CN107382544A - A kind of liquid fertilizer containing medical stone and preparation method thereof - Google Patents
A kind of liquid fertilizer containing medical stone and preparation method thereof Download PDFInfo
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- CN107382544A CN107382544A CN201710817176.XA CN201710817176A CN107382544A CN 107382544 A CN107382544 A CN 107382544A CN 201710817176 A CN201710817176 A CN 201710817176A CN 107382544 A CN107382544 A CN 107382544A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Pest Control & Pesticides (AREA)
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Abstract
The invention discloses a kind of liquid fertilizer containing medical stone, it is made up of the raw material below according to parts by weight：50 55 parts of medical stone extract solution, 38 42 parts of urea, 15 20 parts of potassium dihydrogen phosphate, 12 parts of compound sodium nitrophenolate, 0.7 1.1 parts of diethyl aminoethyl hexanoate, 0.8 1.3 parts of indolebutyric acid sodium, 12 16 parts of potassium fulvate, 47 parts of borax decahydrate, 25 parts of ammonium molybdate tetrahydrate, 7 11 parts of ammonium phosphate, 10 15 parts of zinc sulfate, 35 40 parts of seaweed extracted liquor, 180 200 parts of water.The invention also discloses the preparation method of the liquid fertilizer containing medical stone.The liquid fertilizer can effectively supplement the element of crop missing, improve crop resistance, improve crop yield.
Description
Technical field
The present invention relates to technical field of fertilizers, specifically a kind of liquid fertilizer containing medical stone and preparation method thereof.
Background technology
The development of planting industry in agricultural production be unable to do without fertilizer.The agricultural in China has had the long history of 10,000 years, ancient
Generation fertilizer is referred to as excrement, and fertilising then turns into excrement field.The farmland fertilization in China begins at approximately abundant Shang Dynasty's generation, mainly according to unearthed relics
In dredged up at that time river silt wooden instrument and abundant business's inscriptions on bones or tortoise shells in represented that the fonts such as dung, heap soil or fertilizer over and around the roots are recorded, and have fertilising can
With the fore-telling word of volume increase.Pay attention to the Warring States Period and emphasized farmland fertilization.Ancient Times in China preferably at most by the use of animal wastes as
Fertilizer, decomposed people, animal fecaluria, silkworm faeces, weeds, plant ash, beanstalk, river silt, bone juice etc. are utilized again to the Warring states and Qin Han.In Han dynasty
Pig collected manure is taken much count of.
So far, its species is more and more for Fertilizer development, and liquid fertilizer is exactly one kind therein.Liquid fertilizer, also known as fluid
Fertilizer, liquid fertilizer is commonly called as, is with the fluid product of the nutrient needed for one or more kinds of crops, generally with N, P, K tri-
Big one of nutrient or one of which are the theme, and also usually include many micronutrient elements etc..
Liquid fertilizer, there is advantages below：1st, easily absorb, it is quick；2nd, dissolved dilution does not cool, and easily uniformly divides after
It is distributed in soil, concentrates the local salinity that applies fertilizer high not as solid fertilizer is formed, be not easy frostbite offspring；3rd, can spray, drip irrigation or
Pour, easy to use, cost saving, produce effects fast；4th, be able to can be simultaneously well mixed with insecticide, bactericide, herbicide mixture；5th, will not
Picture solid fertilizer produces isolation in accumulating and quality is uneven；6th, moisture absorption and agglomeration problems are not present in product；7th, production,
Using being not in dust, smog in, transport, pollution is few.So liquid fertilizer is the trend of world today's Growth of Chemical Fertilizer Industry
One of.But there is the defects of single composition, DeGrain, the more excellent Liquid Fertilizer of research and development performance in existing liquid fertilizer
Material has important market value and social value.
The content of the invention
It is an object of the invention to provide a kind of liquid fertilizer containing medical stone and preparation method thereof, to solve the above-mentioned back of the body
The problem of being proposed in scape technology.
