CN107668092A - A kind of pharmaceutical composition used for beetle - Google Patents
A kind of pharmaceutical composition used for beetle Download PDFInfo
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- CN107668092A CN107668092A CN201711094529.4A CN201711094529A CN107668092A CN 107668092 A CN107668092 A CN 107668092A CN 201711094529 A CN201711094529 A CN 201711094529A CN 107668092 A CN107668092 A CN 107668092A
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- extract
- pharmaceutical composition
- beetle
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Pest Control & Pesticides (AREA)
- Mycology (AREA)
- Virology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of pharmaceutical composition used for beetle, including Nidus Vespae extract, fructus ulmi extract, triperygium wilfordii extractive, chun spicebush root extract, Ran She le extract, Periostracum Cicadae extract, Radix Gentianae Macrophyllae extract, iris extract, root of langdu extract and nimbin.Heretofore described pharmaceutical composition can targetedly kill beetle, it is and without any side effects to the natural enemy of beetle, security is good, it is biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small;With preferable permeability and wettability, the central nervous system of polypide is disturbed, suppresses worm's ovum synthesis development, is not susceptible to drug resistance;Quick-acting is good, is adapted to the wide popularization and application in terms of control of insect.
Description
Technical field
The invention belongs to agricultural technology development field, in particular it relates to a kind of pharmaceutical composition used for beetle.
Background technology
Chemical agent plays an important role in terms of crop pest control, but the residual of medicine causes nature
The ecosystem is worsening, and this has turned into international common concern and key subjects urgently to be resolved hurrily.Since China, twentieth century
Because single use chemical pesticide causes agricultural product harmful element exceeded, health and the existence of the people are directly endangered, therefore, state
Family pays much attention to and formulated《Medium-term and long-term scientific and technical development program outline》, it is therefore intended that encourage research and development environment-friendly type fertilizer, agriculture
Medicine." seeking speed " psychology of current peasant is incompatible, and most farmers are still selected using high poison, the chemical pesticide of high residue, this
Chemical pesticide can use only for crop, i.e., kill each class pest for certain crop simultaneously.But this chemical pesticide exists
Today of green and environmental protection is advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, further, since insect
The difference of species, cause each class pest to occur larger difference in terms of the resistance to the action of a drug and drug resistance, so just make killing for chemical agent
Easily there is resistance insect in worm effect, therefore propose to prevent specific insect from just seeming for the insect-proof agent of different insects to have very much must
Will, but yet there are no corresponding report.
The content of the invention
It is good that the technical problems to be solved by the invention are to provide a kind of security, biodegradable good, pollution-free and excitant
Smell, no environment toxic action, in animal body noresidue, specific aim kill the pharmaceutical composition of beetle.
Technical scheme is used by the present invention solves above-mentioned technical problem:A kind of drug regimen used for beetle
Thing, including Nidus Vespae extract, fructus ulmi extract, triperygium wilfordii extractive, chun spicebush root extract, Ran She le extract, cicada slough extraction
Thing, Radix Gentianae Macrophyllae extract, iris extract, root of langdu extract and nimbin.
In order to which the present invention is better achieved, further, contain the honeycomb equivalent to 5-20g honeycomb medicinal materials per 100ml solution
Extract, the fructus ulmi extract of 5-20g fructus ulmi medicinal materials, the triperygium wilfordii extractive of 5-20g tripterygium wilfordiis, 5-20g chun spicebush root medicines
Chun spicebush root extract, Ran She le extract, Periostracum Cicadae extract, the 5- of 5-20g cicada slough medicinal materials of 5-20g Ran She le medicinal materials of material
The Radix Gentianae Macrophyllae extract of 20g gentiana macrophylla medicines, the iris extract of 5-20g iris medicinal materials, the root of langdu extract of 5-20g root of langdu medicinal materials,
Nidus Vespae extract, fructus ulmi extract, triperygium wilfordii extractive, chun spicebush root extract, Ran She le extract, Periostracum Cicadae extract, bark of ash
Extract, iris extract, the usage ratio of root of langdu extract medicinal material are 1:2:2:3:3:1:2:2:2.
In order to which the present invention is better achieved, further, the dosage of the nimbin is 0.005g~5.0g/100ml.
In order to which the present invention is better achieved, further, the dosage of the nimbin is 0.05g~1.0g/100ml.
In order to which the present invention is better achieved, further, described pharmaceutical composition formulation is powder pin or freezed.
