CN101124906A - Nimbin-containing injection formulation for tree trunk and application of nimbin in field of injection for tree trunk - Google Patents

Nimbin-containing injection formulation for tree trunk and application of nimbin in field of injection for tree trunk Download PDF

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Publication number
CN101124906A
CN101124906A CNA2006101093808A CN200610109380A CN101124906A CN 101124906 A CN101124906 A CN 101124906A CN A2006101093808 A CNA2006101093808 A CN A2006101093808A CN 200610109380 A CN200610109380 A CN 200610109380A CN 101124906 A CN101124906 A CN 101124906A
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nimbin
injection
drying agent
agent
cosolvent
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CN101124906B (en
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曾兆华
王玉林
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FUJIAN INSTITUTE OF APPLIED ECOLOGICAL OF AGRICULTURE AND FORESTRY UNIVERSITY
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FUJIAN INSTITUTE OF APPLIED ECOLOGICAL OF AGRICULTURE AND FORESTRY UNIVERSITY
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Abstract

The present invention discloses a truck injection agent with nimbin, which consists of nimbin, latent solvent, osmotic agent, mixing agent and diluent, at the same time, the invention discloses the application of the truck injection agent with nimbin in the truck injection field, namely that the truck injection agent is injected into the truck directly. The injecting part is positioned on the truck with more than 10 cm from the ground, and the injecting depth reaches the xylem. By the method of direct injection, the medicine enters directly into the plant tissue, which reduces the influence of environmental factor to the nimbin, ensures a good suction rate of the plant to the nimbin and reduces correspondingly the relative usage of the nimbin, moreover, the nimbin after entering the plant tissue is able to be conducted primely so as to have longer lasting performance, thus protecting the target plant in a better manner.

