CN108077329A - A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof - Google Patents

A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof Download PDF

Info

Publication number
CN108077329A
CN108077329A CN201711263143.1A CN201711263143A CN108077329A CN 108077329 A CN108077329 A CN 108077329A CN 201711263143 A CN201711263143 A CN 201711263143A CN 108077329 A CN108077329 A CN 108077329A
Authority
CN
China
Prior art keywords
lemon
drying agent
injection drying
extract
injection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711263143.1A
Other languages
Chinese (zh)
Inventor
李贵林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DAXIN COUNTY SCIENCE AND TECHNOLOGY INFORMATION INSTITUTE
Original Assignee
DAXIN COUNTY SCIENCE AND TECHNOLOGY INFORMATION INSTITUTE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DAXIN COUNTY SCIENCE AND TECHNOLOGY INFORMATION INSTITUTE filed Critical DAXIN COUNTY SCIENCE AND TECHNOLOGY INFORMATION INSTITUTE
Priority to CN201711263143.1A priority Critical patent/CN108077329A/en
Publication of CN108077329A publication Critical patent/CN108077329A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/30Polygonaceae [Buckwheat family], e.g. red-knees or rhubarb

Abstract

The invention discloses a kind of lemon nutritive insecticidal injection drying agents and preparation method thereof, are made of the raw material of following weight percent:Herba polygoni hydropiperis extract 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%, preservative 0.6 ~ 0.8%, formamide 10 ~ 12% and deionized water supply 100%.By way of noting and doing, medicament is injected into lemon tree body, lemon pest and disease damage is prevented by tree body intrinsic conduction, it is good to Sooty mould, shot hole, resin disease, coccid, aphid and red spider effect, and contain various nutrient elements, good with rear growing way, quality improves lemon, compared with traditional dispenser water-saving, saving of labor, pollution-free.