The preparation method of the pharmaceutical composition of above-mentioned poisoning beetle is prepared, is comprised the steps:
(1) pharmaceutical composition raw medicinal material honeycomb 50g, fructus ulmi 50g, the tripterygium wilfordii 100g of beetle, chun spicebush root are killed
200g, Ran She le 200g, cicada slough 100g, bark of ash 100g, iris 100g, root of langdu 150g, nimbin 3g;
(2) honeycomb, fructus ulmi, tripterygium wilfordii add water to cook secondary, 2 hours every time, collecting decoction, add ethanol filtering and concentrating, add 3
Amount water again, is sufficiently stirred, and refrigerates 48 hours, and filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby;
(3) chun spicebush root, Ran She le, cicada slough, bark of ash, iris, the root of langdu add water to cook secondary, 1 hour every time, collecting decoction,
Filtration, filtrate is concentrated, is let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relatively close
Spend for 1.20, it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and filtrate is concentrated into relative density as 1.30, adds 3 times
Water to be measured, is sufficiently stirred, is refrigerated 48 hours, filtration, it is 1.15 that filtrate, which is concentrated into relative density,
(4) merge with above-mentioned all decoctions, add 2 times of amount water, be sufficiently stirred, refrigerate 24 hours, filtration, filtrate adds print chinaberry
Element and deionized water water are configured to 1000ml solution, stir evenly, the relative density when relative density of above-mentioned each filtrate is 80 DEG C;
(5) solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution;
(6) filter, it is filling, sterilizing, produce.
The present invention compared with prior art, has advantages below and beneficial effect:
(1) heretofore described pharmaceutical composition can targetedly kill beetle, and to the natural enemy of beetle without
Any toxic side effect, security is good, biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body
Noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small;
(2) low raw-material cost used in heretofore described pharmaceutical composition, there is preferable permeability and wet
Lubricant nature, easily breaks through beetle wax coat, and depth destroys the epidermal structure of polypide and internal protein, makes beetle be not easy to send out
Raw drug resistance;
(3) heretofore described pharmaceutical composition can interfere with the central nervous system of polypide, suppress worm's ovum synthesis hair
Educate;
(4) heretofore described pharmaceutical composition quick-acting is good, and after spray, beetle stopped eating in 20~40 minutes
Death, it is adapted to the wide popularization and application in terms of control of insect.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this
Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention
Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in
In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1:
The present embodiment provides a kind of pharmaceutical composition used for beetle, including Nidus Vespae extract, fructus ulmi extract,
Triperygium wilfordii extractive, chun spicebush root extract, Ran She le extract, Periostracum Cicadae extract, Radix Gentianae Macrophyllae extract, iris extract, the root of langdu
Extract and nimbin, its component are as follows:
Its preparation method:Honeycomb, fructus ulmi, tripterygium wilfordii add water to cook secondary, 2 hours every time, collecting decoction, add ethanol to filter
Concentration, add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby
With;Chun spicebush root, Ran She le, cicada slough, bark of ash, iris, the root of langdu add water to cook it is secondary, 1 hour every time, collecting decoction, filter, concentration
Filtrate, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.20 that filtrate decompression, which is concentrated into relative density,
It is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.30 that filtrate, which is concentrated into relative density, adds 3 times of amount water, fully
Stirring, refrigerate 48 hours, filtration, filtrate is concentrated into relative density as 1.15;Merge with above-mentioned all decoctions, add 2 times of amount water, fill
Point stirring, is refrigerated 24 hours, filtration, filtrate adds nimbin and deionized water water and is configured to 1000ml solution, stirs evenly, above-mentioned each
The relative density when relative density of filtrate is 80 DEG C;Solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution;Filtering,
It is filling, sterilizing, produce.
Wherein, the process for adding ethanol filtering and concentrating is first to filter to get filtrate, and filtrate decompression is concentrated into relative density as 1.27
~1.30, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and decompression filtrate recycling ethanol is simultaneously concentrated into relative
Density is 1.30.Filtrate is concentrated into relative density as 1.25~1.30.The mass percent of the sodium hydroxide solution used is
20%.Solution uses filtering with microporous membrane.
Embodiment 2:
The present embodiment verifies that the pharmaceutical composition insecticide common with market is compared, to the eradicative rate of beetle.
Choose insecticide common on the market:Pale purple purple spore bacterium aqua, nematode killing agent, the agent of special efficacy root line, thiamethoxam disinsection agent.
