CN106946541A - 菱镁防火门芯板及其制备方法 - Google Patents

菱镁防火门芯板及其制备方法 Download PDF

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CN106946541A
CN106946541A CN201710161881.9A CN201710161881A CN106946541A CN 106946541 A CN106946541 A CN 106946541A CN 201710161881 A CN201710161881 A CN 201710161881A CN 106946541 A CN106946541 A CN 106946541A
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马利
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TIANJIN HUAAN ANXIN FIREPROOF MATERIAL Co Ltd
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    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
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    • B28B1/522Producing shaped prefabricated articles from the material specially adapted for producing articles from mixtures containing fibres, e.g. asbestos cement for producing multi-layered articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B17/00Details of, or accessories for, apparatus for shaping the material; Auxiliary measures taken in connection with such shaping
    • B28B17/02Conditioning the material prior to shaping
    • EFIXED CONSTRUCTIONS
    • E06DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06BFIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
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Abstract

本发明菱镁防火门芯板及其制备方法,涉及一种门芯板,特别是涉及一种用于防火门的芯板及其制备方法。其目的是为了提供一种耐火性强、不易粉化、强度大的菱镁防火门芯板及其制备方法。本发明的菱镁防火门芯板按照质量份数包括95~105份氧化镁、85~95份氯化镁水溶液、5~6份菱镁改性剂GX‑0#、8~12份菱镁改性剂GX‑4#、1.9~2.5份发泡剂和0.0016份聚丙烯纤维;所述氯化镁水溶液的浓度为27°Bé。本发明的菱镁防火门芯板耐火性强、不易粉化、强度大。本发明用于防火门生产领域。