To achieve the above object, the present invention provides following technical scheme：
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：Medical stone extract solution 50-55 parts,
Urea 38-42 parts, potassium dihydrogen phosphate 15-20 parts, compound sodium nitrophenolate 1-2 parts, diethyl aminoethyl hexanoate 0.7-1.1 parts, indolebutyric acid sodium 0.8-1.3
Part, potassium fulvate 12-16 parts, borax decahydrate 4-7 parts, ammonium molybdate tetrahydrate 2-5 parts, ammonium phosphate 7-11 parts, zinc sulfate 10-15 parts,
Seaweed extracted liquor 35-40 parts, water 180-200 parts.
As the further scheme of the present invention：It is made up of the raw material below according to parts by weight：Medical stone extract solution 51-54
Part, urea 39-41 parts, potassium dihydrogen phosphate 16-19 parts, compound sodium nitrophenolate 1.3-1.7 parts, diethyl aminoethyl hexanoate 0.8-1.0 parts, indolebutyric acid sodium
0.9-1.2 parts, potassium fulvate 13-15 parts, borax decahydrate 5-6 parts, ammonium molybdate tetrahydrate 3-4 parts, ammonium phosphate 8-10 parts, zinc sulfate
11-14 parts, seaweed extracted liquor 36-39 parts, water 185-195 parts.
As further scheme of the invention：It is made up of the raw material below according to parts by weight：53 parts of medical stone extract solution,
40 parts of urea, 17 parts of potassium dihydrogen phosphate, 1.5 parts of compound sodium nitrophenolate, 0.9 part of diethyl aminoethyl hexanoate, 1.1 parts of indolebutyric acid sodium, potassium fulvate 14
Part, 5 parts of borax decahydrate, 3 parts of ammonium molybdate tetrahydrate, 9 parts of ammonium phosphate, 12 parts of zinc sulfate, 37 parts of seaweed extracted liquor, 190 parts of water.
As further scheme of the invention：The medical stone extract solution is made by following methods：Medical stone is taken, is broken
It is broken, the light-coloured vinegar of 3-5 times of weight is added, after soaking 2-3 days, filtering, the first extract solution and the first extraction residue is obtained, first is carried
Residue calcination processing 1-2h at 450-500 DEG C is taken, after calcining, direct plunges into and quenching is carried out into the first extract solution, obtain
Mixture is obtained, by mixture ball-milling treatment 2-3h, filtering, the second extract solution and the second extraction residue are obtained, by the second extract solution
24-30h is stood, takes supernatant liquid, you can obtains medical stone extract solution.
As further scheme of the invention：The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping,
The water of 10-12 times of weight is added, soaks 2-3h, heating and refluxing extraction 1-2h, obtains reflux extracting liquid and refluxing extraction residue, to
The water of 6-8 times of weight is added in refluxing extraction residue again, soaks 1-2h, ultrasonication 50-60min, ultrasonic wave is obtained and carries
Liquid and ultrasonic wave extraction residue are taken, reflux extracting liquid and ultrasonic extract are merged, you can obtains seaweed extracted liquor.
The preparation method of the liquid fertilizer containing medical stone, step are as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 15-20min is stirred at 75-80 DEG C, obtains second
Mixture；
3）Reactor is cooled to 60-65 DEG C, the first mixture is added into the second mixture, is stirred 25-30min,
Obtain the 3rd mixture；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 15-20min, obtains the 4th mixing
Thing；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
40-50min, discharging, you can.
Compared with prior art, the beneficial effects of the invention are as follows：
Liquid fertilizer prepared by the present invention can promote effective utilization of the crop to phosphate fertilizer, nitrogenous fertilizer and potash fertilizer in soil, and contain
The trace elements such as boron, zinc, molybdenum, the trace element that crop lacks in soil can be quickly supplemented, improve crop yield；It is prepared by the present invention
Liquid fertilizer contain plant growth promoter, the healthy and strong growth of plant health, and medical stone extract solution and marine alga can be promoted
Extract solution can improve crop resistance, reduce crop disease, be advantageous to improve crop yield.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：50 parts of medical stone extract solution, urea
38 parts, 15 parts of potassium dihydrogen phosphate, 1 part of compound sodium nitrophenolate, 0.7 part of diethyl aminoethyl hexanoate, 0.8 part of indolebutyric acid sodium, 12 parts of potassium fulvate, ten water
4 parts of borax, 2 parts of ammonium molybdate tetrahydrate, 7 parts of ammonium phosphate, 10 parts of zinc sulfate, 35 parts of seaweed extracted liquor, 180 parts of water.
