CN107595712A - A kind of blemish clearing gel and preparation method thereof - Google Patents
A kind of blemish clearing gel and preparation method thereof Download PDFInfo
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- CN107595712A CN107595712A CN201711013772.9A CN201711013772A CN107595712A CN 107595712 A CN107595712 A CN 107595712A CN 201711013772 A CN201711013772 A CN 201711013772A CN 107595712 A CN107595712 A CN 107595712A
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Abstract
The invention discloses a kind of blemish clearing gel, is made up of the raw material of following parts by weight：20 25 parts of kuh-seng, 16 20 parts of chrysanthemum indicum, 46 50 parts of honeysuckle, 46 50 parts of garden burnet, 35 45 parts of carbomer.The present invention selects pure natural plant formula, gently non-stimulated to cause secondary injury to human body skin while anti-acne；Raw material is through scientific matching, it is prepared using the advanced extraction such as low temperature circumfluence distillation technology, ultrasonic oscillation extractive technique, film concentration technique, macroreticular resin isolation technics, purification technique, the problem of Heat sensitive active composition is destroyed, volatile active composition scatters is not only avoid, and the content of beary metal being made in product in Chinese medicinal ingredients substantially reduces, the content of small-molecule substance greatly promotes.
Description
Technical field
The present invention relates to technical field of skin care, more particularly to a kind of blemish clearing gel and preparation method thereof.
Background technology
Acne is commonly called as whelk, is chronic inflammation hair follicle sebum gland disease, is one of most common disease of dept. of dermatology.
Skin produce acne the main reason for be：1. cause that grease is excessive, pore is thick because smegma is vigorous
Or block, cuticula thicken, then, grease gradually toward cortical surface swell, thus cause grease block pore, protuberance
Summit oxidation becomes black, result in together with bacterium stirs in pore with grease, makes propionibacterium acnes in anaerobic condition
Lower amount reproduction, then cause inflammation bacterium to invade, become warts, tubercle, last whole hair follicle reddens, inflammation；2. skin is dry
The Crack cause of dryization and acne, because skin water deficient, excessively dry, on the contrary can hypersecretion for skin of moistening
Grease；3. endocrinopathy.
In terms of anti-acne, it need to set about from following several respects：1. improve the moistening effect of skin；2. the grease of regulation skin is put down
Weighing apparatus, suppresses the excessive secretion of sebum；3. suppress the breeding of propionibacterium acnes；4. anti-inflammatory；5. dispel acne print；6. divide in regulation
Secrete.
But in order to pursue anti-acne effect, current market sales of product for resolving poxes often adds some tools in formula
The chemical analysis of toxic side effect, secondary injury is caused to the skin of human body while anti-acne；In addition, traditional preparation method
In need, by high-temperature process, not only to make that the Heat sensitive active composition in formula is destroyed, volatile active composition scatters, and
And refining effect is not good enough, content of beary metal in Chinese medicinal ingredients is higher, small-molecule substance content is relatively low.
The content of the invention
In view of this, the invention provides a kind of anti-acne to coagulate frost and preparation method thereof, and pure natural plant is selected in formula
Formula, product natural no stimulation will not cause secondary injury while anti-acne to human body skin；Using low temperature circumfluence distillation
Advanced extraction, the purification techniques such as technology, ultrasonic oscillation extractive technique, film concentration technique, macroreticular resin isolation technics, not only
The problem of Heat sensitive active composition is destroyed, volatile active composition scatters is avoided, and is made in product Chinese medicinal ingredients
Content of beary metal substantially reduce, the content of small-molecule substance greatly promotes.
In order to achieve the above object, the present invention adopts the following technical scheme that：
A kind of solidifying frost of anti-acne, is made up of the raw material of following parts by weight：Kuh-seng 20-25 parts, chrysanthemum indicum 16-20 parts, honeysuckle
46-50 parts, garden burnet 46-50 parts, carbomer 35-45 parts.
Preferably, in a kind of above-mentioned blemish clearing gel, it is made up of the raw material of following parts by weight：20 parts of kuh-seng, 18 parts of mother chrysanthemum,
48 parts of honeysuckle, 48 parts of garden burnet, 40 parts of carbomer.
