CN107372681B - Novel veterinary compound disinfectant and preparation method thereof - Google Patents
Novel veterinary compound disinfectant and preparation method thereof Download PDFInfo
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- CN107372681B CN107372681B CN201710482464.4A CN201710482464A CN107372681B CN 107372681 B CN107372681 B CN 107372681B CN 201710482464 A CN201710482464 A CN 201710482464A CN 107372681 B CN107372681 B CN 107372681B
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/06—Oxygen or sulfur directly attached to a cycloaliphatic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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Abstract
The invention provides a novel veterinary compound disinfectant and a preparation method thereof, wherein the novel veterinary compound disinfectant comprises the following components in percentage by weight: 1-3% of bamboo leaf extract, 0.5-2% of yucca extract, 0.2-0.5% of O-cymene-5-alcohol, 0.4-1.2% of lemon essential oil, 0.2-0.5% of biguanides, 5-10% of single-chain quaternary ammonium salt, 3-6% of double-chain quaternary ammonium salt, 8-15% of ethanol and the balance of deionized water; the veterinary compound disinfectant prepared by the invention has excellent bactericidal effect on various pathogenic bacteria, and the disinfectant has low toxicity, safety and environmental protection; on the basis, the feed additive has unique fragrance, can effectively remove the bad smell in livestock and poultry breeding places, is stable, and can be stored for a long time.
Description
Technical Field
The invention relates to the field of veterinary disinfectants, in particular to a novel veterinary compound disinfectant and a preparation method thereof.
Background
The disinfection refers to removing or killing pathogenic microorganisms and other harmful microorganisms on the body surfaces of the livestock and poultry and in the living environment thereof by using a proper method according to different production links and objects. Under the current trend of higher and higher intensification degree, diseases of the breeding farm are more and more complicated, and the problem of animal epidemic disease prevention and treatment is very prominent. The occurrence of epidemic diseases in large-scale farms is often the result of a multi-factor combination effect, but the most important of the epidemic diseases is caused by invasion and diffusion of pathogenic microorganisms in the external environment or pollution and diffusion of pathogenic microorganisms of animals in the farms. Effective disinfection is one of important measures for stopping and reducing pathogens in the environment of a farm, cutting off epidemic disease transmission ways and preventing and controlling infectious diseases of the farm.
With the growing food safety problem, the demand of consumers for animal products has gradually shifted from quantity type to quality type, and the restrictions on animal drug use are becoming stricter. Therefore, thorough and standardized disinfection will become the most effective and convenient means for preventing and controlling diseases. At present, the breeding industry of China is going to advance in a large scale, and how to purify pathogenic microorganisms of the breeding farm is an extremely important scientific research and practice direction. Scientific development and reasonable application of the disinfectant play a key role in purification work of a farm, so that development of a low-toxicity, green, environment-friendly and efficient compound disinfectant is a necessary development trend.
Disclosure of Invention
The invention aims to provide a novel veterinary compound disinfectant and a preparation method thereof, the prepared veterinary compound disinfectant has excellent sterilization effect on various pathogenic bacteria, and the veterinary compound disinfectant has low toxicity, is safe and environment-friendly, and is suitable for popularization and application.
In order to achieve the purpose, the invention is realized by the following technical scheme:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 1-3% of bamboo leaf extract, 0.5-2% of yucca extract, 0.2-0.5% of O-cymene-5-alcohol, 0.4-1.2% of lemon essential oil, 0.2-0.5% of biguanides, 5-10% of single-chain quaternary ammonium salt, 3-6% of double-chain quaternary ammonium salt, 8-15% of ethanol and the balance of deionized water.
Preferably, the novel veterinary compound disinfectant consists of the following components in percentage by weight: 2% of bamboo leaf extract, 1.5% of yucca extract, 0.35% of O-cymene-5-alcohol, 1% of lemon essential oil, 3% of biguanides, 8% of single-chain quaternary ammonium salt, 4% of double-chain quaternary ammonium salt, 12% of ethanol and the balance of deionized water.
Preferably, the biguanide is polyhexamethylene biguanide or a salt thereof.
Preferably, the single-chain quaternary ammonium salt is one of tetradecyl dimethyl benzyl ammonium chloride, dodecyl dimethyl benzyl ammonium bromide and dodecyl dimethyl benzyl ammonium chloride.
Preferably, the double-chain quaternary ammonium salt is dioctadecyl dimethyl ammonium chloride or 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride; more preferably, the double-chain quaternary ammonium salt is 2- (2-phenoxyethoxy) ethyltrimethylammonium chloride.