Description

A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof
Technical field
The invention belongs to plant protection and nutritious fertilizer manufacturing method technical fields, and in particular to a kind of lemon nutrition is killed Worm injection drying agent and preparation method thereof.
Background technology
Lemon(Scientific name:Citrus limon (L.) Burm. f.), Rutaceae citrus plant, lemon be also known as lemon fruit, Female fruit of lemon, benefit etc..Dungarunga, branch pierce or are bordering on less stingless, tender leaf and the dark violet red of bud, blade ground paper matter, it is avette or Ellipse.Single flower axillary or few flowers life.Fruit ellipse or avette, pericarp is thick, and usual coarse, lemon yellow, fruit juice acid is to very Acid, seed is small, avette, end point;Kind of skin is smooth, cotyledon milky, usual list or has polyembryony concurrently.The month at florescence 4-5, fruiting period 9-11 Month.
Lemon is because its taste is extremely sour, liver void pregnant woman most eating, therefore claims the female fruit of benefit or beneficial mothers and sons.Contain abundant lemon in lemon Acid, therefore it is known as " citric acid warehouse ".Its fruit juice fleshiness is crisp, there is strong aroma.Because the special acid of taste, therefore can only As first-class flavoring, for modulation beverage dish, cosmetics and drug.In addition, lemon be rich in vitamin C, can preventing phlegm from forming and stopping coughing, It promotes the production of body fluid stomach invigorating.For symptoms such as bronchitis, pertussis, loss of appetite, hypovitaminosis, heatstroke polydipsia, it is " scurvy " Jinx.
Citron fruit nutritive value enriches, and citric acid 6.9g, full sugar 3.1g, protein are contained in every 100ml lemon juices 0.9g, fatty 0.2g, dietary fiber 0.3g, vitamin C 76mg, vitamin B1 0.1mg, vitamin B2 0.2mg, niacin 0.3mg;Potassium 120mg, calcium 24mg, magnesium 12mg, selenium 4.5mg.In addition, lemon is also containing limonin, limonene etc..
Lemon is one of fruit for most having medical value in the world, it is rich in vitamin C, carbohydrate, calcium, phosphorus, iron, vitamin B1, vitamin B2, niacin, quininic acid, citric acid, malic acid, aurantiamarin, aurantiin, coumarin, a large amount potassium element and low amounts sodium Element etc., it is highly beneficial to human body.Vitamin C can maintain the generation of the various tissues of human body and cytoplasm, and keep them just Normal physiological function.The in vivo matrix of people, bonding and collagen etc. are required for vitamin C to protect.When vitamin C lacks, Interstitial between cell --- jelly also just and then tails off.In this way, cell tissue will become fragile, the energy for resisting external force is lost Power, human body are easy for scurvy occur;It also has more multipurpose, and such as preventing cold stimulates the effects that hematopoiesis and anticancer.
Lemon main breed all over the world is promising to make every effort to overcome especially, and Lisbon, Bai Na, graceful appearance Lip river, Xi Er, Fermi are endured hardships, tower Xi Tilaimeng and Meyer lemon occupy a small amount of ratio.The principal item of Chinese cultivated is made every effort to overcome and its Sports strains and megarchidium system to be outstanding, A small amount of cultivation has the kinds such as Meyer lemon, Lisbon, makes every effort to overcome kind especially and strain accounts for more than the 95% of whole varieties of plant.It is near several Year, China sequentially introduced Fino, Wei Erla, Wella Fu Laka lemons and the several kinds of Bill Si lemon from foreign countries.
Especially Appennin sausage is made every effort to overcome, quoted from the U.S., tree vigo(u)r is medium, opens a business, and branch is messy, hangs down loosely, growth potential and resistance, Wide adaptability, blade ellipse, petiole are short.Fruit ellipse is to obovate, early fruiting and high yield, if managing the tree of 3 years or more Single plant yield reaches more than 100kg.Fruit ellipse, apex tool mastoid process, base portion circle, surrounding have radial rill, single fruit weight 100- 200g, maximum fruit weight 600g, pericarp thickness 0.35cm or so, savory dense, essential oil quality is first-class;Acid content 6.4-7.4g/ml fruit juice, Oil content 0.4%-0.6%, 9-22, seed;Mid or late November is ripe, and yielding ability is good, storage tolerance.High containing citric acid, fragrance is good, High yield is stablized, good quality, is the preferred kind of current lemon processing and marketing fresh.
Meyer lemon alias bergamot.Originate in China.It is the cenospecies with lemon, because its resistance is strong, tree performance is short strong, holds The features such as manageability, early fruiting and high yield, lemon high 2.1m, the hat width 3.1m of general 5 years do week 24cm.Branch is messy, drapes over one's shoulders It dissipates, there is spinule.Blade ellipse or ovate-elliptic.Fruit ellipse, mean fruit weight 140g or so, 4 or so, seed, product Matter is medium.Mid-November is ripe, relatively gets bumper crops, compared with storage tolerance.
Lisbon originates in Portugal.Tree vigo(u)r is powerful, makes every effort to overcome resistance to hot and cold and low level management more especially;Fruit oblong, mastoid process Cone, pericarp make every effort to overcome smooth, thick flavor more especially, and going into operation, it is late to make every effort to overcome more especially, but yield is high, the raw tree of general 5 years or more, highest Single plant yield reaches more than 150kg.Its tree body life compared with lunge, and inconvenience manages and easily stabs fruit, and cultivated area is smaller.
The big fruit shape Lay lemon of Ta Xitilaimeng triploids, growth potential is stronger, and branch has short thorn more, and blade ellipse is thicker;Pipe Reason is convenient, compared with Canker-Resistance;Fruit is spherical, and fruit top is micro- prominent, and skin is smooth and thin;Single fruit weight 80g, no seed, fruit juice rate 50%- 56%, acid content 5.4g/100ml;It is the marketing fresh kind promoted.