A kind of preparation method of blemish clearing gel, comprises the following steps：
(1) each raw material is weighed by a kind of parts by weight formula of above-mentioned blemish clearing gel, and each herbal raw material is cleaned, powder
It is broken；
(2) chrysanthemum indicum, garden burnet are mixed chip and extracted using ultrasonic oscillation extractive technique, obtain extract solution A；
(3) kuh-seng, honeysuckle are added mixing chip and extracted using Low Temperature Thermal technique of backflow, obtain extract solution B；
(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate uses film concentration technique, separation, obtains
Film concentrate C；
(5) tubular type seperation film concentrate C, discards precipitation, and centrifugate crosses AB-8 macroporous absorbent resins；
(6) the AB-8 macroporous absorbent resins in above-mentioned steps (5) are subjected to ethanol elution, eluent is in vacuum 0.01-
0.04MPa, concentrate under conditions of 40~50 DEG C, recovery ethanol, be dried to obtain extract product；
(7) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack anti-acne is coagulated
Glue.
Preferably, in a kind of above-mentioned preparation method of blemish clearing gel, the step (2) is by chrysanthemum indicum, the mixing of garden burnet
Chip presses 1 with absolute ethyl alcohol：8~13 weight carries out ultrasonic wave extraction, in 25~50KHZ, 68~85 DEG C of condition than mixing
5~10min of lower reaction.
Preferably, it is specially in a kind of above-mentioned preparation method of blemish clearing gel, the step of step (3)：By kuh-seng,
The mixing chip of honeysuckle presses 1 with water:15~20 weight is added in low temperature circumfluence distillation tank than common, temperature 55-65
DEG C, vacuum 0.2-0.3MPa, add above-mentioned kuh-seng, the mixing chip of honeysuckle and water gross weight 0.1-0.3% chlorination
Sodium, temperature in extractor is then risen into 75~80 DEG C of 2~4h of extraction, collects extract solution.
Preferably, 50%~70% second is selected in a kind of above-mentioned preparation method of blemish clearing gel, in the step (6)
Alcohol.
Through as shown from the above technical solution, compared with prior art, the present disclosure provides a kind of solidifying frost of anti-acne, selecting
Pure natural plant formula, it is prepared through the processing of distinctive processing step, makes the huge sum of money in Chinese medicinal ingredients in the product of gained
Content substantially reduces category, the content of small-molecule substance greatly promotes；The natural plant active composition having in product, it is gentle stingless
Swash, can be antibacterial rapidly, detoxification sore treatment, recover skin, second of injury will not be caused to skin.
Further, the kuh-seng contained in formula has the effect of heat-clearing and damp-drying drug；Contain a variety of effective ingredients in chrysanthemum indicum,
Can play the role of to suppress to kill to various bacteria virus；Contain OPC, biflavone, polypeptide plant cellulose in honeysuckle
The isoreactivity factor, these components can rapid osmotic enter skin, active cell mutual induction, dredge facial microcirculation, there is heat-clearing,
The effect of pacifying skin；Garden burnet has the effect of removing toxic substances sore, while it also has certain antiseptic property, its moderate performance without
Excitant, it is particularly suitable for the use of sensitive skin, it is above-mentioned several with clearing heat and detoxicating natural plants cooperation collocation, make product
Acne-removing has reached optimal.
In preparation process, first, kuh-seng and honeysuckle extract to obtain filtrate A through Low Temperature Thermal technique of backflow, using Low Temperature Thermal
Technique of backflow combines on the basis of traditional Chinese medicine extraction is adhered to and decocts extraction, diafiltration is extracted, adverse current is extracted and backflow extracting
4 kinds of extraction principles synchronously carry out the extraction of Chinese medicine, concentration two procedures, once complete kuh-seng and honeysuckle effective ingredient
Extraction and concentration, and change with pressure in the traditional extractor and high temperature decocting process of normal pressure, using negative pressure of vacuum, boiling point is reduced,
Carry out low temperature extraction low temperature concentration, effectively prevent the Heat sensitive active composition in kuh-seng and Flos Lonicerae extractive solution destroyed,
The problem of volatile active composition scatters.
Secondly, chrysanthemum indicum and garden burnet obtain liquor B through ultrasonic oscillation extractive technique, using ultrasonic oscillation extractive technique
Solvent is set to be rapidly introduced into chrysanthemum indicum and garden burnet, among the organic component contained by them is dissolved in into solvent as fully as possible,
Obtain more composition mixed extracts.Strengthen extraction separation process using ultrasonic technology, chrysanthemum indicum and garden burnet can be effectively improved
Extraction separation rate, shorten extraction time, it is cost-effective, improve product quality and yield, make product small molecular material
Content greatly promotes.
