Add chemical adhesive, it is environmentally protective.
The content of the invention
The present invention provides a kind of medicine perfume for nursing one's health gynaecological disease and its processing technologys.The present invention adopts the following technical scheme that:
A kind of medicine for nursing one's health gynaecological disease is fragrant, and the raw material including following parts by weight is prepared:
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of non-irrigated lotuses Grass, 1-3 portions of rhizoma cyperis, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5 portions of santals, 3-9 parts of Poplar Powders, 10-30 parts of water, 2-6 parts of binding materials.
The present invention provides the processing technology of the medicine perfume of above-mentioned conditioning gynaecological disease:Including weighing each raw material by weight, by benefit Brittle Falsepimpernel Herb, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal are respectively in 45-65 When DEG C dry 6-12 is small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input Poplar Powder, It is stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after water, binding material, mixture is obtained, by mixture Finished medicines perfume is obtained after compression moulding, drying.
Preferably, the present invention provides the processing technology of the medicine perfume of above-mentioned conditioning gynaecological disease:Including weighing each original by weight Material distinguishes motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal When 45-65 DEG C of dry 6-12 is small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input It is stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after Poplar Powder, water, binding material, obtains mixture, it will Mixture is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm, then disk is fragrant into a diameter of 12-15cm, plate-like that weight is 25-30g, Finished medicines perfume is obtained after 45-55 DEG C of drying, the moisture content of finished medicines perfume is 10-12%.
A kind of medicine for nursing one's health gynaecological disease is fragrant, and the raw material including following parts by weight is prepared:
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of non-irrigated lotuses Grass, 1-3 portions of rhizoma cyperis, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5 portions of santals, Poplar Powder, 10-30 parts of water, the 2-6 parts of binding materials of 3-9 parts of modifications.
The present invention also provides the processing technologys of the medicine perfume of above-mentioned conditioning gynaecological disease:It, will including weighing each raw material by weight Motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal are respectively in 45- When 65 DEG C of dry 6-12 are small, 50-80 mesh sieves are crushed, are put into after each raw material after crushing is mixed in mixer, input is modified Poplar Powder, water, stirred 30-90 minutes at 45-65 DEG C, with 200-400 revs/min of rotating speed after binding material, obtain mixture, Finished medicines perfume will be obtained after mixture compression moulding, drying.
Preferably, the present invention also provides above-mentioned conditioning gynaecological disease medicine perfume processing technology:It is each including weighing by weight Raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal point Not when 45-65 DEG C of dry 6-12 is small, 50-80 mesh sieves are crushed, puts into mixer, throws after each raw material after crushing is mixed It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after entering modified Poplar Powder, water, binding material Mixture, is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm by mixture, then disk is into a diameter of 12-15cm, the disk that weight is 25-30g Shape is fragrant, finished medicines perfume is obtained after dry at 45-55 DEG C, the moisture content of finished medicines perfume is 10-12%.
Preferably, the preparation method of the Poplar Powder of the modification includes mixing 25-75g Poplar Powders, 10-40mL ionic liquids It is put into after conjunction in mixer, is 40-45 DEG C, is stirred 30-50 minutes with 200-400 revs/min of rotating speed in temperature, discharge, is close Envelope, is placed in the drying box that temperature is 70-85 DEG C 30-60 minutes, obtains mixture A, and mixture A is added in 120-250g water In, it is stirred 30-60 minutes at 30-45 DEG C, with 100-300 revs/min of rotating speed, filtering, by filtering gained precipitation 30-60g After acetone, the washing of 45-90g ethyl alcohol, when 40-55 DEG C of dry 12-24 is small, modified Poplar Powder is obtained;The ionic liquid is - 3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine are (1-4) in mass ratio:The mixture of (1-4).
