CN106490014A - A kind of plant compound pesticide containing ricidine. and preparation method thereof - Google Patents
A kind of plant compound pesticide containing ricidine. and preparation method thereof Download PDFInfo
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- CN106490014A CN106490014A CN201610928069.XA CN201610928069A CN106490014A CN 106490014 A CN106490014 A CN 106490014A CN 201610928069 A CN201610928069 A CN 201610928069A CN 106490014 A CN106490014 A CN 106490014A
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- ricidine
- plant compound
- compound pesticide
- pesticide containing
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention belongs to technical field of pesticide, and in particular to a kind of plant compound pesticide containing ricidine. and preparation method thereof, the plant compound pesticide containing ricidine. include that the raw material of following parts by weight is made：80 120 parts of 15 parts of ricidine., 5 10 parts of matrine, 35 parts of Sanguinarine, 5 10 parts of pyrethrin, 8 15 parts of rotenone, 26 parts of Oleum Caryophylli, 0 20 parts of organic solvent, 6 15 parts of surfactant, 0 10 parts of synergist, 38 parts of antifreezing agent, 0 2.5 parts of preservative and water.Insecticide of the present invention is rapid-action, and efficacy stability, persistent period are long, does not develop immunity to drugs, degradable, pollution-free, is especially suitable for comprehensive preventing and treating of vegetable-crop pest-insect.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of plant compound pesticide and its preparation side containing ricidine.
Method.
Background technology
Tradition is applied to veterinary antibiotics, the various pesticide of grain are respectively provided with stronger toxicity, and after use, its toxicity is different
Degree it is absorbed into inside veterinary antibiotics, grain, can not be fully erased before eating, serious harm human health, Er Qienong
Medicine is remained and causes certain pollution to environment.In recent years, with the improvement of people's living standards, the extract of plant or plant is added
Work makes insecticide, and which possesses low toxicity, degradable, and Environmental compatibility is good, and to killing natural enemy, insect is not likely to produce drug-fast excellent
Point, is increasingly welcome by people.
Chinese patent CN102239891B discloses a kind of Botanical synergistic compound pesticide containing chinaberry element, and dosage form is
Environment-friendly type cream, microemulsion or aqueous emulsion；Containing chinaberry element 0.1%～20% in preparation, thunder godvine alkaloid 0.1%～20%, its
Remaining for auxiliary agent.But, the patent insecticide lasting period is short.
Chinese patent CN105494472A discloses a kind of novel plant and extracts pesticide, and its raw material includes plant extract activity
Composition, surfactant, synergist, solvent and water.Which has small toxicity, residual amount few, to the killing except the time is short of Pieris rapae,
Effect is good, the advantage of persistent period length.But, the patent pesticide material wide variety, high cost.
Content of the invention
For overcoming drawbacks described above, it is an object of the invention to provide a kind of plant compound pesticide and its system containing ricidine.
Preparation Method.
For achieving the above object, the present invention is adopted the following technical scheme that：
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
Ricidine. 1-5 parts, matrine 5-10 parts, Sanguinarine 3-5 parts, pyrethrin 5-10 parts, rotenone 8-15 parts, Oleum Caryophylli 2-
6 parts, organic solvent 0-20 parts, surfactant 6-15 parts, synergist 0-10 parts, antifreezing agent 3-8 parts, preservative 0-2.5 parts and
Water 80-120 parts.
Preferably, the organic solvent is at least one of glycerol, acetone, Ketohexamethylene and DMF.
Preferably, the surfactant is dodecylbenzene sodium sulfonate, sodium lignin sulfonate, fatty alcohol-polyoxyethylene ether
At least one of with sucrose fatty acid ester.
Preferably, the synergist is at least one of organosilicon, Butacide, alkyl carbonate and laurocapram.
Preferably, the antifreezing agent is ethylene glycol or Propylene Glycol.
Preferably, the preservative is at least one in Sorbitol, sodium benzoate, ethylparaben and sodium salicylate
Kind.