Then, extract solution A and extract solution B mixing, obtains film concentrate C through film concentration technique, using film concentration technique, makes
Effective ingredient loss in formula is few, and especially suitable for heat-sensitive substance, energy consumption is extremely low, its expense about evaporation and concentration or cold
Freeze the 1/3-1/8 of concentration；Moreover, it is typical physical separating process, without chemical reagent and additive, product is not got dirty
Dye.
Finally, the film concentrate C obtained, by combining macroporous absorbent resin, and through ethanol elution, mixing ion exchange is crossed
Resin treatment, the effective ingredient in obtained formula are further purified, and the content of beary metal in product traditional Chinese medicine ingredients is dropped significantly
Low, anti-acne effect reaches optimal.
The solidifying frost of anti-acne provided by the invention from having a clearing heat and detoxicating herbal raw material, in product with natural activity into
Part；The gel as made of the formula and preparation method of offer, traditional Chinese medicine heavy metal content 54%, effectively small point are reduced compared with traditional handicraft
The content lifting 35% of sub- material, product natural no stimulation will not cause secondary injury to skin, and anti-acne effect is splendid.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects
Enclose.
The embodiment of the invention discloses a kind of blemish clearing gel and preparation method thereof, the content of beary metal in product Chinese medicinal ingredients
Substantially reduce, the content of small-molecule substance greatly promotes, product natural no stimulation will not cause secondary injury to skin, anti-acne effect
Fruit is splendid.
A kind of solidifying frost of anti-acne, is made up of the raw material of following parts by weight：Kuh-seng 20-25 parts, chrysanthemum indicum 16-20 parts, honeysuckle
46-50 parts, garden burnet 46-50 parts, carbomer 35-45 parts.
Specific embodiment：
Table 1
The preparation method of above-described embodiment is：
(1) each raw material is weighed by each embodiment percentage；
(2) chrysanthemum indicum, the mixing chip of garden burnet and absolute ethyl alcohol are pressed 1：10 weight carries out ultrasonic wave and carried than mixing
Take, the ultrasonic response 8min under conditions of 25KHZ, 80 DEG C, obtain extract solution A；
(3) kuh-seng, the mixing chip of honeysuckle and water are pressed 1:15 weight adds low temperature circumfluence distillation tank than common
Interior, temperature is 55 DEG C, vacuum 0.2MPa, adds above-mentioned kuh-seng, the mixing chip of honeysuckle and the chlorine of water gross weight 0.2%
Change sodium, temperature in extractor is then risen into 75 DEG C of extraction 3h, obtains extract solution B；
(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate uses film concentration technique, separation, obtains
Film concentrate C；
(5) tubular type seperation film concentrate C, discards precipitation, and centrifugate crosses AB-8 macroporous absorbent resins；
(6) the AB-8 macroporous absorbent resins in above-mentioned steps (5) are subjected to ethanol elution with 60% ethanol, eluent is true
Reciprocal of duty cycle 0.01MPa, concentrate under conditions of 40 DEG C, recovery ethanol, be dried to obtain extract product；
(7) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack anti-acne is coagulated
Glue.
First, blemish clearing gel of the present invention and the common anti-acne effect except acne product are tested：
Choosing 100 skin of face has the women of 17-25 year of acne, is divided equally into five groups of A, B, C, D, E, every group of 20 people；
Wherein, the solidifying frost of anti-acne that A groups, B groups, C groups, D groups are prepared using embodiment 1 to embodiment 4；
E groups are using formula：Zinc carbonate hydroxide 20g, borax 1g, amber powder 15, pearl powder 5g, allantoin 5g, ox
The common of oily fruit tree fruit fat 30g, Angelica roots 5g, Gotu Kola P.E 8g removes acne product；
Each after clean skin in the morning, afternoon and evening daily using once, every night counts to experimenter's skin condition, specific statistics
Situation such as table 2：
Table 2
By contrast test, it can be seen that the blemish clearing gel that formula provided by the invention prepares with method, to skin
There is net skin, anti-acne, reparation, it is gentle non-stimulated, can quickly eliminate small pox, and cure rate is high, and recurrence rate is low.