It is further preferred that the preparation method of the Poplar Powder of the modification is included 25-75g Poplar Powders, 10-40mL ions It is put into after liquid mixing in mixer, is 40-45 DEG C, is stirred 30-50 minutes with 200-400 revs/min of rotating speed in temperature, go out Material, sealing, are placed in the drying box that temperature is 70-85 DEG C 30-60 minutes, obtain mixture A, and mixture A is added in 120- It in 250g water, is stirred 30-60 minutes at 30-45 DEG C, with 100-300 revs/min of rotating speed, filtering, filtering gained precipitation is used After 30-60g acetone, the washing of 45-90g ethyl alcohol, when 40-55 DEG C of dry 12-24 is small, mixture B is obtained, with glacial acetic acid by 15- 45g mass fractions are that the pH of the ethanol water of 85-95% is adjusted to 3-4, add in 0.85-1.7g modifying agent I, are uniformly mixed, Mixed liquor C is obtained, is put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, is 60-75 in temperature DEG C, stirred 50-100 minute with 300-500 revs/min of rotating speed, discharge, when 40-60 DEG C of dry 24-48 is small, be modified Poplar Powder;The ionic liquid is that -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine are (1-4) in mass ratio:(1-4's) is mixed Close object;The modifying agent I is oleamide, vinyltrimethoxysilane, isopropyl three (dioctylphyrophosphoric acid acyloxy) titanium One or more mixture in acid esters.
It is further preferred that the ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4 Mixture.
It is further preferred that the modifying agent I is vinyltrimethoxysilane.
Preferably, the binding material is mixing one or more in sunflower seed dregs adhesive, guar gum, carragheen Object.
It is further preferred that the binding material is sunflower seed dregs adhesive, the preparation method of the sunflower seed dregs adhesive Including 120-240 parts of sunflower seed dregs powder, 200-400 parts of water, 12-18 parts of modifying agent II, 8-12 parts of potassium hydroxide are uniformly mixed, Be warming up to 55-75 DEG C, temperature be 55-75 DEG C, that 3.5-7 is stirred with 200-300 revs/min of rotating speed is small when, naturally cool to 30-45 DEG C, 11.5-23 parts of glutaraldehydes are added in, divides kind at 30-45 DEG C, with 250-400 revs/min of rotating speed stirring 25-45, obtains To sunflower seed dregs adhesive;The modifying agent II is one or more in polyvinyl alcohol, neopelex, urea Mixture.
It is further preferred that it is (3-5) in mass ratio that the modifying agent II, which is polyvinyl alcohol, neopelex,: The mixture of (1-2).
It is further preferred that it is 3 in mass ratio that the modifying agent II, which is polyvinyl alcohol, neopelex,:2 it is mixed Close object.
The medicine of the conditioning gynaecological disease of the present invention is fragrant, can be directly entered lesion according to theoretical make of modern drug matching, have There are nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, it is good to difficult and complicated gynopathy conditioning effect, it has no toxic side effect, green ring It protects, it is easy to use.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be each preferably to get the present invention in any combination Embodiment.
Specific embodiment
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality It applies among a scope.The experimental method of actual conditions is not specified in the following example, according to conventional methods and conditions or according to business Product specification selects.
In following embodiments, primary raw material and instrument used are as follows:
Motherwort, Classification system:Leonurus artemisia (Laur.) S.Y.Hu F have inducing diuresis to remove edema, shrink uterus The effect of effect, is the key medicine that ancient Chinese medicine doctor is used for treating gynaecological disease, and the present invention dries herb using the ground of motherwort.
Radix Salviae Miltiorrhizae, the dry root of labiate Radix Salviae Miltiorrhizae Salvia miltiorrhiza Bge. have promoting blood circulation, promoting menstruation The effect of analgesic, relieving restlessness that clears away heart-fire, cool blood to disappear carbuncle.
Radix Angelicae Sinensis, be umbelliferae angelica Angelica sinensis (Oliv.) Diels dry root, have enrich blood and Blood, menstruction regulating and pain relieving, the effect of moisturize laxation, anticancer.
Rhizome of chuanxiong is the dry rhizome of samphire Rhizoma Chuanxiong Ligusticum chuanxiong Hort., acrid in flavour and warm in nature.Return Liver, courage, pericardium channel, blood-activating and qi-promoting, wind-expelling pain-stopping.
Radix Astragali, specifically used astragalus mongolicus (Classification system:Astragalus membranaceus(Fish) Bungevar.Mongholicus (Bunge) Hsiao) dry root, control shortness of breath and palpitation, weak, collapse, spontaneous perspiration, night sweat, physically weak Edema, chronic nephritis, chronic diarrhea, rectal prolapse, the prolapse of uterus, ulcer is difficult to burst, the long disunion of the open sore part.
Eclipta prostrata is catananche's Eclipta prostrata (Classification system:Eclipta prostrata) ground drying herb, Have effects that tonify the liver and kidney, blood-stanching and blood-cooling.
Rhizoma cyperi, Classification system:Cyperus rotundus L. are the dry rhizome of sedge nutgrass flatsedge, for liver depression The stagnation of the circulation of vital energy, distending pain in the chest and hypochondrium, hernia pain, swollen breasts, the taste stagnation of the circulation of vital energy, gastral cavity abdomen ruffian is bored, turgor pain, irregular menstruation, closed dysmenorrhea.
Rhizoma Atractylodis Macrocephalae, the dry rhizome of feverfew Rhizoma Atractylodis Macrocephalae Atractylodes macrocephala Koidz. have invigorating the spleen The effect of QI invigorating, eliminate dampness and have diuretic effect, hidroschesis, tocolysis, for spleen eating less, abdominal distention diarrhea, phlegm retention anti-dazzle nervous, oedema, spontaneous perspiration, movement of the foetus is not Peace.
