CN107889852A - A kind of quick-acting pharmaceutical compositions for killing heart-eating worm - Google Patents
A kind of quick-acting pharmaceutical compositions for killing heart-eating worm Download PDFInfo
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- CN107889852A CN107889852A CN201711094538.3A CN201711094538A CN107889852A CN 107889852 A CN107889852 A CN 107889852A CN 201711094538 A CN201711094538 A CN 201711094538A CN 107889852 A CN107889852 A CN 107889852A
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- extract
- heart
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- eating worm
- pharmaceutical compositions
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
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- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
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- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Pest Control & Pesticides (AREA)
- Virology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of quick-acting pharmaceutical compositions for killing heart-eating worm, including pepper extract, fruit of Rangoon creeper's extract, Semen Pharbitidis extract, Artemisinin, Semen Pruni extract, Scorpio extract, Rhizoma Polygonati Odorati extract, taro pod extract, cinnamomum cassia extract and toosendanin.Heretofore described pharmaceutical composition can targetedly kill heart-eating worm, it is and without any side effects to the natural enemy of heart-eating worm, security is good, it is biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small;With preferable permeability and wettability, the central nervous system of polypide is disturbed, suppresses worm's ovum synthesis development, is not susceptible to drug resistance;Quick-acting is good, is adapted to the wide popularization and application in terms of control of insect.
Description
Technical field
The invention belongs to agricultural technology development field, in particular it relates to a kind of quick-acting pharmaceutical compositions for killing heart-eating worm.
Background technology
Chemical agent plays an important role in terms of crop pest control, but the residual of medicine causes nature
The ecosystem is worsening, and this has turned into international common concern and key subjects urgently to be resolved hurrily.Since China, twentieth century
Because single use chemical pesticide causes agricultural product harmful element exceeded, health and the existence of the people are directly endangered, therefore, state
Family pays much attention to and formulated《Medium-term and long-term scientific and technical development program outline》, it is therefore intended that encourage research and development environment-friendly type fertilizer, agriculture
Medicine." seeking speed " psychology of current peasant is incompatible, and most farmers are still selected using high poison, the chemical pesticide of high residue, this
Chemical pesticide can use only for crop, i.e., kill each class pest for certain crop simultaneously.But this chemical pesticide exists
Today of green and environmental protection is advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, further, since insect
The difference of species, cause each class pest to occur larger difference in terms of the resistance to the action of a drug and drug resistance, so just make killing for chemical agent
Easily there is resistance insect in worm effect, therefore propose to prevent specific insect from just seeming for the insect-proof agent of different insects to have very much must
Will, but yet there are no corresponding report.
The content of the invention
It is good that the technical problems to be solved by the invention are to provide a kind of security, biodegradable good, pollution-free and excitant
Smell, no environment toxic action, in animal body noresidue, specific aim kill the pharmaceutical composition of heart-eating worm.
Technical scheme is used by the present invention solves above-mentioned technical problem:A kind of quick-acting drug regimens for killing heart-eating worm
Thing, including pepper extract, fruit of Rangoon creeper's extract, Semen Pharbitidis extract, Artemisinin, Semen Pruni extract, scorpio extraction
Thing, Rhizoma Polygonati Odorati extract, taro pod extract, cinnamomum cassia extract and toosendanin.
In order to which the present invention is better achieved, further, contain the Chinese prickly ash equivalent to 10-35g Chinese prickly ash medicinal materials per 100ml solution
Extract, fruit of Rangoon creeper's extract of 10-35g fruit of Rangoon creeper's medicinal materials, the Semen Pharbitidis extract of 10-35g kaladana's medicinal material, 10-35g are blue or green
The Artemisinin of wormwood artemisia medicinal material, the Semen Pruni extract of 10-35g brush-cherry seed medicinal materials, 10-35g scorpio medicinal materials Scorpio extract,
The Rhizoma Polygonati Odorati extract of 10-35g radix polygonati officinalis medicinal materials, the taro pod extract of 10-35g taro pod medicinal materials, the Chinese cassia tree of 10-35g Chinese cassia tree medicinal materials carry
Take thing, pepper extract, fruit of Rangoon creeper's extract, Semen Pharbitidis extract, Artemisinin, Semen Pruni extract, Scorpio extract,
Rhizoma Polygonati Odorati extract, taro pod extract, the usage ratio of cinnamomum cassia extract medicinal material are 1:2:2:3:3:1:2:2:2.
In order to which the present invention is better achieved, further, the dosage of the toosendanin is 0.005g~5.0g/100ml.
In order to which the present invention is better achieved, further, the dosage of the toosendanin is 0.05g~1.0g/100ml.
In order to which the present invention is better achieved, further, described pharmaceutical composition formulation is powder pin or freezed.
The preparation method of the pharmaceutical composition of above-mentioned poisoning heart-eating worm is prepared, is comprised the steps:
(1) pharmaceutical composition raw medicinal material Chinese prickly ash 50g, fruit of Rangoon creeper 100g, the kaladana 100g of heart-eating worm, sweet wormwood are killed
200g, brush-cherry seed 200g, scorpio 100g, radix polygonati officinalis 100g, taro pod 100g, Chinese cassia tree 100g, toosendanin 3g;
(2) Chinese prickly ash, the fruit of Rangoon creeper, kaladana add water to cook secondary, 2 hours every time, collecting decoction, add ethanol filtering and concentrating,
Add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby;
(3) sweet wormwood, brush-cherry seed, scorpio, radix polygonati officinalis, taro pod, Chinese cassia tree add water to cook secondary, 1 hour every time, collecting decoction, filter
Cross, concentrate filtrate, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relative density
For 1.20, it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and filtrate is concentrated into relative density as 1.30, adds 3 times of amounts
Water, it is sufficiently stirred, refrigerates 48 hours, filtration, it is 1.15 that filtrate, which is concentrated into relative density,
(4) merge with above-mentioned all decoctions, add 2 times of amount water, be sufficiently stirred, refrigerate 24 hours, filtration, filtrate adds melia toosendan
Element and deionized water water are configured to 1000ml solution, stir evenly, the relative density when relative density of above-mentioned each filtrate is 80 DEG C;
(5) solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution;
(6) filter, it is filling, sterilizing, produce.
The present invention compared with prior art, has advantages below and beneficial effect:
(1) heretofore described pharmaceutical composition can targetedly kill heart-eating worm, and to the natural enemy of heart-eating worm without
Any toxic side effect, security is good, biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body
Noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small;
(2) low raw-material cost used in heretofore described pharmaceutical composition, there is preferable permeability and wet
Lubricant nature, easily breaks through heart-eating worm wax coat, and depth destroys the epidermal structure of polypide and internal protein, makes heart-eating worm be not easy to send out
Raw drug resistance;
(3) heretofore described pharmaceutical composition can interfere with the central nervous system of polypide, suppress worm's ovum synthesis hair
Educate;
(4) heretofore described pharmaceutical composition quick-acting is good, and after spray, heart-eating worm stopped eating in 20~40 minutes
Death, it is adapted to the wide popularization and application in terms of control of insect.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this
Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention
Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in
In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1:
The present embodiment provides a kind of quick-acting pharmaceutical compositions for killing heart-eating worm, including pepper extract, fruit of Rangoon creeper's extraction
Thing, Semen Pharbitidis extract, Artemisinin, Semen Pruni extract, Scorpio extract, Rhizoma Polygonati Odorati extract, taro pod extract, Chinese cassia tree
Extract and toosendanin, its component are as follows:
Its preparation method:Chinese prickly ash, the fruit of Rangoon creeper, kaladana add water to cook secondary, 2 hours every time, collecting decoction, add ethanol mistake
Filter concentration, add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, decoction
It is standby;Sweet wormwood, brush-cherry seed, scorpio, radix polygonati officinalis, taro pod, Chinese cassia tree add water to cook it is secondary, 1 hour every time, collecting decoction, filter, concentration
Filtrate, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.20 that filtrate decompression, which is concentrated into relative density,
It is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.30 that filtrate, which is concentrated into relative density, adds 3 times of amount water, fully
Stirring, refrigerate 48 hours, filtration, filtrate is concentrated into relative density as 1.15;Merge with above-mentioned all decoctions, add 2 times of amount water, fill
Point stirring, is refrigerated 24 hours, filtration, filtrate adds toosendanin and deionized water water and is configured to 1000ml solution, stirs evenly, above-mentioned each
The relative density when relative density of filtrate is 80 DEG C;Solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution;Filtering,
It is filling, sterilizing, produce.
Wherein, the process for adding ethanol filtering and concentrating is first to filter to get filtrate, and filtrate decompression is concentrated into relative density as 1.27
~1.30, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and decompression filtrate recycling ethanol is simultaneously concentrated into relative
Density is 1.30.Filtrate is concentrated into relative density as 1.25~1.30.The mass percent of the sodium hydroxide solution used is
20%.Solution uses filtering with microporous membrane.
Embodiment 2:
The present embodiment verifies that the pharmaceutical composition insecticide common with market is compared, to the eradicative rate of heart-eating worm.
Choose insecticide common on the market:Pale purple purple spore bacterium aqua, nematode killing agent, the agent of special efficacy root line, thiamethoxam disinsection agent.
It is grouped according to different insecticides, every group prepares to eat the heart in worm's ovum, larva, going out for adult three phases respectively
Each 1000 of worm, then uses insecticide respectively to the heart-eating worm in each stage, tests the eradicative rate of every group of insecticide, such as
Shown in following table:
Killing effect of the insecticide of table one to heart-eating worm
As seen from the above table, each group insecticide is to larval heart-eating worm killing rate highest, and the insecticidal effect of this product is the most
Excellent, insect killing effect is notable, and the worm's ovum for being most difficult to kill also has preferable insect killing effect.
Embodiment 3:
The present embodiment verifies eradicative rate of the pharmaceutical composition to various insects.
Choose heart-eating worm, beetle, mole cricket, red spider, chafer, scale insect, volume noctuid, leafhopper, pear sucker, root knot line
Each 10000 of worm, and be grouped respectively, the decoction of same concentrations is made in the medicine being prepared using embodiment 1, respectively to every group
Insect sprayed, after 1 hour, check the eradicative rate of various insects, it is as a result as shown in the table:
Insect killing effect of the medicine of table two to various insects
Group | Eradicative rate (%) |
Heart-eating worm | 99.96 |
Scale insect | 10.32 |
Beetle | 9.65 |
Mole cricket | 8.75 |
Red spider | 1.02 |
Chafer | 0 |
Leafhopper | 0 |
Root-knot nematode | 1.01 |
Roll up noctuid | 0 |
Pear sucker | 1.24 |
As seen from the above table, the medicine that embodiment 1 is prepared, only there is preferable insect killing effect to heart-eating worm, to other evils
The insect killing effect of worm is very limited, and thus its specific aim of provable this product is stronger, is only capable of using killing for heart-eating worm.
Claims (5)
- A kind of 1. quick-acting pharmaceutical compositions for killing heart-eating worm, it is characterised in that including pepper extract, fruit of Rangoon creeper's extract, Semen Pharbitidis extract, Artemisinin, Semen Pruni extract, Scorpio extract, Rhizoma Polygonati Odorati extract, taro pod extract, Chinese cassia tree carry Take thing and toosendanin.
- 2. a kind of quick-acting pharmaceutical compositions for killing heart-eating worm according to claim 1, it is characterised in that molten per 100ml Liquid contains to be led equivalent to the pepper extract of 10-35g Chinese prickly ash medicinal materials, fruit of Rangoon creeper's extract, the 10-35g of 10-35g fruit of Rangoon creeper's medicinal materials The Semen Pharbitidis extract of ox medicinal material, the Artemisinin of 10-35g Artemisia annuas, the brush-cherry seed of 10-35g brush-cherry seed medicinal materials carry Take thing, the Scorpio extract of 10-35g scorpio medicinal materials, the Rhizoma Polygonati Odorati extract of 10-35g radix polygonati officinalis medicinal materials, the taro of 10-35g taro pod medicinal materials The cinnamomum cassia extract of pod extract, 10-35g Chinese cassia tree medicinal materials, pepper extract, fruit of Rangoon creeper's extract, Semen Pharbitidis extract, sweet wormwood Extract, Semen Pruni extract, Scorpio extract, Rhizoma Polygonati Odorati extract, taro pod extract, the usage ratio of cinnamomum cassia extract medicinal material For 1:2:2:3:3:1:2:2:2.
- A kind of 3. quick-acting pharmaceutical compositions for killing heart-eating worm according to claim 1, it is characterised in that the toosendanin Dosage be 0.005g~5.0g/100ml.
- A kind of 4. quick-acting pharmaceutical compositions for killing heart-eating worm according to claim 3, it is characterised in that the toosendanin Dosage be 0.05g~1.0g/100ml.
- A kind of 5. quick-acting pharmaceutical compositions for killing heart-eating worm according to claim 1 ~ 4 any one, it is characterised in that Described pharmaceutical composition formulation is powder pin or freezed.
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CN201711094538.3A CN107889852A (en) | 2017-11-09 | 2017-11-09 | A kind of quick-acting pharmaceutical compositions for killing heart-eating worm |
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CN201711094538.3A CN107889852A (en) | 2017-11-09 | 2017-11-09 | A kind of quick-acting pharmaceutical compositions for killing heart-eating worm |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111529574A (en) * | 2020-06-29 | 2020-08-14 | 北京生泰尔科技股份有限公司 | Medicinal composition for resisting ichthyophthirius multifiliis and preparation method thereof |
-
2017
- 2017-11-09 CN CN201711094538.3A patent/CN107889852A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111529574A (en) * | 2020-06-29 | 2020-08-14 | 北京生泰尔科技股份有限公司 | Medicinal composition for resisting ichthyophthirius multifiliis and preparation method thereof |
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Application publication date: 20180410 |