Comparative example 1：
(1) kuh-seng 20g, chrysanthemum indicum 18g, honeysuckle 48g, garden burnet 48g, carbomer 40g are weighed；
(2) by chrysanthemum indicum, garden burnet mixing chip through thermophilic digestion, obtain extract solution A；
(3) kuh-seng, the mixing chip of honeysuckle and water are pressed 1:15 weight adds low temperature circumfluence distillation tank than common
Interior, temperature is 55 DEG C, vacuum 0.2MPa, adds above-mentioned kuh-seng, the mixing chip of honeysuckle and the chlorine of water gross weight 0.2%
Change sodium, temperature in extractor is then risen into 75 DEG C of extraction 3h, obtains extract solution B；
(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate uses film concentration technique, separation, obtains
Film concentrate C；
(5) tubular type seperation film concentrate C, discards precipitation, and centrifugate crosses AB-8 macroporous absorbent resins；
(6) the AB-8 macroporous absorbent resins in above-mentioned steps (5) are subjected to ethanol elution with 60% ethanol, eluent is true
Reciprocal of duty cycle 0.01MPa, concentrate under conditions of 40 DEG C, recovery ethanol, be dried to obtain extract product；
(7) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack anti-acne is coagulated
Glue.
Comparative example 2：
(1) kuh-seng 20g, chrysanthemum indicum 18g, honeysuckle 48g, garden burnet 48g, carbomer 40g are weighed；
(2) chrysanthemum indicum, the mixing chip of garden burnet and absolute ethyl alcohol are pressed 1：10 weight carries out ultrasonic wave and carried than mixing
Take, the ultrasonic response 8min under conditions of 25KHZ, 80 DEG C, obtain extract solution A；
(3) by kuh-seng, honeysuckle mixing chip through thermophilic digestion, obtain extract solution B；
(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate uses film concentration technique, separation, obtains
Film concentrate C；
(5) tubular type seperation film concentrate C, discards precipitation, and centrifugate crosses AB-8 macroporous absorbent resins；
(6) the AB-8 macroporous absorbent resins in above-mentioned steps (5) are subjected to ethanol elution with 60% ethanol, eluent is true
Reciprocal of duty cycle 0.01MPa, concentrate under conditions of 40 DEG C, recovery ethanol, be dried to obtain extract product；
(7) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack anti-acne is coagulated
Glue.
Comparative example 3：
(1) kuh-seng 20g, chrysanthemum indicum 18g, honeysuckle 48g, garden burnet 48g, carbomer 40g are weighed；
(2) chrysanthemum indicum, the mixing chip of garden burnet and absolute ethyl alcohol are pressed 1：10 weight carries out ultrasonic wave and carried than mixing
Take, the ultrasonic response 8min under conditions of 25KHZ, 80 DEG C, obtain extract solution A；
(3) kuh-seng, the mixing chip of honeysuckle and water are pressed 1:15 weight adds low temperature circumfluence distillation tank than common
Interior, temperature is 55 DEG C, vacuum 0.2MPa, adds above-mentioned kuh-seng, the mixing chip of honeysuckle and the chlorine of water gross weight 0.2%
Change sodium, temperature in extractor is then risen into 75 DEG C of extraction 3h, obtains extract solution B；
(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate crosses AB-8 macroporous absorbent resins；
(5) the AB-8 macroporous absorbent resins in above-mentioned steps (4) are subjected to ethanol elution with 60% ethanol, eluent is true
Reciprocal of duty cycle 0.01MPa, concentrate under conditions of 40 DEG C, recovery ethanol, be dried to obtain extract product；
(6) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack anti-acne is coagulated
Glue.
2nd, product for resolving poxes is obtained using the blemish clearing gel of preparation method of the present invention acquisition and using comparative example preparation method
Anti-acne effect is tested：
Choosing 80 skin of face has the women of 17-25 year of acne, is divided equally into four groups, every group of 20 people；
Wherein, first group uses the solidifying frost of the anti-acne being formulated by embodiment 1 and prepared by method；
Second group to the 4th group respectively using the product for resolving poxes prepared by the formula and method of comparative example 1 to comparative example 3；
Each after clean skin in the morning, afternoon and evening daily using once, every night counts to experimenter's skin condition, specific statistics
Situation such as table 2：
Table 3
By contrast test, it can be seen that chrysanthemum indicum, garden burnet are mixed chip and extracted using ultrasonic oscillation extractive technique,
Kuh-seng, honeysuckle add mixing chip using Low Temperature Thermal technique of backflow extract, two extract solutions mixing through film concentration extraction technology with
The blemish clearing gel product that macroreticular resin isolation technics prepares, anti-acne effect is optimal, and it has net skin, anti-acne, reparation to skin
Effect, it is gentle non-stimulated, can quickly eliminate small pox, cure rate is high, and recurrence rate is low.