A kind of preparation method of the above-mentioned plant compound pesticide containing ricidine., comprises the following steps：By the weight
The various raw material mixing of number, stir, obtain product.
Positive beneficial effect of the present invention：
1. ricidine. biological activity of the present invention is high, degradable, and significantly, matrine has good prevention effect to insecticidal effect, low
Poison, low-residual, degradable, do not develop immunity to drugs, Sanguinarine has good insecticidal and antifungal effect, Pyrethrum to have paralysis insecticide
Nervus centraliss are acted on, and parasite killing is rapid, and degradable, rotenone is not remained, and respiratory of insect maincenter can be made to benumb and dead, Oleum Caryophylli drive
Worm, good antimicrobial effect, raw material type of the present invention are simple, with low cost, various raw material synergism, make insecticide of the present invention work
Hurry up, efficacy stability, persistent period are long, do not develop immunity to drugs, degradable, pollution-free, microemulsion, medicine is made with the effect of various adjuvants
Effect is stable.
2. organic solvent of the present invention is at least one of glycerol, acetone, Ketohexamethylene and DMF, just
In the abundant dissolving of pyrethrin, rotenone and Oleum Caryophylli, and toxicity is low.The surfactant is DBSA
At least one of sodium, sodium lignin sulfonate, fatty alcohol-polyoxyethylene ether and sucrose fatty acid ester, biological degradation rate are high, low cost
Honest and clean.The synergist is at least one of organosilicon, Butacide, alkyl carbonate and laurocapram, with low surface tension,
Good plate-out ability, permeability and emulsifying dispersivity, effectively suppress or reduction insect is to the anti-poisoning effect of the removing toxic substances of pesticide activity.
The antifreezing agent is ethylene glycol or Propylene Glycol, improves freezing tolerance of the insecticide of the present invention in low temperature environment, is conducive to
Preserve.The preservative is at least one of Sorbitol, sodium benzoate, ethylparaben and sodium salicylate, delays
Insecticide of the present invention rotten.
3. plant compound pesticide preparation method of the present invention containing ricidine. is simple, plant material wide material sources, low cost
Honest and clean, and each raw material synergism, significantly, the lasting period is long for insecticidal effect, is especially suitable for the preventing and treating of vegetable-crop pest-insect.
Specific embodiment
With reference to some specific embodiments, the present invention is further described.
Embodiment 1
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
1 part of ricidine., 5 parts of matrine, 3 parts of Sanguinarine, 5 parts of pyrethrin, 8 parts of rotenone, 2 parts of Oleum Caryophylli, surfactant 6
80 parts of part, 1 part of synergist, 3 parts of antifreezing agent and water.
The surfactant is dodecylbenzene sodium sulfonate.
The synergist is organosilicon.
The antifreezing agent is ethylene glycol.
The preparation method of the above-mentioned plant compound pesticide containing ricidine., comprises the following steps：By above-mentioned parts by weight
The mixing of various raw materials, stir, obtain product.
Embodiment 2
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
1 part of ricidine., 5 parts of matrine, 3 parts of Sanguinarine, 6 parts of pyrethrin, 8 parts of rotenone, 3 parts of Oleum Caryophylli, organic solvent 5
80 parts of part, 6 parts of surfactant, 1 part of synergist, 3 parts of antifreezing agent, 0.5 part of preservative and water.
The organic solvent is glycerol.
The surfactant is sodium lignin sulfonate.
The synergist is organosilicon.
The antifreezing agent is ethylene glycol.
The preservative is Sorbitol.
The preparation method of the above-mentioned plant compound pesticide containing ricidine., comprises the following steps：By above-mentioned parts by weight
The mixing of various raw materials, stir, obtain product.
Embodiment 3
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
2 parts of ricidine., 6 parts of matrine, 3.5 parts of Sanguinarine, 6 parts of pyrethrin, 9 parts of rotenone, 3 parts of Oleum Caryophylli, organic solvent 8
90 parts of part, 7 parts of surfactant, 2 parts of synergist, 4 parts of antifreezing agent, 1 part of preservative and water.
