CN103271401A - Preparation method of honeysuckle flower distillate - Google Patents
Preparation method of honeysuckle flower distillate Download PDFInfo
- Publication number
- CN103271401A CN103271401A CN2013102084806A CN201310208480A CN103271401A CN 103271401 A CN103271401 A CN 103271401A CN 2013102084806 A CN2013102084806 A CN 2013102084806A CN 201310208480 A CN201310208480 A CN 201310208480A CN 103271401 A CN103271401 A CN 103271401A
- Authority
- CN
- China
- Prior art keywords
- distillation
- distillate
- honeysuckle
- deionized water
- carried out
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Landscapes
- Medicines Containing Plant Substances (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses a preparation method of honeysuckle flower distillate. According to the preparation method, the raw honeysuckle flower is processed by steps of cleaning, soaking, extruding, crushing, separating of slag and liquid, atmospheric distilling, distilling in a thermocompression way, adding of other auxiliaries and the like to realize the effective utilization, and the yield and efficacy of honeysuckle flower distillate products are also improved.
Description
Technical field
The present invention relates to a kind of preparation method of the distilled liquid of honeysuckle.
Background technology
Honeysuckle is the general designation of Chinese medicine and plant.The plant honeysuckle has another name called honeysuckle, is the perennial half evergreen winding bejuco of Caprifoliaceae." honeysuckle " one come from Compendium of Material Medica because FLOSLONICERAE just opens and is white, after transfer yellow to, honeysuckle hence obtains one's name.The medicinal material honeysuckle is Caprifoliaceae woodbine honeysuckle and congener dry flower or the first flower of opening of band.Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times.The sweet cold air fragrance of its property, clear heat with drugs of sweet flavour and cold nature and not injuring one's stomach, fragrance reaches thoroughly and can be eliminating evil.Honeysuckle can dispelling wind-heat, and also kind removing summer-heat blood poison is used for various febrile diseases, and as body heat, dermexanthesis, send out cards such as spot, hot carbuncle carbuncle, abscess of throat, all effect is remarkable.
At present, the distilled liquid of honeysuckle mainly is by its effective component is extracted in the boiling of raw material honeysuckle.Though traditional boiling method is easy and simple to handle, its productive rate is limited, and can the plurality of active ingredients in the honeysuckle be damaged, and reduces drug effect.Along with the cost of honeysuckle raw material constantly raises; traditional processing method can't satisfy high yield; low-cost; the production demand of high-drug-effect; traditional boiling method is because it is of poor quality, efficient is low, control difficulty etc.; do not adapt to the scale of distilled liquid of honeysuckle industry, intensive, development of modernization, do not adapted to high-quality, the allegro modern life.Therefore, be necessary to develop a kind of to honeysuckle utilization rate height, when increasing its productive rate, do not destroy the distilled liquid of honeysuckle preparation method of its active ingredient as far as possible.
Summary of the invention
The present invention proposes a kind of preparation method of the distilled liquid of honeysuckle, it is by the cleaning and dipping to the honeysuckle raw material, and extruding is pulverized, slag liquid separates, air-distillation, and the hot pressing distillation also adds step such as other auxiliary material and has realized effective reason to the honeysuckle raw material, improved productive rate, the drug effect of distilled liquid of honeysuckle product.
Particularly, the preparation method of the distilled liquid of honeysuckle of the present invention is:
A kind of preparation method of the distilled liquid of honeysuckle is characterized in that may further comprise the steps:
(1) uses deionized water that fresh honeysuckle is soaked, clean;
(2) honeysuckle that will clean dry to water content be 15%-25%;
(3) extruding of the honeysuckle after will drying is pulverized;
(4) collect the juice that produces in the step (3), and filter, obtain filtrate A; Collect the honeysuckle residue that obtains in the step (3);
(5) filtrate A is carried out air-distillation, collect distillate B; With distillate B cooling, carry out the hot pressing distillation after leaving standstill, collect distillate C;
(6) mix with deionized water collecting the honeysuckle residue that obtains in the step (4), stir the mixed liquor of gained, and it is carried out high temperature high pressure process, be cooled to environment temperature;
(7) afterwards, the mixed liquor in the step (6) is carried out air-distillation, collect distillate D;
(8) distillate C and distillate D mixing are also carried out the hot pressing distillation again, obtain faint yellow oily distillate E;
(9) spent ion exchange resin is handled to the distillate E of gained, and regulated pH value, obtain paste F behind the adding deionized water;
(10) filter paste F, filter the back and add deionized water, salt, xylitol, the dried peppermint leaf distillate obtains mixture G, regulates the pH value, uses microporous barrier that mixture G is filtered, and filtrate is carried out sterilization treatment, and can is namely.