Above rational prescribing designs, and under the support of advanced extractive technique, reduces heavy metal in Chinese medicine compared with traditional handicraft and contains
Amount 54%, and the effectively content lifting 35% of small-molecule substance.Secondary damage is not caused to skin while anti-acne.
Each embodiment is described by the way of progressive in this specification, what each embodiment stressed be and other
The difference of embodiment, between each embodiment identical similar portion mutually referring to.For device disclosed in embodiment
For, because it is corresponded to the method disclosed in Example, so description is fairly simple, related part is said referring to method part
It is bright.
The foregoing description of the disclosed embodiments, professional and technical personnel in the field are enable to realize or using the present invention.
A variety of modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, it is of the invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The most wide scope caused.
Claims (6)
- A kind of 1. blemish clearing gel, it is characterised in that：It is made up of the raw material of following parts by weight：Kuh-seng 20-25 parts, chrysanthemum indicum 16-20 Part, honeysuckle 46-50 parts, garden burnet 46-50 parts, carbomer 35-45 parts.
- A kind of 2. blemish clearing gel according to claim 1, it is characterised in that：It is made up of the raw material of following parts by weight：Kuh-seng 20 parts, 18 parts of chrysanthemum indicum, 48 parts of honeysuckle, 48 parts of garden burnet, 40 parts of carbomer.
- 3. a kind of preparation method of blemish clearing gel, it is characterised in that comprise the following steps：(1) a kind of parts by weight formula of blemish clearing gel as described in claim 1 weighs each raw material, and each herbal raw material is washed Only, crush；(2) chrysanthemum indicum, garden burnet are mixed chip and extracted using ultrasonic oscillation extractive technique, obtain extract solution A；(3) kuh-seng, honeysuckle are added mixing chip and extracted using Low Temperature Thermal technique of backflow, obtain extract solution B；(4) merge extract solution A and B, place 12h, filtering；Filter residue is discarded, filtrate uses film concentration technique, separation, it is dense to obtain film Contracting liquid C；(5) tubular type seperation film concentrate C, discards precipitation, and centrifugate crosses AB-8 macroporous absorbent resins；(6) the AB-8 macroporous absorbent resins in step (5) are subjected to ethanol elution, eluent in vacuum 0.01-0.04MPa, Concentrated under conditions of 40~50 DEG C, recovery ethanol, be dried to obtain extract product.(7) it is the extract product obtained in above-mentioned steps (6) and carbomer is fully fused 48 hours, pack to obtain blemish clearing gel.
- 4. the preparation method of a kind of blemish clearing gel according to claim 3, it is characterised in that the step (2) is by mother chrysanthemum Flower, the mixing chip of garden burnet and absolute ethyl alcohol press 1：8~13 weight carries out ultrasonic wave extraction than mixing, in 25~50KHZ, 5~10min is reacted under conditions of 68~85 DEG C.
- 5. the preparation method of a kind of blemish clearing gel according to claim 3, it is characterised in that the step of step (3) Specially：Kuh-seng, the mixing chip of honeysuckle and water are pressed 1:15~20 weight adds low temperature circumfluence distillation tank than common Interior, temperature is 55-65 DEG C, vacuum 0.2-0.3MPa, adds above-mentioned kuh-seng, the mixing chip of honeysuckle and water gross weight 0.1-0.3% sodium chloride, temperature in extractor is then risen into 75~80 DEG C of 2~4h of extraction, collects extract solution.
- 6. the preparation method of a kind of blemish clearing gel according to claim 3, it is characterised in that selected in the step (6) 50%~70% ethanol.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112618465A (en) * | 2021-01-28 | 2021-04-09 | 广州碧思特生物科技有限公司 | Formula and preparation process of plant acne-removing and red-fading gel |
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| CN104906006A (en) * | 2015-06-23 | 2015-09-16 | 蔡锦瑜 | Cleaning mask |
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| CN104906006A (en) * | 2015-06-23 | 2015-09-16 | 蔡锦瑜 | Cleaning mask |
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| CN112618465A (en) * | 2021-01-28 | 2021-04-09 | 广州碧思特生物科技有限公司 | Formula and preparation process of plant acne-removing and red-fading gel |
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Application publication date: 20180119 |