CN107467084A - A kind of special disinfectant for aquaculture and its preparation - Google Patents

A kind of special disinfectant for aquaculture and its preparation Download PDF

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Publication number
CN107467084A
CN107467084A CN201710481910.XA CN201710481910A CN107467084A CN 107467084 A CN107467084 A CN 107467084A CN 201710481910 A CN201710481910 A CN 201710481910A CN 107467084 A CN107467084 A CN 107467084A
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China
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agent
parts
water
aquaculture
disinfectant
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Chinese (zh)
Inventor
朱蓓
朱岩
张艳侠
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ANHUI HUANGHUAI VETERINARY MEDICINE CO LTD
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ANHUI HUANGHUAI VETERINARY MEDICINE CO LTD
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Publication of CN107467084A publication Critical patent/CN107467084A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
    • A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
    • A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14—Boron; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/045—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing sulfur, e.g. sulfates, thiosulfates, gypsum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/20—Heavy metals or heavy metal compounds

Abstract

The present invention proposes a kind of special disinfectant for aquaculture and its preparation, including mass ratio 3:1.2 1.6 A agent and B agent, the A agent includes tetrakis hydroxymetyl phosphonium sulfuric, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent includes Chinese medicine extract, medical stone, allicin, citric acid, water, preparation technology of the present invention is simple, obtained disinfectant safety and environmental protection, has good sterilization effect compared to traditional chlorine disinfectant, and there is certain improvement to water quality, aquatic products growth, inherently improve the economic benefit of aquaculture.

