CN107098700B - 一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 - Google Patents
一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 Download PDFInfo
- Publication number
- CN107098700B CN107098700B CN201710294356.4A CN201710294356A CN107098700B CN 107098700 B CN107098700 B CN 107098700B CN 201710294356 A CN201710294356 A CN 201710294356A CN 107098700 B CN107098700 B CN 107098700B
- Authority
- CN
- China
- Prior art keywords
- bmn
- stirring
- suspension ink
- suspension
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000725 suspension Substances 0.000 title claims abstract description 55
- 238000007639 printing Methods 0.000 title claims abstract description 38
- 239000007787 solid Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 24
- 239000002243 precursor Substances 0.000 claims description 61
- 239000010955 niobium Substances 0.000 claims description 58
- 238000003756 stirring Methods 0.000 claims description 55
- 239000000843 powder Substances 0.000 claims description 47
- 238000010438 heat treatment Methods 0.000 claims description 40
- 239000000919 ceramic Substances 0.000 claims description 35
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 28
- 229920000642 polymer Polymers 0.000 claims description 21
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Inorganic materials [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims description 20
- 239000000654 additive Substances 0.000 claims description 18
- 230000000996 additive effect Effects 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 17
- 238000005245 sintering Methods 0.000 claims description 14
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 12
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 12
- 239000001095 magnesium carbonate Substances 0.000 claims description 12
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims description 12
- 238000000498 ball milling Methods 0.000 claims description 10
- 238000007873 sieving Methods 0.000 claims description 10
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 9
- 238000009826 distribution Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000003381 stabilizer Substances 0.000 claims description 4
- 229920002873 Polyethylenimine Polymers 0.000 claims description 2
- -1 niobium citrate peroxide Chemical class 0.000 claims 2
- 239000002105 nanoparticle Substances 0.000 claims 1
- 239000000976 ink Substances 0.000 abstract description 43
- 239000008204 material by function Substances 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 description 57
- 238000005303 weighing Methods 0.000 description 32
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 24
- 238000001914 filtration Methods 0.000 description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- 229910021642 ultra pure water Inorganic materials 0.000 description 16
- 239000012498 ultrapure water Substances 0.000 description 16
- 239000011777 magnesium Substances 0.000 description 15
- 238000004519 manufacturing process Methods 0.000 description 11
- 239000007790 solid phase Substances 0.000 description 11
- 238000001816 cooling Methods 0.000 description 8
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 8
- ZKATWMILCYLAPD-UHFFFAOYSA-N niobium pentoxide Inorganic materials O=[Nb](=O)O[Nb](=O)=O ZKATWMILCYLAPD-UHFFFAOYSA-N 0.000 description 8
- 238000000967 suction filtration Methods 0.000 description 8
- 239000006228 supernatant Substances 0.000 description 8
- 239000004697 Polyetherimide Substances 0.000 description 6
- 229920001601 polyetherimide Polymers 0.000 description 6
- 238000011160 research Methods 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 229910052788 barium Inorganic materials 0.000 description 3
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 229910052758 niobium Inorganic materials 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- LRDUPNFEHGGCHQ-UHFFFAOYSA-N 2-(2-hydroperoxy-2-oxoethyl)-2-hydroxybutanedioic acid Chemical compound OOC(=O)CC(O)(C(O)=O)CC(O)=O LRDUPNFEHGGCHQ-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- IJBYNGRZBZDSDK-UHFFFAOYSA-N barium magnesium Chemical compound [Mg].[Ba] IJBYNGRZBZDSDK-UHFFFAOYSA-N 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 238000000349 field-emission scanning electron micrograph Methods 0.000 description 2
- 238000002329 infrared spectrum Methods 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 241000321453 Paranthias colonus Species 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- SHLNMHIRQGRGOL-UHFFFAOYSA-N barium zinc Chemical compound [Zn].[Ba] SHLNMHIRQGRGOL-UHFFFAOYSA-N 0.000 description 1
- BJXXCWDIBHXWOH-UHFFFAOYSA-N barium(2+);oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Ba+2].[Ba+2].[Ba+2].[Ba+2].[Ba+2].[Ta+5].[Ta+5].[Ta+5].[Ta+5] BJXXCWDIBHXWOH-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002977 biomimetic material Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000012778 molding material Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 150000002843 nonmetals Chemical class 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229910052574 oxide ceramic Inorganic materials 0.000 description 1
- 239000011224 oxide ceramic Substances 0.000 description 1
