CN107873758A - A kind of pharmaceutical composition for killing suction pulp worm - Google Patents
A kind of pharmaceutical composition for killing suction pulp worm Download PDFInfo
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- CN107873758A CN107873758A CN201711094506.3A CN201711094506A CN107873758A CN 107873758 A CN107873758 A CN 107873758A CN 201711094506 A CN201711094506 A CN 201711094506A CN 107873758 A CN107873758 A CN 107873758A
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- extract
- pharmaceutical composition
- killing
- medicinal materials
- suction pulp
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/18—Mercury
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Wood Science & Technology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of pharmaceutical composition for killing suction pulp worm, including Alumen extract, pepper extract, calomel mercurous chloride extract, acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, Agkistrodon extract, Radix Flemingiae Philippinensis extract, chun spicebush root extract and matrine.Heretofore described pharmaceutical composition can targetedly kill suction pulp worm, it is and without any side effects to the natural enemy of suction pulp worm, security is good, it is biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small；With preferable permeability and wettability, the central nervous system of polypide is disturbed, suppresses worm's ovum synthesis development, is not susceptible to drug resistance；Quick-acting is good, is adapted to the wide popularization and application in terms of control of insect.
Description
Technical field
The invention belongs to agricultural technology development field, in particular it relates to a kind of pharmaceutical composition for killing suction pulp worm.
Background technology
Chemical agent plays an important role in terms of crop pest control, but the residual of medicine causes nature
The ecosystem is worsening, and this has turned into international common concern and key subjects urgently to be resolved hurrily.Since China, twentieth century
Because single use chemical pesticide causes agricultural product harmful element exceeded, health and the existence of the people are directly endangered, therefore, state
Family pays much attention to and formulated《Medium-term and long-term scientific and technical development program outline》, it is therefore intended that encourage research and development environment-friendly type fertilizer, agriculture
Medicine." seeking speed " psychology of current peasant is incompatible, and most farmers are still selected using high poison, the chemical pesticide of high residue, this
Chemical pesticide can use only for crop, i.e., kill each class pest for certain crop simultaneously.But this chemical pesticide exists
Today of green and environmental protection is advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, further, since insect
The difference of species, cause each class pest to occur larger difference in terms of the resistance to the action of a drug and drug resistance, so just make killing for chemical agent
Easily there is resistance insect in worm effect, therefore propose to prevent specific insect from just seeming for the insect-proof agent of different insects to have very much must
Will, but yet there are no corresponding report.
The content of the invention
It is good that the technical problems to be solved by the invention are to provide a kind of security, biodegradable good, pollution-free and excitant
Smell, no environment toxic action, in animal body noresidue, specific aim kill the pharmaceutical composition of suction pulp worm.
Technical scheme is used by the present invention solves above-mentioned technical problem：A kind of pharmaceutical composition for killing suction pulp worm,
Including Alumen extract, pepper extract, calomel mercurous chloride extract, acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, long-nosed pit viper
Extract, Radix Flemingiae Philippinensis extract, chun spicebush root extract and matrine.
In order to which the present invention is better achieved, further, contain the alum equivalent to 10-20g alum medicinal materials per 100ml solution
Extract, the pepper extract of 10-20g Chinese prickly ash medicinal materials, the calomel mercurous chloride extract of 10-20g calomel mercurous chloride medicinal materials, 10-20g acupuncture needle head medicinal materials
Acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, the 10-20g of 10-20g Chinese cassia tree medicinal materials of 10-20g root tuber of aromatic turmeric medicinal materials beg
The Agkistrodon extract of antidote for snakebite material, the Radix Flemingiae Philippinensis extract of 10-20g waras medicinal materials, the chun spicebush root of 10-20g chun spicebush root medicinal materials carry
Take thing, Alumen extract, pepper extract, calomel mercurous chloride extract, acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, long-nosed pit viper
Extract, Radix Flemingiae Philippinensis extract, the usage ratio of chun spicebush root extract medicinal material are 1：1：1：1：5：3：3：2：6.
In order to which the present invention is better achieved, further, the dosage of the matrine is 0.08g~5.0g/100ml.
In order to which the present invention is better achieved, further, the dosage of the matrine is 0.05g~1.0g/100ml.
In order to which the present invention is better achieved, further, described pharmaceutical composition formulation is powder pin or freezed.
The preparation method of the pharmaceutical composition of above-mentioned killing suction pulp worm is prepared, is comprised the steps：
(1) pharmaceutical composition raw medicinal material alum 40g, Chinese prickly ash 40g, the calomel mercurous chloride 40g of suction pulp worm are killed, it is acupuncture needle head 40g, strongly fragrant
Golden 200g, Chinese cassia tree 120g, long-nosed pit viper 120g, waras 80g, chun spicebush root 160g, matrine 20g；
(2) alum, Chinese prickly ash, calomel mercurous chloride add water to cook secondary, 2 hours every time, collecting decoction, add ethanol filtering and concentrating, add 3 times
Water is measured, is sufficiently stirred, is refrigerated 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby；
(3) acupuncture needle head, root tuber of aromatic turmeric, Chinese cassia tree, long-nosed pit viper, waras, chun spicebush root add water to cook secondary, 1 hour every time, merge and decoct
Liquid, filtration, filtrate is concentrated, is let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relatively
Density is 1.20, and it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, it is 1.30 that filtrate, which is concentrated into relative density, adds 3
Amount water again, is sufficiently stirred, and refrigerates 48 hours, filtration, and it is 1.15 that filtrate, which is concentrated into relative density,
(4) merge with above-mentioned all decoctions, add 2 times of amount water, be sufficiently stirred, refrigerate 24 hours, filtration, filtrate adds kuh-seng
Alkali and deionized water water are configured to 1000ml solution, stir evenly, the relative density when relative density of above-mentioned each filtrate is 80 DEG C；
(5) solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution；
(6) filter, it is filling, sterilizing, produce.
The present invention compared with prior art, has advantages below and beneficial effect：
(1) heretofore described pharmaceutical composition can targetedly kill suction pulp worm, and to the natural enemy of suction pulp worm without
Any toxic side effect, security is good, biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body
Noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small；
(2) low raw-material cost used in heretofore described pharmaceutical composition, there is preferable permeability and wet
Lubricant nature, easily breaks through suction pulp worm wax coat, and depth destroys the epidermal structure of polypide and internal protein, makes suction pulp worm be not easy to send out
Raw drug resistance；
(3) heretofore described pharmaceutical composition can interfere with the central nervous system of polypide, suppress worm's ovum synthesis hair
Educate；
(4) heretofore described pharmaceutical composition quick-acting is good, and after spray, suction pulp worm was stopped eating in 20~40 minutes
Death, it is adapted to the wide popularization and application in terms of control of insect.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this
Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention
Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in
In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1：
The present embodiment provides a kind of pharmaceutical composition for killing suction pulp worm, including Alumen extract, pepper extract, calomel mercurous chloride
Extract, acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, Agkistrodon extract, Radix Flemingiae Philippinensis extract, chun spicebush root extraction
Thing and matrine, its component are as follows：
Its preparation method：Alum, Chinese prickly ash, calomel mercurous chloride add water to cook it is secondary, 2 hours every time, collecting decoction, add ethanol filtering it is dense
Contracting, add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby
With；Acupuncture needle head, root tuber of aromatic turmeric, Chinese cassia tree, long-nosed pit viper, waras, chun spicebush root add water to cook it is secondary, 1 hour every time, collecting decoction, filtration, it is dense
Contracting filtrate, lets cool, and it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relative density and is
1.20, it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.30 that filtrate, which is concentrated into relative density, adds 3 times of amount water,
It is sufficiently stirred, refrigerates 48 hours, filtration, filtrate is concentrated into relative density as 1.15；Merge with above-mentioned all decoctions, add 2 times of amounts
Water, it is sufficiently stirred, refrigerates 24 hours, filtration, filtrate adds matrine and deionized water water is configured to 1000ml solution, stirs evenly,
The relative density when relative density of above-mentioned each filtrate is 80 DEG C；Solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution；
Filtering, it is filling, sterilizing, produce.
Wherein, the process for adding ethanol filtering and concentrating is first to filter to get filtrate, and filtrate decompression is concentrated into relative density as 1.27
~1.30, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and decompression filtrate recycling ethanol is simultaneously concentrated into relative
Density is 1.30.Filtrate is concentrated into relative density as 1.25~1.30.The mass percent of the sodium hydroxide solution used is
20%.Solution uses filtering with microporous membrane.
Embodiment 2：
The present embodiment verifies that the pharmaceutical composition insecticide common with market is compared, to the eradicative rate of suction pulp worm.
Choose insecticide common on the market：Pale purple purple spore bacterium aqua, nematode killing agent, the agent of special efficacy root line, thiamethoxam disinsection agent.
It is grouped according to different insecticides, every group prepares in worm's ovum, larva, the suction pulp worm of adult three phases respectively
Each 1000, insecticide is then used respectively to the suction pulp worm in each stage, tests the eradicative rate of every group of insecticide, it is as follows
Shown in table：
Killing effect of the insecticide of table one to suction pulp worm
As seen from the above table, each group insecticide is to larval suction pulp worm killing rate highest, and the insecticidal effect of this product is the most
Excellent, insect killing effect is notable, and the worm's ovum for being most difficult to kill also has preferable insect killing effect.
Embodiment 3：
The present embodiment verifies eradicative rate of the pharmaceutical composition to various insects.
It is each to choose chafer, beetle, leafhopper, heart-eating worm, pear sucker, scale insect, volume noctuid, mole cricket, fore-telling mud, suction pulp worm
10000, and be grouped respectively, the decoction of same concentrations is made in the medicine being prepared using embodiment 1, respectively the evil to every group
Worm is sprayed, and after 1 hour, checks the eradicative rate of various insects, as a result as shown in the table：
Insect killing effect of the medicine of table two to various insects
| Group | Eradicative rate (%) |
| Suction pulp worm | 99.69 |
| Chafer | 10.32 |
| Beetle | 9.65 |
| Leafhopper | 8.75 |
| Heart-eating worm | 1.02 |
| Pear sucker | 0 |
| Scale insect | 0 |
| Roll up noctuid | 1.01 |
| Mole cricket | 0 |
| Foretell mud | 1.24 |
As seen from the above table, the medicine that embodiment 1 is prepared, only there is preferable insect killing effect to suction pulp worm, to other evils
The insect killing effect of worm is very limited, and thus its specific aim of provable this product is stronger, is only capable of using killing for suction pulp worm.
Claims (5)
1. a kind of pharmaceutical composition for killing suction pulp worm, it is characterised in that carried including Alumen extract, pepper extract, calomel mercurous chloride
Take thing, acupuncture needle head extract, Radix Curcumae extract, cinnamomum cassia extract, Agkistrodon extract, Radix Flemingiae Philippinensis extract, chun spicebush root extract
And matrine.
2. a kind of pharmaceutical composition for killing suction pulp worm according to claim 1, it is characterised in that contain per 100ml solution
The pepper extract of Alumen extract, 10-20g Chinese prickly ash medicinal materials equivalent to 10-20g alum medicinal materials, 10-20g calomel mercurous chloride medicinal materials
Calomel mercurous chloride extract, the acupuncture needle head extract of 10-20g acupuncture needle head medicinal materials, Radix Curcumae extract, the 10-20g meat of 10-20g root tuber of aromatic turmeric medicinal materials
The cinnamomum cassia extract of osmanthus medicinal material, the Agkistrodon extract of 10-20g long-nosed pit viper medicinal materials, 10-20g waras medicinal materials Radix Flemingiae Philippinensis extract,
The chun spicebush root extract of 10-20g chun spicebush root medicinal materials, Alumen extract, pepper extract, calomel mercurous chloride extract, acupuncture needle head extract,
Radix Curcumae extract, cinnamomum cassia extract, Agkistrodon extract, Radix Flemingiae Philippinensis extract, the usage ratio of chun spicebush root extract medicinal material are 1：
1：1：1：5：3：3：2：6.
A kind of 3. pharmaceutical composition for killing suction pulp worm according to claim 1, it is characterised in that the use of the matrine
Measure as 0.08g~5.0g/100ml.
A kind of 4. pharmaceutical composition for killing suction pulp worm according to claim 3, it is characterised in that the use of the matrine
Measure as 0.05g~1.0g/100ml.
5. the pharmaceutical composition of a kind of killing suction pulp worm according to claim 1 ~ 4 any one, it is characterised in that described
Medicine composition dosage form is powder pin or freezed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711094506.3A CN107873758A (en) | 2017-11-09 | 2017-11-09 | A kind of pharmaceutical composition for killing suction pulp worm |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711094506.3A CN107873758A (en) | 2017-11-09 | 2017-11-09 | A kind of pharmaceutical composition for killing suction pulp worm |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107873758A true CN107873758A (en) | 2018-04-06 |
Family
ID=61779525
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711094506.3A Pending CN107873758A (en) | 2017-11-09 | 2017-11-09 | A kind of pharmaceutical composition for killing suction pulp worm |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107873758A (en) |
-
2017
- 2017-11-09 CN CN201711094506.3A patent/CN107873758A/en active Pending
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180406 |
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| WD01 | Invention patent application deemed withdrawn after publication |