CN107711909A - A kind of pharmaceutical composition for killing aphid - Google Patents

A kind of pharmaceutical composition for killing aphid Download PDF

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Publication number
CN107711909A
CN107711909A CN201711094595.1A CN201711094595A CN107711909A CN 107711909 A CN107711909 A CN 107711909A CN 201711094595 A CN201711094595 A CN 201711094595A CN 107711909 A CN107711909 A CN 107711909A
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China
Prior art keywords
extract
pharmaceutical composition
medicinal materials
aphid
arsenolite
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Pending
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CN201711094595.1A
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Chinese (zh)
Inventor
黄伟
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Chengdu Aibike Biotechnology Co Ltd
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Chengdu Aibike Biotechnology Co Ltd
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Priority to CN201711094595.1A priority Critical patent/CN107711909A/en
Publication of CN107711909A publication Critical patent/CN107711909A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12—Powders or granules
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/30—Polygonaceae [Buckwheat family], e.g. red-knees or rhubarb
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Pest Control & Pesticides (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of pharmaceutical composition for killing aphid, including Folium Callicarpae Formosanae extract, arsenolite extract, gemma agrimoninae extract, clear and bright willow extract, Caulis Lonicerae extract, milfoil extract, cinnamomum cassia extract, Radix Dipsaci extract, Herba polygoni hydropiperis extract and d ichlorbenzuron.Heretofore described pharmaceutical composition can targetedly kill aphid, it is and without any side effects to the natural enemy of aphid, security is good, it is biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body noresidue, the ecological balance is not destroyed, crop growth environment is influenceed small；With preferable permeability and wettability, the central nervous system of polypide is disturbed, suppresses worm's ovum synthesis development, is not susceptible to drug resistance；Quick-acting is good, is adapted to the wide popularization and application in terms of control of insect.