It is grouped according to different insecticides, every group prepares in worm's ovum, larva, the crust that goes out of adult three phases respectively
Each 1000 of worm, then uses insecticide respectively to the beetle in each stage, tests the eradicative rate of every group of insecticide, such as
Shown in following table:
Killing effect of the insecticide of table one to beetle
As seen from the above table, each group insecticide is to larval beetle killing rate highest, and the insecticidal effect of this product is the most
Excellent, insect killing effect is notable, and the worm's ovum for being most difficult to kill also has preferable insect killing effect.
Embodiment 3:
The present embodiment verifies eradicative rate of the pharmaceutical composition to various insects.
Choose beetle, penthaleus major duges, mole cricket, red spider, chafer, scale insect, volume noctuid, leafhopper, pear sucker, root knot
Each 10000 of nematode, and be grouped respectively, the decoction of same concentrations is made in the medicine being prepared using embodiment 1, respectively to every
The insect of group is sprayed, and after 1 hour, checks the eradicative rate of various insects, as a result as shown in the table:
Insect killing effect of the medicine of table two to various insects
Group | Eradicative rate (%) |
Beetle | 99.96 |
Scale insect | 10.32 |
Penthaleus major duges | 9.65 |
Mole cricket | 8.75 |
Red spider | 1.02 |
Chafer | 0 |
Leafhopper | 0 |
Root-knot nematode | 1.01 |
Roll up noctuid | 0 |
Pear sucker | 1.24 |
As seen from the above table, the medicine that embodiment 1 is prepared, only there is preferable insect killing effect to beetle, to other evils
The insect killing effect of worm is very limited, and thus its specific aim of provable this product is stronger, is only capable of using killing for beetle.
Claims (5)
1. a kind of pharmaceutical composition used for beetle, it is characterised in that including Nidus Vespae extract, fructus ulmi extract, thunder
Public boisiana extract, chun spicebush root extract, Ran She le extract, Periostracum Cicadae extract, Radix Gentianae Macrophyllae extract, iris extract, the root of langdu carry
Take thing and nimbin.
2. a kind of pharmaceutical composition used for beetle according to claim 1, it is characterised in that molten per 100ml
Liquid contains equivalent to the Nidus Vespae extract of 5-20g honeycomb medicinal materials, the fructus ulmi extract of 5-20g fructus ulmi medicinal materials, 5-20g tripterygium wilfordiis
Triperygium wilfordii extractive, chun spicebush root extract, Ran She le extract, the 5- of 5-20g Ran She le medicinal materials of 5-20g chun spicebush root medicinal materials
The Periostracum Cicadae extract of 20g cicada slough medicinal materials, the Radix Gentianae Macrophyllae extract of 5-20g gentiana macrophylla medicines, 5-20g iris medicinal materials iris extract,
The root of langdu extract of 5-20g root of langdu medicinal materials, Nidus Vespae extract, fructus ulmi extract, triperygium wilfordii extractive, chun spicebush root extract, boa
She le extract, Periostracum Cicadae extract, Radix Gentianae Macrophyllae extract, iris extract, the usage ratio of root of langdu extract medicinal material are 1:2:2:
3:3:1:2:2:2.
A kind of 3. pharmaceutical composition used for beetle according to claim 1, it is characterised in that the nimbin
Dosage be 0.005g~5.0g/100ml.
A kind of 4. pharmaceutical composition used for beetle according to claim 3, it is characterised in that the nimbin
Dosage be 0.05g~1.0g/100ml.
A kind of 5. pharmaceutical composition used for beetle according to claim 1 ~ 4 any one, it is characterised in that
Described pharmaceutical composition formulation is powder pin or freezed.
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CN201711094529.4A CN107668092A (en) | 2017-11-09 | 2017-11-09 | A kind of pharmaceutical composition used for beetle |
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CN201711094529.4A CN107668092A (en) | 2017-11-09 | 2017-11-09 | A kind of pharmaceutical composition used for beetle |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109526663A (en) * | 2018-11-17 | 2019-03-29 | 安徽阜阳金丰生态农业有限公司 | A kind of ecological insect-prevention method of potted lotus |
-
2017
- 2017-11-09 CN CN201711094529.4A patent/CN107668092A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109526663A (en) * | 2018-11-17 | 2019-03-29 | 安徽阜阳金丰生态农业有限公司 | A kind of ecological insect-prevention method of potted lotus |
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