Wherein, the temperature of deionized water is 35-38 ℃ in the above-mentioned steps (1), and soak time is 1-2 hour, comprises in the cleaning process using ultrasonic wave to clean;
Bake out temperature in the above-mentioned steps (2) is 55-58 ℃;
Air-distillation to distillate A in the above-mentioned steps (5) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 110-115 ℃, and 118-120 ℃, 125-128 ℃, the time of each distillation is 20 minutes-30 minutes; Hot pressing distillation to distillate B is carried out three times continuously, and vapo(u)rizing temperature is respectively 130-135 ℃, and 138-140 ℃, 145-148 ℃, the time of each distillation is 20 minutes-30 minutes, and the pressure of hot pressing distillation is 0.15Mpa-0.18Mpa;
The weight ratio that the honeysuckle residue mixes with deionized water in the above-mentioned steps (6) is 1: 5-1: 8, and the condition of HTHP is: 180-190 ℃, 0.45Mpa-0.48Mpa, the processing time is 30 seconds-45 seconds;
Air-distillation to mixed liquor in the above-mentioned steps (7) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 110-115 ℃, and 118-120 ℃, 125-128 ℃, the time of each distillation is 20 minutes-30 minutes;
The temperature of hot pressing distillation is 138-140 ℃ in the above-mentioned steps (8), and the time of distillation is 20 minutes-30 minutes, and the pressure of hot pressing distillation is 0.15Mpa-0.18Mpa.
Above-mentioned steps is adjusted to 7.5-7.8 with the pH value in (9), and the weight of distillate and deionized water is 1: 2-1: 2.5.
In the above-mentioned steps (10), be benchmark with the paste that filters the back gained, deionized water, salt, xylitol, the weight ratio that the dried peppermint leaf distillate adds is respectively: 1: 100-1: 150,1: 0.2-1: 0.3,1: 0.2-1: 0.3,1: 0.1-1: 0.15, regulate the pH value to 4.0-4.5.
Beneficial effect of the present invention is:
1. in the cleaning and dipping process to the honeysuckle raw material, define water temperature and use ultrasonic wave that it is cleaned, namely avoided the destruction to active ingredient in the honeysuckle, reached the purpose of removing impurity in the raw material again;
2. by employing the honeysuckle raw material is pushed and pulverize, slag liquid separates and with the method that slag liquid distills respectively, extracts the active principle in the honeysuckle to greatest extent.
3. in still-process, adopt the distillating method of the segmentation temperature difference, guaranteed the recovery rate to effective ingredient of honeysuckle, the process gentleness has reduced the destruction to active ingredient.
4. choose xylitol, the dried peppermint leaf distillate has improved drug effect and the mouthfeel of the distilled liquid of honeysuckle, and has been suitable for patients with diabetes mellitus as auxiliary material.
Description of drawings
Fig. 1 is the flow chart of a kind of specific embodiment of preparation method of the distilled liquid of honeysuckle provided by the present invention.
The specific embodiment
Please refer to Fig. 1, Fig. 1 is the flow chart of a kind of specific embodiment of preparation method of the distilled liquid of honeysuckle provided by the present invention.