Description

菱镁防火门芯板及其制备方法
技术领域
本发明涉及一种门芯板,特别是涉及一种用于防火门的芯板及其制备方法。
背景技术
按照我国现行的国家标准GB12955—2008《防火门》之规定,防火门被分成钢质防火门、木质防火门、钢木质防火门及其他材质防火门共四大类,现阶段防火门扇内填充物常见的有成型珍珠岩板、硫镁板、发泡水泥板等防火门芯板,这些防火门芯板大都由填充物的生产厂家按照防火门生产厂家的尺寸要求制作成一定尺寸的小块门芯板,然后由防火门生产厂家在制作门扇时,将多块的门芯板裁剪拼接到门扇内,制作成防火门扇。
防火门芯板是防火门结构中的一个关键原材料,防火门性能的优劣,在很大程度上决定于门芯板的性能和质量。但是直到目前为止,国内针对防火门芯板的相关标准还是空白,生产企业遵循的只是《防火门GB12955-2008》中对防火门填充材料的几项描述,除材料必须满足燃烧性不燃(A1级)以及烟气毒性AQ1两项强制条件,材料需要符合环保要求,使用可降解材料外,对更多的材质及理化指标、工艺指标均没有明确的规定,这使得门芯板生产企业在产品标准和质量控制标准上有了较大的可操作空间,导致行业内产品良莠不齐、以次充好的现象普遍存在。
菱镁防火门芯板原材料来源丰富,价格低廉,工艺技术相对容易掌握,可以通过机械化流水线生产,产能潜力大,生产综合成本低,是一种更最具市场前景和竞争力的门芯材料。但是长时间以来出现在菱镁发泡门芯板上的品质问题主要集中在以下几个方面:一、返卤返潮,锈蚀门板;二、板体粉化、泥化,强度衰减;三、吸水性强,吃胶严重,导致用胶成本增加,甚至出现门板脱胶空鼓;四、耐火性能差,芯材质量烧失率过高,导致防火门检验达不到耐火时限要求;另外还存在规格偏差、平整度偏差过大等问题。
发明内容
本发明是为了解决以上技术问题而提供了一种菱镁防火门芯板及其制备方法。
本发明涉及一种菱镁防火门芯板,所述门芯板按照质量份数包括:95~105份氧化镁、85~95份氯化镁水溶液、5~6份菱镁改性剂GX-0#、8~12份菱镁改性剂GX-4#、1.9~2.5份发泡剂和0.0016份聚丙烯纤维;
所述氯化镁水溶液的浓度为27°Bé。
优选地,所述门芯板按照质量份数包括:100份氧化镁、90份氯化镁水溶液、5.4份菱镁改性剂GX-0#、10份菱镁改性剂GX-4#、2.25份发泡剂和0.0016份聚丙烯纤维。
优选地,所述门芯板还包括无纺布。
本发明还涉及一种菱镁防火门芯板的制备方法,所述方法包括以下步骤:
(1)向90份氯化镁水溶液中加入0.0016份聚丙烯纤维,然后加入5.4份菱镁改性剂GX-0#,搅拌均匀,得到混合溶液1;
(2)向混合溶液1中加入100份氧化镁和10份菱镁改性剂GX-4#,搅拌均匀,得到混合溶液2;
(3)向混合溶液2中加入发泡剂,得到混合溶液3,搅拌混合溶液3发泡至混合溶液3体积的9~10倍,即发泡完成;加入的发泡剂与氯化镁水溶液的质量比为1:40;
(4)先向门板模具中铺一层无纺布,然后将发泡完成的混合溶液3倒入门板模具中,再在混合溶液上铺一层无纺布,放置4小时,即制得本发明的菱镁防火门芯板;
上述份数均为质量份数。
优选地,所述步骤(1)中氯化镁水溶液的浓度为27°Bé。
优选地,所述步骤(4)的操作室温为20~25℃。
本发明菱镁防火门芯板及其制备方法与现有技术不同之处在于:
1本发明的菱镁防火门芯板由于使用发泡剂作为粘合剂,板的表面强度高;内部混合时加入了聚丙烯纤维的原因,内部结构拉力强,便于胶合,并且还具备重量轻,体积大,使用方便,防火性能好的优点。
2本发明菱镁防火门芯板的制备方法中设备可以采用全自动生产线,设备分为上下两层,上层有搅拌混料机,完成后,打开闸门,使混合的原料直接流到下层流水线上,根据流水线的速度调节流放的速度,流水线的前面放入模具,传动带自动把模具送入压料机中,压料机缝隙可自动调节,决定产品的厚度,出来的产品根据用户的尺寸自动切割后,送入烘干设备中进行烘干。因此,使得本发明的方法即节省人力、便于操作,又具有精密度高、产量大质量稳定的优点。
具体实施方式
通过以下实施例和验证试验对本发明的菱镁防火门芯板及其制备方法作进一步的说明。
实施例1
本实施例的菱镁防火门芯板按以下步骤制备:
(1)向90kg氯化镁水溶液(氯化镁水溶液的浓度为27°Bé)中加入1.6g聚丙烯纤维,然后加入5.4kg菱镁改性剂GX-0#,搅拌均匀,得到混合溶液1;
(2)向混合溶液1中加入100kg氧化镁和10kg菱镁改性剂GX-4#,搅拌均匀,得到混合溶液2;
(3)向混合溶液2中加入发泡剂,得到混合溶液3,搅拌混合溶液3发泡至混合溶液3体积的9~10倍,即发泡完成;加入的发泡剂的量为2.25kg;
(4)先向门板模具中铺一层无纺布,然后将发泡完成的混合溶液3倒入门板模具中,再在混合溶液上铺一层无纺布,放置4小时,即制得本实施例的菱镁防火门芯板。
实施例2
本实施例的菱镁防火门芯板按以下步骤制备:
(1)向95kg氯化镁水溶液(氯化镁水溶液的浓度为27°Bé)中加入1.5g聚丙烯纤维,然后加入6kg菱镁改性剂GX-0#,搅拌均匀,得到混合溶液1;
(2)向混合溶液1中加入105kg氧化镁和12kg菱镁改性剂GX-4#,搅拌均匀,得到混合溶液2;
(3)向混合溶液2中加入发泡剂,得到混合溶液3,搅拌混合溶液3发泡至混合溶液3体积的9~10倍,即发泡完成;加入的发泡剂的量为1.9kg;
(4)先向门板模具中铺一层无纺布,然后将发泡完成的混合溶液3倒入门板模具中,再在混合溶液上铺一层无纺布,放置4小时,即制得本实施例的菱镁防火门芯板。
实施例3
本实施例的菱镁防火门芯板按以下步骤制备:
(1)向85kg氯化镁水溶液(氯化镁水溶液的浓度为27°Bé)中加入1.7g聚丙烯纤维,然后加入5kg菱镁改性剂GX-0#,搅拌均匀,得到混合溶液1;
(2)向混合溶液1中加入95kg氧化镁和8kg菱镁改性剂GX-4#,搅拌均匀,得到混合溶液2;
(3)向混合溶液2中加入发泡剂,得到混合溶液3,搅拌混合溶液3发泡至混合溶液3体积的9~10倍,即发泡完成;加入的发泡剂的量为2.5kg;
(4)先向门板模具中铺一层无纺布,然后将发泡完成的混合溶液3倒入门板模具中,再在混合溶液上铺一层无纺布,放置4小时,即制得本实施例的菱镁防火门芯板。
对上述实施例中制得的门芯板进行一些基本性能的测定,测定结果见表1。
表1实施例1-3中制得产品的基本性能
由上表可知,本发明制得的产品质地轻、强度高、弯曲度小,容易加工、实用性更强。
虽然以上描述了本发明的具体实施方式,但是本领域的技术人员应当理解,这些仅是举例说明,本发明的保护范围是由所附权利要求书限定的。本领域的技术人员在不背离本发明的原理和实质的前提下,可以对这些实施方式作出多种变更或修改,但这些变更和修改均落入本发明的保护范围。