Description

A kind of injection drying agent and nimbin that contains nimbin annotated dried Application for Field
Technical field
The present invention relates to a kind of injection drying agent and nimbin that contains nimbin and in fruit tree, gardens and forestry, adopt the application of annotating the drying method prevention and elimination of disease and pests.Belong to pesticide field.
Background technology
Nimbin is from the Meliaceae plant, for example print extract in the chinaberry (Azadirachtin indica) efficient, low toxicity, low-residual, the natural agricultural chemicals of environment-friendly type nontoxic to the person poultry safety, non-environmental-pollution, be one of current biopesticide of praising highly the most, can be widely used in damage by disease and insect such as control pest, evil mite and nematode.Its mode of action mainly is, food refusal/repellent action, breed inhibitory action, the repellent action of laying eggs, insect growth regulating action etc., have advantages such as being difficult for developing immunity to drugs, not injuring natural enemy and other non-target organism.Its shortcoming is unstable, studies show that other active ingredient in nimbin and the seal chinaberry decompose under the situation that strong sunshine, high temperature and organic solvent exist easily; They are two years old; plant insecticide must be relatively stable lasting as its food refusal of anti-feedant; if keep the food refusal effect in longer stage; anti-feedant should be in the various piece conduction of plant; the new first portion of plant is lacked a big shortcoming of absorption anti-feedant in the protective effect right and wrong, and these new lives and the position that does not contact anti-feedant may be subjected to the harm of insect.Have report to confirm that nimbin and other seal chinaberry preparations have interior absorption when executing in soil and water, still, nimbin it be unclear that by the conduction of foliage-spray in plant.
Nimbin belongs to four and falls triterpene compound, and the ISO adopted name is Azadirachtin, molecular formula C 35H 44O 16, the CIPAC digital code is 11141-17-6, chemical structural formula:
Figure A20061010938000051
At present, it mainly is by modes such as surface spray, filling roots that nimbin uses as agricultural chemicals, because factors such as high temperature, ultraviolet ray can be quickened the degraded of active ingredient, influences the Expected Results of medicament by the surface spray mode; Can be by the mode of irritating root because soil absorbs and infiltration reduces the absorption efficiency of plant to agricultural chemicals.
Summary of the invention
In order to solve the problem of above-mentioned existence, the purpose of this invention is to provide a kind of injection drying agent that contains nimbin, and the mode by directly injecting, make nimbin directly enter plant tissue inside, reduce the influence of environmental factor to nimbin.
Technical scheme of the present invention is achieved in that a kind of injection drying agent that contains nimbin, is made up of the female medicine (being neem extract) of nimbin, cosolvent, bleeding agent, composite dose and thinner, and its composition proportioning is as follows:
The female medicine of nimbin: for containing the neem extract that nimbin is 1%-60% by weight;
Cosolvent: the amount that adds cosolvent in the female medicine of every gram nimbin is the 1-30 milliliter;
Thinner: be the buffer solution of pH4-7, female medicine of nimbin and cosolvent are diluted to the dilute solution that contains the female medicine 0.001%-30% of nimbin by weight;
Bleeding agent (adding as required): the 0%-1% by female medicine of nimbin and cosolvent dilution back cumulative volume adds.
Composite dose (option):, add 1-2 kind chemical pesticide or other biological agricultural chemicals as auxiliary element according to the needs of controlling object and index for control.
Described cosolvent can be ethanol, acetone or other neutral organic solvents.
Described bleeding agent is the solvent that azone or other have anatonosis (penetrating) effect.
The female medicine of nimbin be from seal chinaberry seed or its hetero-organization through extraction, purify, concentrate the dry powder shape material that forms, can use after must being processed into preparation, directly the female medicine of nimbin is sprayed or annotates that to do technical operability not strong; And on the other hand, the female medicine of nimbin is more stable under normal environmental condition, therefore, adopt that " cocktail method " is now with the current can significantly save the preparation cost and can extend the expiration date, the concrete grammar of its preparation is: the female medicinal cosolvent of nimbin is fully dissolved, add bleeding agent, composite dose as required, do use with thinner dilution back for annotating again, the medicament for preparing is preferably within 24 hours and uses up, in order to avoid the active ingredient degraded.Can be directly used in the nimbin preparation of annotate doing if directly be processed into, then need in process, also need add protectants such as anti-photodissociation agent, stabilizing agent, make behind the preparation because of the degraded in the long term storage process to reduce nimbin as far as possible.
Another object of the present invention provides nimbin annotating dried Application for Field, and nimbin directly is injected in the trunk.
Nimbin is made the injection drying agent that contains nimbin, injection drying agent directly is injected in the trunk
Inject the position and be generally, inject the degree of depth and reach xylem apart from the trunk more than the 10cm of ground.
Compared with prior art, the invention has the beneficial effects as follows:
1, the method by directly injecting can effectively reduce the loss of other application methods (as modes such as surface spray, filling roots) to agricultural chemicals, and to the pollution of environment.
2, the mode that adopts notes to do is directly injected nimbin in the plant corpus, can effectively avoid main active ingredient nimbin to degrade fast because of factor effects such as ultraviolet ray, high temperature.
3, the nimbin that enters in the plant tissue can be well absorbed conduction, can keep the biologically active of long period in plant corpus, thereby protect target plant long-term effectively.
4, because the nimbin mode of action mainly is by food refusal/repellent, and influence reproduction etc., therefore, in the short term, toxic action to insect is not obvious, but can long-term effectively pest population be controlled at reduced levels, and can not impact natural enemy.
Embodiment
Below in conjunction with specific embodiment the present invention is described in further detail, but not as a limitation of the invention.
Embodiment 1: get female medicine 5 grams of the nimbin that contains 39.13% nimbin by weight, 10 milliliters of ethanol with 95% are pre-molten, after to be 5 buffer solution with pH with the mixed liquor of female medicine of nimbin and ethanol be diluted to 150 milliliters, dosage according to 0.5mL/cm, 0.7mL/cm, 0.9mL/cm (diameter of a cross-section of a tree trunk 1.3 meters above the ground) is carried out injection, the injection position is apart from ground 30cm place, the injection degree of depth reaches xylem, and a strain is a repetition, establishes three altogether and repeats and establish the clear water contrast.
Insect population go down rate and preventive effect computational methods:
Figure A20061010938000071
Figure A20061010938000072
Result of the test is as shown in table 1, and along with the increase of dosage, control efficiency increases, and 0.9mL/cm increases not obvious than 0.7mL/cm (diameter of a cross-section of a tree trunk 1.3 meters above the ground) control efficiency, from economical and practical angle, should select 0.7mL/cm (diameter of a cross-section of a tree trunk 1.3 meters above the ground) to be advisable.
Table 1 is that different dose nimbins are annotated the control efficiency of doing olive star chamber wood louse
Dosage Worm before the medicine Behind the medicine 7 days Behind the medicine 15 days Behind the medicine 30 days
mL/cm Number (head) Borer population (head) alive The rate that goes down (%) Preventive effect (%) Borer population (head) alive The rate that goes down (%) Preventive effect (%) Borer population (head) alive The rate that goes down (%) Preventive effect (%)
0.5 0.7 0.9 clear water contrast 436 479 445 398 183 155 133 411 58.0 67.6 70.1 -3.2 59.3 68.6 71.0 - 145 110 97 470 66.7 77.0 78.2 -18.1 71.8 80.6 81.5 - 80 53 43 570 81.7 89.0 90.3 -43.2 87.2 92.3 93.3