Embodiment 1
A kind of preparation method of the distilled liquid of honeysuckle is characterized in that may further comprise the steps:
(1) uses deionized water that fresh honeysuckle is soaked, clean;
(2) honeysuckle that will clean dry to water content be 18%-20%;
(3) extruding of the honeysuckle after will drying is pulverized;
(4) collect the juice that produces in the step (3), and filter, obtain filtrate A; Collect the honeysuckle residue that obtains in the step (3);
(5) filtrate A is carried out air-distillation, collect distillate B; With distillate B cooling, carry out the hot pressing distillation after leaving standstill, collect distillate C;
(6) mix with deionized water collecting the honeysuckle residue that obtains in the step (4), stir the mixed liquor of gained, and it is carried out high temperature high pressure process, be cooled to environment temperature;
(7) afterwards, the mixed liquor in the step (6) is carried out air-distillation, collect distillate D;
(8) distillate C and distillate D mixing are also carried out the hot pressing distillation again, obtain faint yellow oily distillate E;
(9) spent ion exchange resin is handled to the distillate E of gained, and regulated pH value, obtain paste F behind the adding deionized water;
(10) filter paste F, filter the back and add deionized water, salt, xylitol, the dried peppermint leaf distillate obtains mixture G, regulates the pH value, uses microporous barrier that mixture G is filtered, and filtrate is carried out sterilization treatment, and can is namely.
Wherein, the temperature of deionized water is 36 ℃ in the above-mentioned steps (1), and soak time is 1 hour, comprises in the cleaning process using ultrasonic wave to clean;
Bake out temperature in the above-mentioned steps (2) is 57 ℃;
Air-distillation to distillate A in the above-mentioned steps (5) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 113 ℃, and 119 ℃, 127 ℃, the time of each distillation is 20 minutes; Hot pressing distillation to distillate B is carried out three times continuously, and vapo(u)rizing temperature is respectively 133 ℃, and 139 ℃, 146 ℃, the time of each distillation is 30 minutes, and the pressure of hot pressing distillation is 0.16Mpa;
The weight ratio that the honeysuckle residue mixes with deionized water in the above-mentioned steps (6) is 1: 7, and the condition of HTHP is: 185 ℃, and 0.47Mpa, the processing time is 35 seconds;
Air-distillation to mixed liquor in the above-mentioned steps (7) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 113 ℃, and 119 ℃, 127 ℃, the time of each distillation is 20 minutes;
The temperature of hot pressing distillation is 139 ℃ in the above-mentioned steps (8), and the time of distillation is 20 minutes, and the pressure of hot pressing distillation is 0.16Mpa.
Above-mentioned steps is adjusted to 7.5 with the pH value in (9), and the weight of distillate and deionized water is 1: 2.
In the above-mentioned steps (10), be benchmark with the paste that filters the back gained, deionized water, salt, xylitol, the weight ratio that the dried peppermint leaf distillate adds is respectively: 1: 150,1: 0.3,1: 0.2,1: 0.1, regulate pH value to 4.5.
Embodiment 2
A kind of preparation method of the distilled liquid of honeysuckle is characterized in that may further comprise the steps:
(1) uses deionized water that fresh honeysuckle is soaked, clean;
(2) honeysuckle that will clean dry to water content be 15%;
(3) extruding of the honeysuckle after will drying is pulverized;
(4) collect the juice that produces in the step (3), and filter, obtain filtrate A; Collect the honeysuckle residue that obtains in the step (3);
(5) filtrate A is carried out air-distillation, collect distillate B; With distillate B cooling, carry out the hot pressing distillation after leaving standstill, collect distillate C;
(6) mix with deionized water collecting the honeysuckle residue that obtains in the step (4), stir the mixed liquor of gained, and it is carried out high temperature high pressure process, be cooled to environment temperature;
(7) afterwards, the mixed liquor in the step (6) is carried out air-distillation, collect distillate D;
(8) distillate C and distillate D mixing are also carried out the hot pressing distillation again, obtain faint yellow oily distillate E;
(9) spent ion exchange resin is handled to the distillate E of gained, and regulated pH value, obtain paste F behind the adding deionized water;
(10) filter paste F, filter the back and add deionized water, salt, xylitol, the dried peppermint leaf distillate obtains mixture G, regulates the pH value, uses microporous barrier that mixture G is filtered, and filtrate is carried out sterilization treatment, and can is namely.