Radix Paeoniae Alba, Classification system:Cynanchum otophyllum, Ranunculaceae Radix Paeoniae Alba platymiscium are cohosh Chinese herbaceous peonies Dry root, smooth liver and relieve pain, nourishing blood for regulating menstruation, astringing YIN to stop sweating.For dizziness of having a headache, hypochondriac pain, abdominal pain, four limbs contraction pain, blood deficiency chlorosis, Irregular menstruation.
Rhizoma Gastrodiae, orchid Rhizoma Gastrodiae (Classification system:Gastrodia elata Bl.) dry tuber, suppressing hyperactive liver for calming endogenous wind stops Convulsion belongs to the Inflammation Zhijing medicine of medicine for calming liver and calming endopathic wind subordinate classification.
Chinese cassia tree, Classification system:Cinnamomum cassia Presl, for the dry bark of canella Chinese cassia tree, complement Sun, warming spleen and stomach, removing internal cold, promoting blood circulation.
Poria cocos is the dry sclerotia of On Polyporaceae Poria cocos Poria cocos (Schw.) Wolf, for oedema oliguria, Phlegm retention anti-dazzle nervous, spleen eating less, loose stool diarrhea, confused and worried, insomnia of palpitating with fear.
Santal is the heartwood of Santalaceae santal platymiscium santal Santalum album L. trunks.
Poplar Powder, specifically used white poplar (Classification system:Populus alba L) wood powder, 80 mesh of grain size.
Sunflower seed dregs powder, substance of the sunflower seeds after direct leaching squeezes grease, the sunflower seed dregs powder that the present invention uses Meet the primary standard in GB/T 22463-2008,50 mesh of grain size.
- 3 butyl imidazole chlorine of 1- methyl, No. CAS:79917-90-1.
Butyl-pyridinium chlorine, No. CAS:1124-64-7.
Acetone, No. CAS:67-64-1.
Ethyl alcohol, No. CAS:64-17-5.
Glacial acetic acid, No. CAS:64-19-7.
Oleamide, No. CAS:301-02-0.
Vinyltrimethoxysilane, No. CAS:2768-02-7.
Isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, No. CAS:67691-13-8.
Potassium hydroxide, No. CAS:1310-58-3.
Glutaraldehyde, No. CAS:111-30-8.
Polyvinyl alcohol, average degree of polymerization 2400-2500, molecular weight 118000-124000.
Neopelex, No. CAS:25155-30-0.
Urea, No. CAS:57-13-6.
Guar gum, No. CAS:9000-30-0.
In following embodiments, used test method is as follows:
Burning time tests:Medicine prepared by Example is fragrant, lights, and the fragrant completely burned off spent time of record medicine repeats 5 It is secondary, it is averaged.
Flexural strength is tested:Regulation according to GB/T 18416-2009 is tested.
It is further illustrated the present invention below by the mode of embodiment, unless otherwise specified, used number is attached most importance to Measure number.
Embodiment 1
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared:
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of Poplar Powders, 18 parts of water, 2 parts it is viscous Ramming material.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows:Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed 80 mesh sieves are put into after each raw material after crushing is mixed in mixer, at 45 DEG C, with 200 after input Poplar Powder, water, binding material Rev/min rotating speed stir 30 minutes, obtain mixture, mixture be pressed into the perfume (or spice) of a diameter of 4.0mm, then disk is into a diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 2
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared:
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows:Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C 30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is changed The Poplar Powder of property;The ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 4 in mass ratio:1 mixture.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows:Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed 80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C, Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 3
It is substantially the same manner as Example 2, it differs only in, in the present embodiment 3, the preparation method of the Poplar Powder of the modification It is as follows:It is put into after 25g Poplar Powders, 10mL ionic liquids are mixed in mixer, is 40 DEG C, with 300 revs/min of turn in temperature Speed stirring 30 minutes, discharging, sealing are placed in the drying box that temperature is 70 DEG C 30 minutes, obtain mixture A, mixture A is added Enter in 120g water, stirred 30 minutes at 30 DEG C, with 100 revs/min of rotating speed, cross 200 mesh sieves, by filtering gained precipitation 30g After acetone, the washing of 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, modified Poplar Powder is obtained;The ionic liquid is -3 fourth of 1- methyl Base imidazoles chlorine, butyl-pyridinium chlorine are 1 in mass ratio:1 mixture.
Embodiment 4
It is substantially the same manner as Example 2, it differs only in, in the present embodiment 4, the preparation method of the Poplar Powder of the modification It is as follows:It is put into after 25g Poplar Powders, 10mL ionic liquids are mixed in mixer, is 40 DEG C, with 300 revs/min of turn in temperature Speed stirring 30 minutes, discharging, sealing are placed in the drying box that temperature is 70 DEG C 30 minutes, obtain mixture A, mixture A is added Enter in 120g water, stirred 30 minutes at 30 DEG C, with 100 revs/min of rotating speed, cross 200 mesh sieves, by filtering gained precipitation 30g After acetone, the washing of 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, modified Poplar Powder is obtained;The ionic liquid is -3 fourth of 1- methyl Base imidazoles chlorine, butyl-pyridinium chlorine are 1 in mass ratio:4 mixture.
