CN107821479A - A kind of volume noctuid killing agent free from environmental pollution - Google Patents

A kind of volume noctuid killing agent free from environmental pollution Download PDF

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Publication number
CN107821479A
CN107821479A CN201711094568.4A CN201711094568A CN107821479A CN 107821479 A CN107821479 A CN 107821479A CN 201711094568 A CN201711094568 A CN 201711094568A CN 107821479 A CN107821479 A CN 107821479A
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China
Prior art keywords
extract
noctuid
environmental pollution
killing agent
root
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Pending
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CN201711094568.4A
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Chinese (zh)
Inventor
黄伟
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Chengdu Aibike Biotechnology Co Ltd
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Chengdu Aibike Biotechnology Co Ltd
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Priority to CN201711094568.4A priority Critical patent/CN107821479A/en
Publication of CN107821479A publication Critical patent/CN107821479A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10—Animals; Substances produced thereby or obtained therefrom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Pest Control & Pesticides (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Virology (AREA)
  • Toxicology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of volume noctuid killing agent free from environmental pollution, including Nidus Vespae extract, aloe extract, triperygium wilfordii extractive, radish English extract, houttuynia extract, root of langdu extract, small extract of reviving after death, cholla stem extract, Fructus Canarii extract and Osthole.Heretofore described pharmaceutical composition can targetedly kill volume noctuid, and the natural enemy to rolling up noctuid is without any side effects, security is good, it is biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small；With preferable permeability and wettability, the central nervous system of polypide is disturbed, suppresses worm's ovum synthesis development, is not susceptible to drug resistance；Quick-acting is good, is adapted to the wide popularization and application in terms of control of insect.