Originate from Spain in Fino.Fruit is spherical to ellipse, and pericarp is thin, smooth, and fruit colour is yellowish to golden yellow.Tree vigo(u)r Prosperous, spinosity, pole high yield, 5-6 is raw, and tree 667m2 yield may be up to 1.7t.It is observed according to Chongqing Jiangjin farmer, the fruit of Fino It is real maximum, and yield highest, it blooms throughout the year.Seed is more, 15 or so average, and edible rate reaches 62%-68%.
Wei Er pull-ups come from Spain, and tree body is tall and big, opens a business, is stingless.Thick in pericarp, fruit lacks core, 5.6 average, dimension Raw element C contents are high, and fruit texture is good, and fruit shape is oval to factory's ellipse.Usually bloom 2-3 times every year.Fruit tree research institute of Chongqing City It introduces, the kind fruit is small and fruit shape is partially long.
Due to lemon growth quickly, root, which is applied fertilizer, cannot many times meet the requirement of its fast-growth, and root Efficiency of applying fertilizer increases investment, the growth effect of lemon is not also apparent far below note dry application fertilizer.At present to the food of lemon It leaf and notes dry pest and mainly takes and killed with spraying chemical pesticide, long-term medication makes pest generate the resistance to the action of a drug, with chemical agriculture Medicine is killed very undesirable, and also results in environmental pollution, control effect is very poor.
The content of the invention
The present invention is directed to the above-mentioned deficiency of the prior art, provides a kind of lemon nutritive insecticidal injection drying agent, by noting what is done Medicament is injected lemon tree body, lemon pest and disease damage is prevented by tree body intrinsic conduction, to Sooty mould, shot hole, tree by mode Fat disease, coccid, aphid and red spider effect are good, and contain various nutrient elements, and good with rear growing way, quality carries lemon Height, compared with traditional dispenser water-saving, saving of labor, pollution-free.
The technical proposal of the invention is realized in this way:
A kind of injection drying agent for preventing lemon tree pest and disease damage, is made of the raw material of following weight percent:Herba polygoni hydropiperis extract 2.0 ~ 4.0%th, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%, anti- Rotten agent 0.6 ~ 0.8%, formamide 10 ~ 12% and deionized water supply 100%.
Polygonum flaccidum, Chinese medicine name.For polygonaceae arsesmart water pepperPolygonum hydropiper L.Herb.It is distributed in me Each provinces and regions in state north and south.With expelling wind and removing dampness, the effect of removing blood stasis and analgesics, removing toxicity for detumescence, desinsection is antipruritic.It is usually used in dysentery, gastroenteritis, The treatment of the illnesss such as diarrhea, rheumatic arthritis, treating swelling and pain by traumatic injury, functional uterine bleeding;Outside for venomous snake bite, skin eczema.
The preparation method of the Herba polygoni hydropiperis extract is:It will gather or the polygonum flaccidum of buying dry in the shade at room temperature, percolation extraction, Material-water ratio is 1:8 ~ 10, after extracting 5 ~ 7 days, filtrate is recycled, relative density is 1.10 ~ 1.12 medicinal extract when being concentrated into 20 DEG C;Again The ethyl alcohol that volume fraction is more than 85% is added in, refluxing extraction 2 ~ 3 times recycles filtrate, and relative density is 1.16 when being concentrated into 20 DEG C ~ 1.18 medicinal extract, obtains Herba polygoni hydropiperis extract.
Dandelion(Classification system:Taraxacum mongolicum Hand.-Mazz.)Composite family, Dandelion are perennial Herbaceous plant.Root is coniform, surface sepia, shrinkage, and limb edge has wave-formed mouth or a pinniform drastic crack sometimes, base portion gradually narrow Cheng Ye Often band reddish violet, scape top aubergine are close by the long pubescence of spider's thread shape white for handle, petiole and master pulse;Capitulum, involucre clock Shape, achene crineous, long pappus white, 4~October of flowering fruit bearing stage.Dandelion function is clearing heat and detoxicating, dispersing swelling and dissipating binds.It is general in the past It is only used for acute mastitis, sore swells.This product clinically widely uses in recent years, find it except have good antipyretic and antidote functions it Outside, still there is the effect of diuresis, laxative.Surgery sore carbuncle is cannot be only used for, and can use and control internal medicine illness.Clothes match somebody with somebody honeysuckle, cordate houttuynia, Available for the strongly fragrant lung of phlegm heat;It, can be with controlling abscess of throat with Radix Isatidis;It, can be with controlling urine heat gonorrhea with caulis lonicerae, Asiatic plantain;With Cassia Son, yellow chrysanthemum flower, can be with controlling red eye, swell pain;It, can be with controlling jaundice with damp-heat pathogen with cape jasmine, oriental wormwood;It, can be red with acute mastitis is controlled with Snakegourd Fruit, fritillaria It is swollen;With honeysuckle flower, Chinese violet, wild chrysanthemum, available for furuncle swelling toxin;With selfheal, oyster, subcutaneous nodule is gone through available for scrofula.
The preparation method of the dandelion extract is:The dandelion that will be gathered or purchase is more than 75% with volume fraction Ethyl alcohol heating and refluxing extraction 2 ~ 3 times, merging filtrate, relative density is 1.12 ~ 1.15 medicinal extract when being concentrated into 20 DEG C, obtains Pu public affairs English extract.
Soapberry fruit soak is mistake after soapberry fruit is crushed after 3-4 kilograms of per kilogram addition clear water immersion 3-5 days Filter obtained soak.