Embodiment 5
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared:
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows:Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C 30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is mixed Object B is closed, the pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, mixes It closes uniformly, obtains mixed liquor C, put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, in temperature It is stirred 50 minutes for 60 DEG C, with 300 revs/min of rotating speed, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder;Institute State that ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4 mixture;The modifying agent I is Oleamide.
The binding material is guar gum.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows:Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed 80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C, Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 6
It is substantially the same manner as Example 5, it differs only in, in the present embodiment 6, the modifying agent I is vinyl trimethoxy Base silane.
Embodiment 7
It is substantially the same manner as Example 5, it differs only in, in the present embodiment 7, (two is pungent for isopropyl three for the modifying agent I Base pyrophosphoric acid acyloxy) titanate esters.
Comparative example 1
It is substantially the same manner as Example 5, it differs only in, in this comparative example 1, the preparation method of the Poplar Powder of the modification It is as follows:The pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, obtains Mixed liquor is uniformly sprayed at 25g Poplar Powders surface by mixed liquor, then put into mixer in, temperature for 60 DEG C, with 300 turns/ The rotating speed of minute stirs 50 minutes, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder;The modifying agent I is ethylene Base trimethoxy silane.
Embodiment 8
The medicine perfume of gynaecological disease is nursed one's health, the raw material including following parts by weight is prepared:
2.5 portions of motherworts, 3 parts of Radix Salviae Miltiorrhizaes, 2 parts of Radix Angelicae Sinensis, 1.5 parts of rhizome of chuanxiongs, 2 parts of Radix Astragalis, 0.5 portion of Eclipta prostrata, 1 portion of rhizoma cyperi, 1 part Rhizoma Atractylodis Macrocephalae, 1.5 portions of Radix Paeoniae Albas, 0.3 part of Rhizoma Gastrodiae, 0.2 portion of Chinese cassia tree, 1.5 parts of Poria cocos, 0.5 portion of santal, 3 parts of modified Poplar Powders, 18 parts Water, 2 parts of binding materials.
The preparation method of the Poplar Powder of the modification is as follows:Stirring is put into after 25g Poplar Powders, 10mL ionic liquids are mixed In machine, it is 40 DEG C, stirred 30 minutes with 300 revs/min of rotating speed in temperature, discharging, sealing is placed in the drying that temperature is 70 DEG C 30 minutes in case, mixture A is obtained, mixture A is added in 120g water, 30 are stirred at 30 DEG C, with 100 revs/min of rotating speed Minute crosses 200 mesh sieves, filtering gained is precipitated after being washed with 30g acetone, 45g ethyl alcohol, when 40 DEG C of dryings 12 are small, is mixed Object B is closed, the pH for the ethanol water that 15g mass fractions are 95% is adjusted to 3 with glacial acetic acid, 0.85g modifying agent I is added in, mixes It closes uniformly, obtains mixed liquor C, put into after whole mixed liquor C is uniformly sprayed to mixture B surface in mixer, in temperature It is stirred 50 minutes for 60 DEG C, with 300 revs/min of rotating speed, discharging, when 40 DEG C of dryings 24 are small, obtains modified Poplar Powder;Institute State that ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is 1 in mass ratio:4 mixture;The modifying agent I is Vinyltrimethoxysilane.
The binding material is sunflower seed dregs adhesive.
The preparation method of the sunflower seed dregs adhesive is as follows:By 120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent IIth, 8 parts of potassium hydroxide are uniformly mixed, and 55 DEG C are warming up to 2 DEG C/min of speed, are 55 DEG C, with 200 revs/min in temperature When rotating speed stirring 3.5 is small, 30 DEG C are naturally cooled to, adds in 11.5 parts of glutaraldehydes, is stirred at 30 DEG C, with 250 revs/min of rotating speed 25 points of kinds, obtain sunflower seed dregs adhesive;The modifying agent II is polyvinyl alcohol.
The processing technology for nursing one's health the medicine perfume of gynaecological disease is as follows:Weigh each raw material by weight, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal respectively 45 DEG C it is dry 6 it is small when, crushed 80 mesh sieves, will each raw material after crushing mix after put into mixer, put into after modified Poplar Powder, water, binding material 45 DEG C, Stirred 30 minutes with 200 revs/min of rotating speed, obtain mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0mm, then disk into A diameter of 12cm, the plate-like that weight is 25g are fragrant, finished medicines perfume are obtained after dry at 45 DEG C, the moisture content of finished medicines perfume is 10%.
Embodiment 9
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 9, the preparation side of the sunflower seed dregs adhesive Method is as follows:120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/min Speed be warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C, add Enter 11.5 parts of glutaraldehydes, stir 25 points of kinds at 30 DEG C, with 250 revs/min of rotating speed, obtain sunflower seed dregs adhesive;It is described to change Property agent II be neopelex.