Claims (8)

1. injection drying agent that contains nimbin is characterized in that being made up of the female medicine of nimbin, cosolvent, bleeding agent, composite dose and thinner,
The female medicine of nimbin: for containing the neem extract that nimbin is 1%-60% by weight;
Cosolvent: the amount that adds cosolvent in the female medicine of every gram nimbin is the 1-30 milliliter;
Thinner: be the buffer solution of pH4-7, female medicine of nimbin and cosolvent are diluted to the dilute solution that contains the female medicine 0.001%-30% of nimbin by weight;
Bleeding agent: the 0%-1% by female medicine of nimbin and cosolvent dilution back cumulative volume adds.
2. a kind of injection drying agent that contains nimbin according to claim 1 is characterized in that also containing composite dose, according to the needs of controlling object and index for control, adds 1-2 kind chemical pesticide or other biological agricultural chemicals as auxiliary element.
3. a kind of injection drying agent that contains nimbin according to claim 1 is characterized in that described cosolvent is neutral organic solvent.
4. a kind of injection drying agent that contains nimbin according to claim 1 is characterized in that described cosolvent is ethanol or acetone.
5. a kind of injection drying agent that contains nimbin according to claim 1 is characterized in that described bleeding agent is the solvent with anatonosis effect.
6. a kind of injection drying agent that contains nimbin according to claim 1 is characterized in that described bleeding agent is an azone.
7. do Application for Field according to the described a kind of injection drying agent that contains nimbin of claim 1 to 6 at notes, it is characterized in that injection drying agent directly is injected in the trunk.
8. a kind of injection drying agent that contains nimbin according to claim 7 is being annotated dried Application for Field, it is characterized in that injecting the position for apart from the trunk more than the 10cm of ground, injects the degree of depth and reaches xylem.
CN2006101093808A 2006-08-14 2006-08-14 Nimbin-containing injection formulation for tree trunk and application of nimbin in field of injection for tree trunk Expired - Fee Related CN101124906B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102119638A (en) * 2010-11-29 2011-07-13 嘉汉城市生态苗木(苏州)有限公司 Method for promoting rapidly thickening of wood
CN102217611A (en) * 2011-04-19 2011-10-19 浙江农林大学 Milbemycins tree trunk injection liquid and application thereof
CN108077329A (en) * 2017-12-05 2018-05-29 大新县科学技术情报研究所 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1115958C (en) * 1999-08-11 2003-07-30 西北农业大学无公害农药研究服务中心 Injection for tree trunk

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102119638A (en) * 2010-11-29 2011-07-13 嘉汉城市生态苗木(苏州)有限公司 Method for promoting rapidly thickening of wood
CN102217611A (en) * 2011-04-19 2011-10-19 浙江农林大学 Milbemycins tree trunk injection liquid and application thereof
CN108077329A (en) * 2017-12-05 2018-05-29 大新县科学技术情报研究所 A kind of lemon nutritive insecticidal injection drying agent and preparation method thereof

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