CN107429316B - 镍硫化物的制造方法、镍氧化物矿的湿式冶炼方法 - Google Patents

镍硫化物的制造方法、镍氧化物矿的湿式冶炼方法 Download PDF

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Publication number
CN107429316B
CN107429316B CN201580077312.5A CN201580077312A CN107429316B CN 107429316 B CN107429316 B CN 107429316B CN 201580077312 A CN201580077312 A CN 201580077312A CN 107429316 B CN107429316 B CN 107429316B
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China
Prior art keywords
nickel
sulfide
amount
sulfuric acid
nickel sulfide
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Expired - Fee Related
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CN201580077312.5A
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English (en)
Chinese (zh)
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CN107429316A (zh
Inventor
中村真郎
中村真一郎
中井修
三井宏之
柴山敬介
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Sumitomo Metal Mining Co Ltd
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Sumitomo Metal Mining Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/11—Sulfides; Oxysulfides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043—Sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
CN201580077312.5A 2015-03-05 2015-12-01 镍硫化物的制造方法、镍氧化物矿的湿式冶炼方法 Expired - Fee Related CN107429316B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2015043693A JP6222141B2 (ja) 2015-03-05 2015-03-05 ニッケル硫化物の製造方法、ニッケル酸化鉱石の湿式製錬方法
JP2015-043693 2015-03-05
PCT/JP2015/083794 WO2016139858A1 (ja) 2015-03-05 2015-12-01 ニッケル硫化物の製造方法、ニッケル酸化鉱石の湿式製錬方法

Publications (2)

Publication Number Publication Date
CN107429316A CN107429316A (zh) 2017-12-01
CN107429316B true CN107429316B (zh) 2019-04-19

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Country Status (8)

Country Link
US (1) US10017835B2 (enExample)
EP (1) EP3266885B1 (enExample)
JP (1) JP6222141B2 (enExample)
CN (1) CN107429316B (enExample)
AU (1) AU2015384934B2 (enExample)
CA (1) CA2978233C (enExample)
PH (1) PH12017501582B1 (enExample)
WO (1) WO2016139858A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6350684B2 (ja) * 2016-11-30 2018-07-04 住友金属鉱山株式会社 ニッケル酸化鉱石の湿式製錬方法
WO2018101069A1 (ja) * 2016-11-30 2018-06-07 住友金属鉱山株式会社 ニッケル酸化鉱石の湿式製錬方法
JP7035735B2 (ja) * 2018-04-03 2022-03-15 住友金属鉱山株式会社 低ニッケル品位酸化鉱石からのニッケルコバルト混合硫化物の製造方法
CN119301073A (zh) * 2022-06-10 2025-01-10 尤米科尔公司 用于金属硫化的方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1309194A (zh) * 2000-11-28 2001-08-22 华东理工大学 含镍三氯化铁蚀刻废液再生和镍回收方法
CN1736883A (zh) * 2005-07-15 2006-02-22 曹国华 从红土镍矿酸浸液中获得硫化镍的方法
CN101298638A (zh) * 2008-06-27 2008-11-05 中南大学 一种从红土镍矿浸出液分离富集镍钴的方法
CN101466855A (zh) * 2006-03-31 2009-06-24 拜奥特克环保技术公司 硫化镍沉淀方法
US7563421B2 (en) * 2004-05-13 2009-07-21 Sumitomo Metal Mining Co., Ltd. Hydrometallurgical process of nickel oxide ore
CN102918171A (zh) * 2010-07-28 2013-02-06 住友金属矿山株式会社 由低品位氧化镍矿石制造镍铁熔炼原料的方法
CN102994746A (zh) * 2012-11-21 2013-03-27 广西藤县雅照钛白有限公司 工业废酸制取硫化镍精矿的方法
EP2749660A1 (en) * 2011-08-22 2014-07-02 Sumitomo Metal Mining Co., Ltd. Nickel recovery loss reduction method, hydrometallurgical method for nickel oxidized ore, and sulfuration treatment system
CN103946401A (zh) * 2011-11-22 2014-07-23 住友金属矿山株式会社 高纯度硫酸镍的制造方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4547347A (en) * 1983-12-02 1985-10-15 Amax Inc. Granulometric control of nickel sulfide precipitate
JPH0681050A (ja) 1991-10-31 1994-03-22 Taiheiyo Kinzoku Kk ニッケル、コバルトの回収方法
AU2002950815A0 (en) * 2002-08-15 2002-09-12 Wmc Resources Ltd Recovery nickel
JP4762517B2 (ja) 2004-09-09 2011-08-31 株式会社オプトニクス精密 プリンター用トナーの製造方法
JP5572928B2 (ja) * 2008-07-25 2014-08-20 住友金属鉱山株式会社 ニッケル酸化鉱石の湿式製錬方法
US8298501B2 (en) * 2008-06-27 2012-10-30 Bhp Billiton Ssm Development Pty Ltd. Process for forming high density sulfides
JP5257501B2 (ja) * 2011-11-04 2013-08-07 住友金属鉱山株式会社 鉱石スラリーの製造方法及び金属製錬方法
JP5765459B2 (ja) * 2014-04-02 2015-08-19 住友金属鉱山株式会社 ニッケル回収ロスの低減方法、ニッケル酸化鉱石の湿式製錬方法、並びに硫化処理システム

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1309194A (zh) * 2000-11-28 2001-08-22 华东理工大学 含镍三氯化铁蚀刻废液再生和镍回收方法
US7563421B2 (en) * 2004-05-13 2009-07-21 Sumitomo Metal Mining Co., Ltd. Hydrometallurgical process of nickel oxide ore
CN1736883A (zh) * 2005-07-15 2006-02-22 曹国华 从红土镍矿酸浸液中获得硫化镍的方法
CN101466855A (zh) * 2006-03-31 2009-06-24 拜奥特克环保技术公司 硫化镍沉淀方法
CN101298638A (zh) * 2008-06-27 2008-11-05 中南大学 一种从红土镍矿浸出液分离富集镍钴的方法
CN102918171A (zh) * 2010-07-28 2013-02-06 住友金属矿山株式会社 由低品位氧化镍矿石制造镍铁熔炼原料的方法
EP2749660A1 (en) * 2011-08-22 2014-07-02 Sumitomo Metal Mining Co., Ltd. Nickel recovery loss reduction method, hydrometallurgical method for nickel oxidized ore, and sulfuration treatment system
CN103946401A (zh) * 2011-11-22 2014-07-23 住友金属矿山株式会社 高纯度硫酸镍的制造方法
CN102994746A (zh) * 2012-11-21 2013-03-27 广西藤县雅照钛白有限公司 工业废酸制取硫化镍精矿的方法

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Publication number Publication date
CA2978233A1 (en) 2016-09-09
CN107429316A (zh) 2017-12-01
PH12017501582A1 (en) 2018-02-05
AU2015384934A1 (en) 2017-09-21
EP3266885A1 (en) 2018-01-10
US20180044760A1 (en) 2018-02-15
US10017835B2 (en) 2018-07-10
PH12017501582B1 (en) 2022-01-05
WO2016139858A1 (ja) 2016-09-09
JP2016160526A (ja) 2016-09-05
EP3266885A4 (en) 2018-03-07
JP6222141B2 (ja) 2017-11-01
EP3266885B1 (en) 2019-01-23
CA2978233C (en) 2019-10-01
AU2015384934B2 (en) 2019-05-02

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