Soapberry(Classification system:Sapindus mukorossi Gaertn. ), alias:Wood suffers from son(Compendium of Materia Medica), oil Suffer from son(Sichuan)Hardship suffers from tree(Hainan), yellow mesh tree, mesh wave tree(Taiwan), You Luoshu, fruit of washing one's hands, name elsewhere:Rub mesh, vacation with the hands Longan, Devil Frown etc..Soapberry deciduous tree, branch are carried out, leaf alternate;Without stipule;There is handle;Panicle, basidixed and side life; Flower polygamy, corolla light green have shortly clawed;Floral disc cup-shaped;Filigree has fine, soft fur, and medicine back life, and hermaphrodite flower stamen is small, and filigree has soft Hair.Drupe is spherical, yellow or brown color when ripe.Seed is spherical, black, 6~July of florescence.9~October of fruiting period.It is long to originate in China Various regions and South East Asia Mainland various regions, India and Japan on the south the basin of river.Pericarp contains saponin, can do boxboard for soap, timber With wooden comb etc..Root, browse, seed:Bitter, micro-pungent is trembled with fear.It is slightly poisonous.Heat-clearing eliminating the phlegm, disperse accumulation desinsection.For diphtheria, throat swells Bitterly, acute tonsillitis, cough, pertussis, food stagnation malnutrition due to parasitic infestation;Trichomonas vaginalis is used for outside.Benevolence:It is pungent, it puts down.Disperse accumulation wards off evil.For infantile malnutrition due to digestive disturbances or intestinalparasites, roundworm Disease, inflatable in abdomen, halitosis.
The pest and disease damage of lemon once occurs, it is difficult to prevent, traditional control method is mostly by trombone slide, is applied by spray gun Medicine, but most of lemon is grown in mountainous region, forest land or hills, hillside, and diversion is difficult.Insecticide-applying way traditional simultaneously easily draws Worker's poisoning is played, and chemical pesticide is drifted with water, and utilization rate of active components is not high, it is difficult to reach control effect.Inventor is led to After verification experimental verification for many years, find to contain insecticidal constituent in various plants body, by multi-turns screen, determine Herba polygoni hydropiperis extract, Pu Gong English extract and soapberry fruit soak have preferable control effect, the especially bituminous coal to lemon to a variety of pest and disease damages of lemon Disease, shot hole, resin disease, coccid, aphid and red spider have significant prevention and control to act on.
Add in Herba polygoni hydropiperis extract 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0% and soapberry fruit soak 6.0 ~ Co-toxicity coefficient is all higher than 120 under 8.0% blend proportion, has synergistic effect.
Formamide in formula is intensive polar solvent, plays dissolving and dilutes the work of Herba polygoni hydropiperis extract and dandelion extract With since two kinds of extracts are thick medicinal extract, by the use of formamide as retarder thinner, being integrated with water well;In formula Nano-sized carbon is act as:The dissolubility of two kinds of extract components is improved, active ingredient is incorporated in nanometer carbon molecules, promotes lemon Set absorption of the tree body to active ingredient.
The lemon nutritive insecticidal injection drying agent, its preparation method comprise the following steps:Polygonum flaccidum is taken by weight percentage Extract 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%, formamide 10 ~ 12% adds in deionized water dissolving, obtains aqueous solution;In aqueous solution add in preservative 0.6 ~ 0.8%, it is uniformly mixed, is dissolved to transparent;PH value is adjusted to 7 ~ 9 using hydrochloric acid or sodium hydroxide, then with micro-filtrate membrane filtration, It can obtain lemon nutritive insecticidal injection drying agent.
The preservative is formulated by the raw material of following parts by weight:Triethanolamine 5~10, iron chloride 5~10 gather Siloxanes 15~20, bamboo juice 60~80;Preparation method is that above-mentioned raw materials are heated to 20 DEG C~50 DEG C, is stirred evenly, 3~5 points Clock to obtain the final product.
The lemon nutritive insecticidal injection drying agent is used to prevent lemon pest and disease damage:Sooty mould, shot hole, resin disease, Coccid, aphid and red spider.
The application method of the injection drying agent is:The application method of the injection drying agent is:The lemon that tree-walk is selected to be more than 10cm Tree, away from dispenser is injected at 20 ~ 30cm of basal part of stem, by injection drying agent syringe needle, oblique cutting enters in trunk xylem from the top down;Tree The lemon of 10 ~ 20cm of footpath, dosage 5ml, tree-walk are that the lemon dosage of 20 ~ 30cm is 10ml, and tree-walk is more than The lemon dosage of 30cm is 15ml;Observation post administration injection drying agent flow is applied, after medicament fully enters tree body, extracts syringe needle, Wound is blocked with soil, its spontaneous recovery is allowed to can be completed.
Advantages of the present invention:
1st, manufacturing method is simple, and non-environmental-pollution, and manufactured injection drying agent is carried with pure natural Herba polygoni hydropiperis extract, dandelion Based on taking object and soapberry fruit soak, by inject in tree body with achieve the purpose that promote growth and desinsection;
2nd, the application is transported to rapidly the dry of tree, stem, leaf site by the way that medicament is directly injected into trunk with flow liquid in trunk, So as to kill the pest for endangering trees, and trees multiple diseases can be treated, the quick-acting and lasting period is good;
3rd, after using injection drying agent, lemon grows fine, and disease resistance enhancing, during harvest, fruit yield is high;
4th, injection drying agent is easy to use, and tree body will not be damaged, and is improved compared with traditional spray pattern, preventive effect is notable, is lemon Lemon tree prevents the optimal selection of pest and disease damage.
Specific embodiment
The system of 1 injection drying agent active ingredient Herba polygoni hydropiperis extract of embodiment, dandelion extract and soapberry fruit soak It is standby:
The preparation method of Herba polygoni hydropiperis extract:The polygonum flaccidum of acquisition or buying dries in the shade at room temperature, percolation extraction, material-water ratio 1:8~ 10, after extracting 5 ~ 7 days, filtrate is recycled, relative density is 1.10 ~ 1.12 medicinal extract when being concentrated into 20 DEG C;Add volume fraction For more than 85% ethyl alcohol, refluxing extraction 2 ~ 3 times recycles filtrate, and relative density is 1.16 ~ 1.18 medicinal extract when being concentrated into 20 DEG C, Obtain Herba polygoni hydropiperis extract.
The preparation method of dandelion extract is:The dandelion that will be gathered or purchase, with the second that volume fraction is more than 75% Alcohol heating and refluxing extraction 2 ~ 3 times, merging filtrate, relative density is 1.12 ~ 1.15 medicinal extract when being concentrated into 20 DEG C, obtains dandelion and carries Take object.
Soapberry fruit soak is mistake after soapberry fruit is crushed after 3-4 kilograms of per kilogram addition clear water immersion 3-5 days Filter obtained soak.
Lemon nutritive insecticidal injection drying agent, its preparation method comprise the following steps:Herba polygoni hydropiperis extract is taken by weight percentage 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%th, formamide 10 ~ 12% add in deionized water dissolving, obtain aqueous solution;Preservative 0.6 ~ 0.8% is added in aqueous solution, is stirred It mixes uniformly mixed, is dissolved to transparent;PH value is adjusted to 7 ~ 9 using hydrochloric acid or sodium hydroxide, then with micro-filtrate membrane filtration, you can it obtains Lemon nutritive insecticidal injection drying agent.
The formula 1 of 2 injection drying agent of embodiment
Herba polygoni hydropiperis extract 2.0%, dandelion extract 5.0%, soapberry fruit soak 6.0%, nano-sized carbon 1%, molasses 5.0%, anti-corrosion Agent 0.6%, formamide 10% and deionized water supply 100%.
The formula 2 of 3 injection drying agent of embodiment
Herba polygoni hydropiperis extract 3.0%, dandelion extract 7.5%, soapberry fruit soak 7.0%, nano-sized carbon 2%, molasses 7.5%, anti-corrosion Agent 0.7%, formamide 11% and deionized water supply 100%.
The formula 3 of 4 injection drying agent of embodiment
Herba polygoni hydropiperis extract 2.5%, dandelion extract 6.0%, soapberry fruit soak 6.5%, nano-sized carbon 2%, molasses 6.0%, anti-corrosion Agent 0.7%, formamide 11% and deionized water supply 100%.
The formula 4 of 5 injection drying agent of embodiment
Herba polygoni hydropiperis extract 3.5%, dandelion extract 8.0%, soapberry fruit soak 7.5%, nano-sized carbon 2%, molasses 9.0%, anti-corrosion Agent 0.7%, formamide 11% and deionized water supply 100%.
The formula 5 of 6 injection drying agent of embodiment
It is Herba polygoni hydropiperis extract 4.0%, dandelion extract 10.0%, soapberry fruit soak 8.0%, nano-sized carbon 3%, molasses 10.0%, anti- Rotten agent 0.8%, formamide 12% and deionized water supply 100%.
7 injection drying agent of embodiment prevents the field control effectiveness test of lemon pest and disease damage
Inventor has carried out the field control effectiveness test of injection drying agent prevention lemon pest and disease damage, experiment selection on May 11st, 2016 There is the lemon tree that Sooty mould, shot hole, resin disease tentatively occur as controlling object, select the plot lemon age of tree 5 Year or more.
Subjects:200 plants of lemon trees, Sooty mould, shot hole, the moderate generation of resin disease, pest is coccid, Aphid and red spider.
Injection drying agent uses:Tree-walk be more than 10cm lemon, away from 20 ~ 30cm of basal part of stem at injection dispenser, by injection drying agent Oblique cutting enters in trunk xylem syringe needle from the top down;The lemon of 10 ~ 20cm of tree-walk, dosage 5ml, tree-walk 20 The lemon dosage of ~ 30cm is 10ml, and lemon dosage of the tree-walk more than 30cm is 15ml;Apply observation post administration injection drying agent Flow after medicament fully enters tree body, extracts syringe needle, blocks wound with soil, its spontaneous recovery is allowed to can be completed.
As a result investigate:Disease index is investigated before and after experiment, and investigates coccid, aphid and the insect population of red spider. Statistics and result of calculation after 1 month, 2 months and 6 months.
1 injection drying agent of the present invention of table is to lemon Sooty mould field control effectiveness test result
2 injection drying agent of the present invention of table is to lemon shot hole field control effectiveness test result
3 injection drying agent of the present invention of table is to lemon resin disease field control effectiveness test result
4 injection drying agent of the present invention of table is to lemon coccid field control effectiveness test result
5 injection drying agent of the present invention of table is to lemon aphid field control effectiveness test result
6 injection drying agent of the present invention of table is to lemon red spider field control effectiveness test result
Statistics indicate that injection drying agent of the present invention has for lemon Sooty mould, shot hole, resin disease, coccid, aphid and red spider There is significant control effect, this is because:The use of comparison medicament is that conventional trombone slide is sprayed, time-consuming, and is difficult to Spraying is uniform, and trombone slide spraying medicament utilization rate is low.Data show that conventional lasting period difference of spraying is, it is necessary to monthly dispenser.Injection drying agent Principle is the conduction using tree body, and medicament is conducted upwards in tree body, is played a protective role, and the quick-acting and lasting period is not It is wrong.
Meanwhile inventor also found, and after injection drying agent, lemon grows fine, disease resistance enhancing, during harvest, Yield is high.Injection drying agent is easy to use, and tree body will not be damaged, and is improved compared with traditional spray pattern, preventive effect is notable, is lemon Lemon tree prevents the optimal selection of pest and disease damage.

