CN107338103A - 一种抗冻润滑脂 - Google Patents

一种抗冻润滑脂 Download PDF

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CN107338103A
CN107338103A CN201710394891.7A CN201710394891A CN107338103A CN 107338103 A CN107338103 A CN 107338103A CN 201710394891 A CN201710394891 A CN 201710394891A CN 107338103 A CN107338103 A CN 107338103A
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oil
freeze proof
lubricating grease
tbhp
boric acid
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刘秀梅
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/06—Mixtures of thickeners and additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085—Phosphorus oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087—Boron oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/06—Peroxides; Ozonides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/402—Castor oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/02—Groups 1 or 11
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/04—Groups 2 or 12
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/04—Oil-bath; Gear-boxes; Automatic transmissions; Traction drives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

本发明涉及一种抗冻润滑脂，包括基础油、二硫代磷酸锌、叔丁基过氧化氢、硫化鲸鱼油、蓖麻油钾皂、复合锆基稠化剂、硼酸，各组分的质量份数为：基础油20‑40、二硫代磷酸锌10‑15、叔丁基过氧化氢10‑15、硫化鲸鱼油5‑10、蓖麻油钾皂50‑60、复合锆基稠化剂5‑9、硼酸10‑15。本发明抗冻润滑脂采用先进的技术，用于高速齿轮箱零部件上的一种高性能的油脂，含有特殊的聚合物使它具有优异的消音性。适用于高速齿轮箱有抗冻，粘度高，不易跑油，持久高效的优点。

Description

一种抗冻润滑脂
技术领域
本发明涉及一种润滑材料，具体地讲，本发明涉及一种抗冻润滑脂。
背景技术
润滑脂是为了解决设备在运转时产生离心力的状态下，为减少设备摩擦磨损需要的一种润滑材料。
与润滑油相比，由于使用更加容易的原因，被更广泛的应用于润滑各类产业机械的润滑部分。
目前的普遍现象是用国产高温脂使用，频繁停机、注油，影响正常生产，浪费能源，污染环境，劳动强度大，设备养护成本高。一部分企业用进口产品（例如美国LE公司的1275脂），价格昂贵，运输周期长，成本费用高。
发明内容
针对现有技术中存在的上述不足，本发明所要解决的技术问题是提供一种保养效果好的抗冻润滑脂。
本发明解决其技术问题所采用的技术方案是：提供一种抗冻润滑脂，包括基础油、二硫代磷酸锌、叔丁基过氧化氢、硫化鲸鱼油、蓖麻油钾皂、复合锆基稠化剂、硼酸，各组分的质量份数为：基础油20-40、二硫代磷酸锌10-15、叔丁基过氧化氢10-15、硫化鲸鱼油5-10、蓖麻油钾皂50-60、复合锆基稠化剂5-9、硼酸10-15。
作为优选，所述抗冻润滑脂还包括基础油40、二硫代磷酸锌11、叔丁基过氧化氢14、硫化鲸鱼油7、蓖麻油钾皂56、复合锆基稠化剂9、硼酸12。
一种如上述所述的抗冻润滑脂的制备方法，其包括如下步骤：
将所述基础油、硫化鲸鱼油和蓖麻油钾皂加入反应槽中以 400-600 转 / 分速度搅拌，再加入二硫代磷酸锌、叔丁基过氧化氢、硼酸搅拌 20-60 分钟后，加入柠檬复合锆基稠化剂，调速300-500转/分速度搅拌，一小时到一个半小时后，静置完成淡黄色抗冻润滑脂成品。
有益效果，本发明抗冻润滑脂采用先进的技术，用于高速齿轮箱零部件上的一种高性能的油脂，含有特殊的聚合物使它具有优异的消音性。适用于高速齿轮箱有抗冻，粘度高，不易跑油，持久高效的优点。并可延长润滑脂的使用周期，对汽车、火车、船舶、各种汽油机、柴油机均可起到良好的保护作用。
具体实施例：
本发明的一种抗冻润滑脂，包括基础油、二硫代磷酸锌、叔丁基过氧化氢、硫化鲸鱼油、蓖麻油钾皂、复合锆基稠化剂、硼酸，各组分的质量份数为：基础油40、二硫代磷酸锌11、叔丁基过氧化氢14、硫化鲸鱼油7、蓖麻油钾皂56、复合锆基稠化剂9、硼酸12。
一种如上述所述的抗冻润滑脂的制备方法，其包括如下步骤：
将所述基础油、硫化鲸鱼油和蓖麻油钾皂加入反应槽中以 400-600 转 / 分速度搅拌，再加入二硫代磷酸锌、叔丁基过氧化氢、硼酸搅拌 20-60 分钟后，加入柠檬复合锆基稠化剂，调速300-500转/分速度搅拌，一小时到一个半小时后，静置完成淡黄色抗冻润滑脂成品。
以上公开的仅为发明的较佳实施例，但并不用于限制本发明，凡在本发明的精神和原则之内，所作的修改、润色、等同替换等，均应包含在本发明的保护范围之内，此外，本发明未详述之处，均为本技术领域技术人员的公知技术。

Claims (3)

1.一种抗冻润滑脂，其特征在于：包括基础油、二硫代磷酸锌、叔丁基过氧化氢、硫化鲸鱼油、蓖麻油钾皂、复合锆基稠化剂、硼酸，各组分的质量份数为：基础油20-40、二硫代磷酸锌10-15、叔丁基过氧化氢10-15、硫化鲸鱼油5-10、蓖麻油钾皂50-60、复合锆基稠化剂5-9、硼酸10-15。
2.根据权利要求1所述的抗冻润滑脂，其特征在于：所述抗冻润滑脂还包括基础油40、二硫代磷酸锌11、叔丁基过氧化氢14、硫化鲸鱼油7、蓖麻油钾皂56、复合锆基稠化剂9、硼酸12。
3.一种如权利要求 1-2任一所述的抗冻润滑脂的制备方法，其包括如下步骤：
将所述基础油、硫化鲸鱼油和蓖麻油钾皂加入反应槽中以 400-600 转 / 分速度搅拌，再加入二硫代磷酸锌、叔丁基过氧化氢、硼酸搅拌 20-60 分钟后，加入柠檬复合锆基稠化剂，调速300-500转/分速度搅拌，一小时到一个半小时后，静置完成淡黄色抗冻润滑脂成品。
CN201710394891.7A 2017-05-30 2017-05-30 一种抗冻润滑脂 Pending CN107338103A (zh)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102952619A (zh) * 2011-08-25 2013-03-06 中国石油化工股份有限公司 一种复合锆基润滑脂及其制备方法
CN103351923A (zh) * 2013-06-19 2013-10-16 安徽富华电子集团有限公司 铜铝拉丝液及其制备方法
CN104531281A (zh) * 2014-12-22 2015-04-22 无锡市飞天油脂有限公司 炮用润滑脂
CN106590887A (zh) * 2016-11-24 2017-04-26 周淑华 一种抗冻润滑脂

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102952619A (zh) * 2011-08-25 2013-03-06 中国石油化工股份有限公司 一种复合锆基润滑脂及其制备方法
CN103351923A (zh) * 2013-06-19 2013-10-16 安徽富华电子集团有限公司 铜铝拉丝液及其制备方法
CN104531281A (zh) * 2014-12-22 2015-04-22 无锡市飞天油脂有限公司 炮用润滑脂
CN106590887A (zh) * 2016-11-24 2017-04-26 周淑华 一种抗冻润滑脂

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Application publication date: 20171110