Embodiment 10
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 10, the preparation of the sunflower seed dregs adhesive Method is as follows:120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/minute The speed of clock is warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C, 11.5 parts of glutaraldehydes are added in, 25 points of kinds is stirred at 30 DEG C, with 250 revs/min of rotating speed, obtains sunflower seed dregs adhesive;It is described Modifying agent II is urea.
Embodiment 11
It is substantially the same manner as Example 8, it differs only in, in the present embodiment 11, the preparation of the sunflower seed dregs adhesive Method is as follows:120 parts of sunflower seed dregs powder, 200 parts of water, 12 parts of modifying agent, II, 8 part of potassium hydroxide are uniformly mixed, with 2 DEG C/minute The speed of clock is warming up to 55 DEG C, temperature be 55 DEG C, it is small with 200 revs/min of rotating speed stirring 3.5 when, naturally cool to 30 DEG C, 11.5 parts of glutaraldehydes are added in, 25 points of kinds is stirred at 30 DEG C, with 250 revs/min of rotating speed, obtains sunflower seed dregs adhesive;It is described Modifying agent II is that polyvinyl alcohol, neopelex are 3 in mass ratio:2 mixture.
The fracture resistence force test result of the present embodiment 11 is 4.7N, when burning time is 10.4 small.
Test case 1
Medicine incense prescription science of the present invention, plays an important role of nourishing qi and blood, promoting blood circulation for regulating menstruation, removing blood stasis and analgesics, with conditioning gynaecological disease, It is with obvious effects, have no toxic side effect, it is easy to use.
Li Hong, 37 years old, hypogastralgia had leukorrhea, once repeatedly did flushing medicine-feeding, and had little effect, with external itch, waist Tail pain later on the basis of normal developing medicine-feeding treatment, carries out auxiliary treatment using the medicine of the present invention is fragrant, descends tiffin daily The fragrant disk of medicine of the present invention is fired, until the medicine perfume (or spice) after-flame treatment end of one day, after being used continuously 7 days, hypogastralgia mitigates, and leukorrhea is extensive Multiple normal, external itch disappears, and waist tail feeling of pain disappears.
Test case 2
The medicine for the conditioning gynaecological disease that the present invention is processed is fragrant to carry out fracture resistence force test, and test result is shown in Table 1.
Table 1:Fracture resistence force test result table
Fracture resistence force/N
Embodiment 1 2.6
Embodiment 2 2.8
Embodiment 3 2.9
Embodiment 4 3.2
Embodiment 5 3.3
Embodiment 6 3.6
Embodiment 7 3.4
Embodiment 8 4.1
Embodiment 9 4.3
Embodiment 10 3.9
Comparative example 1 2.7
The medicine of the conditioning gynaecological disease of the present invention is fragrant to have good fracture resistance, is hardly damaged, and transports, stores conveniently.With Embodiment 1 is compared, and embodiment 2-4 carries out the aggregate Poplar Powder of medicine perfume ion liquid modified processing, ion liquid modified rear poplar Fibre length, toughness, the surface roughness of wood powder change, and the medicine perfume (or spice) flexural strength for preparing improves.Embodiment 5-7 Surface modification further is carried out to ion liquid modified Poplar Powder, respectively using oleamide, vinyltrimethoxysilane, (dioctylphyrophosphoric acid acyloxy) titanate esters of isopropyl three are as modifying agent, Poplar Powder functionalisation of surfaces after modification, with gluing The combination power of ramming material is improved.Using new sunflower seed dregs adhesive, sunflower seeds gluing when embodiment 8-10 prepares medicine perfume (or spice) Containing substantial amounts of protein in agent, the strand of protein is fully extended by carrying out surface modification to protein, is reused Crosslinking agent is crosslinked, and obtains high viscosity adhesive, the fragrant anti-folding of the medicine processed using sunflower seeds adhesive as binding material Ability further improves.
Test case 3
The fragrant progress burning time test of medicine to the conditioning gynaecological disease that the present invention processes.Test result is shown in Table 2.
Table 2:Burning time test result table
Burning time/h
Embodiment 1 7.6
Embodiment 4 8.3
Embodiment 6 9.0
Embodiment 8 9.4
Embodiment 9 9.5
Embodiment 10 9.2
Comparative example 1 7.9
The medicine of the present invention fragrant burning time is long, and duration of efficacy is long.It was found that compared with embodiment 1-6, embodiment 8-10 Using sunflower seeds adhesive as binding material, medicine perfume (or spice) structure is improved, and burning time extends.
The preferred embodiment of the present invention described in detail above.It should be appreciated that those of ordinary skill in the art without Creative work is needed according to the present invention can to conceive and makes many modifications and variations.Therefore, all technologies in the art Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea Technical solution, all should be in the protection domain being defined in the patent claims.