Claims (8)

1. a kind of lemon nutritive insecticidal injection drying agent, it is characterised in that:It is made of the raw material of following weight percent:Polygonum flaccidum extracts Object 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%th, preservative 0.6 ~ 0.8%, formamide 10 ~ 12% and deionized water supply 100%.
2. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The preparation of the Herba polygoni hydropiperis extract Method is:It will gather or the polygonum flaccidum of buying dry in the shade at room temperature, percolation extraction, material-water ratio 1:8 ~ 10, after extracting 5 ~ 7 days, Filtrate is recycled, relative density is 1.10 ~ 1.12 medicinal extract when being concentrated into 20 DEG C;The ethyl alcohol that volume fraction is more than 85% is added, Refluxing extraction 2 ~ 3 times recycles filtrate, and relative density is 1.16 ~ 1.18 medicinal extract when being concentrated into 20 DEG C, obtains Herba polygoni hydropiperis extract.
3. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The system of the dandelion extract Preparation Method is:It will gather or the dandelion of buying, with the ethyl alcohol heating and refluxing extraction 2 ~ 3 times that volume fraction is more than 75%, merge Filtrate, relative density is 1.12 ~ 1.15 medicinal extract when being concentrated into 20 DEG C, obtains dandelion extract.
4. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The soapberry fruit soak is Per kilogram adds in the soak after 3-4 kilograms of clear water impregnate 3-5 days, being obtained by filtration after soapberry fruit is crushed.
5. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:Its preparation method includes following step Suddenly:Take by weight percentage Herba polygoni hydropiperis extract 2.0 ~ 4.0%, dandelion extract 5.0 ~ 10.0%, soapberry fruit soak 6.0 ~ 8.0%th, nano-sized carbon 1 ~ 3%, molasses 5.0 ~ 10.0%, formamide 10 ~ 12% add in deionized water dissolving, obtain aqueous solution;In aqueous solution Middle addition preservative 0.6 ~ 0.8%, is uniformly mixed, is dissolved to transparent;PH value is adjusted to 7 ~ 9 using hydrochloric acid or sodium hydroxide, Micro-filtrate membrane filtration is used again, you can obtains lemon nutritive insecticidal injection drying agent.
6. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The preservative is by following heavy The raw material of amount number is formulated:Triethanolamine 5~10, iron chloride 5~10, polysiloxanes 15~20, bamboo juice 60~80;It prepares Method is that above-mentioned raw materials are heated to 20 DEG C~50 DEG C, is stirred evenly, and 3~5 minutes to obtain the final product.
7. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The lemon nutritive insecticidal injection Dry agent is used to prevent lemon pest and disease damage:Sooty mould, shot hole, resin disease, coccid, aphid and red spider.
8. lemon nutritive insecticidal injection drying agent according to claim 1, it is characterised in that:The application method of the injection drying agent For:Select tree-walk be more than 10cm lemon, away from 20 ~ 30cm of basal part of stem at injection dispenser, by injection drying agent syringe needle from the top down Oblique cutting enters in trunk xylem;The lemon of 10 ~ 20cm of tree-walk, dosage 5ml, the lemon that tree-walk is 20 ~ 30cm are used Pharmaceutical quantities are 10ml, and lemon dosage of the tree-walk more than 30cm is 15ml;Observation post administration injection drying agent flow is applied, when medicament is whole Into after tree body, syringe needle is extracted, wound is blocked with soil, allows its spontaneous recovery.
CN201711263143.1A 2017-12-05 2017-12-05 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof Pending CN108077329A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711263143.1A CN108077329A (en) 2017-12-05 2017-12-05 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711263143.1A CN108077329A (en) 2017-12-05 2017-12-05 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108077329A true CN108077329A (en) 2018-05-29

