CN107353981A - 一种金属管制造设备所用润滑剂及其制备方法 - Google Patents

一种金属管制造设备所用润滑剂及其制备方法 Download PDF

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CN107353981A
CN107353981A CN201710634472.6A CN201710634472A CN107353981A CN 107353981 A CN107353981 A CN 107353981A CN 201710634472 A CN201710634472 A CN 201710634472A CN 107353981 A CN107353981 A CN 107353981A
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parts
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metal tube
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王诗斌
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Chaohu Pengyuan Metal Pipe Co Ltd
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Abstract

一种金属管制造设备所用润滑剂及其制备方法，包括以下重量份的原料组成：大豆150‑200份、改性胺与聚酰胺混合体10‑15份、丙烯酸丁酯20‑25份；甲基纤维素60‑65份、一氯醋酸10‑13份、丙烯酸5‑6份、烧碱5‑6份、去离子水5‑6份、甲苯二异氰酸酯6‑9份、甲阶酚醛树脂8‑11份、30‑40份环氧有机硅、40‑50份环烷基基础油、抗磨损剂2‑5份、防腐防锈剂5‑10份、清洁因子2‑5份、抗氧化剂5‑15份、金属减活化剂1‑3份和粘度调节剂8‑12份。在控制基础油成本的同时能够保证较好的粘度指数和高抗磨性能；通过助剂的配合添加，能有效去除包覆在引擎零件上浓稠的黑碳泥粒子，延长引擎的使用寿命，降低设备的维护成本，为叉车引擎提供洁净的磨损防护模式；该润滑油的制备方法，步骤简单环保，易于实施。

Description

一种金属管制造设备所用润滑剂及其制备方法
技术领域：
本发明涉及化工领域，具体涉及一种金属管制造设备所用润滑剂及其制备方法。
背景技术：
润滑油是涂在机器轴承表面的油状液体，按其来源分动物油、植物油、石油润滑油和合成润滑油四大类，其具有减少摩擦，避免发热、防止机器磨损等作用。
发明内容：
本发明所要解决的技术问题在于克服现有技术的缺陷，提供一种金属管制造设备所用润滑剂及其制备方法。
本发明所要解决的技术问题采用以下技术方案来实现。
一种金属管制造设备所用润滑剂，其特征在于：包括以下重量份的原料组成：
大豆150-200份、改性胺与聚酰胺混合体10-15份、丙烯酸丁酯20-25份；甲基纤维素60-65份、一氯醋酸10-13份、丙烯酸5-6份、烧碱5-6份、去离子水5-6份、甲苯二异氰酸酯6-9份、甲阶酚醛树脂8-11份、30-40份环氧有机硅、40-50份环烷基基础油、抗磨损剂2-5份、防腐防锈剂5-10份、清洁因子2-5份、抗氧化剂5-15份、金属减活化剂1-3份和粘度调节剂8-12份。
所述的抗磨损剂为硫化脂。
所述的防腐防锈剂为金属酚盐。
所述的抗氧化剂为2,3-二叔丁基对甲酚。
所述的金属减活化剂为硫化物。
所述的粘度调节剂为烷基苯乙烯。
一种金属管制造设备所用润滑剂制备方法制备方法，包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将丙烯酸丁酯与甲基纤维素混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入一氯醋酸、丙烯酸、甲苯二异氰酸酯、甲阶酚醛树脂，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、去离子水；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
本发明的有益效果是：在控制基础油成本的同时能够保证较好的粘度指数和高抗磨性能；通过助剂的配合添加，有效在低温或高温环境下，减少金属管之间的摩擦，降低设备的维护成本，提供洁净的磨损防护模式，同时在此基础上，利用大豆和环氧树脂添加；该润滑油的制备方法，步骤简单环保，易于实施。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
具体实施例1：一种金属管制造设备所用润滑剂，包括以下重量份的原料组成：
大豆150份、改性胺与聚酰胺混合体10份、丙烯酸丁酯20份；甲基纤维素60份、一氯醋酸10份、丙烯酸5份、烧碱5份、去离子水5份、甲苯二异氰酸酯6份、甲阶酚醛树脂8份、30份环氧有机硅、40份环烷基基础油、抗磨损剂2份、防腐防锈剂5份、清洁因子2份、抗氧化剂5份、金属减活化剂1份和粘度调节剂8份。
具体实施例2：一种金属管制造设备所用润滑剂，包括以下重量份的原料组成：
大豆200份、改性胺与聚酰胺混合体15份、丙烯酸丁酯25份；甲基纤维素65份、一氯醋酸13份、丙烯酸6份、烧碱6份、去离子水6份、甲苯二异氰酸酯9份、甲阶酚醛树脂11份、40份环氧有机硅、50份环烷基基础油、抗磨损剂5份、防腐防锈剂10份、清洁因子5份、抗氧化剂15份、金属减活化剂3份和粘度调节剂12份。
所述的抗磨损剂为硫化脂。
所述的防腐防锈剂为金属酚盐。
所述的抗氧化剂为2,3-二叔丁基对甲酚。
所述的金属减活化剂为硫化物。
所述的粘度调节剂为烷基苯乙烯。
一种金属管制造设备所用润滑剂制备方法制备方法，包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将丙烯酸丁酯与甲基纤维素混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入一氯醋酸、丙烯酸、甲苯二异氰酸酯、甲阶酚醛树脂，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、去离子水；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
经试验，对比现有的润滑油的情况：
通过对比可以看出，本法制备的润滑剂粘度指数和高抗磨性能；通过助剂的配合添加，有效在低温或高温环境下，减少金属管之间的摩擦。
以上显示和描述了本发明的基本原理、主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (7)

1.一种金属管制造设备所用润滑剂，其特征在于：包括以下重量份的原料组成：
大豆150-200份、改性胺与聚酰胺混合体10-15份、丙烯酸丁酯20-25份；甲基纤维素60-65份、一氯醋酸10-13份、丙烯酸5-6份、烧碱5-6份、去离子水5-6份、甲苯二异氰酸酯6-9份、甲阶酚醛树脂8-11份、30-40份环氧有机硅、40-50份环烷基基础油、抗磨损剂2-5份、防腐防锈剂5-10份、清洁因子2-5份、抗氧化剂5-15份、金属减活化剂1-3份和粘度调节剂8-12份。
2.根据权利要求中所述的一种金属管制造设备所用润滑剂，其特征在于：所述的抗磨损剂为硫化脂。
3.根据权利要求中所述的一种金属管制造设备所用润滑剂，其特征在于：所述的防腐防锈剂为金属酚盐。
4.根据权利要求中所述的一种金属管制造设备所用润滑剂，其特征在于：所述的抗氧化剂为2,3-二叔丁基对甲酚。
5.根据权利要求中所述的一种金属管制造设备所用润滑剂，其特征在于：所述的金属减活化剂为硫化物。
6.根据权利要求中所述的一种金属管制造设备所用润滑剂，其特征在于：所述的粘度调节剂为烷基苯乙烯。
7.一种金属管制造设备所用润滑剂制备方法制备方法，其特征在于：包括以下步骤：
步骤1：取大豆，分离大豆皮，待用，从大豆中分离蛋白8％-20％、尿素15％-17％、多聚磷酸钠1％-10％，将尿素分散在水中，混合制成尿素溶液，
步骤2：将丙烯酸丁酯与甲基纤维素混合，放入蒸馏瓶内，同时将改性胺与聚酰胺混合体与环烷基基础油混合，待完全混合后，加入环氧有机硅，加入蒸馏内混合，得到基础油；
步骤3：将基础油、防腐防锈剂及抗氧化剂，混合，进行高温低压蒸馏，温度460-480℃、压强0.03-0.06MPa，快速分离轻质油和重质油；
步骤4：将重质油，加入蛋白，在常温下搅拌1-2小时，再加入多聚磷酸钠，继续搅拌2-3小时，然后进行沉淀分离，分离后，取上1/3层油，
步骤5：将大豆皮磨碎，装入提取器中，加入重质油和尿素溶液，在，固液比例为12:1，温度为70-80℃的条件下提取6小时，然后抽滤，对滤液进行真空浓缩，回收溶剂；
步骤6：将步骤4和步骤5混合，采用分级萃取，萃取压力为28-35MPa，温度42-48℃，萃取时间为1.5-2小时，然后进行二级分离，第一级分离压力为8-10MPa，温度为53-57℃，第二季为3-5MPa，温度为30-40℃；
步骤7：依次加入一氯醋酸、丙烯酸、甲苯二异氰酸酯、甲阶酚醛树脂，加热搅拌，加热温度为190℃，时长10分钟、冷却至70℃，加入烧碱、去离子水；
步骤8：将步骤6、步骤7与抗磨损剂、清洁因子、金属减活化剂、粘度调节剂按原料比例混合，过滤，即可。
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CN103526598A (zh) * 2013-10-25 2014-01-22 合肥聚合辐化技术有限公司 一种耐摩擦牢度印花粘合剂及其制备方法
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CN105623752A (zh) * 2016-02-27 2016-06-01 安徽海德石油化工有限公司 一种大豆与植物混合燃料油及其制备方法
CN106634594A (zh) * 2016-12-19 2017-05-10 安徽温禾新材料科技股份有限公司 木地板背面强化防断裂涂层及其制备方法

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CN103526598A (zh) * 2013-10-25 2014-01-22 合肥聚合辐化技术有限公司 一种耐摩擦牢度印花粘合剂及其制备方法
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