Wherein, the medical stone extract solution is made by following methods：Medical stone is taken, is crushed, adds the light-coloured vinegar of 3 times of weight,
After immersion 2 days, filtering, the first extract solution and the first extraction residue are obtained, residue calcination processing at 450 DEG C is extracted by first
1h, after calcining, direct plunge into and quenching is carried out into the first extract solution, mixture is obtained, by mixture ball-milling treatment 2h, mistake
Filter, the second extract solution and the second extraction residue are obtained, the second extract solution is stood into 24h, takes supernatant liquid, you can obtains wheat meal
Stone extract solution；
The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping, the water of 10 times of weight is added, soaks 2h, heat back
Stream extraction 1h, obtains reflux extracting liquid and refluxing extraction residue, adds the water of 6 times of weight, leaching again into refluxing extraction residue
1h, ultrasonication 50min are steeped, ultrasonic extract and ultrasonic wave extraction residue is obtained, reflux extracting liquid and ultrasonic wave is carried
Liquid is taken to merge, you can to obtain seaweed extracted liquor.
In the present embodiment, the preparation method of the liquid fertilizer containing medical stone, step is as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 15min is stirred at 75 DEG C, obtains the second mixture；
3）Reactor is cooled to 60 DEG C, the first mixture is added into the second mixture, is stirred 25min, obtains the
Three mixtures；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 15min, obtains the 4th mixture；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
40min, discharging, you can.
Embodiment 2
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：51 parts of medical stone extract solution, urea
39 parts, 16 parts of potassium dihydrogen phosphate, 1.3 parts of compound sodium nitrophenolate, 0.8 part of diethyl aminoethyl hexanoate, 1.2 parts of indolebutyric acid sodium, 15 parts of potassium fulvate, ten
6 parts of water borax, 4 parts of ammonium molybdate tetrahydrate, 10 parts of ammonium phosphate, 11 parts of zinc sulfate, 36 parts of seaweed extracted liquor, 195 parts of water.
Wherein, the medical stone extract solution is made by following methods：Medical stone is taken, is crushed, adds the white of 3.5 times of weight
Vinegar, after immersion 2 days, filtering, the first extract solution and the first extraction residue are obtained, by the first extraction residue at 460 DEG C at calcining
1.5h is managed, after calcining, direct plunges into and quenching is carried out into the first extract solution, mixture is obtained, by mixture ball-milling treatment
2h, filtering, the second extract solution and the second extraction residue are obtained, the second extract solution is stood into 25h, takes supernatant liquid, you can obtain
Obtain medical stone extract solution；
The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping, the water of 11 times of weight is added, soaks 2h, heat back
Stream extraction 1h, obtains reflux extracting liquid and refluxing extraction residue, adds the water of 6.5 times of weight again into refluxing extraction residue,
1.5h, ultrasonication 53min are soaked, ultrasonic extract and ultrasonic wave extraction residue are obtained, by reflux extracting liquid and ultrasound
Ripple extract solution merges, you can obtains seaweed extracted liquor.
In the present embodiment, the preparation method of the liquid fertilizer containing medical stone, step is as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 16min is stirred at 75 DEG C, obtains the second mixture；
3）Reactor is cooled to 62 DEG C, the first mixture is added into the second mixture, is stirred 27min, obtains the
Three mixtures；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 16min, obtains the 4th mixture；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
42min, discharging, you can.
Embodiment 3
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：53 parts of medical stone extract solution, urea
40 parts, 17 parts of potassium dihydrogen phosphate, 1.5 parts of compound sodium nitrophenolate, 0.9 part of diethyl aminoethyl hexanoate, 1.1 parts of indolebutyric acid sodium, 14 parts of potassium fulvate, ten
5 parts of water borax, 3 parts of ammonium molybdate tetrahydrate, 9 parts of ammonium phosphate, 12 parts of zinc sulfate, 37 parts of seaweed extracted liquor, 190 parts of water.
Wherein, the medical stone extract solution is made by following methods：Medical stone is taken, is crushed, adds the light-coloured vinegar of 4 times of weight,
After immersion 3 days, filtering, the first extract solution and the first extraction residue are obtained, residue calcination processing at 480 DEG C is extracted by first
1.5h, after calcining, direct plunge into and quenching is carried out into the first extract solution, mixture is obtained, by mixture ball-milling treatment
2.5h, filterings, the second extract solution and the second extraction residue are obtained, the second extract solution is stood into 27h, takes supernatant liquid, you can
Obtain medical stone extract solution；
The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping, adds the water of 11 times of weight, soaks 2.5h, heating
Refluxing extraction 1.5h, reflux extracting liquid and refluxing extraction residue are obtained, add 7 times of weight again into refluxing extraction residue
Water, 1.5h, ultrasonication 55min are soaked, obtain ultrasonic extract and ultrasonic wave extraction residue, by reflux extracting liquid and surpassed
Sound wave extract solution merges, you can obtains seaweed extracted liquor.
In the present embodiment, the preparation method of the liquid fertilizer containing medical stone, step is as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 17min is stirred at 78 DEG C, obtains the second mixture；
3）Reactor is cooled to 62 DEG C, the first mixture is added into the second mixture, is stirred 28min, obtains the
Three mixtures；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 17min, obtains the 4th mixture；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
45min, discharging, you can.
Embodiment 4
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：54 parts of medical stone extract solution, urea
41 parts, 19 parts of potassium dihydrogen phosphate, 1.7 parts of compound sodium nitrophenolate, 1.0 parts of diethyl aminoethyl hexanoate, 0.9 part of indolebutyric acid sodium, 13 parts of potassium fulvate, ten
5 parts of water borax, 3 parts of ammonium molybdate tetrahydrate, 8 parts of ammonium phosphate, 14 parts of zinc sulfate, 39 parts of seaweed extracted liquor, 185 parts of water.
Wherein, the medical stone extract solution is made by following methods：Medical stone is taken, is crushed, adds the white of 4.5 times of weight
Vinegar, after immersion 2 days, filtering, the first extract solution and the first extraction residue are obtained, by the first extraction residue at 480 DEG C at calcining
2h is managed, after calcining, direct plunges into and quenching is carried out into the first extract solution, mixture is obtained, by mixture ball-milling treatment
2.5h, filterings, the second extract solution and the second extraction residue are obtained, the second extract solution is stood into 29h, takes supernatant liquid, you can
Obtain medical stone extract solution；
The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping, the water of 11 times of weight is added, soaks 3h, heat back
Stream extraction 1.5h, obtains reflux extracting liquid and refluxing extraction residue, adds the water of 7 times of weight again into refluxing extraction residue,
2h, ultrasonication 58min are soaked, ultrasonic extract and ultrasonic wave extraction residue are obtained, by reflux extracting liquid and ultrasonic wave
Extract solution merges, you can obtains seaweed extracted liquor.
In the present embodiment, the preparation method of the liquid fertilizer containing medical stone, step is as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 18min is stirred at 80 DEG C, obtains the second mixture；
3）Reactor is cooled to 65 DEG C, the first mixture is added into the second mixture, is stirred 30min, obtains the
Three mixtures；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 18min, obtains the 4th mixture；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
45min, discharging, you can.