Family

ID=62173673

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711263143.1A Pending CN108077329A (en) 2017-12-05 2017-12-05 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108077329A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1242935A (en) * 1999-08-11 2000-02-02 西北农业大学无公害农药研究服务中心 Injection for tree trunk
CN1359881A (en) * 2002-01-11 2002-07-24 夏鲁青 Process for preparing nutritive insecticidal injection for poplar
CN101124906A (en) * 2006-08-14 2008-02-20 福建农林大学应用生态研究所 Nimbin-containing injection formulation for tree trunk and application of nimbin in field of injection for tree trunk
CN101147498A (en) * 2007-11-02 2008-03-26 江西省蚕桑茶叶研究所茶厂 Plant insecticide
CN103518784A (en) * 2013-09-30 2014-01-22 横县生产力促进中心 Pollution-free jasmine pesticide
CN103535389A (en) * 2013-10-27 2014-01-29 莫晟琼 Plant source fruit tree insecticide
CN103548895A (en) * 2013-10-27 2014-02-05 来光业 Botanical vegetable insecticide
CN103609618A (en) * 2013-10-30 2014-03-05 桂平市西山茶场 Tea pollution-free pesticide
CN103609416A (en) * 2013-11-30 2014-03-05 桂平市白石洞天仙山铁皮石斛专业合作社 Planting method for dendrobium officinale
CN103814964A (en) * 2014-02-18 2014-05-28 北京联合大学 Emulsion for killing aphid and red spider and its preparation method
CN105284864A (en) * 2015-12-04 2016-02-03 李开森 Forest fruit trunk-injection insecticide and preparation method and application thereof
CN105394092A (en) * 2015-12-28 2016-03-16 北京市农林科学院 Method for preventing and treating aphids by using Lepidium apetalum and Polygonum glabrum extract product