Description

A kind of special disinfectant for aquaculture and its preparation
Technical field
The present invention relates to technical field of aquaculture, and in particular to a kind of special disinfectant for aquaculture and its preparation.
Background technology
According to statistics, aquaculture amount in China's accounts for more than 2/3rds of world aquaculture total amount, as China is intensive The fast development of aquaculture, the pollution that Cultivated water is subject to is increasingly severe, various pathogenic microorganism amount reproductions, result in Aquatic animal disease frequently occurs, and seriously hinders the sound development of culture fishery.On the other hand, raiser uses disinfectant mostly To kill the harmful microorganism in aquatic environment, improve water body environment.The disinfectant commonly used at present on aquatic products is mostly chloride disappears Toxic agent, such as bleaching powder, sym-closene, sodium hypochlorite, chlorine dioxide, sodium trichloro-isocyanurate, chlorinated product cost is relatively low, But inorganic chlorine property is unstable, the influence of easy light, heat and humidity, active ingredient is lost.And research shows, such disinfectant The effect for killing microorganism is had a great influence by water environmental factor, and typically with the rise of temperature, it, which is acted on, strengthens, with the liter of pH value Height, its declines, when content of organics is excessively in water body, its Disinfection Effect is decreased obviously, and these chlorine-containing disinfectant meetings Penetrating odor is produced, larger to the excitant of aquatic livestock, therefore, it is good that urgent need works out a kind of green harmless and Disinfection Effect Aquatic products disinfectant.
The content of the invention
For above-mentioned problem, the present invention proposes a kind of special disinfectant for aquaculture and its preparation, prepares work Skill is simple, and obtained disinfectant safety and environmental protection, has good sterilization effect compared to traditional chlorine disinfectant, and right Water quality, aquatic products growth have certain improvement, inherently improve the economic benefit of aquaculture.
In order to realize above-mentioned purpose, the present invention uses following technical scheme：
A kind of special disinfectant for aquaculture, including mass ratio 3:1.2-1.6 A agent and B agent, the A agent include four hydroxyls Methylsulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, Citric acid, water.
Preferably, each component mass fraction proportioning is tetrakis hydroxymetyl phosphonium sulfuric 28-36 parts, potassium hydrogen persulfate in the A agent 9-15 parts, kodalk 6-10 parts, glacial acetic acid 5-20 parts, water 1-10 parts.
Preferably, the A agent also includes oxygenation agent 3-8 parts, and the oxygenation agent is sodium peroxide or calper calcium peroxide.
Preferably, each component mass fraction proportioning is Chinese medicine extract 22-24 parts, medical stone 36-40 parts, garlic in B agent Plain 4-8 parts, citric acid 5-10 parts, water 5-10 parts.
Preferably, B agent also includes mass fraction at least one in the o-vanillin, caryophyllus oil, ethylmaltol of 2-5 parts Kind.
Preferably, Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko.
Preferably, each component percentage composition is crowndaisy chrysanthemum 25-30%, honeysuckle 20-30%, the Chinese bulbul in Chinese medicine extract 15-30% and gingko surplus.
Preferably, special disinfectant for aquaculture, preparation process are as follows：
1) preparation of A agent：Raw material is weighed by weight, and glacial acetic acid and water are blended, are then added thereto kodalk, Surplus materials is at least added thereto at twice again, after stirring, produces A agent；
2) preparation of B agent：Medical stone, water are blended, then add citric acid thereto, 45 DEG C are stirred 20-25min, so The insulation reaction 1-2h under the conditions of 40 DEG C afterwards, is dried in vacuo to obtain powder after taking-up, be blended, stir by powder and other remaining materials After mixing uniformly, B agent is produced；
3) A agent, B agent are blended, are then fed into comminutor and are granulated, gained particle is crossed 25 mesh sieves and produced.
Due to using above-mentioned technical scheme, the beneficial effects of the invention are as follows：Preparation technology of the present invention is simple, obtained to disappear Toxic agent safety and environmental protection, has good sterilization effect, and water quality, aquatic products are grown compared to traditional chlorine disinfectant With certain improvement, the economic benefit of aquaculture is inherently improved.
The present invention coordinates Chinese medicine extract double sterilization using chemical reagent, cannot be only used for the disinfection of water quality, together When improve the clean-up effect of water quality, coordinate medical stone, citric acid to effectively improve the content and heavy metal of oxygen in water The adsorptivity of ion, in addition, Chinese medical extract has good taste removal effect, reduce excitant of the disinfectant to aquatic products.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the present invention is clearly and completely described.Based on embodiments of the invention, the common skill in this area The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects Enclose.
Embodiment 1:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.4 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 28 parts of tetrakis hydroxymetyl phosphonium sulfuric, 12 parts of potassium hydrogen persulfate, inclined boron in A agent Sour 8 parts of sodium, 15 parts of glacial acetic acid, 6 parts of water, A agent also include 4 parts of oxygenation agent, and the oxygenation agent is sodium peroxide.
Each component mass fraction proportioning is 22 parts of Chinese medicine extract, 38 parts of medical stone, 6 parts of allicin, citric acid 8 in B agent Part, 5 parts of water, B agent also include the o-vanillin that mass fraction is 3 parts and ethylmaltol combination.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 25%, honeysuckle 26%, the Chinese bulbul 18% and gingko surplus.
Special disinfectant for aquaculture, preparation process are as follows：