Wherein, the temperature of deionized water is 35 ℃ in the above-mentioned steps (1), and soak time is 2 hours, comprises in the cleaning process using ultrasonic wave to clean;
Bake out temperature in the above-mentioned steps (2) is 55 ℃;
Air-distillation to distillate A in the above-mentioned steps (5) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 115 ℃, and 120 ℃, 128 ℃, the time of each distillation is 30 minutes; Hot pressing distillation to distillate B is carried out three times continuously, and vapo(u)rizing temperature is respectively 135 ℃, and 140 ℃, 148 ℃, the time of each distillation is 20 minutes, and the pressure of hot pressing distillation is 0.18Mpa;
The weight ratio that the honeysuckle residue mixes with deionized water in the above-mentioned steps (6) is 1: 8, and the condition of HTHP is: 190 ℃, and 0.48Mpa, the processing time is 45 seconds;
Air-distillation to mixed liquor in the above-mentioned steps (7) is carried out three times continuously, and three times vapo(u)rizing temperature is respectively 115 ℃, and 120 ℃, 128 ℃, the time of each distillation is 30 minutes;
The temperature of hot pressing distillation is 140 ℃ in the above-mentioned steps (8), and the time of distillation is 30 minutes, and the pressure of hot pressing distillation is 0.18Mpa.
Above-mentioned steps is adjusted to 7.8 with the pH value in (9), and the weight of distillate and deionized water is 1: 2.5.
In the above-mentioned steps (10), be benchmark with the paste that filters the back gained, deionized water, salt, xylitol, the weight ratio that the dried peppermint leaf distillate adds is respectively: 1: 150,1: 0.3,1: 0.3,1: 0.15, regulate pH value to 4.0.
Compare with traditional boiling method, the productive rate of the distilled liquid of honeysuckle for preparing by method of the present invention has improved about 20%, and content of effective has improved about 15% in the product.
Claims (10)
1. the preparation method of a distilled liquid of honeysuckle is characterized in that, comprises the step of honeysuckle air-distillation and hot pressing distillation.
2. the preparation method of a distilled liquid of honeysuckle is characterized in that may further comprise the steps:
(1) uses deionized water that fresh honeysuckle is soaked, clean;
(2) honeysuckle that will clean dry to water content be 15%-25%;
(3) extruding of the honeysuckle after will drying is pulverized;
(4) collect the juice that produces in the step (3), and filter, obtain filtrate A; Collect the honeysuckle residue that obtains in the step (3);
(5) filtrate A is carried out air-distillation, collect distillate B; With distillate B cooling, carry out the hot pressing distillation after leaving standstill, collect distillate C;
(6) mix with deionized water collecting the honeysuckle residue that obtains in the step (4), stir the mixed liquor of gained, and it is carried out high temperature high pressure process, be cooled to environment temperature;
(7) afterwards, the mixed liquor in the step (6) is carried out air-distillation, collect distillate D;
(8) distillate C and distillate D mixing are also carried out the hot pressing distillation again, obtain faint yellow oily distillate E;
(9) spent ion exchange resin is handled to the distillate E of gained, and regulated pH value, obtain paste F behind the adding deionized water;
(10) filter paste F, filter the back and add deionized water, salt, xylitol, the dried peppermint leaf distillate obtains mixture G, regulates the pH value, uses microporous barrier that mixture G is filtered, and filtrate is carried out sterilization treatment, and can is namely.
3. the described preparation method of claim 2 is characterized in that the temperature of deionized water in the described step (1) is 35-38 ℃, and soak time is 1-2 hour, comprises in the cleaning process and uses ultrasonic wave to clean.
4. the described preparation method of claim 2 is characterized in that the bake out temperature in the described step (2) is 55-58 ℃.
5. the described preparation method of claim 2, it is characterized in that the air-distillation to distillate A is carried out three times continuously in the described step (5), three times vapo(u)rizing temperature is respectively 110-115 ℃, 118-120 ℃, 125-128 ℃, the time of each distillation is 20 minutes-30 minutes; Hot pressing distillation to distillate B is carried out three times continuously, and vapo(u)rizing temperature is respectively 130-135 ℃, and 138-140 ℃, 145-148 ℃, the time of each distillation is 20 minutes-30 minutes, and the pressure of hot pressing distillation is 0.15Mpa-0.18Mpa.
6. the described preparation method of claim 2 is characterized in that the weight ratio that the honeysuckle residue mixes with deionized water in the described step (6) is 1: 5-1: 8, and the condition of HTHP is: 180-190 ℃, 0.45Mpa-0.48Mpa, the processing time is 30 seconds-45 seconds.