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1242935A (en) * 1999-08-11 2000-02-02 西北农业大学无公害农药研究服务中心 Injection for tree trunk
CN1359881A (en) * 2002-01-11 2002-07-24 夏鲁青 Process for preparing nutritive insecticidal injection for poplar
CN101124906A (en) * 2006-08-14 2008-02-20 福建农林大学应用生态研究所 Nimbin-containing injection formulation for tree trunk and application of nimbin in field of injection for tree trunk
CN101147498A (en) * 2007-11-02 2008-03-26 江西省蚕桑茶叶研究所茶厂 Plant insecticide
CN103518784A (en) * 2013-09-30 2014-01-22 横县生产力促进中心 Pollution-free jasmine pesticide
CN103535389A (en) * 2013-10-27 2014-01-29 莫晟琼 Plant source fruit tree insecticide
CN103548895A (en) * 2013-10-27 2014-02-05 来光业 Botanical vegetable insecticide
CN103609618A (en) * 2013-10-30 2014-03-05 桂平市西山茶场 Tea pollution-free pesticide
CN103609416A (en) * 2013-11-30 2014-03-05 桂平市白石洞天仙山铁皮石斛专业合作社 Planting method for dendrobium officinale
CN103814964A (en) * 2014-02-18 2014-05-28 北京联合大学 Emulsion for killing aphid and red spider and its preparation method
CN105284864A (en) * 2015-12-04 2016-02-03 李开森 Forest fruit trunk-injection insecticide and preparation method and application thereof
CN105394092A (en) * 2015-12-28 2016-03-16 北京市农林科学院 Method for preventing and treating aphids by using Lepidium apetalum and Polygonum glabrum extract product

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
冯旭等: "三种东北常见乳汁植物乙醇提取物杀虫性研究", 《东北农业科学》 *
张孝云等: "德宏地区柠檬主要病虫害发生规律及综合防治技术", 《中国热带农业》 *
录丽平等: "无患子皂苷粗提物杀虫活性研究", 《安徽农业科学》 *
龚鹏博: "柠檬树病虫害防治综述", 《农药市场信息》 *

Similar Documents

Publication Publication Date Title
KR101805004B1 (en) Fermentation method using medicinal leaf and skin external composition containing fermented extract by the method
KR101868050B1 (en) Fermentation method using medicinal flower and skin external composition containing fermented extract by the method
JP5864252B2 (en) Medicinal plant extract using smoked product and skin external preparation composition containing the same
KR101405429B1 (en) Cosmetics containing natural grass
CN103053953B (en) Functional bean sprouts prepared from Chinese herbal medicines used as both food and medicine and method for preparing functional bean sprouts
Jansen Dyes and tannins
CN107156828A (en) A kind of full nutrition formula food suitable for patients with inflammatory bowel
CN105379521A (en) Breeding method for organic cherry tomatoes
CN107801443A (en) A kind of method for promoting Gleditsia sinensis Seeds to sprout
CN102604750A (en) Method for preparing forest herbaceous plant biomass detergent
KR20180089696A (en) Removing Method for Residual Agricultural Chemicals of Natural Plant Extracts
CN108029504A (en) A kind of blue or green money willow cuttage and seedling culture matrix
CN106805235A (en) A kind of full nutrition formula food suitable for respiratory disease patient
CN104288577A (en) Traditional Chinese medicine preparation for preventing and curing hog flu and pneumonia, and preparation method thereof
CN106701410A (en) Healthcare wine capable of strengthening stomach and tonifying qi and production method thereof
CN105012769A (en) Traditional Chinese medicine composition for treating diabetes and preparation method of traditional Chinese medicine composition
CN109534915A (en) A kind of biological agent and application for enhancing drug effect and promoting blade function
CN109348972A (en) A kind of numerous implantation methods of grape expansion
CN108496780A (en) A kind of cultural method of organic strawberry
CN107927010A (en) A kind of Chinese olive tree nutritive insecticidal injection drying agent and preparation method thereof
CN107581153A (en) A kind of method of black bottom soft-shelled turtle ecologic breeding
CN108077329A (en) A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof
CN107416919A (en) Efficiently remove the composition of Polychlorinated biphenyls in water body
CN105055597B (en) The Chinese materia medica preparation and its production method for treating peacock enterogastritis
CN104996659A (en) Health-care herb tea contained in cups and production method of health-care herb tea

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180529

RJ01 Rejection of invention patent application after publication