- 238000000059 patterning Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000004528 spin coating Methods 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/495—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on vanadium, niobium, tantalum, molybdenum or tungsten oxides or solid solutions thereof with other oxides, e.g. vanadates, niobates, tantalates, molybdates or tungstates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62218—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic films, e.g. by using temporary supports
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3215—Barium oxides or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/48—Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5445—Particle size related information expressed by the size of the particles or aggregates thereof submicron sized, i.e. from 0,1 to 1 micron
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/602—Making the green bodies or pre-forms by moulding
- C04B2235/6026—Computer aided shaping, e.g. rapid prototyping
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710294356.4A CN107098700B (zh) | 2017-04-28 | 2017-04-28 | 一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710294356.4A CN107098700B (zh) | 2017-04-28 | 2017-04-28 | 一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN107098700A CN107098700A (zh) | 2017-08-29 |
CN107098700B true CN107098700B (zh) | 2020-01-31 |
Family
ID=59657950
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710294356.4A Active CN107098700B (zh) | 2017-04-28 | 2017-04-28 | 一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107098700B (zh) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3790690A4 (en) * | 2018-05-11 | 2022-01-12 | Magna International Inc. | METHOD OF IMPROVING A HIGH-PRESSURE DIE-CASTING CYLINDER BY ADDITIVE FABRICATION OF A METAL MATRIX COMPOSITE INSERT |
CN108424533B (zh) * | 2018-05-30 | 2020-10-27 | 中国科学院兰州化学物理研究所 | 一种3d打印生物医用水凝胶及其制备方法 |
CN110962220B (zh) * | 2019-12-18 | 2021-08-13 | 厦门大学 | 一种聚合物前驱体陶瓷薄膜的直写装置和制作方法 |
CN110954234A (zh) * | 2019-12-18 | 2020-04-03 | 厦门大学 | 一种聚合物前驱体陶瓷薄膜rtd及其制备方法 |
CN111362702B (zh) * | 2020-03-17 | 2022-05-17 | 中国工程物理研究院激光聚变研究中心 | 一种SiOC雷达型吸波材料的制备方法 |
CN112390651A (zh) * | 2020-11-16 | 2021-02-23 | 中国工程物理研究院材料研究所 | 一种基于3D打印成型的AlN陶瓷粉体制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002114571A (ja) * | 2000-07-31 | 2002-04-16 | Kyocera Corp | 圧電磁器及びこれを用いたインクジェット記録ヘッド |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102012219989B4 (de) * | 2012-10-31 | 2016-09-29 | WZR ceramic solutions GmbH | Druckverfahren zur Herstellung eines Grünkörpers, Grünkörper und keramischer Formkörper |
CN103387391B (zh) * | 2013-07-23 | 2015-05-27 | 武汉理工大学 | 采用水溶液凝胶法制备含钽/铌的叠层介电薄膜的方法 |
CN104609861A (zh) * | 2015-01-25 | 2015-05-13 | 济南唯博新材料有限公司 | 利用水溶性溶胶凝胶工艺精细合成Ba(Zn1/3Nb2/3)O3介质陶瓷纳米粉体 |
-
2017
- 2017-04-28 CN CN201710294356.4A patent/CN107098700B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002114571A (ja) * | 2000-07-31 | 2002-04-16 | Kyocera Corp | 圧電磁器及びこれを用いたインクジェット記録ヘッド |
Also Published As
Publication number | Publication date |
---|---|
CN107098700A (zh) | 2017-08-29 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN107098700B (zh) | 一种适用于直写打印的高固含量bmn悬浮液墨水及其制备方法 | |
Zhou et al. | Probing structure− parameter correlations in the molten salt synthesis of BaZrO3 perovskite submicrometer-sized particles | |
KR102457223B1 (ko) | 페라이트 입자, 수지 조성물 및 전자파 쉴드 재료 | |
CN110272263B (zh) | 一种低温共烧陶瓷介质材料及其制备方法 | |
KR101927476B1 (ko) | 은 분말 및 이의 제조방법 | |
KR101483819B1 (ko) | 글라스 분말 및 이의 제조방법 | |
CN106082357B (zh) | 一种四氧化三钴空心多层微球的制备方法 | |
Andrews et al. | Advances in cold sintering: improving energy consumption and unlocking new potential in component manufacturing | |
CN109692971B (zh) | 一种纳米银粉及其制备与在低温固化导电银浆中的应用 | |
CN1294103C (zh) | 一种可低温度烧结的钛酸锌高频介质陶瓷及其制备方法 | |
CN108314078A (zh) | 一种空心球状钛酸锶钡粉体材料的制备方法 | |
Alkathy et al. | Onset of multiferroicity in nickel and lithium co-substituted barium titanate ceramics | |
CN111848153A (zh) | 一种微波介质陶瓷、微波介质陶瓷的制备方法及通信器件 | |
CN107244916B (zh) | 一种铌酸盐系低温烧结微波介质陶瓷材料及其制备方法 | |
CN103708838A (zh) | 一种低温烧结制备具有单斜结构ZnZrNb2O8微波介质陶瓷新方法 | |
CN103755958B (zh) | 一种聚酰亚胺/钛酸铜钙包覆银纳米颗粒复合材料的制备方法 | |
Liu et al. | A novel precipitation-based synthesis for the formation of X8R-type dielectrics composition based on monodispersed submicron Ba0. 991Bi0. 006TiO3@ Nb2O5 particles | |
CN111747745A (zh) | 一种5g滤波器用介质粉体及其制备方法 | |
JP4096053B2 (ja) | 二酸化チタン等の配向性セラミックス焼結体の製造方法 | |
Teixeira et al. | Chemical synthesis and epitaxial growth methods for the preparation of ferroelectric ceramics and thin films | |
Kobayashi et al. | Fabrication of barium titanate nanoparticles/poly (methylmethacrylate) composite films by a combination of deposition process and spin-coating technique | |
CN104445231A (zh) | 一种具有较低烧结温度的硅酸盐纳米粉体及其制备方法 | |
CN115057695A (zh) | 高q值低介电常数ltcc粉、ltcc材料及制备方法、生瓷带及制备方法和应用 | |
CN101269974B (zh) | 用于制备织构层状结构的钙钛矿系陶瓷纳米粉体合成方法 | |
CN106519302A (zh) | 一种激光成型的塑料活性添加剂及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240223 Address after: 572024 Building 9, UFIDA Industrial Park, yazhouwan science and Technology City, Yazhou District, Sanya City, Hainan Province Patentee after: Sanya science and Education Innovation Park Wuhan University of Technology Country or region after: China Address before: 430070 Hubei Province, Wuhan city Hongshan District Luoshi Road No. 122 Patentee before: WUHAN University OF TECHNOLOGY Country or region before: China |
|
TR01 | Transfer of patent right |