7. the described preparation method of claim 2, it is characterized in that the air-distillation to mixed liquor is carried out three times continuously in the described step (7), three times vapo(u)rizing temperature is respectively 110-115 ℃, 118-120 ℃, 125-128 ℃, the time of each distillation is 20 minutes-30 minutes.
8. the described preparation method of claim 2 is characterized in that the temperature of hot pressing distillation in the described step (8) is 138-140 ℃, and the time of distillation is 20 minutes-30 minutes, and the pressure of hot pressing distillation is 0.15Mpa-0.18Mpa.
9. the described preparation method of claim 2 is characterized in that in the described step (9) the pH value being adjusted to 7.5-7.8, and the weight of distillate and deionized water is 1: 2-1: 2.5.
10. the described preparation method of claim 2, it is characterized in that in the described step (10), paste with gained after filtering is benchmark, deionized water, salt, xylitol, the weight ratio that the dried peppermint leaf distillate adds is respectively: 1: 100-1: 150,1: 0.2-1: 0.3,1: 0.2-1: 0.3,1: 0.1-1: 0.15, regulate the pH value to 4.0-4.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310208480.6A CN103271401B (en) | 2013-05-30 | 2013-05-30 | Preparation method of honeysuckle flower distillate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310208480.6A CN103271401B (en) | 2013-05-30 | 2013-05-30 | Preparation method of honeysuckle flower distillate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103271401A true CN103271401A (en) | 2013-09-04 |
| CN103271401B CN103271401B (en) | 2014-05-14 |
Family
ID=49053642
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310208480.6A Active CN103271401B (en) | 2013-05-30 | 2013-05-30 | Preparation method of honeysuckle flower distillate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103271401B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103948629A (en) * | 2014-04-30 | 2014-07-30 | 桂林军供生化技术开发有限公司 | Preparation method for corn cervi pantotrichum extract |
| CN103948129A (en) * | 2014-04-30 | 2014-07-30 | 桂林军供生化技术开发有限公司 | Calcium supplement dew and preparation method thereof |
| CN104146247A (en) * | 2014-07-29 | 2014-11-19 | 桂林实力科技有限公司 | Preparation method of momordica grosvenori syrup |
| CN104432381A (en) * | 2014-12-12 | 2015-03-25 | 广州中国科学院先进技术研究所 | Honeysuckle health beverage and preparation method thereof |
| CN106360219A (en) * | 2016-08-31 | 2017-02-01 | 成都幸有之科技有限公司 | Preparation method of honeysuckle beverage |
| CN108095108A (en) * | 2017-12-09 | 2018-06-01 | 天旺科技股份有限公司 | A kind of preparation method of Pitaya Flower health promoting liquid |
| CN116492382A (en) * | 2023-05-31 | 2023-07-28 | 湖北大别山药业股份有限公司 | Preparation method of antibacterial honeysuckle distilled liquid |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557225A (en) * | 2004-01-15 | 2004-12-29 | 张巨柱 | Honeysuckle dew beverage making method |
| CN102113694A (en) * | 2010-12-28 | 2011-07-06 | 陈国英 | Method for manufacturing Japanese honeysuckle flower liquid |
| CN102485068A (en) * | 2010-12-01 | 2012-06-06 | 郧县正兴农业开发有限公司 | Preparation method of honeysuckle flower beverage |
| CN102935102A (en) * | 2012-10-19 | 2013-02-20 | 湖北楚天舒药业有限公司 | Method for simultaneously producing honeysuckle flower distillate and various active substances |
| CN103120348A (en) * | 2013-03-11 | 2013-05-29 | 朱世超 | Honeysuckle flower distillate beverage and production method thereof |
-
2013
- 2013-05-30 CN CN201310208480.6A patent/CN103271401B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557225A (en) * | 2004-01-15 | 2004-12-29 | 张巨柱 | Honeysuckle dew beverage making method |
| CN102485068A (en) * | 2010-12-01 | 2012-06-06 | 郧县正兴农业开发有限公司 | Preparation method of honeysuckle flower beverage |
| CN102113694A (en) * | 2010-12-28 | 2011-07-06 | 陈国英 | Method for manufacturing Japanese honeysuckle flower liquid |