The preparation method of the novel veterinary compound disinfectant comprises the following steps: weighing the raw materials according to the weight ratio; adding O-cymene-5-alcohol and lemon essential oil into ethanol, stirring, adding deionized water, stirring, sequentially adding biguanides, single chain quaternary ammonium salt, double chain quaternary ammonium salt, bamboo leaf extract and yucca extract, stirring while stirring until the solution is clear, filtering, and bottling.
The invention has the beneficial effects that:
the bamboo leaf extract contains plant flavonoids, and the bamboo leaf flavone has different degrees of inhibition effects on staphylococcus aureus, escherichia coli, streptococcus and staphylococcus epidermidis, particularly has a good inhibition effect on the escherichia coli, and is safe, non-toxic and environment-friendly. The bamboo leaf extract has unique fragrance, and makes the disinfectant taste better. The added yucca extract is mainly used for deodorizing the environment in the sterilization process, because the yucca extract has strong adsorption effect, can directly combine with harmful gases such as ammonia gas, hydrogen sulfide and methylindole, and reduces the concentration of the harmful gases, and has certain sterilization and disinfection effects on the basis.
The single-chain quaternary ammonium salt, the double-chain quaternary ammonium salt and the biguanide are simultaneously added into the disinfectant for livestock, the three substances can act synergistically to further enhance the disinfection effect of the disinfectant, and the bamboo leaf extract, the yucca extract, the lemon essential oil and the ethanol are added, so that the disinfectant is effectively improved, and the sterilization range is wider. On the basis, a small amount of O-cymene-5-alcohol is added, so that the sterilization effect of the disinfectant can reach the best, and the sterilization rate of the disinfectant on staphylococcus aureus, escherichia coli, pasteurella streptoverticillii and hemolytic streptococcus can reach more than 99.99% under the condition that the dilution is 3000 times.
The compound disinfectant for livestock has unique fragrance on the basis of excellent sterilization and disinfection effects, can effectively remove the bad smell in livestock and poultry breeding places, is very stable, can be stored for a long time, does not need to adjust the pH value during preparation and use, and is practical and convenient.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 2% of bamboo leaf extract, 1.5% of yucca extract, 0.35% of O-cymene-5-alcohol, 1% of lemon essential oil, 3% of polyhexamethylene biguanide hydrochloride, 8% of tetradecyl dimethyl benzyl ammonium chloride, 4% of 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride salt, 12% of ethanol and the balance of deionized water.
Example 2:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 3% of bamboo leaf extract, 0.5% of yucca extract, 0.4% of O-cymene-5-alcohol, 0.8% of lemon essential oil, 0.2% of polyhexamethylene biguanide, 8% of dodecyl dimethyl benzyl ammonium chloride, 5% of 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride, 15% of ethanol and the balance of deionized water.
Example 3:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 1.5% of bamboo leaf extract, 2% of yucca extract, 0.5% of O-cymene-5-alcohol, 1.2% of lemon essential oil, 0.5% of polyhexamethylene biguanide hydrochloride, 5% of dodecyl dimethyl benzyl ammonium bromide, 6% of dioctadecyl dimethyl ammonium chloride, 12% of ethanol and the balance of deionized water.
Example 4:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 1% of bamboo leaf extract, 1% of yucca extract, 0.2% of O-cymene-5-alcohol, 0.4% of lemon essential oil, 0.3% of polyhexamethylene biguanide, 10% of tetradecyl dimethyl benzyl ammonium chloride, 3% of 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride, 8% of ethanol and the balance of deionized water.
Example 5:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 2.5% of bamboo leaf extract, 1% of yucca extract, 0.4% of O-cymene-5-ol, 0.7% of lemon essential oil, 0.5% of polyhexamethylene biguanide, 5% of dodecyl dimethyl benzyl ammonium bromide, 4% of 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride, 14% of ethanol and the balance of deionized water.
Example 6:
a novel compound disinfectant for animals comprises the following components in percentage by weight: 1% of bamboo leaf extract, 2% of yucca extract, 0.5% of O-cymene-5-alcohol, 1% of lemon essential oil, 0.4% of polyhexamethylene biguanide, 8% of tetradecyl dimethyl benzyl ammonium chloride, 6% of dioctadecyl dimethyl ammonium chloride, 10% of ethanol and the balance of deionized water.