Description

A kind of pharmaceutical composition for killing aphid
Technical field
The invention belongs to agricultural technology development field, in particular it relates to a kind of pharmaceutical composition for killing aphid.
Background technology
Chemical agent plays an important role in terms of crop pest control, but the residual of medicine causes nature The ecosystem is worsening, and this has turned into international common concern and key subjects urgently to be resolved hurrily.Since China, twentieth century Because single use chemical pesticide causes agricultural product harmful element exceeded, health and the existence of the people are directly endangered, therefore, state Family pays much attention to and formulated《Medium-term and long-term scientific and technical development program outline》, it is therefore intended that encourage research and development environment-friendly type fertilizer, agriculture Medicine." seeking speed " psychology of current peasant is incompatible, and most farmers are still selected using high poison, the chemical pesticide of high residue, this Chemical pesticide can use only for crop, i.e., kill each class pest for certain crop simultaneously.But this chemical pesticide exists Today of green and environmental protection is advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, further, since insect The difference of species, cause each class pest to occur larger difference in terms of the resistance to the action of a drug and drug resistance, so just make killing for chemical agent Easily there is resistance insect in worm effect, therefore propose to prevent specific insect from just seeming for the insect-proof agent of different insects to have very much must Will, but yet there are no corresponding report.
The content of the invention
It is good that the technical problems to be solved by the invention are to provide a kind of security, biodegradable good, pollution-free and excitant Smell, no environment toxic action, in animal body noresidue, specific aim kill the pharmaceutical composition of aphid.
Technical scheme is used by the present invention solves above-mentioned technical problem：A kind of pharmaceutical composition for killing aphid, bag Include Folium Callicarpae Formosanae extract, arsenolite extract, gemma agrimoninae extract, clear and bright willow extract, Caulis Lonicerae extract, milfoil extract, Cinnamomum cassia extract, Radix Dipsaci extract, Herba polygoni hydropiperis extract and d ichlorbenzuron.
In order to which the present invention is better achieved, further, contain the purple equivalent to 10-25g folium callicarpae pedunculatae medicinal materials per 100ml solution Pearl leaf extract, the arsenolite extract of 10-25g arsenolite medicinal materials, gemma agrimoninae extract, the 10-25g of 10-25g gemma agrimoninae medicinal materials are clear The clear and bright willow extract of bright willow medicinal material, the Caulis Lonicerae extract of 10-25g caulis lonicerae medicinal materials, the milfoil of 10-25g milfoil medicinal materials carry Take thing, the cinnamomum cassia extract of 10-25g Chinese cassia tree medicinal materials, the Radix Dipsaci extract of 10-25g teasel root medicinal materials, 10-25g polygonum flaccidum medicinal materials it is peppery Knotweed extract, Folium Callicarpae Formosanae extract, arsenolite extract, gemma agrimoninae extract, clear and bright willow extract, Caulis Lonicerae extract, milfoil Extract, cinnamomum cassia extract, Radix Dipsaci extract, the usage ratio of Herba polygoni hydropiperis extract medicinal material are 1：2：1：3：5：4：1：2：1.
In order to which the present invention is better achieved, further, the dosage of the d ichlorbenzuron is 0.08g~5.0g/100ml.
In order to which the present invention is better achieved, further, the dosage of the d ichlorbenzuron is 0.05g~1.0g/100ml.
In order to which the present invention is better achieved, further, described pharmaceutical composition formulation is powder pin or freezed.
The preparation method of the pharmaceutical composition of above-mentioned killing aphid is prepared, is comprised the steps：
(1) pharmaceutical composition raw medicinal material folium callicarpae pedunculatae 50g, arsenolite 100g, the gemma agrimoninae 50g of aphid, clear and bright willow are killed 150g, caulis lonicerae 250g, milfoil 200g, Chinese cassia tree 50g, teasel root 100g, polygonum flaccidum 50g, d ichlorbenzuron 20g；
(2) folium callicarpae pedunculatae, arsenolite, gemma agrimoninae add water to cook secondary, 2 hours every time, collecting decoction, add ethanol filtering and concentrating, Add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, and decoction is standby；
(3) clear and bright willow, caulis lonicerae, milfoil, Chinese cassia tree, teasel root, polygonum flaccidum add water to cook secondary, 1 hour every time, collecting decoction, Filtration, filtrate is concentrated, is let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relatively close Spend for 1.20, it is 70% to add ethanol to make containing amount of alcohol, stands overnight, filters, and filtrate is concentrated into relative density as 1.30, adds 3 times Water to be measured, is sufficiently stirred, is refrigerated 48 hours, filtration, it is 1.15 that filtrate, which is concentrated into relative density,
(4) merge with above-mentioned all decoctions, add 2 times of amount water, be sufficiently stirred, refrigerate 24 hours, filtration, filtrate adds children of going out Urea and deionized water water are configured to 1000ml solution, stir evenly, the relative density when relative density of above-mentioned each filtrate is 80 DEG C；
(5) solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution；
(6) filter, it is filling, sterilizing, produce.
The present invention compared with prior art, has advantages below and beneficial effect：
(1) heretofore described pharmaceutical composition can targetedly kill aphid, and to the natural enemy of aphid without any Toxic side effect, security is good, biodegradable good, pollution-free and penetrating odor, no environment toxic action, in animal body without residual Thing is stayed, does not destroy the ecological balance, crop growth environment is influenceed small；
(2) low raw-material cost used in heretofore described pharmaceutical composition, there is preferable permeability and wet Lubricant nature, easily breaks through aphid wax coat, and depth destroys the epidermal structure of polypide and internal protein, is not susceptible to aphid resistance to The property of medicine；
(3) heretofore described pharmaceutical composition can interfere with the central nervous system of polypide, suppress worm's ovum synthesis hair Educate；
(4) heretofore described pharmaceutical composition quick-acting is good, and after spray, aphid stopped eating dead in 20~40 minutes Die, be adapted to the wide popularization and application in terms of control of insect.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1：
The present embodiment provides a kind of pharmaceutical composition for killing aphid, including Folium Callicarpae Formosanae extract, arsenolite extract, crane grass Bud extract, clear and bright willow extract, Caulis Lonicerae extract, milfoil extract, cinnamomum cassia extract, Radix Dipsaci extract, polygonum flaccidum extraction Thing and d ichlorbenzuron, its component are as follows：
Its preparation method：Folium callicarpae pedunculatae, arsenolite, gemma agrimoninae add water to cook secondary, 2 hours every time, collecting decoction, add ethanol mistake Filter concentration, add 3 times of amount water, be sufficiently stirred, refrigerate 48 hours, filtration, it is about 1.15 that filtrate decompression, which is concentrated into relative density, decoction It is standby；Clear and bright willow, caulis lonicerae, milfoil, Chinese cassia tree, teasel root, polygonum flaccidum add water to cook it is secondary, 1 hour every time, collecting decoction, filtration, it is dense Contracting filtrate, lets cool, and it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, filtrate decompression is concentrated into relative density and is 1.20 it is 70% to add ethanol to make containing amount of alcohol, standing overnight, filter, it is 1.30 that filtrate, which is concentrated into relative density, adds 3 times of amount water, It is sufficiently stirred, refrigerates 48 hours, filtration, filtrate is concentrated into relative density as 1.15；Merge with above-mentioned all decoctions, add 2 times of amounts Water, it is sufficiently stirred, refrigerates 24 hours, filtration, filtrate adds d ichlorbenzuron and deionized water water is configured to 1000ml solution, stirs evenly, The relative density when relative density of above-mentioned each filtrate is 80 DEG C；Solution ph is adjusted to 6.5-8.5 with sodium hydroxide solution； Filtering, it is filling, sterilizing, produce.
Wherein, the process for adding ethanol filtering and concentrating is first to filter to get filtrate, and filtrate decompression is concentrated into relative density as 1.27 ~1.30, let cool, it is 65% to add ethanol to make containing amount of alcohol, stands overnight, filters, and decompression filtrate recycling ethanol is simultaneously concentrated into relative Density is 1.30.Filtrate is concentrated into relative density as 1.25~1.30.The mass percent of the sodium hydroxide solution used is 20%.Solution uses filtering with microporous membrane.
Embodiment 2：
The present embodiment verifies that the pharmaceutical composition insecticide common with market is compared, to the eradicative rate of aphid.
Choose insecticide common on the market：Pale purple purple spore bacterium aqua, nematode killing agent, the agent of special efficacy root line, thiamethoxam disinsection agent.
Be grouped according to different insecticides, every group prepare respectively it is each in worm's ovum, larva, the aphid of adult three phases 1000, insecticide is then used respectively to the aphid in each stage, tests the eradicative rate of every group of insecticide, such as following table institute Show：
Killing effect of the insecticide of table one to aphid
As seen from the above table, each group insecticide is the most excellent to larval aphid killing rate highest, the insecticidal effect of this product Good, insect killing effect is notable, and the worm's ovum for being most difficult to kill also has preferable insect killing effect.
Embodiment 3：
The present embodiment verifies eradicative rate of the pharmaceutical composition to various insects.
It is each to choose chafer, beetle, leafhopper, heart-eating worm, pear sucker, scale insect, volume noctuid, mole cricket, fore-telling mud, aphid 10000, and be grouped respectively, the decoction of same concentrations is made in the medicine being prepared using embodiment 1, respectively the evil to every group Worm is sprayed, and after 1 hour, checks the eradicative rate of various insects, as a result as shown in the table：
Insect killing effect of the medicine of table two to various insects
Group Eradicative rate (%)
Aphid 99.47
Chafer 10.32
Beetle 9.65
Leafhopper 8.75
Heart-eating worm 1.02
Pear sucker 0
Scale insect 0
Roll up noctuid 1.01
Mole cricket 0
Foretell mud 1.24
As seen from the above table, the medicine that embodiment 1 is prepared, only there is preferable insect killing effect to aphid, to other insects Insect killing effect it is very limited, thus its specific aim of provable this product is stronger, is only capable of using and being killed for aphid.