Description

A kind of volume noctuid killing agent free from environmental pollution
Technical field
The invention belongs to agricultural technology development field, in particular it relates to a kind of volume noctuid killing agent free from environmental pollution.
Background technology
Chemical agent plays an important role in terms of crop pest control, but the residual of medicine causes nature The ecosystem is worsening, and this has turned into international common concern and key subjects urgently to be resolved hurrily.Since China, twentieth century Because single use chemical pesticide causes agricultural product harmful element exceeded, health and the existence of the people are directly endangered, therefore, state Family pays much attention to and formulated《Medium-term and long-term scientific and technical development program outline》, it is therefore intended that encourage research and development environment-friendly type fertilizer, agriculture Medicine." seeking speed " psychology of current peasant is incompatible, and most farmers are still selected using high poison, the chemical pesticide of high residue, this Chemical pesticide can use only for crop, i.e., kill each class pest for certain crop simultaneously.But this chemical pesticide exists Today of green and environmental protection is advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, further, since insect The difference of species, cause each class pest to occur larger difference in terms of the resistance to the action of a drug and drug resistance, so just make killing for chemical agent Easily there is resistance insect in worm effect, therefore propose to prevent specific insect from just seeming for the insect-proof agent of different insects to have very much must Will, but yet there are no corresponding report.
The content of the invention
It is good that the technical problems to be solved by the invention are to provide a kind of security, biodegradable good, pollution-free and excitant Smell, no environment toxic action, in animal body noresidue, specific aim volume noctuid killing agent free from environmental pollution.
Technical scheme is used by the present invention solves above-mentioned technical problem：A kind of volume noctuid free from environmental pollution is killed Agent, including the extraction of Nidus Vespae extract, aloe extract, triperygium wilfordii extractive, radish English extract, houttuynia extract, the root of langdu Thing, small extract of reviving after death, cholla stem extract, Fructus Canarii extract and Osthole.
In order to which the present invention is better achieved, further, contain the honeycomb equivalent to 1-10g honeycomb medicinal materials per 100ml solution Extract, the aloe extract of 1-10g aloe medicinal materials, the triperygium wilfordii extractive of 1-10g tripterygium wilfordiis, 1-10g radish English medicines Radish English extract, the houttuynia extract of 1-10g Herba Houttuyniaes, root of langdu extract, the 1- of 1-10g root of langdu medicinal materials of material The small extract of reviving after death of the small medicinal materials of reviving after death of 10g, the cholla stem extract of 1-10g cholla stem medicinal materials, the Chinese olive of 1-10g Chinese olive medicinal materials Extract, Nidus Vespae extract, aloe extract, triperygium wilfordii extractive, radish English extract, houttuynia extract, root of langdu extraction Thing, small extract of reviving after death, cholla stem extract, the usage ratio of Fructus Canarii extract medicinal material are 1：2：1：2：3：2：3：2：3.
In order to which the present invention is better achieved, further, the dosage of the Osthole is 0.005g~5.0g/100ml.
In order to which the present invention is better achieved, further, the dosage of the Osthole is 0.05g~1.0g/100ml.
In order to which the present invention is better achieved, further, described pharmaceutical composition formulation is powder pin or freezed.
The preparation method of above-mentioned volume noctuid killing agent free from environmental pollution is prepared, is comprised the steps：
(1) volume noctuid killing agent raw medicinal material honeycomb 50g free from environmental pollution, aloe 100g, tripterygium wilfordii 50g, radish English 100g, cordate houttuynia 150g, root of langdu 100g, the small 150g that revives after death, cholla stem 100g, Chinese olive 150g, Osthole 3g；
(2) honeycomb, aloe, tripterygium wilfordii add water to cook secondary, 2 hours every time, collecting decoction, add ethanol filtering and concentrating, add 3 Amount water again, is sufficiently stirred, and refrigerates 48 hours, and filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby；
(3) radish English, cordate houttuynia, the root of langdu, it is small revive after death, cholla stem, Chinese olive add water to cook it is secondary, 1 hour every time, merge decoct Liquid, filtration, filtrate is concentrated, is let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relatively Density is 1.20, and it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, it is 1.30 that filtrate, which is concentrated into relative density, adds 3 Amount water again, is sufficiently stirred, and refrigerates 48 hours, filtration, and it is 1.15 that filtrate, which is concentrated into relative density,
(4) merge with above-mentioned all decoctions, add 2 times of amount water, be sufficiently stirred, refrigerate 24 hours, filtration, filtrate adds cnidium monnieri Sub- element and deionized water water are configured to 1000ml solution, stir evenly, relatively close when the relative density of above-mentioned each filtrate is 80 DEG C Degree；
(5) solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution；
(6) filter, it is filling, sterilizing, produce.
The present invention compared with prior art, has advantages below and beneficial effect：
(1) heretofore described pharmaceutical composition can targetedly kill volume noctuid, and to roll up noctuid natural enemy without Any toxic side effect, security is good, biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body Noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small；
(2) low raw-material cost used in heretofore described pharmaceutical composition, there is preferable permeability and wet Lubricant nature, easily breaks through volume noctuid wax coat, and depth destroys the epidermal structure of polypide and internal protein, makes volume noctuid be not easy to send out Raw drug resistance；
(3) heretofore described pharmaceutical composition can interfere with the central nervous system of polypide, suppress worm's ovum synthesis hair Educate；
(4) heretofore described pharmaceutical composition quick-acting is good, and after spray, volume noctuid stopped eating in 20~40 minutes Death, it is adapted to the wide popularization and application in terms of control of insect.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1：
The present embodiment provides a kind of volume noctuid killing agent free from environmental pollution, including Nidus Vespae extract, aloe extract, thunder Public boisiana extract, radish English extract, houttuynia extract, root of langdu extract, small extract of reviving after death, cholla stem extract, green grass or young crops Berry extract and Osthole, its component are as follows：
Its preparation method：Honeycomb, aloe, tripterygium wilfordii add water to cook secondary, 2 hours every time, collecting decoction, add ethanol to filter Concentration, add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby With；Radish English, cordate houttuynia, the root of langdu, it is small revive after death, cholla stem, Chinese olive add water to cook it is secondary, 1 hour every time, collecting decoction, filtration, Filtrate is concentrated, is let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relative density and is 1.20, it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and it is 1.30 that filtrate, which is concentrated into relative density, adds 3 times of amount water, It is sufficiently stirred, refrigerates 48 hours, filtration, filtrate is concentrated into relative density as 1.15；Merge with above-mentioned all decoctions, add 2 times of amounts Water, it is sufficiently stirred, refrigerates 24 hours, filtration, filtrate adds Osthole and deionized water water is configured to 1000ml solution, stirs It is even, the relative density when relative density of above-mentioned each filtrate is 80 DEG C；Solution ph is adjusted to 6.5- with sodium hydroxide solution 8.5；Filtering, it is filling, sterilizing, produce.
Wherein, the process for adding ethanol filtering and concentrating is first to filter to get filtrate, and filtrate decompression is concentrated into relative density as 1.27 ~1.30, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and decompression filtrate recycling ethanol is simultaneously concentrated into relative Density is 1.30.Filtrate is concentrated into relative density as 1.25~1.30.The mass percent of the sodium hydroxide solution used is 20%.Solution uses filtering with microporous membrane.
Embodiment 2：
The present embodiment verifies that the pharmaceutical composition insecticide common with market is compared, the eradicative rate to rolling up noctuid.
Choose insecticide common on the market：Pale purple purple spore bacterium aqua, nematode killing agent, the agent of special efficacy root line, thiamethoxam disinsection agent.
It is grouped according to different insecticides, every group prepares to roll up night in worm's ovum, larva, going out for adult three phases respectively Each 1000 of moth, then uses insecticide respectively to the volume noctuid in each stage, tests the eradicative rate of every group of insecticide, such as Shown in following table：
Killing effect of the insecticide of table one to volume noctuid
As seen from the above table, each group insecticide is to larval volume noctuid killing rate highest, and the insecticidal effect of this product is the most Excellent, insect killing effect is notable, and the worm's ovum for being most difficult to kill also has preferable insect killing effect.
Embodiment 3：
The present embodiment verifies eradicative rate of the pharmaceutical composition to various insects.
Choose chafer, beetle, leafhopper, heart-eating worm, pear sucker, scale insect, volume noctuid, mole cricket, fore-telling mud, root-knot nematode Each 10000, and be grouped respectively, the decoction of same concentrations is made in the medicine being prepared using embodiment 1, respectively to every group Insect is sprayed, and after 1 hour, checks the eradicative rate of various insects, as a result as shown in the table：
Insect killing effect of the medicine of table two to various insects
Group Eradicative rate (%)
Roll up noctuid 99.96
Chafer 10.32
Beetle 9.65
Leafhopper 8.75
Heart-eating worm 1.02
Pear sucker 0
Scale insect 0
Root-knot nematode 1.01
Mole cricket 0
Foretell mud 1.24
As seen from the above table, the medicine that embodiment 1 is prepared, only there is preferable insect killing effect to volume noctuid, to other evils The insect killing effect of worm is very limited, and thus its specific aim of provable this product is stronger, is only capable of using for rolling up killing for noctuid.