| CN102935102A (en) * | 2012-10-19 | 2013-02-20 | 湖北楚天舒药业有限公司 | Method for simultaneously producing honeysuckle flower distillate and various active substances |
| CN103120348A (en) * | 2013-03-11 | 2013-05-29 | 朱世超 | Honeysuckle flower distillate beverage and production method thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103948629A (en) * | 2014-04-30 | 2014-07-30 | 桂林军供生化技术开发有限公司 | Preparation method for corn cervi pantotrichum extract |
| CN103948129A (en) * | 2014-04-30 | 2014-07-30 | 桂林军供生化技术开发有限公司 | Calcium supplement dew and preparation method thereof |
| CN104146247A (en) * | 2014-07-29 | 2014-11-19 | 桂林实力科技有限公司 | Preparation method of momordica grosvenori syrup |
| CN104432381A (en) * | 2014-12-12 | 2015-03-25 | 广州中国科学院先进技术研究所 | Honeysuckle health beverage and preparation method thereof |
| CN104432381B (en) * | 2014-12-12 | 2017-07-14 | 广州中国科学院先进技术研究所 | A kind of honeysuckle health-care beverage and preparation method thereof |
| CN106360219A (en) * | 2016-08-31 | 2017-02-01 | 成都幸有之科技有限公司 | Preparation method of honeysuckle beverage |
| CN108095108A (en) * | 2017-12-09 | 2018-06-01 | 天旺科技股份有限公司 | A kind of preparation method of Pitaya Flower health promoting liquid |
| CN116492382A (en) * | 2023-05-31 | 2023-07-28 | 湖北大别山药业股份有限公司 | Preparation method of antibacterial honeysuckle distilled liquid |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103271401B (en) | 2014-05-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103271401B (en) | Preparation method of honeysuckle flower distillate | |
| CN102813064B (en) | Plant extract feed additive for piglets | |
| CN101502534B (en) | Method for extracting medicinal material from Periplaneta americana | |
| CN104041602A (en) | Hyperlipidemia hypertension prevention health care sesame oil and preparation method thereof | |
| CN103892393A (en) | Preparation method for honeysuckle beverage | |
| CN107279446A (en) | A kind of betel nut colloid chews piece | |
| CN101658232A (en) | Method for preparing green tea confection | |
| CN104284601A (en) | Pleuropterus multiflorus extract and dipsacus asperoides extract for secreting insulin-like growth factor and promoting bone structure growth, and method for preparing same | |
| CN103816209A (en) | Eu-commin intragastric administration agent for cows and preparation method thereof | |
| KR101333152B1 (en) | Honey containing lavender | |
| CN105533598A (en) | Health-care honey and preparation method thereof | |
| CN102228473B (en) | Extraction method for active substances in cornua cervi pantotrichum | |
| CN101709076A (en) | Method for preparing hoof nail polypeptide | |
| CN104054863A (en) | Maca wolfberry Pu'er tea paste for improving energy and enhancing immunity and preparation method thereof | |
| CN108785358A (en) | A kind of preparation method of Honegsukle flower P.E | |
| CN108783159A (en) | A kind of Pitaya Flower Healthy Drink and preparation method thereof | |
| CN104026255A (en) | Health-care sesame oil capable of reducing cholesterol and preparation method thereof | |
| CN104026252A (en) | Health-care sesame oil with efficacies of nourishing lungs and removing dryness and preparation method thereof | |
| KR20090079653A (en) | Arrowroot Beverage and Manufacturing Method Thereof | |
| JPS58116650A (en) | Preparation of tonic food using sugar cane as raw material | |
| CN109602781A (en) | A kind of preparation method of Honegsukle flower P.E | |
| CN103005426A (en) | Preparation method for gingko biloba sarcotesta extracting solution | |
| CN103120347B (en) | Production method of vegetable beverage | |
| CN103907717B (en) | A kind of preparation method of green tea dew | |
| CN104222400A (en) | Pu'er tea cream with functions of dispelling alcohol effect, protecting liver, nourishing heart and tranquilizing mind and processing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |