CN107001314B - 制备4-苯基二苯并噻吩的方法 - Google Patents

制备4-苯基二苯并噻吩的方法 Download PDF

Info

Publication number
CN107001314B
CN107001314B CN201580067301.9A CN201580067301A CN107001314B CN 107001314 B CN107001314 B CN 107001314B CN 201580067301 A CN201580067301 A CN 201580067301A CN 107001314 B CN107001314 B CN 107001314B
Authority
CN
China
Prior art keywords
reaction
lithium
sulfur
range
phenyllithium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201580067301.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN107001314A (zh
Inventor
E.L.威廉斯
D.K.霍伦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WR Grace and Co Conn
Original Assignee
Albemarle Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Albemarle Corp filed Critical Albemarle Corp
Publication of CN107001314A publication Critical patent/CN107001314A/zh
Application granted granted Critical
Publication of CN107001314B publication Critical patent/CN107001314B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
    • C07D333/50—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom condensed with carbocyclic rings or ring systems
    • C07D333/76—Dibenzothiophenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201580067301.9A 2014-12-12 2015-12-01 制备4-苯基二苯并噻吩的方法 Expired - Fee Related CN107001314B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201462091119P 2014-12-12 2014-12-12
US62/091119 2014-12-12
PCT/US2015/063237 WO2016094135A1 (en) 2014-12-12 2015-12-01 Process for the preparation of 4-phenyldibenzothiophene

Publications (2)

Publication Number Publication Date
CN107001314A CN107001314A (zh) 2017-08-01
CN107001314B true CN107001314B (zh) 2020-03-27

Family

ID=55024252

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580067301.9A Expired - Fee Related CN107001314B (zh) 2014-12-12 2015-12-01 制备4-苯基二苯并噻吩的方法

Country Status (7)

Country Link
US (1) US9951037B2 (https=)
EP (1) EP3230271B1 (https=)
JP (1) JP6793643B2 (https=)
CN (1) CN107001314B (https=)
CA (1) CA2967439A1 (https=)
TW (1) TWI691492B (https=)
WO (1) WO2016094135A1 (https=)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013012296A1 (en) * 2011-07-21 2013-01-24 Rohm And Haas Electronic Materials Korea Ltd. Novel organic electroluminescence compounds and organic electroluminescence device using the same
US20130069049A1 (en) * 2010-05-26 2013-03-21 Duksan High Metal Co., Ltd. Compound comprising a five-membered hetero ring, an organic electrical element using the same and a terminal thereof
CN103509036A (zh) * 2012-06-27 2014-01-15 三星显示有限公司 新型稠环化合物、有机发光装置和有机发光显示仪器

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102154705B1 (ko) * 2013-04-25 2020-09-11 삼성디스플레이 주식회사 헤테로고리 화합물 및 이를 포함한 유기 발광 소자

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20130069049A1 (en) * 2010-05-26 2013-03-21 Duksan High Metal Co., Ltd. Compound comprising a five-membered hetero ring, an organic electrical element using the same and a terminal thereof
WO2013012296A1 (en) * 2011-07-21 2013-01-24 Rohm And Haas Electronic Materials Korea Ltd. Novel organic electroluminescence compounds and organic electroluminescence device using the same
CN103509036A (zh) * 2012-06-27 2014-01-15 三星显示有限公司 新型稠环化合物、有机发光装置和有机发光显示仪器

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
Derivatives of Dibenzofuran and Dibenzothiophen. Part 11.Free-radical Phenylation of Dibenxothiophen;E.B.MCCAL等;《Jouranl of organic chemistry》;19620101;5287-5290页 *
Dibenzothiophene: Orientation and Derivatives;H.Gilman;《Jouranl of organic chemistry》;19380517;第3卷;108-119页 *
Syntheses of dibenzo[c,e][1,2]diselenin and related novel chalcogenide heterocyclic compounds;Shizuaki Murata和Toshiyasu Suzuki;《Journal of Heterocyclic Chemistry》;19910101;第28卷(第2期);433-438页 *
Synthesis, structure, and reactions of the first stable aromatic S-nitrosothiol bearing a novel dendrimer-type steric protection group;Goto Kei等;《Chemistry Letters》;20011231(第12期);1204-1205页 *
Two Efficient Routes to m-Terphenyls from 1,3-Dichlorobenzenes;Akbar Saednya和Harold Hart;《Synthesis》;19961201;1455-1458页 *

Also Published As

Publication number Publication date
CN107001314A (zh) 2017-08-01
EP3230271A1 (en) 2017-10-18
TWI691492B (zh) 2020-04-21
WO2016094135A1 (en) 2016-06-16
US20180022725A1 (en) 2018-01-25
JP2018501210A (ja) 2018-01-18
JP6793643B2 (ja) 2020-12-02
CA2967439A1 (en) 2016-06-16
US9951037B2 (en) 2018-04-24
TW201620891A (zh) 2016-06-16
EP3230271B1 (en) 2019-05-01

Similar Documents

Publication Publication Date Title
EP0169101B1 (en) Process for preparing (hydrocarbylthio)cyclic amines
CN109071409A (zh) 制备取代的双环[1 1 1]戊烷的方法
Rodygin et al. Calcium carbide as a convenient acetylene source in the synthesis of unsaturated sulfides, promising functionalized monomers
KR20100114893A (ko) 1-플루오로-2-치환된-3-클로로벤젠의 선택적 탈양성자화 및 관능화 방법
CN107001314B (zh) 制备4-苯基二苯并噻吩的方法
JP4531410B2 (ja) オキセタン化合物及びその製造方法
JP4407062B2 (ja) ジフェニルジスルフィド誘導体の製造法
KR930000290B1 (ko) 퍼플루오로알킬 브로마이드의 합성
JP6620142B2 (ja) ２，２，２−トリフルオロエタンチオールの合成
EP0866049B1 (en) Chlorination of aromatic compounds and catalysts therefor
EP1044965B1 (en) Process for the preparation of aromatic sulfur compounds
JP4570768B2 (ja) 環状フェノール硫化物の製造方法
HU196349B (en) Process for producing chlorobenzotrifluoride compounds
JPH08245558A (ja) 芳香族またはヘテロ芳香族スルフィド化合物の製造方法
US4393241A (en) Synthesis of alkoxy and phenoxy substituted aryl sulfides
JP2001031666A (ja) オキセタン環を有するビナフタレン誘導体
JP3827029B2 (ja) 環状フェノール硫化物の製造方法
US7772443B2 (en) Iodine-containing fluoropolyether and process for producing the same
SU859360A1 (ru) Способ получени дифенилсульфида
JPS6391340A (ja) ハロゲンアルコールの製法
JP5751569B2 (ja) 超原子価臭素体、及びシリル芳香族スルホナート化合物の製造方法
TW202313638A (zh) 噁二矽環戊烷化合物之製造方法
JP2807029B2 (ja) ビス［（４−ヒドロキシ−３−フェニル）フェニル］スルフィドの製造方法
JPH11255778A (ja) シリルチオアルケン化合物及びその製造方法
EP0203827A1 (en) Process for preparing ortho-(alkylthio) phenols

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20210929

Address after: American Maryland

Patentee after: W.R. GRACE & CO.-CONN.

Address before: louisiana

Patentee before: Albemarle Corp.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20200327

CF01 Termination of patent right due to non-payment of annual fee