Claims (5)

1. a kind of volume noctuid killing agent free from environmental pollution, it is characterised in that including Nidus Vespae extract, aloe extract, Thunder God Boisiana extract, radish English extract, houttuynia extract, root of langdu extract, small extract of reviving after death, cholla stem extract, Chinese olive Extract and Osthole.
2. a kind of volume noctuid killing agent free from environmental pollution according to claim 1, it is characterised in that per 100ml solution Nidus Vespae extract containing equivalent to 1-10g honeycomb medicinal materials, the aloe extracts of 1-10g aloe medicinal materials, 1-10g tripterygium wilfordiis Radish English extract, the houttuynia extract of 1-10g Herba Houttuyniaes, the 1- of triperygium wilfordii extractive, 1-10g radish English medicinal materials Small extract of reviving after death, the cholla stem of 1-10g cholla stem medicinal materials of the small medicinal material of reviving after death of root of langdu extract, 1-10g of 10g root of langdu medicinal materials The Fructus Canarii extract of extract, 1-10g Chinese olive medicinal materials, Nidus Vespae extract, aloe extract, triperygium wilfordii extractive, radish English carry Take thing, houttuynia extract, root of langdu extract, old Lei extracts, cholla stem extract, the usage ratio of Fructus Canarii extract medicinal material For 1：2：1：2：3：2：3：2：3.
A kind of 3. volume noctuid killing agent free from environmental pollution according to claim 1, it is characterised in that the Osthole Dosage be 0.005g~5.0g/100ml.
A kind of 4. volume noctuid killing agent free from environmental pollution according to claim 3, it is characterised in that the Osthole Dosage be 0.05g~1.0g/100ml.
A kind of 5. volume noctuid killing agent free from environmental pollution according to claim 1 ~ 4 any one, it is characterised in that institute Medicine composition dosage form is stated as powder pin or lyophilized.
CN201711094568.4A 2017-11-09 2017-11-09 A kind of volume noctuid killing agent free from environmental pollution Pending CN107821479A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711094568.4A CN107821479A (en) 2017-11-09 2017-11-09 A kind of volume noctuid killing agent free from environmental pollution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711094568.4A CN107821479A (en) 2017-11-09 2017-11-09 A kind of volume noctuid killing agent free from environmental pollution

Publications (1)

Publication Number Publication Date
CN107821479A true CN107821479A (en) 2018-03-23

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Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

Country Link
CN (1) CN107821479A (en)

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Application publication date: 20180323

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