Embodiment 5
A kind of liquid fertilizer containing medical stone, is made up of the raw material below according to parts by weight：55 parts of medical stone extract solution, urea
42 parts, 20 parts of potassium dihydrogen phosphate, 2 parts of compound sodium nitrophenolate, 1.1 parts of diethyl aminoethyl hexanoate, 1.3 parts of indolebutyric acid sodium, 16 parts of potassium fulvate, ten water
7 parts of borax, 5 parts of ammonium molybdate tetrahydrate, 11 parts of ammonium phosphate, 15 parts of zinc sulfate, 40 parts of seaweed extracted liquor, 200 parts of water.
Wherein, the medical stone extract solution is made by following methods：Medical stone is taken, is crushed, adds the light-coloured vinegar of 5 times of weight,
After immersion 3 days, filtering, the first extract solution and the first extraction residue are obtained, residue calcination processing at 500 DEG C is extracted by first
2h, after calcining, direct plunge into and quenching is carried out into the first extract solution, mixture is obtained, by mixture ball-milling treatment 3h, mistake
Filter, the second extract solution and the second extraction residue are obtained, the second extract solution is stood into 30h, takes supernatant liquid, you can obtains wheat meal
Stone extract solution；
The seaweed extracted liquor is made by following methods：Marine alga is taken, after chopping, the water of 12 times of weight is added, soaks 3h, heat back
Stream extraction 2h, obtains reflux extracting liquid and refluxing extraction residue, adds the water of 8 times of weight, leaching again into refluxing extraction residue
2h, ultrasonication 60min are steeped, ultrasonic extract and ultrasonic wave extraction residue is obtained, reflux extracting liquid and ultrasonic wave is carried
Liquid is taken to merge, you can to obtain seaweed extracted liquor.
In the present embodiment, the preparation method of the liquid fertilizer containing medical stone, step is as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 20min is stirred at 80 DEG C, obtains the second mixture；
3）Reactor is cooled to 65 DEG C, the first mixture is added into the second mixture, is stirred 30min, obtains the
Three mixtures；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 20min, obtains the 4th mixture；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
50min, discharging, you can.
Liquid fertilizer prepared by the present invention can promote effective utilization of the crop to phosphate fertilizer, nitrogenous fertilizer and potash fertilizer in soil, and
Containing trace elements such as boron, zinc, molybdenums, the trace element that crop lacks in soil can be quickly supplemented, improves crop yield；The present invention
The liquid fertilizer of preparation contains plant growth promoter, can promote the healthy and strong growth of plant health, and medical stone extract solution and
Seaweed extracted liquor can improve crop resistance, reduce crop disease, be advantageous to improve crop yield.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula, can also be on the premise of present inventive concept not be departed from one skilled in the relevant art's possessed knowledge
Various changes can be made.
Claims (6)
1. a kind of liquid fertilizer containing medical stone, it is characterised in that be made up of the raw material below according to parts by weight：Medical stone carries
Take liquid 50-55 parts, urea 38-42 parts, potassium dihydrogen phosphate 15-20 parts, compound sodium nitrophenolate 1-2 parts, diethyl aminoethyl hexanoate 0.7-1.1 parts, indoles
Sodium butyrate 0.8-1.3 parts, potassium fulvate 12-16 parts, borax decahydrate 4-7 parts, ammonium molybdate tetrahydrate 2-5 parts, ammonium phosphate 7-11 parts, sulphur
Sour zinc 10-15 parts, seaweed extracted liquor 35-40 parts, water 180-200 parts.
2. the liquid fertilizer according to claim 1 containing medical stone, it is characterised in that by below according to the original of parts by weight
Material composition：Medical stone extract solution 51-54 parts, urea 39-41 parts, potassium dihydrogen phosphate 16-19 parts, compound sodium nitrophenolate 1.3-1.7 parts, amine
Fresh ester 0.8-1.0 parts, indolebutyric acid sodium 0.9-1.2 parts, potassium fulvate 13-15 parts, borax decahydrate 5-6 parts, ammonium molybdate tetrahydrate 3-4
Part, ammonium phosphate 8-10 parts, zinc sulfate 11-14 parts, seaweed extracted liquor 36-39 parts, water 185-195 parts.