Claims (5)

1. a kind of pharmaceutical composition for killing aphid, it is characterised in that including Folium Callicarpae Formosanae extract, arsenolite extract, gemma agrimoninae Extract, clear and bright willow extract, Caulis Lonicerae extract, milfoil extract, cinnamomum cassia extract, Radix Dipsaci extract, Herba polygoni hydropiperis extract And d ichlorbenzuron.
2. a kind of pharmaceutical composition for killing aphid according to claim 1, it is characterised in that contain phase per 100ml solution When in the Folium Callicarpae Formosanae extract of 10-25g folium callicarpae pedunculatae medicinal materials, the arsenolite extract of 10-25g arsenolite medicinal materials, 10-25g gemma agrimoninae medicines The caulis lonicerae extraction of the gemma agrimoninae extract of material, the clear and bright willow extract of 10-25g Clear and Bright willow medicinal materials, 10-25g caulis lonicerae medicinal materials Thing, the milfoil extract of 10-25g milfoil medicinal materials, the cinnamomum cassia extract of 10-25g Chinese cassia tree medicinal materials, the teasel root of 10-25g teasel root medicinal materials The Herba polygoni hydropiperis extract of extract, 10-25g polygonum flaccidum medicinal materials, Folium Callicarpae Formosanae extract, arsenolite extract, gemma agrimoninae extract, clear and bright willow Extract, Caulis Lonicerae extract, milfoil extract, cinnamomum cassia extract, Radix Dipsaci extract, the usage ratio of Herba polygoni hydropiperis extract medicinal material For 1：2：1：3：5：4：1：2：1.
A kind of 3. pharmaceutical composition for killing aphid according to claim 1, it is characterised in that the dosage of the d ichlorbenzuron For 0.08g~5.0g/100ml.
A kind of 4. pharmaceutical composition for killing aphid according to claim 3, it is characterised in that the dosage of the d ichlorbenzuron For 0.05g~1.0g/100ml.
A kind of 5. pharmaceutical composition of killing aphid according to claim 1 ~ 4 any one, it is characterised in that the medicine Compositions formulation is powder pin or freezed.
CN201711094595.1A 2017-11-09 2017-11-09 A kind of pharmaceutical composition for killing aphid Pending CN107711909A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711094595.1A CN107711909A (en) 2017-11-09 2017-11-09 A kind of pharmaceutical composition for killing aphid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711094595.1A CN107711909A (en) 2017-11-09 2017-11-09 A kind of pharmaceutical composition for killing aphid

Publications (1)

Publication Number Publication Date
CN107711909A true CN107711909A (en) 2018-02-23

Family

ID=61214083

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711094595.1A Pending CN107711909A (en) 2017-11-09 2017-11-09 A kind of pharmaceutical composition for killing aphid

Country Status (1)

Country Link
CN (1) CN107711909A (en)

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