The organic solvent is acetone.
The surfactant is that sodium lignin sulfonate and fatty alcohol-polyoxyethylene ether, both weight compare 1：1.
The synergist is alkyl carbonate.
The antifreezing agent is Propylene Glycol.
The preservative is sodium benzoate.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Embodiment 4
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
3 parts of ricidine., 8 parts of matrine, 4 parts of Sanguinarine, 7 parts of pyrethrin, 10 parts of rotenone, 4 parts of Oleum Caryophylli, organic solvent 10
100 parts of part, 8 parts of surfactant, 5 parts of synergist, 5 parts of antifreezing agent, 1.5 parts of preservative and water.
The organic solvent is DMF.
The surfactant is fatty alcohol-polyoxyethylene ether.
The synergist is laurocapram.
The antifreezing agent is Propylene Glycol.
The preservative is ethylparaben.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Embodiment 5
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
3 parts of ricidine., 8 parts of matrine, 4 parts of Sanguinarine, 7 parts of pyrethrin, 2 parts of Celastrus angulatus, 10 parts of rotenone, Oleum Caryophylli 4
100 parts of part, 10 parts of organic solvent, 8 parts of surfactant, 5 parts of synergist, 5 parts of antifreezing agent, 1.5 parts of preservative and water.
It is anesthetic action and toxic action that the present embodiment adds Celastrus angulatus model of action, mainly prevents and treats biting mouthparts evil
Worm, and do not develop immunity to drugs, do not kill natural enemy, with each raw material synergism, comprehensive parasite killing, insecticidal effect strengthen.
The organic solvent is DMF.
The surfactant is fatty alcohol-polyoxyethylene ether.
The synergist is laurocapram.
The antifreezing agent is Propylene Glycol.
The preservative is ethylparaben.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Embodiment 6
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
4 parts of ricidine., 8.5 parts of matrine, 4 parts of Sanguinarine, 8 parts of pyrethrin, 12 parts of rotenone, 4.5 parts of Oleum Caryophylli, You Jirong
110 parts of 15 parts of agent, 10 parts of surfactant, 6 parts of synergist, 6 parts of antifreezing agent, 2 parts of preservative and water.
The organic solvent is Ketohexamethylene.
The surfactant is sucrose fatty acid ester.
The synergist is Butacide and alkyl carbonate, and both weight ratios are 1:1.
The antifreezing agent is ethylene glycol.
The preservative is sodium salicylate.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Embodiment 7
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
4.5 parts of ricidine., 9 parts of matrine, 5 parts of Sanguinarine, 9 parts of pyrethrin, 13 parts of rotenone, 5 parts of Oleum Caryophylli, organic solvent
18 parts, 12 parts of surfactant, 8 parts of synergist, 7 parts of antifreezing agent, 120 parts of 2.5 parts of preservative and water.
The organic solvent is glycerol and DMF, and both amount ratios are 1：1.
The surfactant is fatty alcohol-polyoxyethylene ether.
The synergist is Butacide.
The antifreezing agent is ethylene glycol.
The preservative is ethylparaben.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Embodiment 8
A kind of plant compound pesticide containing ricidine., the raw material including following parts by weight are made：
5 parts of ricidine., 10 parts of matrine, 5 parts of Sanguinarine, 10 parts of pyrethrin, 15 parts of rotenone, 6 parts of Oleum Caryophylli, organic solvent
20 parts, 15 parts of surfactant, 10 parts of synergist, 8 parts of antifreezing agent, 120 parts of 2.5 parts of preservative and water.
The organic solvent is Ketohexamethylene.
The surfactant is dodecylbenzene sodium sulfonate.
The synergist is laurocapram.
The antifreezing agent is ethylene glycol.
The preservative is Sorbitol and sodium salicylate, and both amount ratios are 1：1.
The preparation method of the above-mentioned plant compound pesticide containing ricidine. is shown in embodiment 2.
Comparative example 1
Plant compound pesticide of the present embodiment containing ricidine. is substantially the same manner as Example 4, and difference is：
The plant compound pesticide containing ricidine. includes that the raw material of following parts by weight is made：
8 parts of matrine, 4 parts of Sanguinarine, 7 parts of pyrethrin, 10 parts of rotenone, 4 parts of Oleum Caryophylli, 10 parts of organic solvent, surface are lived
Property 100 parts of 8 parts of agent, 5 parts of synergist, 5 parts of antifreezing agent, 1.5 parts of preservative and water.
Comparative example 2
Plant compound pesticide of the present embodiment containing ricidine. is substantially the same manner as Example 4, and difference is：
The plant compound pesticide containing ricidine. includes that the raw material of following parts by weight is made：
3 parts of ricidine., 8 parts of matrine, 4 parts of Sanguinarine, 10 parts of rotenone, 4 parts of Oleum Caryophylli, 10 parts of organic solvent, surface activity
100 parts of 8 parts of agent, 5 parts of synergist, 5 parts of antifreezing agent, 1.5 parts of preservative and water.
Comparative example 3
Plant compound pesticide of the present embodiment containing ricidine. is substantially the same manner as Example 4, and difference is：
The plant compound pesticide containing ricidine. includes that the raw material of following parts by weight is made：
3 parts of ricidine., 8 parts of matrine, 4 parts of Sanguinarine, 7 parts of pyrethrin, 4 parts of Oleum Caryophylli, 10 parts of organic solvent, surface activity
100 parts of 8 parts of agent, 5 parts of synergist, 5 parts of antifreezing agent, 1.5 parts of preservative and water.
Application test
Experimental field：The a certain Chinese cabbage field in Anyang, breeds of Chinese cabbage are rich anti-70, and subregion is planted, per 20 m of area's area2, minizone
Protection row is left, protection line-spacing is 1.0m.
Reagent agent：Test group is using embodiment of the present invention 1-8 and the insecticide of comparative example 1-3, positive controls
Using 4.5% r, safe matched group adopts clear water, formulation rate 50g/ mus.
Process of the test：Embodiment 1-8, the insecticide of comparative example 1-3 and 4.5% r are equal
1000 times are diluted with water, carry out dispenser with conventional manual aerosol apparatus, carry out the 1st time in field first meeting Pieris rapae larva and apply
Medicine, interval 15d carry out not spraying other insect prevention medicaments in the 2nd dispenser, treatment region, and other field management measures are normal with land for growing field crops
Rule.Each 10th area of test random selection, chooses 10 plants per area, investigates insect population before dispenser, after dispenser 1d, 5d, 10d and
15d investigates remaining borer population alive, the results are shown in Table 1.
Revision insect recluced rate=[（Population number after population number-dispenser before dispenser）Population number before/dispenser] × 100%
Prevention effect=[（Treatment region Revision insect recluced rate-safe check plot Revision insect recluced rate）/（1- is safe, and check plot insect population goes down
Rate）] × 100%.
Plant compound pesticide insecticidal effect testing result of 1 embodiment of the present invention 1-8 of table containing ricidine.
As shown in Table 1, growth over time, plant compound pesticide 1d residual worm of embodiment of the present invention 1-8 containing ricidine.
Amount has somewhat declined, and the residual worm amounts of 5d and 10d are decreased obviously, and the residual worm amounts of 15d somewhat increased, 1d prevention effects
Only more than 27%, 5d just reach more than 60%, and 10d and 15d prevention effects may be up to more than 80%, and safety is compareed
As time goes on, residual worm amount is increased considerably group, and plant compound pesticide of embodiment of the present invention 1-8 containing ricidine. is described
Significantly, the lasting period is long for insecticidal effect.Positive controls are compared to, although chemical pesticide significantly prevents and treats Pieris rapae in a short time,
It is that As time goes on preventive effect effect declines substantially.Comparative example 1-3 is compared to, comparative example 1,2 and 3 distinguishes
Ricidine., pyrethrin and rotenone is eliminated, prevention effect contains the plant compound pesticide of ricidine. significantly lower than the present invention,
The each raw material synergism of plant compound pesticide of the present invention containing ricidine. is obvious.
Claims (7)
1. a kind of plant compound pesticide containing ricidine., it is characterised in that the raw material including following parts by weight is made：
Ricidine. 1-5 parts, matrine 5-10 parts, Sanguinarine 3-5 parts, pyrethrin 5-10 parts, rotenone 8-15 parts, Oleum Caryophylli 2-
6 parts, organic solvent 0-20 parts, surfactant 6-15 parts, synergist 0-10 parts, antifreezing agent 3-8 parts, preservative 0-2.5 parts and
Water 80-120 parts.
2. the plant compound pesticide containing ricidine. according to claim 1, it is characterised in that the organic solvent is third
At least one of triol, acetone, Ketohexamethylene and DMF.
3. the plant compound pesticide containing ricidine. according to claim 1, it is characterised in that the surfactant is
At least one of dodecylbenzene sodium sulfonate, sodium lignin sulfonate, fatty alcohol-polyoxyethylene ether and sucrose fatty acid ester.
4. the plant compound pesticide containing ricidine. according to claim 1, it is characterised in that the synergist is organic
At least one of silicon, Butacide, alkyl carbonate and laurocapram.
5. the plant compound pesticide containing ricidine. according to claim 1, it is characterised in that the antifreezing agent is second two
Alcohol or Propylene Glycol.
6. the plant compound pesticide containing ricidine. according to claim 1, it is characterised in that the preservative is Pyrusussuriensiss
At least one of alcohol, sodium benzoate, ethylparaben and sodium salicylate.
7. the preparation method of the plant compound pesticide containing ricidine. described in a kind of any one of claim 1-6, its feature exist
In comprising the following steps：By the various raw material mixing of the parts by weight, stir, obtain product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610928069.XA CN106490014A (en) | 2016-10-31 | 2016-10-31 | A kind of plant compound pesticide containing ricidine. and preparation method thereof |
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| CN201610928069.XA CN106490014A (en) | 2016-10-31 | 2016-10-31 | A kind of plant compound pesticide containing ricidine. and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108353927A (en) * | 2018-04-28 | 2018-08-03 | 赖振明 | A kind of composition pesticide containing Imiprothrin and sanguinarine |
| CN109673661A (en) * | 2019-01-30 | 2019-04-26 | 福建省三明市烟草物流有限责任公司 | A kind of tobacco leaf insect prevention pulvis and preparation method thereof |
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| CN103518751A (en) * | 2013-10-28 | 2014-01-22 | 上海市农业科学院 | Plant composite insecticide |
| CN104938543A (en) * | 2015-06-10 | 2015-09-30 | 朱云 | Pesticide for preventing cotton bollworms on vegetable leaves |
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2016
- 2016-10-31 CN CN201610928069.XA patent/CN106490014A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103518751A (en) * | 2013-10-28 | 2014-01-22 | 上海市农业科学院 | Plant composite insecticide |
| CN104938543A (en) * | 2015-06-10 | 2015-09-30 | 朱云 | Pesticide for preventing cotton bollworms on vegetable leaves |
Non-Patent Citations (1)
| Title |
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| 徐汉虹: "杀虫植物与植物性杀虫剂", 《杀虫植物与植物性杀虫剂》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108353927A (en) * | 2018-04-28 | 2018-08-03 | 赖振明 | A kind of composition pesticide containing Imiprothrin and sanguinarine |
| CN109673661A (en) * | 2019-01-30 | 2019-04-26 | 福建省三明市烟草物流有限责任公司 | A kind of tobacco leaf insect prevention pulvis and preparation method thereof |
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