Claims (10)

1. a kind of medicine for nursing one's health gynaecological disease is fragrant, which is characterized in that the raw material including following parts by weight is prepared:
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of Eclipta prostratas, 1-3 Part rhizoma cyperi, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5 Part santal, 3-9 parts of Poplar Powders, 10-30 parts of water, 2-6 parts of binding materials.
2. a kind of medicine for nursing one's health gynaecological disease is fragrant, which is characterized in that the raw material including following parts by weight is prepared:
2.5-5 portions of motherworts, 3-6 parts of Radix Salviae Miltiorrhizaes, 2-4 parts of Radix Angelicae Sinensis, 1.5-3 parts of rhizome of chuanxiongs, 2-4 parts of Radix Astragalis, 0.5-1 parts of Eclipta prostratas, 1-3 Part rhizoma cyperi, 1-3 parts of Rhizoma Atractylodis Macrocephalaes, 1.5-4.5 portions of Radix Paeoniae Albas, 0.3-1 parts of Rhizoma Gastrodiaes, 0.2-0.6 portions of Chinese cassia trees, 1.5-3 parts of Poria cocos, 0.5-1.5 Part santal, Poplar Powder, 10-30 parts of water, the 2-6 parts of binding materials of 3-9 parts of modifications.
3. the medicine of conditioning gynaecological disease according to claim 2 is fragrant, which is characterized in that the preparation side of the Poplar Powder of the modification Method includes:Will 25-75g Poplar Powders, 10-40mL ionic liquids mix after put into mixer in, temperature for 40-45 DEG C, with 200-400 revs/min of rotating speed stirs 30-50 minutes, and discharging, sealing are placed in 30-60 in the drying box that temperature is 70-85 DEG C Minute, mixture A is obtained, mixture A is added in 120-250g water, is stirred at 30-45 DEG C, with 100-300 revs/min of rotating speed It mixes 30-60 minutes, filters, after filtering gained precipitation is washed with 30-60g acetone, 45-90g ethyl alcohol, in 40-55 DEG C of dry 12- 24 it is small when, obtain modified Poplar Powder;The ionic liquid is -3 butyl imidazole chlorine of 1- methyl, butyl-pyridinium chlorine is in mass ratio (1-4):The mixture of (1-4).
4. the medicine of the conditioning gynaecological disease according to Claims 2 or 3 is fragrant, which is characterized in that the system of the Poplar Powder of the modification Preparation Method includes:Will 25-75g Poplar Powders, 10-40mL ionic liquids mix after put into mixer in, temperature for 40-45 DEG C, It is stirred 30-50 minutes with 200-400 revs/min of rotating speed, discharging, sealing are placed in 30- in the drying box that temperature is 70-85 DEG C 60 minutes, mixture A is obtained, mixture A is added in 120-250g water, at 30-45 DEG C, with 100-300 revs/min of rotating speed Stirring 30-60 minutes, filtering, after filtering gained precipitation is washed with 30-60g acetone, 45-90g ethyl alcohol, in 40-55 DEG C of drying When 12-24 is small, obtain mixture B, with glacial acetic acid by the pH for the ethanol water that 15-45g mass fractions are 85-95% adjust to 3-4 adds in 0.85-1.7g modifying agent I, is uniformly mixed, obtains mixed liquor C, uniformly sprays whole mix to mixture B surface It is put into after closing liquid C in mixer, is 60-75 DEG C, is stirred 50-100 minutes with 300-500 revs/min of rotating speed in temperature, go out Material when 40-60 DEG C of dry 24-48 is small, obtains modified Poplar Powder;The ionic liquid for -3 butyl imidazole chlorine of 1- methyl, Butyl-pyridinium chlorine is (1-4) in mass ratio:The mixture of (1-4);The modifying agent I is oleamide, vinyl trimethoxy One or more mixture in silane, isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters.