1) preparation of A agent：Raw material is weighed by weight, and glacial acetic acid and water are blended, are then added thereto kodalk, Surplus materials is added thereto at twice again, after stirring, produces A agent；
2) preparation of B agent：Medical stone, water are blended, then add citric acid thereto, 45 DEG C are stirred 20-25min, so The insulation reaction 1-2h under the conditions of 40 DEG C afterwards, is dried in vacuo to obtain powder after taking-up, be blended, stir by powder and other remaining materials After mixing uniformly, B agent is produced；
3) A agent, B agent are blended, are then fed into comminutor and are granulated, gained particle is crossed 25 mesh sieves and produced.
Embodiment 2:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.5 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 32 parts of tetrakis hydroxymetyl phosphonium sulfuric, 10 parts of potassium hydrogen persulfate, inclined boron in A agent Sour 6 parts of sodium, 20 parts of glacial acetic acid, 5 parts of water, A agent also include 3 parts of oxygenation agent, and the oxygenation agent is calper calcium peroxide.
Each component mass fraction proportioning is 23 parts of Chinese medicine extract, 36 parts of medical stone, 7 parts of allicin, citric acid 8 in B agent Part, 8 parts of water, B agent also include the ethylmaltol that mass fraction is 4 parts.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 30%, honeysuckle 24%, the Chinese bulbul 22% and gingko surplus.
The present embodiment preparation process is the same as embodiment 1.
Embodiment 3:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.6 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 30 parts of tetrakis hydroxymetyl phosphonium sulfuric, 15 parts of potassium hydrogen persulfate, inclined boron in A agent Sour 6 parts of sodium, 10 parts of glacial acetic acid, 10 parts of water, A agent also include 8 parts of oxygenation agent, and the oxygenation agent is sodium peroxide.
Each component mass fraction proportioning is 24 parts of Chinese medicine extract, 40 parts of medical stone, 8 parts of allicin, citric acid 6 in B agent Part, 10 parts of water, B agent also include the o-vanillin that mass fraction is 4 parts.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 28%, honeysuckle 28%, the Chinese bulbul 25% and gingko surplus.
The present embodiment preparation process is the same as embodiment 1.
Embodiment 4:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.5 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 35 parts of tetrakis hydroxymetyl phosphonium sulfuric, 13 parts of potassium hydrogen persulfate, inclined boron in A agent Sour 9 parts of sodium, 12 parts of glacial acetic acid, 1 part of water, A agent also include 5 parts of oxygenation agent, and the oxygenation agent is sodium peroxide.
Each component mass fraction proportioning is 24 parts of Chinese medicine extract, 40 parts of medical stone, 4 parts of allicin, citric acid 10 in B agent Part, 8 parts of water, B agent also include the o-vanillin that mass fraction is 5 parts.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 28%, honeysuckle 30%, the Chinese bulbul 30% and gingko surplus.
The present embodiment preparation process is the same as embodiment 1.
Embodiment 5:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.6 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 36 parts of tetrakis hydroxymetyl phosphonium sulfuric, 9 parts of potassium hydrogen persulfate, metaboric acid in A agent 10 parts of sodium, 5 parts of glacial acetic acid, 5 parts of water, A agent also include 4 parts of oxygenation agent, and the oxygenation agent is calper calcium peroxide.
Each component mass fraction proportioning is 22 parts of Chinese medicine extract, 36 parts of medical stone, 8 parts of allicin, citric acid 10 in B agent Part, 6 parts of water, B agent also include the caryophyllus oil that mass fraction is 4 parts, ethylmaltol composition.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 26%, honeysuckle 25%, the Chinese bulbul 15% and gingko surplus.
The present embodiment preparation process is the same as embodiment 1.
Embodiment 6:
A kind of special disinfectant for aquaculture, including mass ratio 3:1.5 A agent and B agent, the A agent include tetra methylol Sulfuric acid phosphorus, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent include Chinese medicine extract, medical stone, allicin, lemon Acid, water.
Wherein, each component mass fraction proportioning is 34 parts of tetrakis hydroxymetyl phosphonium sulfuric, 11 parts of potassium hydrogen persulfate, inclined boron in A agent Sour 8 parts of sodium, 14 parts of glacial acetic acid, 7 parts of water, A agent also include 6 parts of oxygenation agent, and the oxygenation agent is calcium oxide.
Each component mass fraction proportioning is 23 parts of Chinese medicine extract, 38 parts of medical stone, 5 parts of allicin, citric acid 5 in B agent Part, 5 parts of water, B agent also include the o-vanillin that mass fraction is 3 parts, ethylmaltol composition.
Chinese medicine extract includes crowndaisy chrysanthemum, honeysuckle, the Chinese bulbul and gingko, and each component percentage composition is Tong in Chinese medicine extract Wormwood artemisia 25%, honeysuckle 20%, the Chinese bulbul 24% and gingko surplus.
The present embodiment preparation process is the same as embodiment 1.
Product made from the embodiment of the present invention 1 is subjected to performance test, cancels toxic agent 100g and is watered 1000kg uses, uniformly Fish pond surface is sprayed on, sprays once after first sprinkling, sprays 3 times altogether every three days.
To spray beginning timing for the last time, observation uses different time sections water quality index after disinfectant：
From above table data, disinfectant of the present invention has excellent water correction effect.
In addition, sterilising index (sterilization rate, %) after different extension rates is used to be counted (same to disinfectant of the present invention Sample is with timing after the completion of spraying three times), data are as follows：
Staphylococcus aureus Escherichia coli Bacillus subtilis
1：100 100 100 100
1:500 100 100 100
1:1000 100 100 83
1:5000 99 99 70
1:10000 96.8 97.2 41
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (8)

  1. A kind of 1. special disinfectant for aquaculture, it is characterised in that：Including mass ratio 3:1.2-1.6 A agent and B agent, the A agent Including tetrakis hydroxymetyl phosphonium sulfuric, potassium hydrogen persulfate, kodalk, glacial acetic acid, water, the B agent includes Chinese medicine extract, wheat meal Stone, allicin, citric acid, water.
  2. 2. special disinfectant for aquaculture according to claim 1, it is characterised in that：Each component mass parts in the A agent Number proportioning is tetrakis hydroxymetyl phosphonium sulfuric 28-36 parts, potassium hydrogen persulfate 9-15 parts, kodalk 6-10 parts, glacial acetic acid 5-20 parts, water 1-10 parts.
  3. 3. special disinfectant for aquaculture according to claim 2, it is characterised in that：The A agent also includes oxygenation agent 3-8 Part, the oxygenation agent is sodium peroxide or calper calcium peroxide.
  4. 4. special disinfectant for aquaculture according to claim 1, it is characterised in that：Each component mass parts in the B agent Number proportioning is Chinese medicine extract 22-24 parts, medical stone 36-40 parts, allicin 4-8 parts, citric acid 5-10 parts, water 5-10 parts.
  5. 5. special disinfectant for aquaculture according to claim 4, it is characterised in that：The B agent also includes mass fraction At least one of o-vanillin, caryophyllus oil, ethylmaltol for 2-5 parts.
  6. 6. special disinfectant for aquaculture according to claim 1, it is characterised in that：The Chinese medicine extract includes Tong Wormwood artemisia, honeysuckle, the Chinese bulbul and gingko.
  7. 7. special disinfectant for aquaculture according to claim 6, it is characterised in that：Each component in the Chinese medicine extract Percentage composition is crowndaisy chrysanthemum 25-30%, honeysuckle 20-30%, Chinese bulbul 15-30% and gingko surplus.
  8. 8. according to the special disinfectant for aquaculture described in claim any one of 1-7, it is characterised in that preparation process is as follows：
    1) preparation of A agent：Raw material is weighed by weight, and glacial acetic acid and water are blended, are then added thereto kodalk, then will Surplus materials is at least added thereto at twice, after stirring, produces A agent；
    2) preparation of B agent：Medical stone, water are blended, then add citric acid, 45 DEG C of stirrings 20-25min, Ran Hou thereto Insulation reaction 1-2h under the conditions of 40 DEG C, is dried in vacuo to obtain powder after taking-up, be blended by powder and other remaining materials, stirring is equal After even, B agent is produced；
    3) A agent, B agent are blended, are then fed into comminutor and are granulated, gained particle is crossed 25 mesh sieves and produced.
CN201710481910.XA 2017-06-22 2017-06-22 A kind of special disinfectant for aquaculture and its preparation Pending CN107467084A (en)

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CN108244104A (en) * 2017-12-29 2018-07-06 常州市阿曼特化工有限公司 A kind of preparation method of ornamental fish disinfection tablet
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CN110623005A (en) * 2019-09-16 2019-12-31 江西省农业科学院蔬菜花卉研究所 Compound plant extract for inhibiting bitter gourd fusarium wilt and preparation method thereof
CN110623005B (en) * 2019-09-16 2021-06-29 江西省农业科学院蔬菜花卉研究所 Compound plant extract for inhibiting bitter gourd fusarium wilt and preparation method thereof

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Application publication date: 20171215