Claims (6)

1.一种菱镁防火门芯板,其特征在于:所述门芯板按照质量份数包括:95~105份氧化镁、85~95份氯化镁水溶液、5~6份菱镁改性剂GX-0#、8~12份菱镁改性剂GX-4#、1.9~2.5份发泡剂和0.0015~0.0017份聚丙烯纤维;
所述氯化镁水溶液的浓度为27°Bé。
2.根据权利要求1所述的菱镁防火门芯板,其特征在于:所述门芯板按照质量份数包括:100份氧化镁、90份氯化镁水溶液、5.4份菱镁改性剂GX-0#、10份菱镁改性剂GX-4#、2.25份发泡剂和0.0016份聚丙烯纤维。
3.根据权利要求2所述的菱镁防火门芯板,其特征在于:所述门芯板还包括无纺布。
4.一种菱镁防火门芯板的制备方法,其特征在于:所述方法包括以下步骤:
(1)向90份氯化镁水溶液中加入0.0016份聚丙烯纤维,然后加入5.4份菱镁改性剂GX-0#,搅拌均匀,得到混合溶液1;
(2)向混合溶液1中加入100份氧化和10份菱镁改性剂GX-4#,搅拌均匀,得到混合溶液2;
(3)向混合溶液2中加入发泡剂,得到混合溶液3,搅拌混合溶液3发泡至混合溶液3体积的9~10倍,即发泡完成;加入的发泡剂与氯化镁水溶液的质量比为1:40;
(4)先向门板模具中铺一层无纺布,然后将发泡完成的混合溶液3倒入门板模具中,再在混合溶液上铺一层无纺布,放置4小时,即制得本发明的菱镁防火门芯板;
上述份数均为质量份数。
5.根据权利要求4所述的菱镁防火门芯板的制备方法,其特征在于:所述步骤(1)中氯化镁水溶液的浓度为27°Bé。
6.根据权利要求5所述的菱镁防火门芯板的制备方法,其特征在于:所述步骤(4)的操作室温为20~25℃。
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Application publication date: 20170714