5. the medicine of conditioning gynaecological disease according to claim 1 or 2 is fragrant, which is characterized in that the binding material is sunflower seed dregs One or more mixtures in adhesive, guar gum, carragheen.
6. the medicine of conditioning gynaecological disease according to claim 5 is fragrant, which is characterized in that the preparation of the sunflower seed dregs adhesive Method includes:120-240 parts of sunflower seed dregs powder, 200-400 parts of water, 12-18 parts of modifying agent II, 8-12 parts of potassium hydroxide are mixed Uniformly, be warming up to 55-75 DEG C, temperature be 55-75 DEG C, that 3.5-7 is stirred with 200-300 revs/min of rotating speed is small when, it is naturally cold But to 30-45 DEG C, 11.5-23 parts of glutaraldehydes are added in, at 30-45 DEG C, with 250-400 revs/min of 25-45 points of rotating speed stirring Kind, obtain sunflower seed dregs adhesive;The modifying agent II for polyvinyl alcohol, neopelex, one kind in urea or A variety of mixtures.
7. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 1, which is characterized in that including weighing by weight Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer, It stirs 30-90 minutes, is mixed at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into Poplar Powder, water, binding material Material obtains finished medicines perfume after mixture compression moulding, drying.
8. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 2, which is characterized in that including weighing by weight Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer, It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into modified Poplar Powder, water, binding material To mixture, finished medicines perfume is obtained after mixture compression moulding, drying.
9. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to claim 8, which is characterized in that including weighing by weight Each raw material, by motherwort, Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, rhizome of chuanxiong, Radix Astragali, Eclipta prostrata, rhizoma cyperi, Rhizoma Atractylodis Macrocephalae, Radix Paeoniae Alba, Rhizoma Gastrodiae, Chinese cassia tree, Poria cocos, santal Respectively when 45-65 DEG C of dry 6-12 is small, crushed 50-80 mesh sieves, put into after each raw material after crushing is mixed in mixer, It stirs 30-90 minutes, obtains at 45-65 DEG C, with 200-400 revs/min of rotating speed after putting into modified Poplar Powder, water, binding material To mixture, mixture is pressed into the perfume (or spice) of a diameter of 4.0-4.2mm, then disk into a diameter of 12-15cm, weight be 25-30g's Plate-like is fragrant, and finished medicines perfume is obtained after dry at 45-55 DEG C.
10. the processing technology of the medicine perfume of gynaecological disease is nursed one's health according to any one of claim 7-9, which is characterized in that finished product The moisture content of medicine perfume is 10-12%.
CN201711382846.6A 2017-12-20 2017-12-20 Medicinal incense for conditioning gynecopathy and processing technology thereof Active CN108096473B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711382846.6A CN108096473B (en) 2017-12-20 2017-12-20 Medicinal incense for conditioning gynecopathy and processing technology thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711382846.6A CN108096473B (en) 2017-12-20 2017-12-20 Medicinal incense for conditioning gynecopathy and processing technology thereof

Publications (2)

Publication Number Publication Date
CN108096473A true CN108096473A (en) 2018-06-01
CN108096473B CN108096473B (en) 2021-02-23

Family

ID=62211321

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711382846.6A Active CN108096473B (en) 2017-12-20 2017-12-20 Medicinal incense for conditioning gynecopathy and processing technology thereof

Country Status (1)

Country Link
CN (1) CN108096473B (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1695700A (en) * 2005-05-24 2005-11-16 李洪国 'Yimu' ointment and preparation method
CN103223687A (en) * 2013-05-07 2013-07-31 中国林业科学研究院林产化学工业研究所 Poplar powder acetylation modified processing method
CN106729569A (en) * 2017-01-19 2017-05-31 沈阳耀灸生物科技有限公司 Medicine perfume (or spice) for gynaecology and preparation method thereof
CN107007735A (en) * 2017-03-07 2017-08-04 沈阳耀灸生物科技有限公司 Medicine perfume (or spice) dirty for aligning and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1695700A (en) * 2005-05-24 2005-11-16 李洪国 'Yimu' ointment and preparation method
CN103223687A (en) * 2013-05-07 2013-07-31 中国林业科学研究院林产化学工业研究所 Poplar powder acetylation modified processing method
CN106729569A (en) * 2017-01-19 2017-05-31 沈阳耀灸生物科技有限公司 Medicine perfume (or spice) for gynaecology and preparation method thereof
CN107007735A (en) * 2017-03-07 2017-08-04 沈阳耀灸生物科技有限公司 Medicine perfume (or spice) dirty for aligning and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张连城: "月经病治验五则", 《天津中医》 *
李凤凤 等: "杨木粉在EmimAC离子液体中溶解性能的研究", 《林产化学与工业》 *

Also Published As

Publication number Publication date
CN108096473B (en) 2021-02-23

Similar Documents

Publication Publication Date Title
CN102178809B (en) Externally-applied medicament for skin and method for processing medicament into preparation
CN101380386A (en) Traditional Chinese medicine composition for tonifying the kidney yang
CN101983703A (en) Traditional Chinese medicine composition and traditional Chinese medicine preparation
CN107007735B (en) Medicinal incense for regulating heart and preparation method thereof
CN110638987A (en) Moxibustion medicinal moxibustion stick for dispelling cold and eliminating dampness and preparation method thereof
CN110013470A (en) Application of the kidney treasured piece in preparation treatment sequelae of pelvic inflammatory disease drug
WO2017220052A2 (en) Formulation treating rheumatoid bone pain
CN106539882A (en) Traditional Chinese medicine composition for foot bath and preparation method thereof
CN104826074A (en) Traditional Chinese medicine preparation for sinus bradycardia and its preparation method
CN108079260A (en) A kind of Chinese medicine preparation for treating the proliferation of mammary gland and preparation method thereof
CN107913377A (en) It is a kind of treat rheumatic disease harvest sub- wine and preparation method thereof
CN108096473A (en) Nurse one's health the medicine perfume and its processing technology of gynaecological disease
CN106389972A (en) Rhodomyrtus tomentosa wine for treating rheumatic diseases and preparation method thereof
CN106729100A (en) With anti-inflammatory, the external application Chinese medicine health care preparation of beauty and preparation method thereof
CN101816774A (en) Medicinal powder for nourishing blood, regulating menstruation and removing maculae
CN112138096A (en) Pharmaceutical composition for scalp health care, hair blacking and hair growth, preparation method and application thereof
CN105148240A (en) Medicinal preparation used for treating chronic cardiac failure
CN110559417A (en) gout-relieving moxibustion stick and preparation method thereof
CN104840891A (en) Traditional Chinese medicine preparation used for treating alcoholic cardiomyopathy and preparation method thereof
CN110585285A (en) A Chinese medicinal composition for consolidating hair, promoting hair growth, nourishing hair, blackening hair, regulating stomach and tranquilizing mind, and its preparation method
CN103446535A (en) Miao ethnomedicine for treating coronary heart disease
CN108607055A (en) Treat carcinoid Chinese medicine composition in uterus and preparation method thereof
CN108114112A (en) A kind of blood-activating analgetic plaster and preparation method thereof
CN108704040B (en) Traditional Chinese medicine composition and application thereof
CN106177075A (en) The cold compress bag for the treatment of allergic skin and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information

Inventor after: Zhu Xueming

Inventor after: Wang Yao

Inventor after: Ruan Xiaojun

Inventor before: Ruan Xiaojun

CB03 Change of inventor or designer information
TA01 Transfer of patent application right

Effective date of registration: 20210202

Address after: No.66, Fengqi West Road, Kechuang Park, Tongxiang Economic Development Zone, Jiaxing, Zhejiang 314000

Applicant after: JIAXING SOFTTER BIOTECHNOLOGY Co.,Ltd.

Address before: 331400 Room 102, unit 1, building 1, No.2 Anping Road, Baqiu Town, Xiajiang County, Ji'an City, Jiangxi Province

Applicant before: Ruan Xiaojun

TA01 Transfer of patent application right
GR01 Patent grant
GR01 Patent grant