3. the liquid fertilizer according to claim 2 containing medical stone, it is characterised in that by below according to the original of parts by weight
Material composition：53 parts of medical stone extract solution, 40 parts of urea, 17 parts of potassium dihydrogen phosphate, 1.5 parts of compound sodium nitrophenolate, 0.9 part of diethyl aminoethyl hexanoate, Yin
1.1 parts of diindyl sodium butyrate, 14 parts of potassium fulvate, 5 parts of borax decahydrate, 3 parts of ammonium molybdate tetrahydrate, 9 parts of ammonium phosphate, 12 parts of zinc sulfate, sea
37 parts of algae extract solution, 190 parts of water.
4. the liquid fertilizer according to claim 1 containing medical stone, it is characterised in that the medical stone extract solution by with
Lower section method is made：Medical stone is taken, is crushed, adds the light-coloured vinegar of 3-5 times of weight, after soaking 2-3 days, filtering, obtains the first extract solution
With first extraction residue, by first extract residue calcination processing 1-2h at 450-500 DEG C, after calcining, direct plunge into
Carry out quenching in first extract solution, obtain mixture, by mixture ball-milling treatment 2-3h, filtering, obtain the second extract solution and the
Two extraction residues, stand 24-30h by the second extract solution, take supernatant liquid, you can obtain medical stone extract solution.
5. the liquid fertilizer according to claim 1 containing medical stone, it is characterised in that the seaweed extracted liquor is by following
Method is made：Marine alga is taken, after chopping, the water of 10-12 times of weight is added, soaks 2-3h, heating and refluxing extraction 1-2h, flowed back
Extract solution and refluxing extraction residue, add the water of 6-8 times of weight into refluxing extraction residue again, soak 1-2h, at ultrasonic wave
50-60min is managed, obtains ultrasonic extract and ultrasonic wave extraction residue, reflux extracting liquid and ultrasonic extract are merged, i.e.,
Seaweed extracted liquor can be obtained.
A kind of 6. preparation method of liquid fertilizer containing medical stone as described in claim 1-5 is any, it is characterised in that step
It is rapid as follows：
1）Potassium fulvate, borax decahydrate, ammonium molybdate tetrahydrate, ammonium phosphate and zinc sulfate are weighed, merges, after being uniformly mixed, obtains
Obtain the first mixture；
2）Water and potassium dihydrogen phosphate are weighed, is put into reactor, 15-20min is stirred at 75-80 DEG C, obtains second
Mixture；
3）Reactor is cooled to 60-65 DEG C, the first mixture is added into the second mixture, is stirred 25-30min,
Obtain the 3rd mixture；
4）Reactor is cooled to 55 DEG C, adds urea and medical stone extract solution, is stirred 15-20min, obtains the 4th mixing
Thing；
5）Reactor is cooled to 40 DEG C, compound sodium nitrophenolate, diethyl aminoethyl hexanoate, indolebutyric acid sodium and seaweed extracted liquor is added, is stirred
40-50min, discharging, you can.
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| CN108129243A (en) * | 2018-03-16 | 2018-06-08 | 常国占 | A kind of mineral element biological compound fertilizer |
| CN108456040A (en) * | 2018-05-28 | 2018-08-28 | 隋皓为 | A kind of oil shale making siliceous fertilizer technique |
| CN113860951A (en) * | 2021-10-13 | 2021-12-31 | 山东荣华生物科技股份有限公司 | Foliar fertilizer for improving resistance and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108129243A (en) * | 2018-03-16 | 2018-06-08 | 常国占 | A kind of mineral element biological compound fertilizer |
| CN108456040A (en) * | 2018-05-28 | 2018-08-28 | 隋皓为 | A kind of oil shale making siliceous fertilizer technique |
| CN113860951A (en) * | 2021-10-13 | 2021-12-31 | 山东荣华生物科技股份有限公司 | Foliar fertilizer for improving resistance and preparation method thereof |
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