The preparation method of the novel veterinary compound disinfectant in the embodiments 1 to 6 comprises the following steps: weighing the raw materials according to the weight ratio; adding O-cymene-5-alcohol and lemon essential oil into ethanol, stirring, adding deionized water, stirring, sequentially adding biguanides, single chain quaternary ammonium salt, double chain quaternary ammonium salt, bamboo leaf extract and yucca extract, stirring while stirring until the solution is clear, filtering, and bottling.
The performance test of the compound disinfectant for animals comprises the following steps:
1. test method
The test is carried out according to the method of 'veterinary disinfectant identification test technical specification' of Ministry of agriculture, and a bacterial suspension quantitative method is adopted.
2. Test strains: including Escherichia coli, Staphylococcus aureus, and Bacillus cereus.
3. And (3) sterilizing various test strains by using disinfectants with different solubilities for 4min, and calculating the sterilization rate after sterilization.
4. The results of the test of the compound disinfectant for animals in examples 1-2 of the present invention on killing the strains are shown in table 1:
TABLE 1 results of the test for killing strains by the inventive compound disinfectant for animals
As can be seen from Table 1, the veterinary compound disinfectant has excellent bactericidal effect on Escherichia coli 8099, Staphylococcus aureus ATCC6538 and Bacillus cereus SSI C1/1 even under the condition of large dilution times, is low in toxicity, safe and environment-friendly, and is suitable for popularization and application.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (5)
1. A novel compound disinfectant for animals is characterized by comprising the following components in percentage by weight: 1-3% of bamboo leaf extract, 0.5-2% of yucca extract, 0.2-0.5% of O-cymene-5-alcohol, 0.4-1.2% of lemon essential oil, 0.2-0.5% of biguanides, 5-10% of single-chain quaternary ammonium salt, 3-6% of double-chain quaternary ammonium salt, 8-15% of ethanol and the balance of deionized water;
the biguanide is polyhexamethylene biguanide or a salt thereof;
the single-chain quaternary ammonium salt is one of tetradecyl dimethyl benzyl ammonium chloride, dodecyl dimethyl benzyl ammonium bromide and dodecyl dimethyl benzyl ammonium chloride;
the double-chain quaternary ammonium salt is dioctadecyl dimethyl ammonium chloride or 2- (2-phenoxyethoxy) ethyl trimethyl ammonium chloride.
2. A novel veterinary compound disinfectant according to claim 1, wherein the double-chain quaternary ammonium salt is 2- (2-phenoxyethoxy) ethyltrimethyl ammonium chloride.
3. A method of preparation of a novel veterinary compound disinfectant according to any of claims 1-2, characterized in that it comprises the following steps: weighing the raw materials according to the weight ratio; adding O-cymene-5-alcohol and lemon essential oil into ethanol, stirring, adding deionized water, stirring, sequentially adding biguanides, single chain quaternary ammonium salt, double chain quaternary ammonium salt, bamboo leaf extract and yucca extract, stirring while stirring until the solution is clear, filtering, and bottling.
4. Use of a novel veterinary compound disinfectant according to any of claims 1-2 for killing pathogenic bacteria in non-therapeutic destinations.
5. The use according to claim 4, wherein the pathogenic bacteria are Staphylococcus aureus, Escherichia coli, Streptococcus hemolyticus, Pasteurella streptoverticillata and Bacillus cereus.
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108294069A (en) * | 2018-02-07 | 2018-07-20 | 合肥华盖生物科技有限公司 | A kind of disinfectant for animals and preparation method thereof |
| CN111096340A (en) * | 2019-12-02 | 2020-05-05 | 安徽启威生物科技有限公司 | Disinfectant concentrated solution for pet hospitals and preparation method thereof |
| CN111466416A (en) * | 2020-04-20 | 2020-07-31 | 重庆森盟新能源开发有限公司 | Composite disinfectant using photocatalysis technology |
| CN111789796A (en) * | 2020-04-28 | 2020-10-20 | 广东分子态生物股份有限公司 | Disinfectant with liposome-encapsulated bactericidal component and preparation method thereof |
| CN115119848A (en) * | 2021-10-19 | 2022-09-30 | 湖南坤源生物科技有限公司 | Disinfectant for livestock and poultry and preparation method thereof |
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| CN104886186A (en) * | 2015-05-14 | 2015-09-09 | 青岛国航祥玉技术服务有限公司 | Efficient bactericidal disinfectant for livestock breeding house |
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| CN104886186A (en) * | 2015-05-14 | 2015-09-09 | 青岛国航祥玉技术服务有限公司 | Efficient bactericidal disinfectant for livestock breeding house |
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