CN107474915A - 一种金属管拉伸减少摩擦划痕的润滑油及其制备方法 - Google Patents

一种金属管拉伸减少摩擦划痕的润滑油及其制备方法 Download PDF

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CN107474915A
CN107474915A CN201710634470.7A CN201710634470A CN107474915A CN 107474915 A CN107474915 A CN 107474915A CN 201710634470 A CN201710634470 A CN 201710634470A CN 107474915 A CN107474915 A CN 107474915A
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metal tube
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王诗斌
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Chaohu Pengyuan Metal Pipe Co Ltd
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Abstract

一种金属管拉伸减少摩擦划痕的润滑油及其制备方法，包括以下重量份的原料组成：大豆150‑200份、改性胺与聚酰胺混合体10‑15份、滑石粉20‑25份；环氧树脂60‑65份、间本二胺10‑13份、苯酚5‑6份、烧碱5‑6份、氢氧化铵5‑6份、二乙烯三胺6‑9份、磷酸三甲酚酯8‑11份、30‑40份环氧有机硅、40‑50份环烷基基础油、抗磨损剂2‑5份、防腐防锈剂5‑10份、清洁因子2‑5份、抗氧化剂5‑15份、金属减活化剂1‑3份和粘度调节剂8‑12份。在控制基础油成本的同时能够保证较好的粘度指数和高抗磨性能；通过助剂的配合添加，有效在低温或高温环境下，减少金属管之间的摩擦，降低设备的维护成本，提供洁净的磨损防护模式，同时在此基础上，利用大豆和环氧树脂添加。

Description

一种金属管拉伸减少摩擦划痕的润滑油及其制备方法
技术领域：
本发明涉及化工领域，具体涉及一种金属管拉伸减少摩擦划痕的润滑油及其制备方法。
背景技术：
润滑油是涂在机器轴承表面的油状液体，按其来源分动物油、植物油、石油润滑油和合成润滑油四大类，其具有减少摩擦，避免发热、防止机器磨损等作用。
发明内容：
本发明所要解决的技术问题在于克服现有技术的缺陷，提供一种金属管拉伸减少摩擦划痕的润滑油及其制备方法。
本发明所要解决的技术问题采用以下技术方案来实现。
一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：包括以下重量份的原料组成：
大豆150-200份、改性胺与聚酰胺混合体10-15份、滑石粉20-25份；环氧树脂60-65份、间本二胺10-13份、苯酚5-6份、烧碱5-6份、氢氧化铵5-6份、二乙烯三胺6-9份、磷酸三甲酚酯8-11份、30-40份环氧有机硅、40-50份环烷基基础油、抗磨损剂2-5份、防腐防锈剂5-10份、清洁因子2-5份、抗氧化剂5-15份、金属减活化剂1-3份和粘度调节剂8-12份。
所述的抗磨损剂为硫化脂。
所述的防腐防锈剂为金属酚盐。
所述的抗氧化剂为2,3-二叔丁基对甲酚。
所述的金属减活化剂为硫化物。
所述的粘度调节剂为烷基苯乙烯。
一种金属管拉伸减少摩擦划痕的润滑油制备方法制备方法，包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将滑石粉与环氧树脂混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入间本二胺、苯酚、二乙烯三胺、磷酸三甲酚酯，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、氢氧化铵；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
本发明的有益效果是：在控制基础油成本的同时能够保证较好的粘度指数和高抗磨性能；通过助剂的配合添加，有效在低温或高温环境下，减少金属管之间的摩擦，降低设备的维护成本，提供洁净的磨损防护模式，同时在此基础上，利用大豆和环氧树脂添加；该润滑油的制备方法，步骤简单环保，易于实施。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
具体实施例1：一种金属管拉伸减少摩擦划痕的润滑油，包括以下重量份的原料组成：
大豆150份、改性胺与聚酰胺混合体10份、滑石粉20份；环氧树脂60份、间本二胺10份、苯酚5份、烧碱5份、氢氧化铵5份、二乙烯三胺6份、磷酸三甲酚酯8份、30份环氧有机硅、40份环烷基基础油、抗磨损剂2份、防腐防锈剂5份、清洁因子2份、抗氧化剂5份、金属减活化剂1份和粘度调节剂8份。
具体实施例2：一种金属管拉伸减少摩擦划痕的润滑油，包括以下重量份的原料组成：
大豆200份、改性胺与聚酰胺混合体15份、滑石粉25份；环氧树脂65份、间本二胺13份、苯酚6份、烧碱6份、氢氧化铵6份、二乙烯三胺9份、磷酸三甲酚酯11份、40份环氧有机硅、50份环烷基基础油、抗磨损剂5份、防腐防锈剂10份、清洁因子5份、抗氧化剂15份、金属减活化剂3份和粘度调节剂12份。
所述的抗磨损剂为硫化脂。
所述的防腐防锈剂为金属酚盐。
所述的抗氧化剂为2,3-二叔丁基对甲酚。
所述的金属减活化剂为硫化物。
所述的粘度调节剂为烷基苯乙烯。
一种金属管拉伸减少摩擦划痕的润滑油制备方法制备方法，包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将滑石粉与环氧树脂混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入间本二胺、苯酚、二乙烯三胺、磷酸三甲酚酯，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、氢氧化铵；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
经试验，对比现有的润滑油的情况：
通过对比可以看出，本法制备的润滑剂粘度指数和高抗磨性能；通过助剂的配合添加，有效在低温或高温环境下，减少金属管之间的摩擦。
以上显示和描述了本发明的基本原理、主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (7)

1.一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：包括以下重量份的原料组成：
大豆150-200份、改性胺与聚酰胺混合体10-15份、滑石粉20-25份；环氧树脂60-65份、间本二胺10-13份、苯酚5-6份、烧碱5-6份、氢氧化铵5-6份、二乙烯三胺6-9份、磷酸三甲酚酯8-11份、30-40份环氧有机硅、40-50份环烷基基础油、抗磨损剂2-5份、防腐防锈剂5-10份、清洁因子2-5份、抗氧化剂5-15份、金属减活化剂1-3份和粘度调节剂8-12份。
2.根据权利要求中所述的一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：所述的抗磨损剂为硫化脂。
3.根据权利要求中所述的一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：所述的防腐防锈剂为金属酚盐。
4.根据权利要求中所述的一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：所述的抗氧化剂为2,3-二叔丁基对甲酚。
5.根据权利要求中所述的一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：所述的金属减活化剂为硫化物。
6.根据权利要求中所述的一种金属管拉伸减少摩擦划痕的润滑油，其特征在于：所述的粘度调节剂为烷基苯乙烯。
7.一种金属管拉伸减少摩擦划痕的润滑油制备方法制备方法，其特征在于：包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将滑石粉与环氧树脂混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入间本二胺、苯酚、二乙烯三胺、磷酸三甲酚酯，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、氢氧化铵；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
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CN102585988A (zh) * 2011-12-30 2012-07-18 大连三达奥克化学股份有限公司 无缝钢管拉拔润滑乳化油及生产方法
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CN104073206A (zh) * 2014-06-23 2014-10-01 安徽神舟飞船胶业有限公司 改性环氧树脂粘胶剂配方及其制备工艺
CN105623752A (zh) * 2016-02-27 2016-06-01 安徽海德石油化工有限公司 一种大豆与植物混合燃料油及其制备方法

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CN102585988A (zh) * 2011-12-30 2012-07-18 大连三达奥克化学股份有限公司 无缝钢管拉拔润滑乳化油及生产方法
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